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NZ783737B2 - Novel b-galactosidase - Google Patents
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NZ783737B2 - Novel b-galactosidase - Google Patents

Novel b-galactosidase

Info

Publication number
NZ783737B2
NZ783737B2 NZ783737A NZ78373716A NZ783737B2 NZ 783737 B2 NZ783737 B2 NZ 783737B2 NZ 783737 A NZ783737 A NZ 783737A NZ 78373716 A NZ78373716 A NZ 78373716A NZ 783737 B2 NZ783737 B2 NZ 783737B2
Authority
NZ
New Zealand
Prior art keywords
enzyme
galactosidase
amino acid
galactosidase enzyme
acid sequence
Prior art date
Application number
NZ783737A
Other versions
NZ783737A (en
Inventor
Masayuki Hojo
Akio Horii
Yukiko Hoshi
Masamichi Okada
Original Assignee
Amano Enzyme Inc
Filing date
Publication date
Application filed by Amano Enzyme Inc filed Critical Amano Enzyme Inc
Publication of NZ783737A publication Critical patent/NZ783737A/en
Publication of NZ783737B2 publication Critical patent/NZ783737B2/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C07H3/06Oligosaccharides, i.e. having three to five saccharide radicals attached to each other by glycosidic linkages
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N15/00Mutation or genetic engineering; DNA or RNA concerning genetic engineering, vectors, e.g. plasmids, or their isolation, preparation or purification; Use of hosts therefor
    • C12N15/09Recombinant DNA-technology
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N5/00Undifferentiated human, animal or plant cells, e.g. cell lines; Tissues; Cultivation or maintenance thereof; Culture media therefor
    • C12N5/10Cells modified by introduction of foreign genetic material
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N9/00Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
    • C12N9/14Hydrolases (3)
    • C12N9/24Hydrolases (3) acting on glycosyl compounds (3.2)
    • C12N9/2402Hydrolases (3) acting on glycosyl compounds (3.2) hydrolysing O- and S- glycosyl compounds (3.2.1)
    • C12N9/2468Hydrolases (3) acting on glycosyl compounds (3.2) hydrolysing O- and S- glycosyl compounds (3.2.1) acting on beta-galactose-glycoside bonds, e.g. carrageenases (3.2.1.83; 3.2.1.157); beta-agarase (3.2.1.81)
    • C12N9/2471Beta-galactosidase (3.2.1.23), i.e. exo-(1-->4)-beta-D-galactanase
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/14Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12YENZYMES
    • C12Y302/00Hydrolases acting on glycosyl compounds, i.e. glycosylases (3.2)
    • C12Y302/01Glycosidases, i.e. enzymes hydrolysing O- and S-glycosyl compounds (3.2.1)
    • C12Y302/01023Beta-galactosidase (3.2.1.23), i.e. exo-(1-->4)-beta-D-galactanase

Abstract

The present invention has a purpose of providing a novel ß-galactosidase enzyme useful for the production of oligosaccharides. Disclosed is a ß-galactosidase enzyme comprising the amino acid sequence of any one of SEQ ID NOs: 1 to 4 or an amino acid sequence that is 80% or more identical to said amino acid sequence

Claims (17)

1. A ß-galactosidase enzyme comprising an amino acid sequence that is 90% or 5 more identical to any one of SEQ ID NOs: 1 to 4.
2. The ß-galactosidase enzyme according to claim 1, wherein the amino acid sequence consists of an amino acid sequence having a length equal to or less than that of the amino acid sequence of SEQ ID NO: 1.
3. The ß-galactosidase enzyme according to claim 1 or claim 2, wherein the amino acid sequence comprises the amino acid sequence of any one of SEQ ID NOs: 1 to 4.
4. A ß-galactosidase enzyme according to claim 1 which possesses the following 15 enzymological properties: (1) an enzymatic action by which the enzyme has a lactose hydrolyzing activity and a transgalactosylation activity, wherein the activity of the enzyme to transfer a galactosyl residue via ß-1,4-linkage is superior to that via ß-1,6-, ß-1,3-, or ß-1,2- linkage; 20 (2) an optimum temperature of 70°C; and (3) a molecular weight of about 104 kDa, about 64 kDa, or about 61 kDa (by SDS-PAGE) for the enzyme without sugar chains.
5. The ß-galactosidase enzyme according to claim 4, which further possesses the 25 following enzymological properties: (4) an optimum pH of 4 to 5; (5) a pH stability in which the enzyme is stable in a range of pH 2 to 8 (at 40°C for 30 minutes); and (6) a thermostability in which the enzyme is stable in a temperature range of 30 30°C to 60°C (at pH 6.0 for 30 minutes).
6. The ß-galactosidase enzyme according to claim 4, which further possesses the following enzymological properties: (4) an optimum pH of 4 to 5; 35 (5) a pH stability in which the enzyme is stable in a range of pH 2 to 9 (at 40°C for 30 minutes); and (6) a thermostability in which the enzyme is stable in a temperature range of 30°C to 65°C (at pH 6.0 for 30 minutes). 5
7. An enzyme preparation comprising, as an active ingredient, the ß-galactosidase enzyme according to any one of claims 1 to 6.
8. A ß-galactosidase gene consisting of a DNA selected from the group consisting 10 (a) a DNA encoding the amino acid sequences of any one of SEQ ID NOs: 1 to (b) a DNA consisting of the base sequence of any one of SEQ ID NOs: 5 to 8 and 16; and (c) a DNA comprising a base sequence that is 90% or more identical to that of 15 any one of SEQ ID NOs: 5 to 8 and 16 and encoding a protein with ß-galactosidase activity.
9. A recombinant DNA comprising the ß-galactosidase gene according to claim 8. 20
10. A microorganism carrying the recombinant DNA according to claim 9.
11. A method for producing a ß-galactosidase enzyme according to any one of claims 1 to 6, comprising the steps of: (1) culturing cells of Cryptococcus terrestris; and 25 (2) collecting the ß-galactosidase enzyme from the cultured medium and/or cells.
12. The method according to claim 11, wherein the Cryptococcus terrestris is Cryptococcus terrestris strain MM13-F2171 or a mutant strain thereof.
13. A method for producing a ß-galactosidase enzyme, comprising the steps of: (i) culturing the microorganism of claim 10 under conditions allowing the production of protein encoded by the gene; and (ii) collecting the protein that has been produced.
14. A method for producing oligosaccharides, comprising a step of subjecting the ß-galactosidase enzyme according to any one of claims 1 to 6 to a reaction with a disaccharide, oligosaccharide, or polysaccharide having at least one of ß-1,3-, ß-1,4-, and ß-1,6-linkages.
15. A method for producing oligosaccharides, comprising a step of subjecting the ß-galactosidase enzyme according to any one of claims 1 to 6 to a reaction with lactose.
16. The method according to claim 14 or 15, wherein the reaction temperature in 10 the step is from 30°C to 75°C.
17. Use of the ß-galactosidase enzyme according to any one of claims 1 to 6 for the production of oligosaccharides. DRAWINGS
NZ783737A 2016-12-27 Novel b-galactosidase NZ783737B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2015257705 2015-12-29
NZ744061A NZ744061B2 (en) 2016-12-27 Novel ?-galactosidase

Publications (2)

Publication Number Publication Date
NZ783737A NZ783737A (en) 2025-09-26
NZ783737B2 true NZ783737B2 (en) 2026-01-06

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