JP2594082B2 - Aromatic jellified composition - Google Patents
Aromatic jellified compositionInfo
- Publication number
- JP2594082B2 JP2594082B2 JP62333212A JP33321287A JP2594082B2 JP 2594082 B2 JP2594082 B2 JP 2594082B2 JP 62333212 A JP62333212 A JP 62333212A JP 33321287 A JP33321287 A JP 33321287A JP 2594082 B2 JP2594082 B2 JP 2594082B2
- Authority
- JP
- Japan
- Prior art keywords
- fragrance
- water
- aromatic
- encapsulated
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000203 mixture Substances 0.000 title claims description 14
- 125000003118 aryl group Chemical group 0.000 title claims description 7
- 239000003205 fragrance Substances 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 8
- 238000010521 absorption reaction Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 description 8
- 239000002304 perfume Substances 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- -1 alkali metal acrylate Chemical class 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- QIVUCLWGARAQIO-OLIXTKCUSA-N (3s)-n-[(3s,5s,6r)-6-methyl-2-oxo-1-(2,2,2-trifluoroethyl)-5-(2,3,6-trifluorophenyl)piperidin-3-yl]-2-oxospiro[1h-pyrrolo[2,3-b]pyridine-3,6'-5,7-dihydrocyclopenta[b]pyridine]-3'-carboxamide Chemical compound C1([C@H]2[C@H](N(C(=O)[C@@H](NC(=O)C=3C=C4C[C@]5(CC4=NC=3)C3=CC=CN=C3NC5=O)C2)CC(F)(F)F)C)=C(F)C=CC(F)=C1F QIVUCLWGARAQIO-OLIXTKCUSA-N 0.000 description 3
- 229910021417 amorphous silicon Inorganic materials 0.000 description 3
- 238000013329 compounding Methods 0.000 description 3
- VWTINHYPRWEBQY-UHFFFAOYSA-N denatonium Chemical compound [O-]C(=O)C1=CC=CC=C1.C=1C=CC=CC=1C[N+](CC)(CC)CC(=O)NC1=C(C)C=CC=C1C VWTINHYPRWEBQY-UHFFFAOYSA-N 0.000 description 3
- 229960001610 denatonium benzoate Drugs 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 3
- 235000010234 sodium benzoate Nutrition 0.000 description 3
- 239000004299 sodium benzoate Substances 0.000 description 3
- 108010010803 Gelatin Proteins 0.000 description 2
- 229920000084 Gum arabic Polymers 0.000 description 2
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 description 2
- 241000978776 Senegalia senegal Species 0.000 description 2
- 239000004288 Sodium dehydroacetate Substances 0.000 description 2
- 239000000205 acacia gum Substances 0.000 description 2
- 235000010489 acacia gum Nutrition 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- NPERTKSDHFSDLC-UHFFFAOYSA-N ethenol;prop-2-enoic acid Chemical compound OC=C.OC(=O)C=C NPERTKSDHFSDLC-UHFFFAOYSA-N 0.000 description 2
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 2
- 239000008273 gelatin Substances 0.000 description 2
- 229920000159 gelatin Polymers 0.000 description 2
- 235000019322 gelatine Nutrition 0.000 description 2
- 235000011852 gelatine desserts Nutrition 0.000 description 2
- 239000001863 hydroxypropyl cellulose Substances 0.000 description 2
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 description 2
- 235000015110 jellies Nutrition 0.000 description 2
- 239000008274 jelly Substances 0.000 description 2
- 229940094522 laponite Drugs 0.000 description 2
- XCOBTUNSZUJCDH-UHFFFAOYSA-B lithium magnesium sodium silicate Chemical compound [Li+].[Li+].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Na+].[Na+].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3.O1[Si](O2)([O-])O[Si]3([O-])O[Si]1([O-])O[Si]2([O-])O3 XCOBTUNSZUJCDH-UHFFFAOYSA-B 0.000 description 2
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 2
- 238000005191 phase separation Methods 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 2
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 2
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 229940079839 sodium dehydroacetate Drugs 0.000 description 2
- 235000019259 sodium dehydroacetate Nutrition 0.000 description 2
- DSOWAKKSGYUMTF-GZOLSCHFSA-M sodium;(1e)-1-(6-methyl-2,4-dioxopyran-3-ylidene)ethanolate Chemical compound [Na+].C\C([O-])=C1/C(=O)OC(C)=CC1=O DSOWAKKSGYUMTF-GZOLSCHFSA-M 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 229920003002 synthetic resin Polymers 0.000 description 2
- 239000000057 synthetic resin Substances 0.000 description 2
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 description 1
- UBVSIAHUTXHQTD-UHFFFAOYSA-N 2-n-(4-bromophenyl)-1,3,5-triazine-2,4-diamine Chemical compound NC1=NC=NC(NC=2C=CC(Br)=CC=2)=N1 UBVSIAHUTXHQTD-UHFFFAOYSA-N 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 238000012695 Interfacial polymerization Methods 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 1
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229960000686 benzalkonium chloride Drugs 0.000 description 1
- CADWTSSKOVRVJC-UHFFFAOYSA-N benzyl(dimethyl)azanium;chloride Chemical compound [Cl-].C[NH+](C)CC1=CC=CC=C1 CADWTSSKOVRVJC-UHFFFAOYSA-N 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000012732 erythrosine Nutrition 0.000 description 1
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 1
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 229920000578 graft copolymer Polymers 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000002502 liposome Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- DVEKCXOJTLDBFE-UHFFFAOYSA-N n-dodecyl-n,n-dimethylglycinate Chemical compound CCCCCCCCCCCC[N+](C)(C)CC([O-])=O DVEKCXOJTLDBFE-UHFFFAOYSA-N 0.000 description 1
- XULSCZPZVQIMFM-IPZQJPLYSA-N odevixibat Chemical compound C12=CC(SC)=C(OCC(=O)N[C@@H](C(=O)N[C@@H](CC)C(O)=O)C=3C=CC(O)=CC=3)C=C2S(=O)(=O)NC(CCCC)(CCCC)CN1C1=CC=CC=C1 XULSCZPZVQIMFM-IPZQJPLYSA-N 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229960003885 sodium benzoate Drugs 0.000 description 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 1
- 229960004025 sodium salicylate Drugs 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000001593 sorbitan monooleate Substances 0.000 description 1
- 235000011069 sorbitan monooleate Nutrition 0.000 description 1
- 229940035049 sorbitan monooleate Drugs 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Landscapes
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Description
【発明の詳細な説明】 ［産業上の利用分野］ 本発明は、新規な芳香剤に関するものである。Description: TECHNICAL FIELD The present invention relates to a novel fragrance.
［従来の技術］ 高吸水性粒子を用いて芳香剤に利用する方法として、
高吸水性粒子、香料、界面活性剤、水等を配合しゼリー
状の芳香剤を各種容器に入れ一定の形状をしたもの、及
１、吸水性合成樹脂、油性香料、含水無晶形酸化ケイ素
等を主成分とし水を加えることによりゲル化する芳香性
ゼリー化用成型組成物（特開昭57ー183854）がある。[Prior art] As a method of using a superabsorbent particle as a fragrance,
Highly water-absorbing particles, fragrance, surfactant, water, etc., into which various forms of jelly-like fragrance are put in various containers, and water-absorbing synthetic resin, oily fragrance, hydrous amorphous silicon oxide, etc. There is a molding composition (JP-A-57-183854) for forming an aromatic jelly, which is made into a gel by adding water and containing water as a main component.
［発明が解決しようとする問題点］ 上記の手段において、最初から、一定形状をなす芳香
剤は、使用者が任意の容器を使用することはできず、、
又、その使用量を調整するのは困難である。又、水を加
える事によりゲル化する芳香性ゼリー化組成物において
は、含水無晶形酸化ケイ素等を使用している為、その触
媒活性により香料が経時的に変化し、長期間保存するこ
とができない。[Problems to be Solved by the Invention] In the above-mentioned means, from the beginning, a fragrance having a certain shape cannot be used by a user in an arbitrary container,
Also, it is difficult to adjust the amount used. Further, in the aromatic jellified composition which gels by adding water, since hydrated amorphous silicon oxide or the like is used, the fragrance changes over time due to its catalytic activity, and it can be stored for a long time. Can not.
［問題を解決するための手段］ 本発明は、それらの問題を解決する為に、少なくとも
吸水倍率50の粒子及び水溶性のカプセル化膜によりカプ
セル化した香料を含有することを特徴とする芳香性ゼリ
ー化組成物を提供するものである。[Means for Solving the Problems] In order to solve these problems, the present invention is characterized by containing at least particles having a water absorption ratio of 50 and a fragrance encapsulated by a water-soluble encapsulating film. It provides a jellified composition.
本発明に用いられる高吸水性粒子としては、現在市販
されている澱粉あるいはセルロースと無水マレイン酸等
とのグラフト重合体の架橋物（特公昭53ー46199、特公
昭53ー46200。市販品としては、三洋化成工業株式会社
製“サンウエット”がある。）、ビニルエステルと（メ
タ）アクリル酸エステルとの共重合体の鹸化物（特公昭
53ー37994。市販品としては、住友化学株式会社製“ス
ミカゲル”がある。）、アクリル酸アルカリ金属塩から
得られる自己架橋型アクリル酸アルカリ金属塩重合体
（特開昭53ー46389）、αーオレフィン類または重合性
ビニル化合物と無水マレイン酸誘導体との共重合体また
はそのアルカリ中和物の架橋体（特開昭56ー36504。市
販品としては、株式会社 クラレ製“イソバンゲル”が
ある。）、二酸化ケイ素、酸化マグネシウム等の混合物
（市販品としては、イギリス、ラポルテ インダストリ
リミデッド社製“ラポナイト”がある。）等がある
が、これらの中から使用目的に合ったものを用いればよ
い。Examples of the superabsorbent particles used in the present invention include crosslinked products of currently available starch or graft polymers of cellulose and maleic anhydride (JP-B-53-46199, JP-B-53-46200). Sanyo Kasei Kogyo Co., Ltd. “Sunwet”), a saponified product of a copolymer of vinyl ester and (meth) acrylic acid ester
53-37994. As a commercially available product, "Sumikagel" manufactured by Sumitomo Chemical Co., Ltd. is available. ), A self-crosslinkable alkali metal acrylate polymer obtained from an alkali metal acrylate (JP-A-53-46389), a copolymer of an α-olefin or a polymerizable vinyl compound and a maleic anhydride derivative, or an alkali thereof. Crosslinked product of neutralized product (JP-A-56-36504; commercially available products include "Isovangel" manufactured by Kuraray Co., Ltd.), and mixtures of silicon dioxide, magnesium oxide, etc. (commercially available products include Laporte Industry, UK) There is a "Laponite" manufactured by Limited, Inc.), and among them, those suitable for the purpose of use may be used.
本発明で用いられる香料は、天然香料、調合香料、及
び、それらの素材となる単品香料も含む香気物質全体を
言う。The fragrance used in the present invention refers to a natural fragrance, a compounded fragrance, and a whole fragrance substance including a single fragrance as a material thereof.
本発明でもちいられる香料のカプセル化法として、水
溶液からの相分離法、有機溶液系からの相分離法、界面
重合法、スプレードライング法、in situ重合法、液中
硬化被覆法（オリフィス法）、気中懸濁被覆法等があ
る。カプセルの大きさは,1nm〜10mmの範囲である。ま
た、水溶性のカプセル化膜の種類としては、水溶性高分
子、例えば、ゼラチン、アラビアゴム、ヒドロキシプロ
ピルセルロース、カルボキシメチルセルロース、ポリビ
ニルアルコール、ポリビニルピロリドン、ポリエチレン
グリコール等、やリポソーム等から使用目的に合った任
意のものを用いればよい。As a method for encapsulating a fragrance used in the present invention, a phase separation method from an aqueous solution, a phase separation method from an organic solution system, an interfacial polymerization method, a spray drying method, an in situ polymerization method, a curing-in-liquid coating method (orifice method). And an air suspension coating method. Capsule size ranges from 1 nm to 10 mm. The type of the water-soluble encapsulating film may be selected from water-soluble polymers such as gelatin, gum arabic, hydroxypropylcellulose, carboxymethylcellulose, polyvinyl alcohol, polyvinylpyrrolidone, polyethylene glycol, etc., and liposomes. Any arbitrary one may be used.
本発明で用いられるカプセル化膜と香料の配合比は、
カプセル化膜100に対し、香料１〜20の範囲（重量％）
である。又、高吸水性粒子とカプセル化した香料（カプ
セル化膜及び香料の量）の配合比は、高吸水性粒子100
に対し、カプセル化した香料１〜10000（重量％０）で
ある。The compounding ratio of the encapsulating film and the fragrance used in the present invention,
Perfume in the range of 1 to 20 (% by weight) based on the encapsulated membrane 100
It is. The mixing ratio of the superabsorbent particles and the encapsulated perfume (the amount of the encapsulated film and the perfume) is 100 superabsorbent particles.
In contrast, the encapsulated fragrance is 1 to 10000 (% by weight 0).
又、上記組成物に、例えば、赤色３号、赤色213号、
黄色４号、緑色３号、青色205号・・・等のタール系色
素、ソルビタンモノオレエート、ポリオキシエチレン
（40）硬化ヒマシ油、ラウリル硫酸ナトリウム、塩化ベ
ンザルコニウム、ラウリルジメチルアミノ酢酸ベタイン
・・・等の界面活性剤、安息香酸ナトリウム、サリチル
酸ナトリウム、デヒドロ酢酸ナトリウム、パラオキシ安
息香酸エチル・・・等の殺菌、防腐剤、安息香酸デナト
ニウム等の苦味剤を加えてもよい。Further, in the above composition, for example, Red No. 3, Red No. 213,
Tar dyes such as yellow No. 4, green No. 3, blue No. 205, etc., sorbitan monooleate, polyoxyethylene (40) hydrogenated castor oil, sodium lauryl sulfate, benzalkonium chloride, betaine lauryl dimethylaminoacetate. A surfactant such as sodium benzoate, sodium salicylate, sodium dehydroacetate, ethyl parahydroxybenzoate, etc., a preservative, and a bittering agent such as denatonium benzoate may be added.
［発明の作用］ 本発明の芳香性ゼリー化組成物は、香料が水溶性カプ
セル化膜によりカプセル化されている為、直接他の成分
による影響を受けることなく、長期の保存に耐えるもの
である。[Action of the Invention] The aromatic jellified composition of the present invention is resistant to long-term storage without being directly affected by other components since the flavor is encapsulated by the water-soluble encapsulating film. .
使用にあたっては、本発明の芳香性ゼリー化組成物１
に対し、0.1〜1000倍の水を加えることにより、瞬時に
水溶性カプセル化膜が溶解すると共に、高吸水性粒子に
より組成物全体がゲル化して、衝撃等によっても流動し
ない芳香を有するゼリーを形成する。Before use, the aromatic jellified composition 1 of the present invention
On the other hand, by adding 0.1 to 1000 times of water, the water-soluble encapsulating film is instantaneously dissolved, and the entire composition is gelled by the highly water-absorbing particles, and a jelly having an aroma that does not flow even by impact etc. Form.
［実施例］ 実施例によって本発明を更に詳細に説明する。尚、本
発明はこれにより限定されるものではない。配合量は重
量％である。[Examples] The present invention will be described in more detail with reference to Examples. Note that the present invention is not limited by this. The compounding amount is% by weight.
実施例ー１ （１）カプセル化香料 （香料：ゼラチン＝1:5） 60.0 （２）サンウエット 40.0 （３）黄色203号 微量 （製法） 成分（１）〜（３）を混合し製品とする。Example-1 (1) Encapsulated fragrance (flavor: gelatin = 1: 5) 60.0 (2) Sun wet 40.0 (3) Yellow No. 203 trace (Production method) Mix components (1) to (3) to obtain a product .
実施例ー２ （１）カプセル化香料 （香料：アラビアゴム＝1:9） 50.0 （２）スミカゲル 50.0 （３）安息香酸デナトニウム 微量 （製法） 成分（１）〜（３）を混合し製品とする。Example-2 (1) Encapsulated flavor (flavor: gum arabic = 1: 9) 50.0 (2) Sumika gel 50.0 (3) Trace amount of denatonium benzoate (Production method) Mix components (1) to (3) to obtain a product .
実施例ー３ （１）カプセル化香料 （香料：ヒドロキシプロピルセルロース＝1:20） 70.0 （２）イソバンゲル 29.8 （３）安息香酸ナトリウム 0.2 （製法） 成分（１）〜（３）を混合し製品とする。Example-3 (1) Encapsulated fragrance (perfume: hydroxypropylcellulose = 1: 20) 70.0 (2) Isovan gel 29.8 (3) Sodium benzoate 0.2 (Production method) Components (1) to (3) were mixed and mixed with a product. I do.
実施例ー４ （１）カプセル化香料 （香料：ポリビニルアルコール＝1:18） 19.0 （２）ラポナイト 80.5 （３）安息香酸ナトリウム 0.5 （製法） 成分（１）〜（３）を混合し製品とする。Example-4 (1) Encapsulated perfume (perfume: polyvinyl alcohol = 1: 18) 19.0 (2) Laponite 80.5 (3) Sodium benzoate 0.5 (Production method) Components (1) to (3) are mixed to form a product. .
実施例ー５ （１）カプセル化香料 （香料：ポリビニルピロリドン＝1:13） 70.0 （２）イソバンゲル 30.0 （３）青色205号 微量 （４）デヒドロ酢酸ナトリウム 微量 （５）安息香酸デナトニウム 微量 （製法） 成分（１）〜（５）を混合し製品とする。Example-5 (1) Encapsulated perfume (perfume: polyvinylpyrrolidone = 1: 13) 70.0 (2) Isovangel 30.0 (3) Blue No. 205 trace (4) Sodium dehydroacetate trace (5) Denatonium benzoate trace (production method) Components (1) to (5) are mixed to obtain a product.
［発明の効果］ 本発明により、香料が経時的に反応することがなく、
安定な香調を保つことができる。[Effect of the Invention] According to the present invention, the fragrance does not react with time,
A stable incense tone can be maintained.
従来の技術である粉体に香料を含浸させる方法（比較
例ー１、２）と実施例１〜５の香調の安定性をテストし
た。配合量は重量％である。A conventional technique of impregnating a powder with a fragrance (Comparative Examples 1 and 2) and the stability of the fragrance of Examples 1 to 5 were tested. The compounding amount is% by weight.
比較例ー１ （１）香料 5.0 （２）タルク 55.0 （３）サンウェット 45.0 （製法） 成分（１）を成分（２）に含浸させ成分（３）と混合し
製品とする。Comparative Example-1 (1) Fragrance 5.0 (2) Talc 55.0 (3) Sunwet 45.0 (Production method) The component (1) is impregnated with the component (2) and mixed with the component (3) to obtain a product.
比較例ー２ （１）香料 22.0 （２）結晶セルロース 15.0 （３）含水無晶形酸化ケイ素末 （ホワイト カーボン） 25.0 （４）粉末状シリカゲル 15.0 （５）イソバン系合成樹脂 23.0 （製法） 成分（１）〜（５）を混合して得た混合末を打錠機にか
け、常法により、製錠する。Comparative Example-2 (1) Fragrance 22.0 (2) Crystalline cellulose 15.0 (3) Hydrous amorphous silicon oxide powder (white carbon) 25.0 (4) Powdered silica gel 15.0 (5) Isoban synthetic resin 23.0 (Production method) Component (1) ) To (5) are mixed, and the resulting mixture is set on a tableting machine and tableted in a conventional manner.
（実験例） 香調の安定性を検討する為に、実施例１〜５及び、比
較例ー１、２の製品を密封容器に入れ、所定の期間40℃
に保った。その後各製品4gを200mlの水に加え、香調の
変化を検討した。(Experimental example) In order to examine the stability of the incense tone, the products of Examples 1 to 5 and Comparative Examples 1 and 2 were put in a sealed container and kept at 40 ° C for a predetermined period.
Kept. Thereafter, 4 g of each product was added to 200 ml of water, and the change of the incense tone was examined.
その結果を以下に示す。 The results are shown below.
以上の実験例から、本発明が従来の技術に比較して香
調の安定性が高く優れているとがわかる。 From the experimental examples described above, it can be seen that the present invention has higher and higher incense tone stability than the conventional technique.
以上のことから、本発明により、従来の技術にはな
い、経時的な香調の安定性が高く長期間の保存ができ、
室内又は戸外に於て、ガラスコップ、紙コップ、空かん
・・・等の任意の容器と水があれば必要に応じて自ら芳
香剤を作れる、芳香性ゼリー化組成物を提供する事がで
きる。From the above, according to the present invention, the stability of fragrance over time is high and can be stored for a long period of time, which is not available in the prior art.
Indoor or outdoor, it is possible to provide an aromatic jellified composition that can make a fragrance by itself if there is water and any container such as a glass cup, a paper cup, an empty can, etc. and water. .
───────────────────────────────────────────────────── フロントページの続き (56)参考文献 特開 昭63−260567（ＪＰ，Ａ) 特開 昭57−52458（ＪＰ，Ａ) 実開 昭63−158343（ＪＰ，Ｕ) 実開 昭63−40942（ＪＰ，Ｕ) 実開 昭57−163245（ＪＰ，Ｕ) ──────────────────────────────────────────────────続 き Continuation of the front page (56) References JP-A-63-260567 (JP, A) JP-A-57-52458 (JP, A) Actually open 1988-158343 (JP, U) Actually open 1988 40942 (JP, U) Actually open 57-163245 (JP, U)
Claims (1)
のカプセル化膜によりカプセル化した香料を含有するこ
とを特徴とする芳香性ゼリー化組成物。1. An aromatic jellified composition comprising at least particles having a water absorption ratio of 50 times and a fragrance encapsulated by a water-soluble encapsulating film.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62333212A JP2594082B2 (en) | 1987-12-28 | 1987-12-28 | Aromatic jellified composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62333212A JP2594082B2 (en) | 1987-12-28 | 1987-12-28 | Aromatic jellified composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH01171558A JPH01171558A (en) | 1989-07-06 |
| JP2594082B2 true JP2594082B2 (en) | 1997-03-26 |
Family
ID=18263570
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62333212A Expired - Fee Related JP2594082B2 (en) | 1987-12-28 | 1987-12-28 | Aromatic jellified composition |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2594082B2 (en) |
-
1987
- 1987-12-28 JP JP62333212A patent/JP2594082B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH01171558A (en) | 1989-07-06 |
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