DE2504961B2 - Process for processing mink fats - Google Patents
Process for processing mink fatsInfo
- Publication number
- DE2504961B2 DE2504961B2 DE19752504961 DE2504961A DE2504961B2 DE 2504961 B2 DE2504961 B2 DE 2504961B2 DE 19752504961 DE19752504961 DE 19752504961 DE 2504961 A DE2504961 A DE 2504961A DE 2504961 B2 DE2504961 B2 DE 2504961B2
- Authority
- DE
- Germany
- Prior art keywords
- fats
- mink
- sulfur
- iodine
- degrees celsius
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000772415 Neovison vison Species 0.000 title claims description 11
- 239000003925 fat Substances 0.000 title claims description 11
- 238000000034 method Methods 0.000 title claims description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 10
- 229910052717 sulfur Inorganic materials 0.000 claims description 10
- 239000011593 sulfur Substances 0.000 claims description 10
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 5
- 239000002537 cosmetic Substances 0.000 claims description 5
- 229910052740 iodine Inorganic materials 0.000 claims description 5
- 239000011630 iodine Substances 0.000 claims description 5
- 235000019197 fats Nutrition 0.000 description 8
- 239000003921 oil Substances 0.000 description 5
- 230000032683 aging Effects 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 125000005456 glyceride group Chemical group 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 230000000622 irritating effect Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 230000037368 penetrate the skin Effects 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Dermatology (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
Es ist bekannt, Nerzfett, welches Glyceride von Myristinsäure, Palrnitinsäure, Stearinsäure, Oleinsäure und Linolsäure zusammen mit Spuren von GIyceriden anderer Fettsäuren enthält, zu raffinieren, vor allem zwecks besserer Haltbarkeit gegenüber Alterserscheinungen, wie Ranzigwerden. Wegen seines besonders guten Benetzungsvermögen auf Haut und Haar, die sich aus der niedrigen Oberflächenspannung von nur etwa 31 dyn/cm2 ergeben, bietet das Nerzfett insbesondere für kosmetische und pharmazeutische Zwecke wichtige Vorteile, abgesehen von Verwendungen für andere gewerbliche Zwecke. Aber gerade bei Verwendung für kosmetische und pharmazeutische Zwecke ist der bis jetzt erzielte Stabilisierungsgrad mittels bereits bekannter Raffinations- und Konservierungsmethoden noch unzureichend.It is known to refine mink fat, which contains glycerides of myristic acid, palrnitic acid, stearic acid, oleic acid and linoleic acid together with traces of glycerides of other fatty acids, above all for the purpose of better durability against signs of aging such as rancidity. Because of its particularly good wetting properties on skin and hair, which result from the low surface tension of only about 31 dynes / cm 2 , the mink fat offers important advantages in particular for cosmetic and pharmaceutical purposes, apart from uses for other commercial purposes. But especially when used for cosmetic and pharmaceutical purposes, the degree of stabilization achieved up to now by means of already known refining and preservation methods is still inadequate.
Es ist nun gefunden worden, daß chemische Umsetzungen mit Schwefel oder mit Schwefel und Jod auch in sehr geringen Mengen die Stabilität von Nerzfett so bedeutend steigert, wie es für Verwendung zu kosmetischen Zwecken unbedingt notwendig ist. Etwa 0,1 bis J % sind für die besagte Stabilisierung in der Regel ausreichend.It has now been found that chemical reactions with sulfur or with sulfur and iodine also in very small amounts increases the stability of mink fat as significantly as it does for cosmetic use Purposes is absolutely necessary. About 0.1 to J% are for said stabilization in the Usually sufficient.
Es ist so gelungen, alle besagten Schwierigkeiten in einem Verfahrensschritt zu beseitigen.It was thus possible to eliminate all of the aforementioned difficulties in one procedural step.
Erfindungsgemäß erfolgt die chemische Umsetzung mit Schwefel oder mit Schwefel und Jod bei Temperaturen bis 100 Grad Celsius.According to the invention, the chemical reaction with sulfur or with sulfur and iodine takes place at temperatures up to 100 degrees Celsius.
Mit allen der besagten chemisch wirksamen Zusatzstoffe erzielt man überraschenderweise auch aus dem unhomogenen Originalnerzfett oder aus Nerzfett, das in an sich bekannter Weise vorraffiniert wurde, völlig homogene klare öle, frei von Trübungsstoffen, von goldgelber Farbe bei Behandlung mit Schwefel, von dunkelbrauner Farbe bei Behandlung mit Jod und Schwefel.With all of the said chemically active additives is surprisingly also obtained from the inhomogeneous original mink fat or from mink fat which has been pre-refined in a manner known per se became, completely homogeneous clear oils, free of opacities, of golden yellow color when treated with Sulfur, dark brown in color when treated with iodine and sulfur.
Diese dringen in die Haut oder ins Haar rasch und vollständig ein, bemerkenswerterweise ohne daß Reizwirkungen erkennbar sind.These penetrate the skin or hair quickly and completely, notably without it Irritant effects are recognizable.
1. In einem mit Doppelmantel für Niederdruckdampf oder für elektrische Heizung eingerichteten Mischer werden 1000 Kilo rohes, unhomogenes nicht vorraffiniertes Nerzfett bei ständig1. In one furnished with a double jacket for low pressure steam or for electric heating Mixers turn 1000 kilos of raw, inhomogeneous, not pre-refined mink fat at constant
is laufendem Mischer mit 5 Kilo Jod und Schwefel im Atomverhältnis S: J = 2:2 eingeschmolzen und bei allmählich ansteigender Temperatur innerhalb von 30 bis 60 Minuten bis auf 100 Grad Celsius erhitzt.Is a running mixer with 5 kilos of iodine and sulfur in an atomic ratio of S: J = 2: 2 melted down and with gradually increasing temperature within 30 to 60 minutes up to 100 degrees Celsius heated.
Dadurch erfolgt völlige Homogenisierung in ein dunkelbraun gefärbtes Öi, frei von Fest- und Schwebestoffen.This results in complete homogenization in a dark brown colored oil, free of solid and Suspended matter.
Mit Erreichung der 100 Grad Celsius ist der Prozeß abgeschlossen und das öl kann in Lagerbehältern abgelassen werden.When 100 degrees Celsius has been reached, the process is complete and the oil can be stored in storage containers be drained.
Seine Beständigkeit ohne Alterserscheinungen beträgt normalerweise drei Jahre oder mehr. Es ist hauptsächlich für pharmazeutische Zwecke bestimmt, für Einreibe-Massageöle etc.Its persistence with no signs of aging is usually three years or more. It is mainly intended for pharmaceutical purposes, for rub-in massage oils, etc.
2. Im Mischgefäß gemäß Beispiel 1 werden als Zusatzwirkstoff für 1000 Kilo des besagten Nerzfettes
100 Kilo Schwefelblüte angewendet. Ansonsten wird der Prozeß so geleitet wie in Beispiel 1
angegeben. Die Beständigkeit des Produktes ohne Alterserscheinungen beträgt normalerweise
zwei Jahr«· oder mehr. Es ist für kosmetische
Zwecke, wie 1 *aut- und Haarpflegemittel, bestimmt.
Die Zusatzmengen können je nach Verwendungszweck einzeln oder in beliebiger Kombination abgeändert
werden. Auch die Behandlungstemperaturen können je nach Herkunft und Eigenart der Nerzfette
unterschiedlich sein, aber in der Regel nahe 100 Grad
Celsius. Die dem fertigen öl im kalten Zustand noch zuzusetzenden Wirkstoffe, einschließlich Riechstoffen,
sind bekannt.2. In the mixing vessel according to Example 1, 100 kilos of sulfur blossom are used as an additional active ingredient for 1000 kilos of said mink fat. Otherwise the process is carried out as indicated in Example 1. The durability of the product without any signs of aging is normally two years or more. It is intended for cosmetic purposes such as 1 * car and hair care products.
The additional amounts can be changed individually or in any combination, depending on the intended use. The treatment temperatures can also differ depending on the origin and nature of the mink fats, but are usually close to 100 degrees Celsius. The active ingredients to be added to the finished oil in the cold state, including fragrances, are known.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752504961 DE2504961B2 (en) | 1975-02-06 | 1975-02-06 | Process for processing mink fats |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752504961 DE2504961B2 (en) | 1975-02-06 | 1975-02-06 | Process for processing mink fats |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2504961A1 DE2504961A1 (en) | 1976-08-19 |
| DE2504961B2 true DE2504961B2 (en) | 1980-01-31 |
| DE2504961C3 DE2504961C3 (en) | 1980-09-25 |
Family
ID=5938238
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752504961 Granted DE2504961B2 (en) | 1975-02-06 | 1975-02-06 | Process for processing mink fats |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE2504961B2 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2535200A1 (en) * | 1982-11-03 | 1984-05-04 | Partouche Josette | Vison oil-based cosmetic product for multiple use |
-
1975
- 1975-02-06 DE DE19752504961 patent/DE2504961B2/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE2504961A1 (en) | 1976-08-19 |
| DE2504961C3 (en) | 1980-09-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: SALMOCID GMBH, 5135 SELFKANT, DE |
|
| 8339 | Ceased/non-payment of the annual fee |