WO2018042537A1 - Container - Google Patents
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- WO2018042537A1 WO2018042537A1 PCT/JP2016/075453 JP2016075453W WO2018042537A1 WO 2018042537 A1 WO2018042537 A1 WO 2018042537A1 JP 2016075453 W JP2016075453 W JP 2016075453W WO 2018042537 A1 WO2018042537 A1 WO 2018042537A1
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- WIPO (PCT)
- Prior art keywords
- container
- main body
- extrapolation
- container main
- container body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D21/00—Nestable, stackable or joinable containers; Containers of variable capacity
- B65D21/08—Containers of variable capacity
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
Definitions
- the present invention relates to a container, particularly a container suitable for sample analysis.
- a container for an analysis sample for example, there is a container called a vial having a general size and volume corresponding to a gas chromatograph autosampler (see, for example, Patent Document 1 below).
- a sample handled in such a container may be pretreated before being placed in the container and set in the autosampler.
- the sample is concentrated by a centrifugal concentrator.
- the amount of the sample before concentration by the centrifugal concentrator is large.
- Such a large sample cannot fit into a vial of constant size and volume. Therefore, since a large amount of sample is first subjected to pretreatment such as concentration by a centrifugal concentrator, it is pretreated in a larger volume pretreatment container separate from the vial. After that, the pretreated sample is transferred from the pretreatment container to the vial, and the vial is set in the autosampler.
- the object of the present invention is to provide a container that can easily cope with a large change in the volume of the contained items.
- the present invention is a container comprising an extrapolation container main body having a first accommodation part and an insertion container main body having a second accommodation part, and the insertion container main body is inserted into the extrapolation container main body, By sliding the insertion container main body relative to the extrapolation container main body, the volume of the storage part composed of the first storage part and the second storage part increases or decreases, and the extrapolation container main body and the insertion container main body change the sliding direction. Relative rotation as a rotation axis is restricted, and the inner container body includes a pressure seal portion that presses and seals the inner surface of the first housing portion of the extrapolation container body regardless of the slide position. About.
- the extrapolation container body is formed of a material that is more easily deformed than the insertion container body.
- one of the extrapolation container body and the insertion container body has a convex part for realizing sliding and restricting relative rotation
- the other of the extrapolation container body or the insertion container body is convex.
- a recessed portion in which the portion is disposed, and has a recessed portion for realizing sliding and restricting relative rotation, and the protruding portion and the recessed portion are relative to the extrapolation container body and the insertion container body at a predetermined angle. It is preferable to allow general rotation.
- the extrapolation container body and the insertion container body can be held at an arbitrary slide position by pressing the pressing seal portion.
- the lower container body is more sample than the upper container body.
- the material is formed from a material having high resistance to.
- the extrapolation container main body and the extrapolation container main body after being concentrated by centrifugal concentrating with the centrifugal concentrator for concentrating the sample accommodated in the accommodating portion in a state where the extrapolation container main body is slid and extended.
- it is preferably used for sample analysis in which the centrifugally concentrated sample is analyzed by a sample analyzer while the insertion container body is slid and contracted.
- FIG. 3 is a cross-sectional view taken along line AA in FIG. 2. It is a longitudinal view seen in the state where the container concerning this embodiment was extended. It is a longitudinal view which shows the extrapolation container main body which comprises the container which concerns on this embodiment. It is a top view which shows the extrapolation container main body which comprises the container which concerns on this embodiment. It is a side view which shows the insertion container main body which comprises the container which concerns on this embodiment.
- FIG. 8 is a cross-sectional view taken along line BB in FIG. 7. It is the elements on larger scale which expand and show the C arrow part of FIG.
- FIG. 1 is a perspective view showing a state in which the container 1 is contracted in the container 1 assembled by inserting the insertion container body 3 into the extrapolation container body 2.
- FIG. 2 is a partially longitudinal front view showing the container 1 of FIG. 3 is a cross-sectional view showing the container 1 of FIG. 1 cut along the line AA of FIG.
- FIG. 4 is a longitudinal sectional view showing the container 1 of FIG. 1 in an extended state.
- FIG. 5 is a longitudinal sectional view showing the extrapolation container main body 2 constituting the container 1 of FIG. 1 as a single unit.
- FIG. 6 is a plan view of the extrapolation container body 2 shown in FIG. FIG.
- FIG. 7 is a side view showing the insertion container main body 3 constituting the container 1 of FIG. 1 as a single unit.
- FIG. 8 is a cross-sectional view taken along line BB in FIG.
- FIG. 9 is a partially enlarged view showing the portion indicated by the arrow C in FIG. 4 in an enlarged manner.
- the container 1 includes an extrapolation container main body 2 having a first accommodation part 20, an insertion container main body 3 having a second accommodation part 30, a lid (Not shown).
- the first accommodating portion 20 and the second accommodating portion 30 constitute the entire accommodating portion 10 of the container 1.
- the extrapolation container main body 2 will be described with reference to FIG. 5, FIG. 6, FIG.
- the extrapolation container main body 2 is a lower container main body that constitutes the lower half of the container 1, and includes a first storage portion 20 (described later), a peripheral wall 21, a bottom wall 22, and a sample reservoir 23.
- the peripheral wall 21 has a cylindrical shape and extends from the upper end to the lower end of the extrapolation container main body 2.
- the bottom wall 22 is connected to a predetermined height H1 and a high portion (hereinafter also referred to as “continuous portion 215”) from the lower end of the peripheral wall 21.
- An inner peripheral surface (inner surface) 211 in a range (height) H5 from the upper end of the peripheral wall 21 to the height H1 of the continuous portion 215 is a cylindrical surface except for a convex portion 212 and an annular convex portion 213 described later.
- the bottom wall 22 is continuous with the peripheral wall 21 at the continuous portion 215.
- the bottom wall 22 extends downward gently from the continuous portion 215 toward the central axis CL ⁇ b> 1 of the peripheral wall 21, and continues to the upper end of the sample reservoir 23.
- the sample reservoir 23 is a small concave space arranged concentrically with the peripheral wall 21.
- the vertical wall 231 extends downward from the upper end and reaches the bottom 232.
- the inner space of the bottom portion 232 has an inverted conical shape and has a deepest portion 233 at a position that coincides with the central axis CL1 of the peripheral wall 21.
- the lower end of the bottom portion 232 is located at the same height as the lower end of the peripheral wall 21.
- the upper end portion of the peripheral wall 21 is provided with four convex portions 212 protruding inward in the radial direction from the inner peripheral surface 211 in plan view.
- the four convex portions 212 are arranged at an interval of approximately 90 ° from each other along the circumferential direction of the peripheral wall 21.
- Each convex part 212 is substantially the same in size and shape.
- each convex portion 212 includes a first inclined surface 2121 extending obliquely downward from the upper end of the inner peripheral surface 211, a predetermined height H2 from the upper end of the inner peripheral surface 211, and an obliquely upward from a lower portion.
- a second inclined surface 2122 extending to the upper surface, a protruding surface 2123 connecting the lower end edge of the first inclined surface 2121 and the upper end edge of the second inclined surface 2122, a first side surface 2124 (see FIG. 5), 2 side surfaces 2125 (see FIG. 5).
- each convex portion 212 is disposed substantially parallel to the inner peripheral surface 211.
- the protruding amount of each convex portion 212 that is, the radial distance P1 between the inner peripheral surface 211 and the protruding surface 2123 is the same.
- the second inclined surface 2122 has a gentler gradient with respect to the inner peripheral surface 211.
- the first side surface 2124 and the second side surface 2125 are slightly inclined with respect to the vertical surface so that the distance between the first side surface 2124 and the second side surface 2125 increases.
- annular convex portion protruding inward in the radial direction from the inner peripheral surface 211 through a region of the inner peripheral surface 211 to a predetermined height H3 (> H2) and a lower portion from the upper end of each convex portion 212 of the peripheral wall 21 213 is provided.
- the annular convex portion 213 is provided along the circumferential direction of the peripheral wall 21 without a 360 ° break (on the entire circumference).
- the annular convex portion 213 has an annular protruding edge 2131 that protrudes most inward in the radial direction from the inner peripheral surface 211.
- the curved surface on the upper side of the protruding edge 2131 is bent and connected to the inner peripheral surface 211.
- the inclined surface on the lower side of the protruding edge 2131 is smoothly connected to the inner peripheral surface 211.
- the protrusion amount P2 of the annular protrusion 213 (that is, the radial distance P2 between the inner peripheral surface 211 and the protrusion edge 2131) is smaller than the protrusion amount P1 of each protrusion 212 (P2 ⁇ P1).
- the space occupied by the insertion container body 3 in the state where the container 1 is extended is excluded from the space surrounded by the peripheral wall 21, the bottom wall 22 and the sample reservoir 23 from the upper end of the extrapolation container body 2.
- the space constitutes the first housing part 20.
- the first accommodating part 20 has an inner diameter R1 and a central axis CL1.
- the insertion container body 3 will be described with reference to FIGS. 7, 8, 9 and the like.
- the insertion container main body 3 has the 2nd accommodating part 30 so that it may mention later.
- the insertion container body 3 has a substantially cylindrical shape penetrating from the upper end to the lower end.
- the insertion container body 3 has a center axis CL2.
- the insertion container body 3 has a state in which the container 1 is contracted (see FIG. 2) and a state in which the container 1 is extended (see FIG. 4) in the state inserted in the extrapolation container body 2. Configured to slide between.
- the insertion container main body 3 includes a pressing seal portion 31, a rotation restricting portion 32, and a mouth portion 33 in order from the bottom to the top.
- the pressure seal portion 31 is always located inside the insertion container main body 3 during use.
- the rotation restricting portion 32 is located inside the insertion container main body 3 when the container 1 is contracted during use.
- the rotation restricting portion 32 is located outside the insertion container main body 3 when the container 1 is extended during use.
- the mouth portion 33 is always located outside the insertion container body 3 (regardless of the expansion and contraction of the container 1).
- the pressure seal part 31 occupies from the lower end of the insertion container body 3 to a position at a predetermined height.
- the pressing seal portion 31 has a cylindrical shape and includes an outer peripheral reference surface 311, a first annular seal portion 312, a second annular seal portion 313, and an inner peripheral surface 314.
- the diameter R2 of the outer peripheral reference surface 311 is smaller than the inner diameter R1 of the first housing portion 20 (R2 ⁇ R1).
- the inner peripheral surface 314 has a diameter R3.
- the protrusion amount P2 of the annular convex portion 213 in the extrapolation container body 2 is half of the difference (R1 ⁇ R2) between the inner diameter R1 of the first accommodating portion 20 and the diameter R2 of the outer peripheral reference surface 311 of the pressure seal portion 31. be equivalent to.
- R1 R2 + 2 ⁇ P2
- the first annular seal portion 312 protrudes radially outward from the outer peripheral reference surface 311 at the lower end of the pressure seal portion 31. As shown in FIG. 9, the first annular seal portion 312 has an annular seal edge 3121 that protrudes most outward in the radial direction from the outer peripheral reference surface 311. The curved surface on the upper side of the seal edge 3121 is smoothly connected to the outer peripheral reference surface 311. The curved surface on the lower side of the seal edge portion 3121 continues to the lower surface of the press seal portion 31.
- the second annular seal portion 313 protrudes radially outward from the outer peripheral reference surface 311 via the region of the outer peripheral reference surface 311 above the first annular seal portion 312. As shown in FIG. 9, the second annular seal portion 313 has an annular seal edge portion 3131 that protrudes most outward in the radial direction from the outer peripheral reference surface 311, similarly to the first annular seal portion 312. The curved surface on the upper side of the seal edge 3131 and the curved surface on the lower side of the seal edge 3131 are smoothly connected to the outer peripheral reference surface 311.
- the outer diameter R4 of the first annular seal portion 312 and the second annular seal portion 313 is larger than the inner diameter R1 of the first accommodating portion 20 (R4> R1).
- the protrusion amount P ⁇ b> 3 of the first annular seal portion 312 that is, the radial distance P ⁇ b> 3 between the outer peripheral reference surface 311 and the seal edge portion 3121
- the amount P3 that is, the radial distance P3 between the outer peripheral reference surface 311 and the seal edge 3131) is the same.
- the protrusion amount P3 of the first annular seal portion 312 and the second annular seal portion 313 is larger than the protrusion amount P2 of the annular convex portion 213 in the extrapolation container body 2 (P3> P2). Therefore, it is a case where the 1st annular seal part 312 and the 2nd annular seal part 313 in insertion container body 3 are inserted in arbitrary height in the 1st storage part 20 of extrapolation container body 2, and The annular seal edge 3121 of the first annular seal portion 312 and the annular seal edge portion 3131 of the second annular seal portion 313 are arranged so that the inner peripheral surface 211 of the first accommodating portion 20 faces radially outward. It can be pressed and sealed.
- the rotation restricting portion 32 is disposed adjacent to and above the pressure seal portion 31.
- the rotation restricting portion 32 has a cylindrical shape and includes an outer peripheral surface 321, four concave portions 322, an upper flange 323, and an inner peripheral surface 324.
- the diameter R2 of the outer circumferential surface 321 is the same as the diameter R2 of the outer circumferential reference surface 311 of the pressing seal portion 31.
- the diameter R3 of the inner peripheral surface 324 is the same as the diameter R3 of the inner peripheral surface 314 of the pressing seal portion 31.
- a space surrounded by the inner peripheral surface 314 of the pressing seal portion 31 and the inner peripheral surface 324 of the rotation restricting portion 32 constitutes the second accommodating portion 30.
- the second accommodating portion 30 has an inner diameter R3 and a central axis CL2.
- the four recesses 322 are recesses scraped from the outer peripheral surface 321 inward in the radial direction from the upper end to the lower end of the outer peripheral surface 321.
- Each recess 322 is provided over a range of approximately 90 ° along the circumferential direction of the rotation restricting portion 32.
- the four concave portions 322 are arranged at an interval of approximately 90 ° from each other along the circumferential direction of the rotation restricting portion 32.
- Each recess 322 is substantially the same in size and shape.
- each recess 322 includes an inner side surface 3221 arranged in parallel to the outer peripheral surface 321 on the radially inner side of the outer peripheral surface 321, and an upper surface 3222 continuous from the lower surface of the upper flange 323 to the inner side thereof. It has a lower surface 3223 serving as an upper surface of the pressure seal portion 31, a first side surface 3224 (see FIG. 8), and a second side surface 3225 (see FIG. 8).
- the rotation restricting portion 32 is formed by removing the four concave portions 322 on the outer peripheral surface 321, and as a result, the remaining outer peripheral surface 321 extending in the vertical direction and the first side surface 3224 of the concave portion 322 adjacent to the right side thereof. And four rib-shaped protrusions constituted by the second side surface 3225 of another concave portion 322 adjacent to the left side, and spaced apart from each other by approximately 90 ° along the circumferential direction of the rotation restricting portion 32. If placed, you can see it.
- each recess 322 that is, the radial distance D1 between the outer peripheral surface 321 and the inner side surface 3221
- the protrusion amount P1 of each protrusion 212 in the extrapolation container body 2 is the protrusion of the annular protrusion 213 in the extrapolation container body 2.
- the rotation restricting portion 32 in the insertion container main body 3 is inserted into the extrapolation container main body 2, the four convex portions 212 of the first accommodating portion 20 in the extrapolation container main body 2 are rotated in the insertion container main body 3.
- Each of the four recessed portions 322 of the restricting portion 32 is accommodated.
- the relative rotation of the extrapolation container body 2 and the insertion container body 3 is such that the four convex portions 212 in the extrapolation container main body 2 are located within the four concave portions 322 in the insertion container main body 3 (that is, In the range of about 90 °).
- the inner container body 3 can be moved in and out of the outer container body 2 within the range of the rotation restricting portion 32. Specifically, as shown in FIG. 2, the insertion container main body 3 can be inserted into the extrapolation container main body 2 until the lower surface of the upper flange 323 is in contact with the upper surface of the extrapolation container main body 2. At this time, the container 1 is in a contracted state. Therefore, the length H4 (see FIG. 4, the length H4 from the lower surface of the upper flange 323 to the lower end of the pressure seal portion 31) including the pressure seal portion 31 and the rotation restriction portion 32 in the insertion container body 3 is extrapolated. It is shorter than the length H5 (see FIG. 4) from the upper end of the container body 2 to the continuous portion 215 between the peripheral wall 21 and the bottom wall 22.
- the insertion container body 3 has a boundary 315 (see FIG. 9, that is, the lower surface 3223 of the rotation restriction part 32) between the pressure seal part 31 and the rotation restriction part 32. It can be pulled out of the extrapolation container main body 2 up to a height H6 that contacts the second inclined surface 2122 of the convex portion 212. At this time, the container 1 is in an extended state. Thus, the insertion container body 3 can slide with respect to the extrapolation container body 2.
- the lower surface 3223 of the rotation restricting portion 32 in the insertion container main body 3 contacts the second inclined surface 2122 of the convex portion 212 in the extrapolation container main body 2 in a state where the container 1 is extended. Because of the contact, the insertion container main body 3 cannot be pulled out from the extrapolation container main body 2 any more. Therefore, the insertion container body 3 is prevented from coming off from the outer container body 2 accurately.
- the mouth portion 33 continues above the rotation restricting portion 32.
- the mouth portion 33 has a cylindrical shape and includes an outer peripheral surface 331, a screw thread 332, and an inner peripheral surface 333.
- the screw thread 332 is for screwing with a corresponding screw thread provided on a lid (not shown).
- the inner peripheral surface 333 of the mouth portion 33 has a smaller diameter than the inner peripheral surfaces 314 and 324 of the pressing seal portion 31 and the rotation restricting portion 32.
- the container 1 is assembled by inserting the insertion container body 3 into the outer insertion container body 2 by press fitting.
- the insertion container main body 3 and the extrapolation container main body 2 can be relatively slid in the axial direction between the contracted state shown in FIG. 2 and the extended state shown in FIG. is there. Therefore, by sliding the insertion container main body 3 and the extrapolation container main body 2 relative to each other, the volume of the accommodating portion 10 of the container 1 is arbitrarily increased or decreased within a design possible range.
- the volume of the container 10 of the container 1 is a volume obtained by adding the volume of the first container 20 and the volume of the second container 30.
- the volume of the second storage portion 30 occupies the most volume of the first storage portion 20 instead, it is slightly smaller than that approximated to the volume of the second storage portion 30.
- a large volume is the volume of the accommodating portion 10 of the container 1. For example, it is possible to store a larger amount of sample in the container 1 in the extended state by using the container 1 that conforms to the standard of the autosampler in the contracted state.
- the relative rotation of the extrapolation container main body 2 and the insertion container main body 3 with the sliding directions as the rotation axes CL1 and CL2 is restricted.
- the convex portion 212 of the extrapolation container body 2 and the concave portion 322 of the insertion container body 3 are provided in order to realize sliding and to restrict relative rotation. More specifically, the four convex portions 212 of the first accommodating portion 20 in the extrapolation container main body 2 are respectively accommodated and arranged in the four concave portions 322 of the rotation restricting portion 32 in the interpolated container main body 3.
- relative rotation of the extrapolation container main body 2 and the insertion container main body 3 is a range in which the four convex portions 212 in the extrapolation container main body 2 are located inside the four concave portions 322 in the interpolation container main body 3 (that is, about 90 ° range).
- the extrapolation container body 2 is formed of a material that is more easily deformed than the insertion container body 3.
- the extrapolation container body 2 is made of PFA (polytetrafluoroethylene) because high resistance to the sample is required.
- the insertion container body 3 is made of PP (polypropylene) or PE (polyethylene), which is less expensive than PFA because it is difficult to directly contact the sample. PFA is more easily deformed than PP and PE.
- the extrapolation container body 2 and the insertion container body 3 are formed by injection molding, cutting, or the like.
- the first annular seal portion 312 and the second annular seal portion 313 of the pressure seal portion 31 in the insertion container body 3 are arranged at any slide position from the contracted state to the extended state. 2, the inner peripheral surface 211 of the first accommodating portion 20 can be pressed and sealed.
- the pressure seal with respect to the 1st accommodating part 20 of the external container body 2 by the press seal part 31 of the internal container body 3 is exhibited in arbitrary slide positions, the internal container body 3 and the external container body 2 Can be held at an arbitrary slide position by pressing the pressing seal portion 31.
- the extrapolation container body 2 is more easily deformed than the insertion container body 3 by making the extrapolation container body 2 made of PFA and the insertion container body 3 made of PP or PE. Therefore, when the first annular seal portion 312 and the second annular seal portion 313 of the press seal portion 31 in the insertion container body 3 press-seal the inner peripheral surface 211 of the first storage portion 20 in the extrapolation container body 2. In addition, the inner peripheral surface 211 of the first accommodating portion 20 is pushed outward by the first annular seal portion 312 and the second annular seal portion 313 of the pressing seal portion 31 and expands somewhat.
- the combination of the PFA extrapolating container main body 2 and the PP or PE interpolating container main body 3 is also a point that holds the interpolating container main body 3 and the extrapolating container main body 2 at an arbitrary slide position. The effect of enhancing the holding function is exhibited.
- the container 1 is a sample accommodated in the first accommodation part 20 and the second accommodation part 30. It is used as a container for centrifugal concentration in which the solution is concentrated with a centrifugal concentrator. As shown in FIG. 4, the container 1 is firmly locked by the sealing function and the holding function at the position where the inner container body 3 is extended from the outer container body 2 to the maximum extent. The reason for this is that, as shown in FIG.
- the outer edge of the boundary 315 between the pressure seal portion 31 and the rotation restricting portion 32 in the insertion container body 3 is formed on the second inclined surface 2122 of the convex portion 212 in the insertion container body 2. This is because they abut and receive a reaction force from the inclined surface 2122. In this state, the container 1 is put on a centrifugal concentrator as will be described later.
- the container 1 is a container for sample analysis in which the extrapolated container body 2 and the inserted container body 3 are slid and contracted to analyze the centrifugally concentrated sample with a sample analyzer. Used as. Moreover, the container 1 used as a container for centrifugal concentration and the container 1 used as a container for sample analysis are the same containers that are simply deformed from a stretched state to a contracted state. No transfer is required.
- the container 1 is relatively slidable from the contracted state shown in FIG. 2 to the extended state shown in FIG. Thereby, the volume of the accommodating part 10 of the container 1 can be arbitrarily increased / decreased in the range which can be designed. Therefore, for example, the container 1 can be manufactured in a contracted state with a size and volume that conforms to the standard of a predetermined device. And this container 1 can accommodate a larger amount of sample exceeding the standard in the stretched state.
- the relative rotation of the extrapolation container main body 2 and the insertion container main body 3 is a range in which the four convex portions 212 in the extrapolation container main body 2 are positioned inside the four concave portions 322 in the insertion container main body 3 ( That is, it is limited to a range of about 90 °. Therefore, for example, when the extrapolation container body 2 is rotated when the container 1 is set in a predetermined device, the insertion container body 3 rotates with the extrapolation container body 2 only by a delay of about 90 degrees at the maximum. Thus, integral rotation of the extrapolation container body 2 and the insertion container body 3 can be realized.
- each of the four recesses 322 in the insertion container main body 3 is provided over a range of, for example, 60 ° or more, specifically, a range of approximately 90 ° along the circumferential direction of the rotation restricting portion 32. It is done.
- the formation of the wide concave portion 322 is easier than the formation of the narrow concave portion. Therefore, the rotation restricting portion 32 and the insertion container main body 3 and, as a result, the container 1 can be manufactured at a relatively low cost.
- a slide is realized by a combination of a convex portion and a concave portion that are substantially not allowed to rotate, it is necessary to form a thin and long concave portion. However, formation of such a recess is not easy.
- rotation of a predetermined angle is allowed, that is, if the width of the recess can be increased, the formation of the recess is easy.
- the first annular seal portion 312 and the second annular seal portion 313 of the pressure seal portion 31 in the insertion container main body 3 are located at any position from the contracted state to the expanded state.
- the inner peripheral surface 211 of the first accommodating portion 20 in the extrapolation container main body 2 is pressed and sealed without change. For this reason, when the container 1 is expanded and contracted, it is possible to avoid the possibility of foreign matters entering the container 1.
- the extrapolation container body 2 (for example, made of PFA) is formed of a material that is more easily deformed than the insertion container body 3 (for example, made of PP or PE). Therefore, the first annular seal portion 312 and the second annular seal portion 313 of the pressure seal portion 31 can easily secure a large amount of pressure displacement of the inner peripheral surface 211 of the first accommodating portion 20 in the extrapolation container body 2 and are stable. It is easy to realize a seal by pressing.
- the extrapolation container body 2 and the insertion container body 3 can be held at an arbitrary slide position by pressing of the pressing seal portion 31. Therefore, the holding can be realized without providing another configuration for holding at an arbitrary slide position.
- the container body in which the sample is stored is referred to as the lower container body, and the other container body is referred to as the upper container body. It is formed from a material that is highly resistant to A material having high resistance to a sample often has limitations such as being relatively expensive and having low moldability. If only the lower container main body is formed from a material having high resistance to the sample, the upper container main body can employ a material that avoids restrictions.
- the container 1 is for centrifugal concentration in which the sample accommodated in the first accommodating part 20 and the second accommodating part 30 is concentrated by a centrifugal concentrator in a state where the extrapolating container body 2 and the inserting container body 3 are slid and extended.
- the sample is analyzed by a sample analyzer in a state where the extrapolation container body 2 and the insertion container body 3 are slid and contracted. Therefore, it is possible to use for sample analysis without transferring the centrifugally concentrated sample to another container for sample analysis. Therefore, contamination of the sample when the container 1 is transferred can be suppressed.
- first annular seal portion 312 and the second annular seal portion 313 are provided in the press seal portion 31, but the present invention is not limited to this.
- the second annular seal portion 313 may be omitted, and the pressure seal portion 31 may be configured with only the first annular seal portion 312.
- the extrapolation container body 2 is made of PFA and the insertion container body 3 is made of PP or PE.
- the present invention is not limited to this.
- the insertion container body 3 may be made of PFA.
- the convex part 212 was provided in the inner peripheral surface 211 in the extrapolation container main body 2, and the recessed part 322 was provided in the outer peripheral surface 321 of the rotation control part 32 in the insertion container main body 3, it is not limited to this.
- a concave portion may be provided on the inner peripheral surface 211 of the extrapolation container main body 2, and a convex portion may be provided on the outer peripheral surface 321 of the rotation restricting portion 32 of the inner case 3.
- the extrapolation container main body 2 was made into the lower container main body, and the insertion container main body 3 was made into the upper container main body, it is not limited to this.
- the insertion container main body 3 may be a lower container main body, and the extrapolation container main body 2 may be an upper container main body.
- the insertion container body 3 as the lower container body may be made of PFA since a material having high resistance to the sample is required, and the extrapolation container body 2 as the upper container body may be made of PP or PE.
- the present invention can be applied to containers other than those for sample analysis and centrifugal concentration.
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Abstract
Description
本発明は、容器、特に試料分析用に好適な容器に関する。 The present invention relates to a container, particularly a container suitable for sample analysis.
分析試料用の容器として、例えば、ガスクロマトグラフオートサンプラ用に対応する一般的な寸法及び容積を有するバイアルと呼ばれる容器がある(例えば、下記特許文献1参照)。このような容器で取り扱う試料は、容器に入れてオートサンプラにセットされる前に、前処理を施される場合がある。例えば、試料は、遠心濃縮機によって濃縮される。
As a container for an analysis sample, for example, there is a container called a vial having a general size and volume corresponding to a gas chromatograph autosampler (see, for example,
近時、上記のバイアルで取り扱う試料について、例えば、遠心濃縮機による濃縮前の試料の分量が大量である場合も発生している。他の前処理でも、同様の場合がある。
このような大量の試料は、寸法及び容積が一定のバイアルには入りきれない。そのため、大量の試料は、まず、遠心濃縮機による濃縮など前処理を施されるために、バイアルとは別のより大容量の前処理用の容器に入れて前処理を施される。そしてその後、前処理が施された試料は、前処理用の容器からバイアルに移し換えられ、バイアルは、オートサンプラにセットされる。
Recently, with regard to the sample handled in the above-mentioned vial, for example, the amount of the sample before concentration by the centrifugal concentrator is large. The same applies to other pre-processing.
Such a large sample cannot fit into a vial of constant size and volume. Therefore, since a large amount of sample is first subjected to pretreatment such as concentration by a centrifugal concentrator, it is pretreated in a larger volume pretreatment container separate from the vial. After that, the pretreated sample is transferred from the pretreatment container to the vial, and the vial is set in the autosampler.
しかしながら、このような作業順序で取り扱われる試料は、前処理用の容器からバイアルに移し換える際にコンタミネーションの発生とロスが懸念される。また、このような問題点は、試料分析用及び遠心濃縮用の容器以外の容器においても、同様に発生し得る。 However, there is a concern that the sample handled in such a work order may cause contamination and loss when it is transferred from the pretreatment container to the vial. Further, such a problem may occur in a container other than the sample analysis container and the centrifugal concentration container.
本発明は、収容される収容物の容積が大幅に変更になることに容易に対応することができる容器を提供することを目的とする。 The object of the present invention is to provide a container that can easily cope with a large change in the volume of the contained items.
本発明は、第1収容部を有する外挿容器本体と、第2収容部を有する内挿容器本体とを備える容器であって、内挿容器本体が外挿容器本体に内挿されると共に、内挿容器本体が外挿容器本体に対してスライドすることで、第1収容部と第2収容部とからなる収容部の容積が増減し、外挿容器本体及び内挿容器本体は、スライド方向を回転軸とする相対的な回転が規制されており、内挿容器本体は、スライド位置に拘わらず、外挿容器本体の第1収容部の内面を押圧してシールする押圧シール部を備える、容器に関する。 The present invention is a container comprising an extrapolation container main body having a first accommodation part and an insertion container main body having a second accommodation part, and the insertion container main body is inserted into the extrapolation container main body, By sliding the insertion container main body relative to the extrapolation container main body, the volume of the storage part composed of the first storage part and the second storage part increases or decreases, and the extrapolation container main body and the insertion container main body change the sliding direction. Relative rotation as a rotation axis is restricted, and the inner container body includes a pressure seal portion that presses and seals the inner surface of the first housing portion of the extrapolation container body regardless of the slide position. About.
また、外挿容器本体は、内挿容器本体よりも変形しやすい素材から形成される、ことが好ましい。 Further, it is preferable that the extrapolation container body is formed of a material that is more easily deformed than the insertion container body.
また、外挿容器本体又は内挿容器本体の一方は、スライドを実現するため及び相対的な回転を規制するための凸部を有し、外挿容器本体又は内挿容器本体の他方は、凸部が配置される凹部であって、スライドを実現するため及び相対的な回転を規制するための凹部を有し、凸部及び凹部は、外挿容器本体及び内挿容器本体に所定角度の相対的な回転を許容する、ことが好ましい。 Further, one of the extrapolation container body and the insertion container body has a convex part for realizing sliding and restricting relative rotation, and the other of the extrapolation container body or the insertion container body is convex. A recessed portion in which the portion is disposed, and has a recessed portion for realizing sliding and restricting relative rotation, and the protruding portion and the recessed portion are relative to the extrapolation container body and the insertion container body at a predetermined angle. It is preferable to allow general rotation.
また、外挿容器本体及び内挿容器本体は、押圧シール部の押圧により任意のスライド位置に保持可能である、ことが好ましい。 In addition, it is preferable that the extrapolation container body and the insertion container body can be held at an arbitrary slide position by pressing the pressing seal portion.
また、外挿容器本体又は内挿容器本体のうち試料が収容される容器本体を下容器本体といい、他方の容器本体を上容器本体という場合に、下容器本体は、上容器本体よりも試料に対する耐性が高い素材から形成される、ことが好ましい。 In addition, when the outer container body or the inner container body in which the sample is stored is referred to as the lower container body and the other container body is referred to as the upper container body, the lower container body is more sample than the upper container body. It is preferable that the material is formed from a material having high resistance to.
また、外挿容器本体及び内挿容器本体をスライドさせて伸ばした状態で収容部に収容された試料を遠心濃縮機で濃縮させる遠心濃縮用であると共に、遠心濃縮がされた後に外挿容器本体及び内挿容器本体をスライドさせて縮めた状態で、遠心濃縮された試料を試料分析器で分析させる試料分析用である、ことが好ましい。 Also, the extrapolation container main body and the extrapolation container main body after being concentrated by centrifugal concentrating with the centrifugal concentrator for concentrating the sample accommodated in the accommodating portion in a state where the extrapolation container main body is slid and extended. In addition, it is preferably used for sample analysis in which the centrifugally concentrated sample is analyzed by a sample analyzer while the insertion container body is slid and contracted.
本発明によれば、収容される収容物の容積が大幅に変更になることに容易に対応することができる容器を提供することができる。 According to the present invention, it is possible to provide a container that can easily cope with a large change in the volume of the accommodated item.
以下、本発明の一実施形態に係る容器について、図面を参照しながら説明する。図1は、内挿容器本体3が外挿容器本体2に内挿されて組み立てられた容器1において、容器1を縮めた状態で示す斜視図である。図2は、図1の容器1を一部縦断面にして示す部分縦断正面図である。図3は、図1の容器1を図2のA-A線に沿って切断して示す横断面図である。図4は、図1の容器1を伸ばした状態で示す縦断視図である。図5は、図1の容器1を構成する外挿容器本体2を単体で示す縦断視図である。図6は、図4に示す外挿容器本体2の平面図である。図7は、図1の容器1を構成する内挿容器本体3を単体で示す側視図である。図8は、図7のB-B線に沿って切断した横断視図である。図9は、図4のC矢視部分を拡大して示す部分拡大図である。
Hereinafter, a container according to an embodiment of the present invention will be described with reference to the drawings. FIG. 1 is a perspective view showing a state in which the
図1~図8に示すように、本実施形態に係る容器1は、第1収容部20を有する外挿容器本体2と、第2収容部30を有する内挿容器本体3と、蓋体(図示せず)と、を備える。第1収容部20と第2収容部30とは、容器1の全体の収容部10を構成する。
まず、図5、図6、図9などを参照して外挿容器本体2について説明する。
As shown in FIGS. 1 to 8, the
First, the extrapolation container
[外挿容器本体2]
外挿容器本体2は、容器1の下半分を構成する下容器本体であり、第1収容部20(後述)と、周壁21と、底壁22と、試料溜め23と、を備える。周壁21は、円筒状を呈し、外挿容器本体2の上端から下端まで延びる。周壁21の下端から所定の高さH1、高い部分(以下「連なり部215」ともいう)には、底壁22が連なる。周壁21の上端から連なり部215の高さH1までの範囲(高さ)H5における内周面(内面)211は、後述する凸部212及び環状凸部213を除き、円筒面である。
[Extrapolation container body 2]
The extrapolation container
底壁22は、連なり部215において周壁21と連なる。底壁22は、この連なり部215から周壁21の中心軸線CL1に向けて緩やかに下向きに延びて、試料溜め23の上端に連なる。試料溜め23は、周壁21と同心に配置される小さな凹状の空間である。試料溜め23は、上端から縦壁231が下方へ延びて、底部232に至る。底部232の内部空間は、逆円錐状を呈し、周壁21の中心軸線CL1と一致する位置に最深部233を有する。底部232の下端は、周壁21の下端と同じ高さに位置する。
The
図6に示すように、周壁21の上端部には、平面視で内周面211から半径方向内向きに突出する凸部212が、4つ設けられる。4つの凸部212は、周壁21の円周方向に沿って互いに略90°の間隔を置いて配置される。各凸部212は、大きさ、形状ともに略同一である。
As shown in FIG. 6, the upper end portion of the
図9に示すように、各凸部212は、内周面211の上端から斜め下方に延びる第1の傾斜面2121と、内周面211の上端から所定の高さH2、低い部分から斜め上方に延びる第2の傾斜面2122と、第1の傾斜面2121の下端縁と第2の傾斜面2122の上端縁とを繋ぐ突出面2123と、第1の側面2124(図5参照)と、第2の側面2125(図5参照)と、を有する。
As shown in FIG. 9, each
縦断面視において、各凸部212の突出面2123は、内周面211と略平行に配置される。各凸部212の突出量、すなわち内周面211と突出面2123との間の半径方向の距離P1は、いずれも同一である。
In the longitudinal sectional view, the
第1の傾斜面2121に比べて、第2の傾斜面2122は、内周面211に対する勾配がより緩やかである。図5に示すように、第1の側面2124及び第2の側面2125は、垂直面に対して、上方よりも下方に近づくにつれて互いの間の距離が離れるように僅かに傾斜している。
Compared with the first
周壁21の各凸部212の上端から所定の高さH3(>H2)、低い部分には、内周面211の領域を介して、内周面211から半径方向内向きに突出する環状凸部213が設けられる。環状凸部213は、周壁21の円周方向に沿って360°切れ目なく(全周に)設けられる。
An annular convex portion protruding inward in the radial direction from the inner
図9に示すように、環状凸部213は、内周面211から半径方向内向きに最も突出する環状の突出縁部2131を有する。突出縁部2131の上側における湾曲面は、内周面211に対して屈曲して連なる。突出縁部2131の下側における傾斜面は、内周面211と滑らかに連なる。
As shown in FIG. 9, the annular
環状凸部213の突出量P2(すなわち内周面211と突出縁部2131との間の半径方向の距離P2)は、各凸部212の突出量P1よりも小さい(P2<P1)。
The protrusion amount P2 of the annular protrusion 213 (that is, the radial distance P2 between the inner
図4に示すように、外挿容器本体2の上端から周壁21、底壁22及び試料溜め23によって囲まれる空間のうち、容器1を伸ばした状態において内挿容器本体3によって占められる領域を除く空間は、第1収容部20を構成する。第1収容部20は、内径R1、中心軸線CL1を有する。
As shown in FIG. 4, the space occupied by the
次に、図7、図8、図9などを参照して、内挿容器本体3について説明する。
[内挿容器本体3]
内挿容器本体3は、後述するように、第2収容部30を有する。
内挿容器本体3は、上端から下端まで貫通した略円筒状を呈する。内挿容器本体3は、中心軸線CL2を有する。内挿容器本体3は、後述するように、外挿容器本体2に内挿された状態において、容器1を縮めた状態(図2参照)と、容器1を伸ばした状態(図4参照)との間をスライドするように構成される。
Next, the
[Insertion container body 3]
The insertion container
The
内挿容器本体3は、下から上へ順に、押圧シール部31と、回転規制部32と、口部33と、を備える。押圧シール部31は、内挿容器本体3が外挿容器本体2に圧入により一旦内挿されると、使用中においては、常時、内挿容器本体3の内部に位置する。回転規制部32は、使用中において、容器1を縮めた状態では、内挿容器本体3の内部に位置する。回転規制部32は、使用中において、容器1を伸ばした状態では、内挿容器本体3の外方に位置する。口部33は、常時(容器1の伸縮に拘わらず)、内挿容器本体3の外方に位置する。
The insertion container
押圧シール部31は、内挿容器本体3の下端から所定高さの位置まで占める。押圧シール部31は、円筒状を呈し、外周基準面311と、第1の環状シール部312と、第2の環状シール部313と、内周面314と、を備える。図9に示すように、外周基準面311の直径R2は、第1収容部20の内径R1よりも小さい(R2<R1)。図8、図9に示すように、内周面314は、直径R3を有する。
The
上記の外挿容器本体2における環状凸部213の突出量P2は、第1収容部20の内径R1と、押圧シール部31の外周基準面311の直径R2との差(R1-R2)の半分に等しい。すなわち、押圧シール部31の外周基準面311の直径R2に、環状凸部213の突出量P2の2倍を加味すると、第1収容部20の内径R1と一致する(R1=R2+2×P2)。そのため、外挿容器本体2における第1収容部20の環状凸部213の位置に、内挿容器本体3における押圧シール部31の外周基準面311が内挿される場合、外挿容器本体2の中心軸線CL1と、内挿容器本体3の中心軸線CL2とは、互いに芯合わせされて一致することができる。
The protrusion amount P2 of the annular
第1の環状シール部312は、押圧シール部31の下端において、外周基準面311から半径方向外向きに突出する。
図9に示すように、第1の環状シール部312は、外周基準面311から半径方向外向きに最も突出する環状のシール縁部3121を有する。シール縁部3121の上側における湾曲面は、外周基準面311と滑らかに連なる。シール縁部3121の下側における湾曲面は、押圧シール部31の下面に連なる。
The first
As shown in FIG. 9, the first
第2の環状シール部313は、第1の環状シール部312の上方において、外周基準面311の領域を介して、外周基準面311から半径方向外向きに突出する。
図9に示すように、第2の環状シール部313は、第1の環状シール部312と同様に、外周基準面311から半径方向外向きに最も突出する環状のシール縁部3131を有する。シール縁部3131の上側における湾曲面も、シール縁部3131の下側における湾曲面も、外周基準面311と滑らかに連なる。
The second
As shown in FIG. 9, the second
第1の環状シール部312及び第2の環状シール部313の外径R4は、第1収容部20の内径R1よりも大きい(R4>R1)。押圧シール部31において、第1の環状シール部312の突出量P3(すなわち外周基準面311とシール縁部3121との間の半径方向の距離P3)、及び、第2の環状シール部313の突出量P3(すなわち外周基準面311とシール縁部3131との間の半径方向の距離P3)は、同一である。
The outer diameter R4 of the first
第1の環状シール部312及び第2の環状シール部313の突出量P3は、上記の外挿容器本体2における環状凸部213の突出量P2よりも大きい(P3>P2)。そのため、外挿容器本体2の第1収容部20における任意の高さに、内挿容器本体3における第1の環状シール部312及び第2の環状シール部313が内挿された場合であっても、第1の環状シール部312の環状のシール縁部3121、及び第2の環状シール部313の環状のシール縁部3131は、第1収容部20の内周面211を半径方向外向きに押圧して、シールすることができる。
The protrusion amount P3 of the first
図7、図8に示すように、回転規制部32は、押圧シール部31の上方に隣接して配置される。回転規制部32は、円筒状を呈し、外周面321と、4つの凹部322と、上部フランジ323と、内周面324と、を備える。外周面321の直径R2は、押圧シール部31の外周基準面311の直径R2と同一である。内周面324の直径R3は、押圧シール部31の内周面314の直径R3と同一である。押圧シール部31の内周面314及び回転規制部32の内周面324によって囲まれる空間は、第2収容部30を構成する。第2収容部30は、内径R3、中心軸線CL2を有する。
7 and 8, the
4つの凹部322は、外周面321の上端から下端まで、外周面321から半径方向内向きに削り取られた凹部である。各凹部322は、回転規制部32の円周方向に沿って略90°の範囲に亘って設けられる。4つの凹部322は、回転規制部32の円周方向に沿って互いに略90°の間隔を置いて配置される。各凹部322は、大きさ、形状ともに略同一である。
The four
図7に示すように、各凹部322は、外周面321よりも半径方向内側に外周面321と平行に配置される内側面3221と、上部フランジ323の下面からその奥側に連なる上面3222と、押圧シール部31の上面となる下面3223と、第1の側面3224(図8参照)と、第2の側面3225(図8参照)と、を有する。
As shown in FIG. 7, each
見方を変えると、回転規制部32は、外周面321において4つの凹部322が削り取られた結果、残りの上下方向に延びる外周面321と、その右方に隣接する凹部322の第1の側面3224と、左方に隣接する別の凹部322の第2の側面3225とによって構成されるリブ状の突起が4つ、回転規制部32の円周方向に沿って互いに略90°の間隔を置いて配置されていると、見ることもできる。
In other words, the
各凹部322の深さD1(すなわち外周面321と内側面3221との間の半径方向の距離D1)は、いずれも同一である。
上記の外挿容器本体2における各凸部212の突出量P1(すなわち内周面211と突出面2123との間の半径方向の距離P1)は、外挿容器本体2における環状凸部213の突出量P2(すなわち内周面211と突出縁部2131との間の半径方向の距離P2)よりも大きく(P1>P2)、そして、環状凸部213の突出量に各凹部322の深さを加えた距離よりも小さい(P1<P2+D1)。
The depth D1 of each recess 322 (that is, the radial distance D1 between the outer
The protrusion amount P1 of each
そのため、内挿容器本体3における回転規制部32が外挿容器本体2に内挿される場合、外挿容器本体2における第1収容部20の4つの凸部212は、内挿容器本体3における回転規制部32の4つの凹部322に、それぞれ収容される。
その結果、外挿容器本体2及び内挿容器本体3の相対的回転は、外挿容器本体2における4つの凸部212が内挿容器本体3における4つの凹部322の内部に位置する範囲(すなわち約90°の範囲)に制限されることができる。
Therefore, when the
As a result, the relative rotation of the
内挿容器本体3は、回転規制部32の範囲内において、外挿容器本体2に対して出没可能である。
具体的には、図2に示すように、内挿容器本体3は、上部フランジ323の下面が外挿容器本体2の上面に接する高さまで、外挿容器本体2に挿入されることができる。このとき、容器1は、縮めた状態にある。
そのため、内挿容器本体3における押圧シール部31及び回転規制部32を加えた長さH4(図4参照。上部フランジ323の下面から押圧シール部31の下端までの長さH4)は、外挿容器本体2の上端から周壁21と底壁22との連なり部215までの長さH5(図4参照)よりも短い。
The
Specifically, as shown in FIG. 2, the insertion container
Therefore, the length H4 (see FIG. 4, the length H4 from the lower surface of the
また、図4に示すように、内挿容器本体3は、押圧シール部31と回転規制部32との境界315(図9参照。すなわち回転規制部32の下面3223)が外挿容器本体2における凸部212の第2の傾斜面2122に当接する高さH6まで、外挿容器本体2から引き出されることができる。このとき、容器1は、伸ばした状態にある。
このように、内挿容器本体3は、外挿容器本体2に対してスライドすることができる。
As shown in FIG. 4, the
Thus, the
図4、図9に示すように、容器1を伸ばした状態において、内挿容器本体3における回転規制部32の下面3223が外挿容器本体2における凸部212の第2の傾斜面2122に当接するため、内挿容器本体3は、外挿容器本体2からこれ以上引き出されることができない。そのため、外挿容器本体2からの内挿容器本体3の抜けは、的確に防止される。
As shown in FIGS. 4 and 9, the
口部33は、回転規制部32の上方に連なる。図4に示すように、口部33は、円筒状を呈し、外周面331と、ねじ山332と、内周面333と、を備える。ねじ山332は、蓋体(不図示)に設けられる対応するねじ山と螺合するためのものである。口部33の内周面333は、押圧シール部31及び回転規制部32の内周面314、324よりも小径である。
The
[外挿容器本体2と内挿容器本体3との連携]
次に、全図を参照して、本実施形態に係る容器1について説明する。
すなわち、内挿容器本体3を外挿容器本体2に圧入により内挿して容器1を組み立てる。組み立てられた容器1において、内挿容器本体3及び外挿容器本体2は、図2に示す縮めた状態と、図4に示す伸ばした状態との間を、軸線方向に相対的にスライド可能である。そのため、内挿容器本体3及び外挿容器本体2を相対的にスライドさせることにより、容器1の収容部10の容積は、設計上可能な範囲で任意に増減する。
[Cooperation between
Next, the
That is, the
具体的には、図4に示す伸ばした状態では、容器1の収容部10の容積は、第1収容部20の容積及び第2収容部30の容積を加えた容積となる。一方、図2に示す縮めた状態では、第1収容部20の大部分の容積をそれに代わって第2収容部30の容積が占めるため、第2収容部30の容積に近似したそれよりも僅かに大きい容積が、容器1の収容部10の容積となる。
例えば、縮めた状態でオートサンプラの規格に適合する容器1を用いて、伸ばした状態において、より大量の試料を容器1に収容することが可能となる。
Specifically, in the extended state shown in FIG. 4, the volume of the
For example, it is possible to store a larger amount of sample in the
容器1において、外挿容器本体2及び内挿容器本体3は、スライド方向を回転軸CL1、CL2とする相対的な回転が規制される。外挿容器本体2の凸部212及び内挿容器本体3の凹部322は、スライドを実現するため及び相対的な回転を規制するために設けられる。詳述すると、外挿容器本体2における第1収容部20の4つの凸部212は、内挿容器本体3における回転規制部32の4つの凹部322に、それぞれ収容されて配置される。そのため、外挿容器本体2及び内挿容器本体3の相対的回転は、外挿容器本体2における4つの凸部212が内挿容器本体3における4つの凹部322の内部に位置する範囲(すなわち約90°の範囲)に制限される。
In the
外挿容器本体2は、内挿容器本体3よりも変形しやすい素材から形成される。外挿容器本体2は、試料に対する高い耐性が要求されるため、PFA(ポリテトラフルオロエチレン)で作製する。内挿容器本体3は、試料に直接接触しにくいため、PFAに比べてより安価なPP(ポリプロピレン)、PE(ポリエチレン)で作製する。PFAは、PP、PEに比べてより変形しやすい。外挿容器本体2及び内挿容器本体3は、射出成形、切削加工などにより形成される。
The
内挿容器本体3における押圧シール部31の第1の環状シール部312及び第2の環状シール部313は、容器1を縮めた状態から伸ばした状態までの任意のスライド位置において、外挿容器本体2における第1収容部20の内周面211を押圧シールすることができる。
加えて、内挿容器本体3の押圧シール部31による外挿容器本体2の第1収容部20に対する押圧シールが任意のスライド位置で発揮されるため、内挿容器本体3及び外挿容器本体2は、押圧シール部31の押圧により任意のスライド位置に保持可能である。
The first
In addition, since the pressure seal with respect to the
具体的には、外挿容器本体2をPFA製とし、内挿容器本体3をPP又はPE製とすることにより、外挿容器本体2は、内挿容器本体3に比べてより変形しやすい。そのため、内挿容器本体3における押圧シール部31の第1の環状シール部312及び第2の環状シール部313が外挿容器本体2における第1収容部20の内周面211を押圧シールする際に、第1収容部20の内周面211は、押圧シール部31の第1の環状シール部312及び第2の環状シール部313によって外方へ押されて、いくらか膨らむ。そして、第1収容部20の内周面211は、その膨らみを元の状態に復元する方向に作用するため、押圧シール部31の第1の環状シール部312及び第2の環状シール部313と協働するシール面をより強固にシールする結果となる。
Specifically, the
加えて、内挿容器本体3及び外挿容器本体2を任意のスライド位置に保持する点でも、PFA製の外挿容器本体2と、PP又はPE製の内挿容器本体3との組み合わせは、その保持機能をより高める作用を発揮する。
In addition, the combination of the PFA extrapolating container
容器1の実際の応用では、例えば、外挿容器本体2及び内挿容器本体3をスライドさせて伸ばした状態において、容器1は、第1収容部20及び第2収容部30に収容された試料を遠心濃縮機で濃縮させる遠心濃縮用の容器として使用される。図4に示すように、内挿容器本体3を外挿容器本体2から最大限まで伸ばした位置において、容器1は、上記のシール機能及び保持機能により強固にロックされる。その理由は、図9に示すように、内挿容器本体3における押圧シール部31と回転規制部32との境界315の外縁が外挿容器本体2における凸部212の第2の傾斜面2122に当接して、傾斜面2122からの反力を受けるからである。容器1は、この状態で、後述するように、遠心濃縮機に掛けられる。
In an actual application of the
一方、遠心濃縮がされた後に、外挿容器本体2及び内挿容器本体3をスライドさせて縮めた状態において、容器1は、遠心濃縮された試料を試料分析器で分析させる試料分析用の容器として使用される。しかも、遠心濃縮用の容器として使用される容器1と、試料分析用の容器として使用される容器1は、容器1を伸ばした状態から縮めた状態に変形させただけの同じ容器であり、試料の移し換えは不要である。
On the other hand, after centrifugal concentration, the
[実施形態の効果]
上述した本実施形態の容器1によれば、例えば、以下のような様々な効果が奏される。
容器1は、内挿容器本体3及び外挿容器本体2を、図2に示す縮めた状態から図4に示す伸ばした状態まで、相対的にスライド可能である。それにより、容器1の収容部10の容積は、設計上可能な範囲で任意に増減可能である。
そのため、例えば、縮めた状態で所定の装置の規格に適合する寸法及び容積で容器1を作製することができる。そして、この容器1には、伸ばした状態で規格を上回るより大量の試料を収容することができる。
[Effect of the embodiment]
According to the
The
Therefore, for example, the
容器1において、外挿容器本体2及び内挿容器本体3の相対的回転は、外挿容器本体2における4つの凸部212が内挿容器本体3における4つの凹部322の内部に位置する範囲(すなわち約90°の範囲)に制限される。
そのため、例えば、容器1を所定の装置にセットする際に外挿容器本体2を回転させた場合に、内挿容器本体3は、最大約90°遅れるだけで外挿容器本体2と共に回転することができて、外挿容器本体2及び内挿容器本体3の一体的回転を実現することができる。
In the
Therefore, for example, when the
容器1において、内挿容器本体3における4つの凹部322の各々は、回転規制部32の円周方向に沿って、例えば60°以上の範囲、具体的には略90°の範囲に亘って設けられる。このように幅の広い凹部322の成形は、幅の狭い凹部の成形に比べてより容易である。そのため、回転規制部32ひいては内挿容器本体3を、そしてその結果、容器1を、比較的低コストで作製することができる。
換言すれば、回転が実質的に許容されない凸部と凹部との組合せでスライドを実現する場合、細く長い凹部を形成する必要がある。しかし、そのような凹部の形成は容易ではない。一方、所定角度の回転が許容されれば、すなわち、凹部の幅を広くできれば、凹部の形成は容易である。
In the
In other words, when a slide is realized by a combination of a convex portion and a concave portion that are substantially not allowed to rotate, it is necessary to form a thin and long concave portion. However, formation of such a recess is not easy. On the other hand, if rotation of a predetermined angle is allowed, that is, if the width of the recess can be increased, the formation of the recess is easy.
容器1において、内挿容器本体3における押圧シール部31の第1の環状シール部312及び第2の環状シール部313は、容器1を縮めた状態から伸ばした状態までどの位置にあっても、外挿容器本体2における第1収容部20の内周面211を変わりなく押圧シールする。
そのため、容器1を伸縮する際に、容器1内に異物が混入する虞を未然に回避することができる。
In the
For this reason, when the
外挿容器本体2(例えばPFA製)は、内挿容器本体3(例えばPP製、PE製)よりも変形しやすい素材から形成される。
そのため、押圧シール部31の第1の環状シール部312及び第2の環状シール部313による外挿容器本体2における第1収容部20の内周面211の押圧変移量を多く確保しやすく、安定した押圧によるシールを実現しやすい。
The extrapolation container body 2 (for example, made of PFA) is formed of a material that is more easily deformed than the insertion container body 3 (for example, made of PP or PE).
Therefore, the first
外挿容器本体2及び内挿容器本体3は、押圧シール部31の押圧により任意のスライド位置に保持可能である。
そのため、任意のスライド位置に保持させるための別の構成を設けなくても、保持を実現できる。
The
Therefore, the holding can be realized without providing another configuration for holding at an arbitrary slide position.
外挿容器本体2又は内挿容器本体3のうち試料が収容される容器本体を下容器本体といい、他方の容器本体を上容器本体という場合に、下容器本体は、上容器本体よりも試料に対する耐性が高い素材から形成される。
試料に対する耐性が高い素材は、比較的高価であったり、成形性が低い等の制約が有ることが多い。下容器本体だけ試料に対する耐性が高い素材から形成すれば、上容器本体は、制約を回避する素材を採用できる。
Of the
A material having high resistance to a sample often has limitations such as being relatively expensive and having low moldability. If only the lower container main body is formed from a material having high resistance to the sample, the upper container main body can employ a material that avoids restrictions.
容器1は、外挿容器本体2及び内挿容器本体3をスライドさせて伸ばした状態で第1収容部20及び第2収容部30に収容された試料を遠心濃縮機で濃縮させる遠心濃縮用であると共に、遠心濃縮がされた後に外挿容器本体2及び内挿容器本体3をスライドさせて縮めた状態で、遠心濃縮された試料を試料分析器で分析させる試料分析用である。
そのため、遠心濃縮された試料を試料分析用の別の容器に移し換えなくても、試料分析に用いることができるため、容器1を移し換えるときの試料へのコンタミネーションを抑制することができる。
The
Therefore, it is possible to use for sample analysis without transferring the centrifugally concentrated sample to another container for sample analysis. Therefore, contamination of the sample when the
[変形例]
以上、本発明の好適な実施形態について説明したが、本発明は、上述した実施形態に限定されることなく、種々の形態で実施することができる。
[Modification]
As mentioned above, although preferred embodiment of this invention was described, this invention can be implemented with a various form, without being limited to embodiment mentioned above.
上記実施形態では、押圧シール部31に第1の環状シール部312及び第2の環状シール部313を設けたが、これに限定されない。例えば、第2の環状シール部313を省略して、第1の環状シール部312のみで押圧シール部31を構成してもよい。
In the above embodiment, the first
また、上記実施形態では、外挿容器本体2をPFA製とし、内挿容器本体3をPP又はPE製としたが、これに限定されない。例えば、外挿容器本体2だけでなく内挿容器本体3についても試料に対する耐性が高い素材が求められる場合には、内挿容器本体3をPFA製としてもよい。
In the above embodiment, the
また、上記実施形態では、外挿容器本体2における内周面211に凸部212を設け、内挿容器本体3における回転規制部32の外周面321に凹部322を設けたが、これに限定されない。例えば、外挿容器本体2における内周面211に凹部を設け、内挿容器本体3における回転規制部32の外周面321に凸部を設けてもよい。
Moreover, in the said embodiment, although the
また、上記実施形態では、外挿容器本体2を下容器本体とし、内挿容器本体3を上容器本体としたが、これに限定されない。例えば、内挿容器本体3を下容器本体とし、外挿容器本体2を上容器本体としてもよい。その場合、下容器本体としての内挿容器本体3は、試料に対する耐性が高い素材が求められるからPFA製とし、上容器本体としての外挿容器本体2は、PP又はPE製としてもよい。
本発明は、試料分析用及び遠心濃縮用の容器以外の容器に適用することができる。
Moreover, in the said embodiment, although the extrapolation container
The present invention can be applied to containers other than those for sample analysis and centrifugal concentration.
1 容器
10 収容部
2 外挿容器本体(下容器本体)
20 第1収容部
211 内周面(内面)
212 凸部
3 内挿容器本体(上容器本体)
30 第2収容部
31 押圧シール部
322 凹部
CL1 中心軸線(回転軸)
CL2 中心軸線(回転軸)
DESCRIPTION OF
20
212 Convex 3 Insertion container body (upper container body)
30
CL2 center axis (rotary axis)
Claims (6)
前記内挿容器本体が前記外挿容器本体に内挿されると共に、前記内挿容器本体が前記外挿容器本体に対してスライドすることで、前記第1収容部と前記第2収容部とからなる収容部の容積が増減し、
前記外挿容器本体及び前記内挿容器本体は、スライド方向を回転軸とする相対的な回転が規制されており、
前記内挿容器本体は、スライド位置に拘わらず、前記外挿容器本体の前記第1収容部の内面を押圧してシールする押圧シール部を備える、容器。 A container comprising an extrapolation container body having a first housing part and an insertion container body having a second housing part,
The insertion container main body is inserted into the extrapolation container main body, and the insertion container main body slides with respect to the extrapolation container main body, thereby including the first storage portion and the second storage portion. The volume of the storage part increases or decreases,
The extrapolation container body and the insertion container body are restricted in relative rotation with the slide direction as the rotation axis,
The said insertion container main body is a container provided with the press seal part which presses and seals the inner surface of the said 1st accommodating part of the said extrapolation container main body irrespective of a slide position.
前記凸部及び前記凹部は、前記外挿容器本体及び前記内挿容器本体に所定角度の相対的な回転を許容する、請求項1又は2に記載の容器 One of the extrapolation container body or the insertion container body has a convex part for realizing sliding and restricting relative rotation, and the other of the extrapolation container body or the insertion container body is A concave portion in which the convex portion is disposed, and has a concave portion for realizing sliding and restricting relative rotation,
The container according to claim 1, wherein the convex part and the concave part allow relative rotation of a predetermined angle to the extrapolation container body and the insertion container body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2016/075453 WO2018042537A1 (en) | 2016-08-31 | 2016-08-31 | Container |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2016/075453 WO2018042537A1 (en) | 2016-08-31 | 2016-08-31 | Container |
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| Publication Number | Publication Date |
|---|---|
| WO2018042537A1 true WO2018042537A1 (en) | 2018-03-08 |
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| Application Number | Title | Priority Date | Filing Date |
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|---|---|---|---|---|
| US3905528A (en) * | 1974-04-10 | 1975-09-16 | Hugh V Maiocco | Two-piece concentric centrifuge sample container |
| JPS57180634U (en) * | 1982-01-07 | 1982-11-16 | ||
| JPH06130812A (en) * | 1992-10-22 | 1994-05-13 | Ricoh Co Ltd | Toner supply device |
| JP3020665U (en) * | 1995-02-06 | 1996-02-06 | 高明 加藤 | 2-stage tube |
| JP2006289222A (en) * | 2005-04-08 | 2006-10-26 | Dai Ichi Seiyaku Co Ltd | Method and centrifuge tube for collecting marrow of experimental small animal |
| JP2011515149A (en) * | 2008-03-21 | 2011-05-19 | サイエンティフィック プラスティック プロダクツ インコーポレイテッド | Filter vial having a tubular piston, a retaining cup, and a filter |
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| JP2015502851A (en) * | 2011-12-06 | 2015-01-29 | バム ハ リー, | Centrifuge container |
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2016
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3905528A (en) * | 1974-04-10 | 1975-09-16 | Hugh V Maiocco | Two-piece concentric centrifuge sample container |
| JPS57180634U (en) * | 1982-01-07 | 1982-11-16 | ||
| JPH06130812A (en) * | 1992-10-22 | 1994-05-13 | Ricoh Co Ltd | Toner supply device |
| JP3020665U (en) * | 1995-02-06 | 1996-02-06 | 高明 加藤 | 2-stage tube |
| JP2006289222A (en) * | 2005-04-08 | 2006-10-26 | Dai Ichi Seiyaku Co Ltd | Method and centrifuge tube for collecting marrow of experimental small animal |
| JP2011515149A (en) * | 2008-03-21 | 2011-05-19 | サイエンティフィック プラスティック プロダクツ インコーポレイテッド | Filter vial having a tubular piston, a retaining cup, and a filter |
| JP2012115829A (en) * | 2010-11-09 | 2012-06-21 | Jms Co Ltd | Separation container, and separation method |
| JP2015502851A (en) * | 2011-12-06 | 2015-01-29 | バム ハ リー, | Centrifuge container |
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