AU603566B2 - Silicon nitride powders for ceramics by carbothermic reduction and the process for the manufacture thereof - Google Patents
Silicon nitride powders for ceramics by carbothermic reduction and the process for the manufacture thereofInfo
- Publication number
- AU603566B2 AU603566B2 AU71037/87A AU7103787A AU603566B2 AU 603566 B2 AU603566 B2 AU 603566B2 AU 71037/87 A AU71037/87 A AU 71037/87A AU 7103787 A AU7103787 A AU 7103787A AU 603566 B2 AU603566 B2 AU 603566B2
- Authority
- AU
- Australia
- Prior art keywords
- manufacture
- ceramics
- silicon nitride
- powders
- carbothermal reduction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 4
- 239000000843 powder Substances 0.000 title abstract 4
- 229910052581 Si3N4 Inorganic materials 0.000 title abstract 3
- 239000000919 ceramic Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 title abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 4
- 238000006722 reduction reaction Methods 0.000 abstract 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 239000008187 granular material Substances 0.000 abstract 2
- 239000000377 silicon dioxide Substances 0.000 abstract 2
- 239000011230 binding agent Substances 0.000 abstract 1
- 230000001747 exhibiting effect Effects 0.000 abstract 1
- 238000005121 nitriding Methods 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 239000011148 porous material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/068—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with silicon
- C01B21/0685—Preparation by carboreductive nitridation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Ceramic Products (AREA)
- Silicon Compounds (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Silicon Polymers (AREA)
Abstract
Silicon nitride Si3N4 powders by a silica carbothermal reduction and nitriding route, capable of being employed especially for the manufacture of ceramics and exhibiting a specific surface of at least 30 m<2>/g. Process for the manufacture of the powders comprising the following stages: a) From silica, from a binder generating carbon not later than during the carbothermal reduction reaction and, if appropriate, from additional carbon, manufacture of granules with a controlled pore volume. b) Carbothermal reduction reaction of the granules obtained under a, in the presence of an atmosphere containing nitrogen. c) Decarburisation. d) Obtaining powders. h
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8604764A FR2596746B1 (en) | 1986-04-03 | 1986-04-03 | POWDERS FOR CARBOTHERMAL REDUCTION SILICON NITRIDE CERAMICS AND THEIR MANUFACTURING METHOD |
| FR8604764 | 1986-04-03 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU7103787A AU7103787A (en) | 1987-10-08 |
| AU603566B2 true AU603566B2 (en) | 1990-11-22 |
Family
ID=9333845
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU71037/87A Ceased AU603566B2 (en) | 1986-04-03 | 1987-04-03 | Silicon nitride powders for ceramics by carbothermic reduction and the process for the manufacture thereof |
Country Status (12)
| Country | Link |
|---|---|
| EP (1) | EP0240414B1 (en) |
| JP (1) | JP2610867B2 (en) |
| CN (1) | CN1007888B (en) |
| AT (1) | ATE72204T1 (en) |
| AU (1) | AU603566B2 (en) |
| DE (1) | DE3776376D1 (en) |
| DK (1) | DK167865B1 (en) |
| ES (1) | ES2039468T3 (en) |
| FR (1) | FR2596746B1 (en) |
| GR (1) | GR3004228T3 (en) |
| IE (1) | IE59544B1 (en) |
| NO (1) | NO170208C (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2678602A1 (en) * | 1991-07-02 | 1993-01-08 | Atochem | PROCESS FOR THE PREPARATION OF SILICON NITRIDE BY SILICA CARBONITRURATION AND SILICON NITRIDE AS PARTICLES EXEMPT FROM WHISKEY. |
| JP4844709B2 (en) * | 2005-03-18 | 2011-12-28 | 戸田工業株式会社 | Method for producing silicon nitride powder |
| RU2572425C2 (en) * | 2009-10-30 | 2016-01-10 | Алкоа Инк. | Reactor for carbothermal obtaining of titanium diboride |
| CN106348762B (en) * | 2016-08-23 | 2019-02-05 | 安徽科创中光科技有限公司 | Synthetic method of silicon nitride powder for laser equipment |
| CN111555114A (en) * | 2020-05-11 | 2020-08-18 | 欧菲微电子技术有限公司 | Vertical cavity surface emitting laser, preparation method and camera module |
| CN116813354B (en) * | 2023-06-06 | 2024-10-18 | 东莞理工学院 | A method for in-situ preparation of silicon nitride ceramics, prepared silicon nitride ceramics and applications thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1028977A (en) * | 1962-02-24 | 1966-05-11 | Eric Campbell Shears | Improvements in or relating to the manufacture of silicon nitride and oxynitride |
| DE2800174A1 (en) * | 1978-01-03 | 1979-07-12 | Max Planck Gesellschaft | PROCESS FOR SINTERING SILICON NITRIDE SHAPED BODIES |
| JPS6036311A (en) * | 1983-08-08 | 1985-02-25 | Nippon Cement Co Ltd | Production of alpha-type silicon nitride |
| US4626422A (en) * | 1985-06-24 | 1986-12-02 | Gte Products Corporation | High purity high surface area silicon nitride |
-
1986
- 1986-04-03 FR FR8604764A patent/FR2596746B1/en not_active Expired
-
1987
- 1987-03-23 IE IE75587A patent/IE59544B1/en not_active IP Right Cessation
- 1987-03-25 DE DE8787400664T patent/DE3776376D1/en not_active Expired - Fee Related
- 1987-03-25 AT AT87400664T patent/ATE72204T1/en not_active IP Right Cessation
- 1987-03-25 ES ES198787400664T patent/ES2039468T3/en not_active Expired - Lifetime
- 1987-03-25 EP EP19870400664 patent/EP0240414B1/en not_active Expired - Lifetime
- 1987-04-01 JP JP62082177A patent/JP2610867B2/en not_active Expired - Lifetime
- 1987-04-02 NO NO871373A patent/NO170208C/en unknown
- 1987-04-02 DK DK168087A patent/DK167865B1/en not_active IP Right Cessation
- 1987-04-03 AU AU71037/87A patent/AU603566B2/en not_active Ceased
- 1987-04-03 CN CN87102970A patent/CN1007888B/en not_active Expired
-
1992
- 1992-04-01 GR GR920400598T patent/GR3004228T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IE59544B1 (en) | 1994-03-09 |
| DK167865B1 (en) | 1993-12-27 |
| ATE72204T1 (en) | 1992-02-15 |
| DK168087D0 (en) | 1987-04-02 |
| DK168087A (en) | 1987-10-04 |
| NO871373D0 (en) | 1987-04-02 |
| NO170208B (en) | 1992-06-15 |
| CN87102970A (en) | 1987-10-21 |
| ES2039468T3 (en) | 1993-10-01 |
| FR2596746A1 (en) | 1987-10-09 |
| NO170208C (en) | 1992-09-23 |
| AU7103787A (en) | 1987-10-08 |
| EP0240414B1 (en) | 1992-01-29 |
| DE3776376D1 (en) | 1992-03-12 |
| CN1007888B (en) | 1990-05-09 |
| FR2596746B1 (en) | 1988-06-03 |
| GR3004228T3 (en) | 1993-03-31 |
| JP2610867B2 (en) | 1997-05-14 |
| JPS62241810A (en) | 1987-10-22 |
| EP0240414A1 (en) | 1987-10-07 |
| IE870755L (en) | 1987-10-03 |
| NO871373L (en) | 1987-10-05 |
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