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GB2116454A - Coating sheets - Google Patents
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GB2116454A - Coating sheets - Google Patents

Coating sheets Download PDF

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Publication number
GB2116454A
GB2116454A GB08207390A GB8207390A GB2116454A GB 2116454 A GB2116454 A GB 2116454A GB 08207390 A GB08207390 A GB 08207390A GB 8207390 A GB8207390 A GB 8207390A GB 2116454 A GB2116454 A GB 2116454A
Authority
GB
United Kingdom
Prior art keywords
coating
aluminium
welding
inert atmosphere
adhesive
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB08207390A
Other versions
GB2116454B (en
Inventor
Patrick George Selwood
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BL Technology Ltd
Original Assignee
BL Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BL Technology Ltd filed Critical BL Technology Ltd
Priority to GB08207390A priority Critical patent/GB2116454B/en
Publication of GB2116454A publication Critical patent/GB2116454A/en
Application granted granted Critical
Publication of GB2116454B publication Critical patent/GB2116454B/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/14Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to metal, e.g. car bodies
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/26After-treatment
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/26After-treatment
    • C23C2/261After-treatment in a gas atmosphere, e.g. inert or reducing atmosphere
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D2202/00Metallic substrate
    • B05D2202/20Metallic substrate based on light metals
    • B05D2202/25Metallic substrate based on light metals based on Al
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/04Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to gases
    • B05D3/0486Operating the coating or treatment in a controlled atmosphere
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/06Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation
    • B05D3/068Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation using ionising radiations (gamma, X, electrons)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/10Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by other chemical means
    • B05D3/102Pretreatment of metallic substrates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Welding Or Cutting Using Electron Beams (AREA)
  • Lining Or Joining Of Plastics Or The Like (AREA)
  • Laminated Bodies (AREA)

Abstract

The process is provided for depositing on a sheet of aluminium or aluminium alloy a coating material comprising (1) treating the sheet to expose the virgin surface, (2) protecting the exposed surface from exposure to oxygen by means of an inert atmosphere, (3) applying coating material while so protected and (4) subjecting the coating to a stabilising process. Components so fabricated then subsequently be joined by the use of an adhesive or by welding or by both joining processes.

Description

SPECIFICATION Process for coating sheets This invention relates to a process for the coating of sheets of aluminium or of its alloys, and to the use of sheet material so coated. It is particularly concerned with providing such a process to enable components fabricated from sheets so coated to be bonded either by the use of adhesive or welding or both to each other or to another material.
In the vehicle body industry spot welding is widely used in the fabrication of bodies from mild steel sheet. The quest for lighter vehicle bodies has led to the use of aluminium and its alloys.
However the use of spot welding with aluminium raises problems including welding electrode contamination and reduced weld strength by comparison with mild steel welds. The aircraft industry has for many years made use of adhesive bonding to fabricate load bearing structures of aluminium and its alloys. It has been found that the adhesive bond occurs between the relatively weak oxide layers on the metal surface rather than between the metal surfaces themselves. An improvement in bonding has been achieved by stripping of the naturally occuring oxide layer and replacing it with an oxide layer which has been generated with optimised physical properties for subsequent bonding.
According to the present invention there is provided a process for the coating of sheet aluminium of aluminium alloy comprising the steps of: (1) passing the sheet material through a bath or other treatment step to expose a surface of virgin metal or alloy; (2) protecting the exposed surface on formation from oxidation by means of an inert atmosphere; (3) depositing on the exposed surface, while protected by the inert atmosphere, a coating material; and (4) subjecting the coating material to a stabilizing process following which the coating is stabilized and bonded to the previously exposed surface so as to protect the surface from subsequent oxidation.
Preferably the process is carried out on a continuous basis with the sheet in the form of a continuous band.
Preferably the inert atmosphere is formed by an inert gas such as nitrogen.
Preferably the stabilizing process comprises curing or polymerising the coating material by means of an electron beam or other radiation source.
Subsequent to the coating process components prepared from the sheet material can be incorporated into structures, such as vehicle bodies, by the use of adhesives or by a welding process or by a combination of the two.
To protect people in the vicinity of the radiation shielding 23 while the electrom beam guns are in operation the shielding is provided with an angled passage 25 so that no straight path for the passage of radiation to the enclosure outlet 26 is available. A suitable angled path for the strip after curing is provided by rollers 27.
In considering the embodiment it should be born in mind that it is diagrammatic. Thus although only one degreasing and one etching tank is shown it may be necessary in practice to have more than one of each. In addition the coating stage is shown being carried out on both sides of the strip simultaneously. It may be necessary for each side to be coated and cured separately. The provision of an inert atmosphere with a suitably limited oxygen content can be dealt with by conventional means and is not detailed here.
Thereafter the sheet material can be subjected to conventional press or other fabrication processes to provide components which are capable of fabrication into structure, by the use of adhesive or by welding process or by using both adhesive and welding.
1. A process for the coating of sheet aluminium or aluminium alloy comprising the steps of: (1) passing the sheet material through a bath or other treatment step to expose a surface of virgin metal or alloy; (2) protecting the exposed surface on formation from oxidation by means of an inert atmosphere; (3) depositing on the exposed surface, while protected by the inert atmosphere, a coating material; and (4) subjecting the coating material to a stabilising process following which the coating is stabilised and bonded to the previously exposed surface so as to protect the surface from subsequent oxidation.
2. A process as claimed in claim 1 adapted for a continuous operation where the sheet material is in the form of a continuous band.
3. A process as claimed in any preceding claim wherein the inert atmosphere is made up of nitrogen gas.
4. A process as claimed in any preceding claim wherein the stabilizing process comprises curing or polymerising the coating material by means of an electron beam or other radiation source.
5. A process as herein before described with reference to, and as illustrated by, the accompanying drawing.
6. A process as claimed in any preceding claim comprising the further step of incorporating the sheet material, or a portion thereof, in to a fabrication by the application of an adhesive and/or welding process.
7. A component comprising sheet material prepared according to the process for any of the preceding claims 1 to 5.
**WARNING** end of DESC field may overlap start of CLMS **.

Claims (8)

**WARNING** start of CLMS field may overlap end of DESC **. SPECIFICATION Process for coating sheets This invention relates to a process for the coating of sheets of aluminium or of its alloys, and to the use of sheet material so coated. It is particularly concerned with providing such a process to enable components fabricated from sheets so coated to be bonded either by the use of adhesive or welding or both to each other or to another material. In the vehicle body industry spot welding is widely used in the fabrication of bodies from mild steel sheet. The quest for lighter vehicle bodies has led to the use of aluminium and its alloys. However the use of spot welding with aluminium raises problems including welding electrode contamination and reduced weld strength by comparison with mild steel welds. The aircraft industry has for many years made use of adhesive bonding to fabricate load bearing structures of aluminium and its alloys. It has been found that the adhesive bond occurs between the relatively weak oxide layers on the metal surface rather than between the metal surfaces themselves. An improvement in bonding has been achieved by stripping of the naturally occuring oxide layer and replacing it with an oxide layer which has been generated with optimised physical properties for subsequent bonding. According to the present invention there is provided a process for the coating of sheet aluminium of aluminium alloy comprising the steps of: (1) passing the sheet material through a bath or other treatment step to expose a surface of virgin metal or alloy; (2) protecting the exposed surface on formation from oxidation by means of an inert atmosphere; (3) depositing on the exposed surface, while protected by the inert atmosphere, a coating material; and (4) subjecting the coating material to a stabilizing process following which the coating is stabilized and bonded to the previously exposed surface so as to protect the surface from subsequent oxidation. Preferably the process is carried out on a continuous basis with the sheet in the form of a continuous band. Preferably the inert atmosphere is formed by an inert gas such as nitrogen. Preferably the stabilizing process comprises curing or polymerising the coating material by means of an electron beam or other radiation source. Subsequent to the coating process components prepared from the sheet material can be incorporated into structures, such as vehicle bodies, by the use of adhesives or by a welding process or by a combination of the two. To protect people in the vicinity of the radiation shielding 23 while the electrom beam guns are in operation the shielding is provided with an angled passage 25 so that no straight path for the passage of radiation to the enclosure outlet 26 is available. A suitable angled path for the strip after curing is provided by rollers 27. In considering the embodiment it should be born in mind that it is diagrammatic. Thus although only one degreasing and one etching tank is shown it may be necessary in practice to have more than one of each. In addition the coating stage is shown being carried out on both sides of the strip simultaneously. It may be necessary for each side to be coated and cured separately. The provision of an inert atmosphere with a suitably limited oxygen content can be dealt with by conventional means and is not detailed here. Thereafter the sheet material can be subjected to conventional press or other fabrication processes to provide components which are capable of fabrication into structure, by the use of adhesive or by welding process or by using both adhesive and welding. CLAIMS
1. A process for the coating of sheet aluminium or aluminium alloy comprising the steps of: (1) passing the sheet material through a bath or other treatment step to expose a surface of virgin metal or alloy; (2) protecting the exposed surface on formation from oxidation by means of an inert atmosphere; (3) depositing on the exposed surface, while protected by the inert atmosphere, a coating material; and (4) subjecting the coating material to a stabilising process following which the coating is stabilised and bonded to the previously exposed surface so as to protect the surface from subsequent oxidation.
2. A process as claimed in claim 1 adapted for a continuous operation where the sheet material is in the form of a continuous band.
3. A process as claimed in any preceding claim wherein the inert atmosphere is made up of nitrogen gas.
4. A process as claimed in any preceding claim wherein the stabilizing process comprises curing or polymerising the coating material by means of an electron beam or other radiation source.
5. A process as herein before described with reference to, and as illustrated by, the accompanying drawing.
6. A process as claimed in any preceding claim comprising the further step of incorporating the sheet material, or a portion thereof, in to a fabrication by the application of an adhesive and/or welding process.
7. A component comprising sheet material prepared according to the process for any of the preceding claims 1 to 5.
8. A fabrication comprising of an assembly in which a component as claimed in claim 7 is incorporated by means of an application of an adhesive and/or a welding process.
GB08207390A 1982-03-13 1982-03-13 Coating sheets Expired GB2116454B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB08207390A GB2116454B (en) 1982-03-13 1982-03-13 Coating sheets

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB08207390A GB2116454B (en) 1982-03-13 1982-03-13 Coating sheets

Publications (2)

Publication Number Publication Date
GB2116454A true GB2116454A (en) 1983-09-28
GB2116454B GB2116454B (en) 1985-08-29

Family

ID=10528991

Family Applications (1)

Application Number Title Priority Date Filing Date
GB08207390A Expired GB2116454B (en) 1982-03-13 1982-03-13 Coating sheets

Country Status (1)

Country Link
GB (1) GB2116454B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0201992A3 (en) * 1985-03-18 1987-12-02 Illinois Tool Works Inc. Method and apparatus for plating and coating and articles so produced
GB2248419A (en) * 1990-10-05 1992-04-08 Secr Defence Method for improving adhesive bonding
DE4424979C1 (en) * 1994-07-15 1996-01-25 C D Waelzholz Poduktions Ges M Process for making a ski edge

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB558926A (en) * 1942-07-23 1944-01-27 Ernest Windsor Bowen Improvements in and relating to treating aluminium and aluminium base alloy surfaces in preparation for applying an adherent coating to them
GB666820A (en) * 1948-09-16 1952-02-20 Alais & Froges & Camarque Cie Improvements relating to the coating or enamelling of copper articles
GB1271096A (en) * 1969-04-14 1972-04-19 Minnesota Mining & Mfg Coating of solid substrates
GB1486979A (en) * 1974-03-12 1977-09-28 Nasa Joining of aluminium containing components

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB558926A (en) * 1942-07-23 1944-01-27 Ernest Windsor Bowen Improvements in and relating to treating aluminium and aluminium base alloy surfaces in preparation for applying an adherent coating to them
GB666820A (en) * 1948-09-16 1952-02-20 Alais & Froges & Camarque Cie Improvements relating to the coating or enamelling of copper articles
GB1271096A (en) * 1969-04-14 1972-04-19 Minnesota Mining & Mfg Coating of solid substrates
GB1486979A (en) * 1974-03-12 1977-09-28 Nasa Joining of aluminium containing components

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0201992A3 (en) * 1985-03-18 1987-12-02 Illinois Tool Works Inc. Method and apparatus for plating and coating and articles so produced
GB2248419A (en) * 1990-10-05 1992-04-08 Secr Defence Method for improving adhesive bonding
DE4424979C1 (en) * 1994-07-15 1996-01-25 C D Waelzholz Poduktions Ges M Process for making a ski edge

Also Published As

Publication number Publication date
GB2116454B (en) 1985-08-29

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Date Code Title Description
PCNP Patent ceased through non-payment of renewal fee

Effective date: 19940313