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CN103976921B - A kind of Herba Moslae Cavaleriei extracting solution and its preparation method and application - Google Patents
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CN103976921B - A kind of Herba Moslae Cavaleriei extracting solution and its preparation method and application - Google Patents

A kind of Herba Moslae Cavaleriei extracting solution and its preparation method and application Download PDF

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CN103976921B
CN103976921B CN201410242102.4A CN201410242102A CN103976921B CN 103976921 B CN103976921 B CN 103976921B CN 201410242102 A CN201410242102 A CN 201410242102A CN 103976921 B CN103976921 B CN 103976921B
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herba moslae
extracting solution
moslae cavaleriei
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CN103976921A (en
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杨广群
李苏
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Guangzhou Q Max Biotechnology Co ltd
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Guangzhou Danqi Daily Chemical Co Ltd
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Abstract

The invention discloses a kind of Herba Moslae Cavaleriei extracting solution and its preparation method and application.The Herba Moslae Cavaleriei extracting solution that the present invention obtains through refining through water; it has the effect significantly removing skin toxins; this characteristic makes Herba Moslae Cavaleriei extracting solution possess the effect improving skin immunization power, is applied in cosmetics have and significantly repairs and protect sensitive-skinned effect.

Description

一种七星剑提取液及其制备方法和应用A kind of Qixingjian extract and its preparation method and application

技术领域technical field

本发明涉及化妆品领域,特别是涉及一种七星剑提取液及其制备方法和应用。The invention relates to the field of cosmetics, in particular to a Qixingjian extract and a preparation method and application thereof.

背景技术Background technique

随着人们生活水平的提高,美容化妆品已经成为人们生活中必备品。但是人们却对于化妆品的质量要求非常之高,不但要求效果好,而且要求没有副作用。随着美容化妆品行业的发展,天然植物类产品由于使用安全、作用温和、效果明显等优点而得到欢迎。一般是通过相应加工得到含有有效成分的植物提取物,并添加到化妆品中。With the improvement of people's living standards, beauty cosmetics have become a must-have in people's lives. But people have very high requirements for the quality of cosmetics, not only require good effects, but also require no side effects. With the development of the beauty and cosmetics industry, natural plant products are welcomed due to their advantages such as safe use, mild effect, and obvious effect. Generally, plant extracts containing active ingredients are obtained through corresponding processing and added to cosmetics.

目前化妆品中的植物提取物,大都采用水提、醇提、超声波提取、微波提取等方法提取所得,提取工艺复杂,经过浓缩干燥等工序,还要加入防腐剂以使提取物的保质期更长久。这样带来的弊端,一个是浪费资源,在提取过程中,溶液浓缩,一般只取浓缩出来的小部分精华,而大部分溶液则是扔掉。其实这部分溶液还是会含有活性成分的,还可以再次利用,而直接扔掉就造成了资源的浪费。另一个弊端是,在提取物中加入防腐剂固然可以使提取物获得更长的保质期,但是同时也为皮肤带来致敏源。At present, most of the plant extracts in cosmetics are extracted by water extraction, alcohol extraction, ultrasonic extraction, microwave extraction and other methods. The extraction process is complicated. The disadvantages brought about in this way are a waste of resources. During the extraction process, the solution is concentrated, and generally only a small part of the concentrated essence is taken, while most of the solution is thrown away. In fact, this part of the solution will still contain active ingredients and can be reused, and throwing it away directly will cause a waste of resources. Another disadvantage is that adding preservatives to the extract can certainly make the extract have a longer shelf life, but it also brings allergens to the skin.

敏感皮肤是当前化妆品界人士想攻克的难题,造成敏感肌肤的根本原因是:皮肤细胞受损而使皮肤的免疫力下降,角质层变薄导致皮肤滋润度不够,最终导致肌肤的屏障功能过于薄弱,无法抵御外界刺激;接着皮肤的神经纤维由于经常受到外界刺激,从而易于产生瘙痒、红肿、刺痛、粉刺、脱皮等不适现象的产生。Sensitive skin is a problem that people in the cosmetics industry want to overcome. The root cause of sensitive skin is: skin cells are damaged, which reduces the skin's immunity, and the thinning of the stratum corneum leads to insufficient moisture of the skin, which eventually leads to the skin's barrier function being too weak , unable to resist external stimuli; then the nerve fibers of the skin are prone to itching, redness, tingling, acne, peeling and other discomforts due to frequent external stimuli.

因此,选择何种植物,如何简单、安全、有效地对该植物提取进行,并将其安全的应用到化妆品中保护敏感皮肤,是亟待解决的问题。Therefore, what kind of plant to choose, how to extract the plant simply, safely and effectively, and how to safely apply it to cosmetics to protect sensitive skin are problems to be solved urgently.

发明内容Contents of the invention

基于此,本发明目的在于提供一种七星剑提取液及其制备方法和应用。Based on this, the purpose of the present invention is to provide a Qixingjian extract and its preparation method and application.

解决上述技术问题的具体技术方案如下:The concrete technical scheme that solves the above-mentioned technical problem is as follows:

一种七星剑提取液的制备方法,包括以下步骤:A preparation method of Qixingjian extract, comprising the following steps:

将七星剑干燥粉碎,用灭菌过的800-1000目纱布袋装好,置于真空均质乳化锅中,按七星剑的重量,加入8-12倍量的去离子水,于90-100℃提取,即可制得七星剑提取液。Dry and crush the Seven Star Sword, pack it in a sterilized 800-1000 mesh gauze bag, place it in a vacuum homogeneous emulsification pot, add 8-12 times the amount of deionized water according to the weight of the Seven Star Sword, and put it at 90-100 ℃ extraction, the Qixingjian extract can be prepared.

在其中一些实施例中,所述提取的时间为20-50min。In some of these embodiments, the extraction time is 20-50 minutes.

在其中一些实施例中,将七星剑干燥粉碎,用灭菌过的800-1000目纱布袋装好,置于真空均质乳化锅中,提取完成后,直接将纱布袋拿出,余下的溶液即为七星剑提取液。该方法中由于采用真空均质乳化锅,其可在提取完成后,直接将其他化妆品辅料加进去,进行化妆品生产,而不需要用专门的植物提取设备提取,节约了成本;另外,采用纱布袋装七星剑粉,提取完后直接将纱布袋取出即可,不用过滤,简化提取工艺,提高效率。In some of these embodiments, the Seven Star Sword is dried and pulverized, packed in a sterilized 800-1000 mesh gauze bag, and placed in a vacuum homogenizing emulsification pot. After the extraction is completed, the gauze bag is directly taken out, and the remaining solution It is the extract of Seven Star Sword. In this method, due to the use of a vacuum homogeneous emulsification pot, it can directly add other cosmetic auxiliary materials after the extraction is completed, and carry out cosmetic production without using special plant extraction equipment for extraction, which saves costs; in addition, gauze bags are used Packed with Qixingjian powder, just take out the gauze bag directly after extraction, no need to filter, simplify the extraction process and improve efficiency.

上述方法简单易操作,七星剑提取物可现提现用,不需添加防腐剂,显著减少对皮肤的致敏源。化妆品配方中,本身就添加有防腐剂,将本发明提取物现提加进去,避免了因放置而产生变质问题。The above method is simple and easy to operate, and the extract of Seven Star Sword can be used immediately without adding preservatives, which can significantly reduce the allergens to the skin. In the cosmetic formula, preservatives are already added, and the extract of the present invention is added in place to avoid the problem of deterioration due to storage.

上述方法所制得的七星剑提取液在制备具有修复和保护敏感皮肤功效的化妆品中的应用。The application of the Qixingjian extract prepared by the above method in the preparation of cosmetics with the functions of repairing and protecting sensitive skin.

在其中一些实施例中,所述化妆品中七星剑提取液的含量为58-95wt%。In some of the embodiments, the content of the Qixingjian extract in the cosmetic is 58-95wt%.

在其中一些实施例中,所述化妆品为营养霜。In some of these embodiments, the cosmetic is nutritional cream.

本发明提供一种营养霜,所述营养霜包括下述重量百分比的组分:The invention provides a nutritional cream, which comprises the following components in weight percentage:

乳化剂:3.5-6.3wt%,Emulsifier: 3.5-6.3wt%,

润肤剂:5-10wt%,Emollient: 5-10wt%,

抗氧化剂:0.2-0.8wt%,Antioxidant: 0.2-0.8wt%,

保湿剂:5-15wt%,Humectant: 5-15wt%,

增稠剂:0.05-0.15wt%,Thickener: 0.05-0.15wt%,

防腐剂:0.3-0.7wt%,Preservatives: 0.3-0.7wt%,

上述制备方法制得的七星剑提取液:余量,The Seven Star Sword extract that above-mentioned preparation method makes: surplus,

所述乳化剂为鲸蜡硬脂醇/鲸蜡硬脂基葡糖苷、鲸蜡硬脂醇、甘油硬脂酸酯/PEG-100硬脂酸酯、聚丙烯酰胺/C13-14异链烷烃/月桂醇聚醚-7或甲基葡糖倍半硬脂酸酯中的至少一种;The emulsifier is cetearyl alcohol/cetaryl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/ At least one of laureth-7 or methyl glucose sesquistearate;

所述润肤剂为环五聚二甲基硅氧烷/环己硅氧烷、聚二甲基硅氧烷、辛酸/癸酸甘油三酯或氢化霍霍巴油中的至少一种;The emollient is at least one of cyclopentasiloxane/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;

所述抗氧化剂为生育酚或迷迭提取物中的至少一种;The antioxidant is at least one of tocopherol or rosemary extract;

所述保湿剂为丙二醇、甘油、透明质酸钠、低聚果糖或山梨醇中的至少一种;The moisturizing agent is at least one of propylene glycol, glycerin, sodium hyaluronate, fructooligosaccharide or sorbitol;

所述增稠剂为黄原胶或羧甲基纤维素钠中的至少一种;The thickener is at least one of xanthan gum or sodium carboxymethyl cellulose;

所述防腐剂为苯氧乙醇/乙基己基甘油、苯甲酸钠或杰马中的至少一种。The preservative is at least one of phenoxyethanol/ethylhexylglycerin, sodium benzoate or Genma.

在其中一些实施例中,所述营养霜包括下述重量百分比的组分:In some of these embodiments, the nutritional cream includes the following components in weight percentage:

乳化剂:4.9-6.3wt%,Emulsifier: 4.9-6.3wt%,

润肤剂:6.4-7.6wt%,Emollient: 6.4-7.6wt%,

抗氧化剂:0.4-0.6wt%,Antioxidant: 0.4-0.6wt%,

保湿剂:8-12.15wt%,Humectant: 8-12.15wt%,

增稠剂:0.09-0.11wt%,Thickener: 0.09-0.11wt%,

防腐剂:0.4-0.6wt%,Preservatives: 0.4-0.6wt%,

上述制备方法制得的七星剑提取液:余量,The Seven Star Sword extract that above-mentioned preparation method makes: surplus,

所述乳化剂为鲸蜡硬脂醇/鲸蜡硬脂基葡糖苷、鲸蜡硬脂醇、甘油硬脂酸酯/PEG-100硬脂酸酯或聚丙烯酰胺/C13-14异链烷烃/月桂醇聚醚-7中的至少一种;The emulsifier is cetearyl alcohol/cetaryl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearate or polyacrylamide/C13-14 isoparaffin/ At least one of laureth-7;

所述润肤剂为环五聚二甲基硅氧烷/环己硅氧烷、聚二甲基硅氧烷或辛酸/癸酸甘油三酯中的至少一种;The emollient is at least one of cyclopentasiloxane/cyclohexasiloxane, polydimethylsiloxane or caprylic/capric triglyceride;

所述抗氧化剂为生育酚;The antioxidant is tocopherol;

所述保湿剂为丙二醇、甘油、透明质酸钠或低聚果糖中的至少一种;The humectant is at least one of propylene glycol, glycerin, sodium hyaluronate or fructooligosaccharide;

所述增稠剂为黄原胶;The thickener is xanthan gum;

所述防腐剂为苯氧乙醇/乙基己基甘油。The preservative is phenoxyethanol/ethylhexylglycerin.

在其中一些实施例中,所述营养霜包括下述重量百分比的组分:In some of these embodiments, the nutritional cream includes the following components in weight percentage:

鲸蜡硬脂醇/鲸蜡硬脂基葡糖苷:2.3-2.7wt%,Cetearyl Alcohol/Cetearyl Glucoside: 2.3-2.7wt%,

鲸蜡硬脂醇:1-1.4wt%,Cetearyl Alcohol: 1-1.4wt%,

甘油硬脂酸酯/PEG-100硬脂酸酯1-1.4wt%,Glyceryl Stearate/PEG-100 Stearate 1-1.4wt%,

环五聚二甲基硅氧烷/环己硅氧烷:1.8-2.2wt%,Cyclopentasiloxane/Cyclohexasiloxane: 1.8-2.2 wt%,

聚二甲基硅氧烷:1.8-2.2wt%,Polydimethylsiloxane: 1.8-2.2wt%,

辛酸/癸酸甘油三酯:2.8-3.2wt%,Caprylic/capric triglycerides: 2.8-3.2wt%,

生育酚:0.4-0.6wt%,Tocopherol: 0.4-0.6wt%,

丙二醇:4-6wt%,Propylene glycol: 4-6wt%,

甘油:4-6wt%,Glycerin: 4-6wt%,

黄原胶:0.09-0.11wt%,Xanthan gum: 0.09-0.11wt%,

透明质酸钠:0.015-0.025wt%,Sodium hyaluronate: 0.015-0.025wt%,

聚丙烯酰胺/C13-14异链烷烃/月桂醇聚醚-7:0.6-0.8wt%,Polyacrylamide/C13-14 Isoparaffin/Laureth-7: 0.6-0.8wt%,

苯氧乙醇/乙基己基甘油:0.4-0.6wt%,Phenoxyethanol/Ethylhexylglycerin: 0.4-0.6 wt%,

低聚果糖:0.08-0.11wt%,Fructooligosaccharides: 0.08-0.11wt%,

上述的七星剑提取液:余量。The above-mentioned Qixingjian extract: surplus.

本发明所述一种七星剑提取液及其制备方法和应用具有以下优点和有益效果:A Qixingjian extract of the present invention and its preparation method and application have the following advantages and beneficial effects:

本发明经发明人大量的实验和研究,得出在最优工艺——水提下所制得的七星剑提取液,其具有显著的清除皮肤毒素的作用,这种特性使得七星剑提取液具备提高皮肤免疫力的作用,将其应用于化妆品中具有显著的修复和保护敏感皮肤的功效。After a large number of experiments and researches by the inventors, the present invention has obtained the Qixingjian extract prepared under the optimal process—water extraction, which has a significant effect of removing skin toxins. This characteristic makes the Qixingjian extract possess It has the effect of improving skin immunity, and its application in cosmetics has a significant effect of repairing and protecting sensitive skin.

具体实施方式detailed description

本发明所述七星剑唇形科植物细叶七星剑的全草,生于海拔The whole herb of the seven-star sword of the present invention Lamiaceae plant thin-leaved seven-star sword, born at altitude

700-1600m的山坡草地、疏林下或山谷地带,主要分布于浙江、江西、湖北、广东、广西、四川、贵州、云南等地。七星剑味辛,性微温。治狂犬、毒蛇咬伤,皮肤湿疹,疮毒,发汗解暑,利湿角毒。本发明将七星剑经水提制得七星剑提取液,将其用于制备具有修复和保护敏感皮肤化妆品中。700-1600m hillside grassland, sparse forest or valley area, mainly distributed in Zhejiang, Jiangxi, Hubei, Guangdong, Guangxi, Sichuan, Guizhou, Yunnan and other places. Qixingjian is pungent in taste and slightly warm in nature. Control rabies, venomous snake bites, skin eczema, sores, sweating to relieve summer heat, dampness and horny poison. In the present invention, the seven-star sword is extracted with water to obtain the seven-star sword extract, which is used to prepare cosmetics for repairing and protecting sensitive skin.

以下将结合具体实施例对本发明做进一步说明。The present invention will be further described below in conjunction with specific examples.

以下实施例中所用到的成分名称均为国际化妆品原料命名(InternationalNomenclatureCosmeticIngredient,INCI)所规定的名称,例如苯氧乙醇/乙基己基甘油、甘油硬脂酸酯/PEG-100硬脂酸酯、环五聚二甲基硅氧烷/环己硅氧烷、鲸蜡硬脂醇/鲸蜡硬脂基葡糖苷、辛酸/癸酸甘油三酯、聚丙烯酰胺/C13-14异链烷烃/月桂醇聚醚-7。The names of the ingredients used in the following examples are the names specified by the International Nomenclature Cosmetic Ingredient (INCI), such as phenoxyethanol/ethylhexylglycerin, glyceryl stearate/PEG-100 stearate, cyclic Pentamethicone/Cyclohexasiloxane, Cetearyl Alcohol/Cetearyl Glucoside, Caprylic/Capric Triglyceride, Polyacrylamide/C13-14 Isoparaffin/Lauryl Alcohol Polyether-7.

实施例1营养霜Embodiment 1 nutrition cream

本实施例所述营养霜中含有七星剑提取液,所述七星剑提取液的制备方法,包括以下步骤:将1公斤七星剑洗净,晾干,干燥粉碎至100目,用灭菌过的1000目纱布袋装好,将其用灭菌过的纱布袋装好,封紧,置于真空均质乳化锅中,加入12公斤的去离子水,于100℃浸提50min,将纱布袋取出,剩余的溶液,即得七星剑提取液。The nutrition cream described in this embodiment contains Qixingjian extract, and the preparation method of said Qixingjian extract comprises the following steps: wash 1 kg of Qixingjian, dry, dry and pulverize to 100 mesh, and use sterilized Pack it in a 1000-mesh gauze bag, pack it in a sterilized gauze bag, seal it tightly, put it in a vacuum homogeneous emulsification pot, add 12 kg of deionized water, extract at 100°C for 50 minutes, and take out the gauze bag , the remaining solution is the Seven Star Sword extract.

所述营养霜的组分和含量见表1:The composition and content of described nutrient cream are shown in Table 1:

表1营养霜的组分和含量The composition and content of table 1 nutritional cream

对比例1营养霜Comparative example 1 nutritional cream

所述营养霜的组分和含量见表2:The composition and content of described nutrient cream are shown in Table 2:

表2营养霜的组分和含量The composition and content of table 2 nutritional cream

成分Element 重量百分比(wt%)Weight percent (wt%) 去离子水Deionized water 余量margin 鲸蜡硬脂醇/鲸蜡硬脂基葡糖苷Cetearyl Alcohol/Cetearyl Glucoside 2.52.5 鲸蜡硬脂醇cetearyl alcohol 1.21.2 甘油硬脂酸酯/PEG-100硬脂酸酯Glyceryl Stearate/PEG-100 Stearate 1.21.2 环五聚二甲基硅氧烷/环己硅氧烷Cyclopentasiloxane/Cyclohexasiloxane 22 聚二甲基硅氧烷Polydimethylsiloxane 22 辛酸/癸酸甘油三酯Caprylic/Capric Triglycerides 33 生育酚(维生素E)Tocopherol (Vitamin E) 0.50.5 丙二醇Propylene Glycol 55 甘油glycerin 55 黄原胶xanthan gum 0.10.1 透明质酸钠Sodium hyaluronate 0.020.02 聚丙烯酰胺/C13-14异链烷烃/月桂醇聚醚-7Polyacrylamide/C13-14 Isoparaffin/Laureth-7 0.70.7 苯氧乙醇/乙基己基甘油Phenoxyethanol/Ethylhexylglycerin 0.50.5 低聚果糖fructooligosaccharide 0.10.1 合计total 100100

实施例2功效评价Embodiment 2 efficacy evaluation

一、实验目的1. Purpose of the experiment

通过对比分析评价上述各实施例中所制得的化妆品的修复和保护敏感皮肤的效果。The effects of repairing and protecting sensitive skin of the cosmetics prepared in the above-mentioned embodiments were evaluated by comparative analysis.

二、实验方法2. Experimental method

本实验分为实验组和对照组,其中,实验组分为:实施例1-营养霜;对照组为对比例1-营养霜、某一市售具有修复和保护敏感肌肤的精华素。This experiment is divided into an experimental group and a control group, wherein the experimental group is: Example 1 - nutritional cream; the control group is comparative example 1 - nutritional cream, a commercially available essence that repairs and protects sensitive skin.

征集敏感皮肤200名志愿者试用上述各产品28天后,观察结果。其中,女性120人,男性80人,最大年龄30岁,最小年龄15岁,平均年龄22岁。After recruiting 200 volunteers with sensitive skin to try the above products for 28 days, observe the results. Among them, there are 120 women and 80 men, the oldest is 30 years old, the youngest is 15 years old, and the average age is 22 years old.

所述敏感皮肤的表现为:瘙痒、红肿、刺痛、粉刺、脱皮。The manifestations of the sensitive skin are: pruritus, redness, tingling, acne, peeling.

三、实验结果3. Experimental results

结果参见表3。See Table 3 for the results.

表3实验组和对照组的功效结果表Table 3 Efficacy result table of experimental group and control group

从表3可知:对照组各产品即对比例1-营养霜、某一市售精华素和实验组各产品实施例1-营养霜对瘙痒、红肿、刺痛、粉刺、脱皮均有不同程度的改善,从实验数据可以看出,实验组中各产品对瘙痒、红肿、刺痛、粉刺、脱皮改善程度明显比对照组中各产品的改善程度要高,由此可知,含有七星剑提取液的化妆品具有显著的修复和保护敏感皮肤的功效。As can be seen from Table 3: each product of the control group is comparative example 1-nutrition cream, a certain commercially available essence and each product embodiment 1-nutrition cream of the experimental group has different degrees of effects on pruritus, redness, tingling pain, acne, and peeling. It can be seen from the experimental data that the improvement degree of each product in the experimental group on itching, redness, tingling, acne, and peeling is significantly higher than that of the products in the control group. Cosmetics have a remarkable effect on repairing and protecting sensitive skin.

以上所述实施例仅表达了本发明的几种实施方式,其描述较为具体和详细,但并不能因此而理解为对本发明专利范围的限制。应当指出的是,对于本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进,这些都属于本发明的保护范围。因此,本发明专利的保护范围应以所附权利要求为准。The above-mentioned embodiments only express several implementation modes of the present invention, and the descriptions thereof are relatively specific and detailed, but should not be construed as limiting the patent scope of the present invention. It should be noted that those skilled in the art can make several modifications and improvements without departing from the concept of the present invention, and these all belong to the protection scope of the present invention. Therefore, the protection scope of the patent for the present invention should be based on the appended claims.

Claims (1)

1. a nourishing cream, it is characterised in that described nourishing cream includes the component of following weight percentage ratio: breast Agent: 3.5-6.3wt%, emollient: 5-10wt%, antioxidant: 0.2-0.8wt%, wetting agent: 5-15wt%, increase Thick dose: 0.05-0.15wt%, preservative: 0.3-0.7wt%, Herba Moslae Cavaleriei extracting solution: surplus;
Described emulsifying agent is cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate / PEG-100 stearate, polyacrylamide/C13-14 isoparaffin/laureth-7 or methyl times At least one in semi-solid fat acid esters;Described emollient is ring five polydimethylsiloxane/cyclohexasiloxane, gathers At least one in dimethyl siloxane, caprylic/capric triglyceride or hydrogenated jojoba oil;Described antioxidation Agent is at least one in tocopherol or fan's repeatedly extract;Described wetting agent is propylene glycol, glycerol, hyalomitome At least one in acid sodium, oligofructose or sorbitol;Described thickening agent is xanthan gum or carboxymethyl cellulose At least one in sodium;Described preservative is in phenoxyethanol/Sensiva SC50, sodium benzoate or germall At least one;
Described Herba Moslae Cavaleriei extracting solution through the following steps that preparation: be dry, pulverize by Herba Moslae Cavaleriei, loading is gone out The 800-1000 mesh gauze bag that bacterium crosses, is placed in vacuum emulsifying pot, by the weight of Herba Moslae Cavaleriei, adds The deionized water of 8-12 times amount, in 90-100 DEG C of extraction,.
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