JP2782591B2 - Perfuming molding materials and perfumes - Google Patents

Description

DETAILED DESCRIPTION OF THE INVENTION

[0001]

BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a perfume molding material obtained by mixing granules containing fine powder of Chinese herbs, and to a perfume formed using the same.
Add the excipient to the Chinese herb spice fine powder or a mixture of several Chinese herb spice fine powders, add a pigment and a binder, and granulate each different color to obtain the desired color pattern of the image. It is intended to provide an incense molding material obtained by mixing at least two or more kinds in order to produce it, or an incense molded into a predetermined shape using the same.

[0002]

2. Description of the Related Art Incense is used to create a world of scent from the scent when fired. And, as for each incense product, a product having a uniform aroma and a small variation was regarded as a good product. In addition, regarding the coloring of the appearance of the incense itself, conventionally, a dye or a pigment is kneaded at the time of manufacture and colored and extruded into a shape of incense. The method used is to add letters and patterns, alternately extrude or coextrude different-colored kneaded materials, and laminate or bind them together, but in any case, to obtain incense products with color changes Was difficult. Moreover, it was impossible to change the scent over time during incense burning.

[0003]

SUMMARY OF THE INVENTION According to the present invention, it is possible to make a shape with a color change in the appearance of an incense product,
Further, it is an object of the present invention to provide a molding compound for incense which can change its scent with the passage of time when burning an incense product, or an incense with a color pattern formed using the same.

[0004]

SUMMARY OF THE INVENTION The object of the present invention is to provide at least two kinds of granules containing (1) fine powder of Chinese herbs and having different colors and / or fragrances according to the present invention. (2) The incense molding material according to (1) above, wherein the granulated product has a particle size of 150 to 1300 μm, and (3) Chinese herbal medicine. A molding material for incense comprising a mixture of at least two kinds of granules having different colors and / or scents, including a fine powder of fragrance,
A molding material for incense, characterized in that the difference in density of the granulated material is in the range of 0 to 0.2 g / ml, and (4) containing fine powder of Chinese herb and having different colors and / or scents What is claimed is: 1. A molding material for incense which is obtained by mixing at least two kinds of granules, wherein a difference in density of said granules is in a range of 0 to 0.2 g / ml, and an average particle diameter or a distribution of particle diameters. The incense molding material having the same range and (5) the incense molding material according to any one of the above (1) to (4) are put into a molding die and compression molded. Achieved by incense, which is characterized by

[0005]

BEST MODE FOR CARRYING OUT THE INVENTION Hereinafter, the incense molding material and the incense according to the present invention will be described in detail. The molding material for incense of the present invention is prepared by first mixing fine powder of Chinese herbs, excipients, and inorganic components, adding a desired pigment, adding a binder, and granulating to produce a single-color granulated product. And then mixing the granules having different colors. Here, as the Chinese herb spice fine powder, fine powders such as kara, agarwood, white temple, cinnamon barn, cinch, sweet pine, frankincense, benzoin, Karaki incense, cold scent, Daifeng incense, etc. Alternatively, they may be used by mixing as desired. Next, as an excipient, crystalline cellulose,
Corn starch, potato starch, lactose, fructose and the like. Further, examples of the inorganic component include light anhydrous silicic acid, heavy anhydrous silicic acid, aluminum silicate, titanium oxide, calcium carbonate, magnesium hydroxide, and inorganic salts, hydroxides, and oxides exemplified by aluminum hydroxide. . These inorganic components function as excipients and play an important role together with pigments for the color shaping of the appearance of the incense in the present invention. Further, the inorganic component used here is related to the density of the granulated material obtained through granulation, and is also important in relation to the uniformity of dispersion of the granulated material in the molding process of the molding material for aroma.
Pigments added for coloring the granules include red-based food red No. 102, food red No. 2, food red No. 106,
Examples include yellow food yellow No. 4 such as rhodamine, blue food blue No. 1, methyl violet, methylene blue, and malachite green. The pigments used are important factors in relation to the colouration of the incense surface. Further, examples of the binder include pastes such as hydroxypropylcellulose, carboxymethylcellulose, and starch paste. Usually, these are used as an aqueous solution or an aqueous solution (an aqueous solution containing a solvent compatible with water, methanol, ethanol, propanol, acetone, tetrahydrofuran, etc.). The solution of the paste used here is colored with a dye pigment or the like, and by using this as a binder, it is possible to color the granulated material. can do.

[0006] Granulation is performed using a machine such as a basket granulator, a centrifugal granulator, a tumbling granulator, a fluidized bed granulator, a rotating disk fluidized bed granulator or the like, using materials other than a binder. Mix. The resulting mixture is allowed to adhere to the surface of the mixture particles while spraying an aqueous paste solution or aqueous solution. In order to uniformly adhere the binder to the particle surfaces of the mixture, it is preferable to spray the aqueous paste solution or aqueous solution intermittently several times and granulate while repeating spraying and drying of the particles. The granules thus obtained are sieved through a mesh screen. The mixture is sieved using a sieve having an opening of 1300 μm to remove large particles remaining on the sieve. Further, a 150 μm sieve is used to remove particles smaller than this, thus obtaining a granulated product having a particle size of 150 μm to 1300 μm. The particle size after sizing is preferably 150 μm to 1300 μm,
If it is small, it scatters during molding, and if it is large, moldability is poor. From the viewpoint of utilizing the difference in density when adjusting the composition for incense, and in addition, expressing the change in the scent at the time of perfume and the change in the apparent color, the thickness is preferably 180 μm to 850 μm. The granules obtained here can be further divided into several sizes by using sieves having different sizes of openings. For example, 1180, 858, 500, 355, 18
Screen with a 0 μm sieve. As a result, granules having different densities can be obtained, and depending on which size is used more frequently, there is a relation with the density of the pattern on the incense surface described later.

The granules thus obtained have different colors (fine powder of Chinese herbs, excipients (including inorganic components),
And at least two kinds thereof (including coloring based on a material such as a binder) are mixed to obtain an incense molding material. Here, when the perfume molding material is molded into perfume, a lubricant may be added so that the perfume molding material can be easily filled into a molding die, and the lubricant may be talc. , Magnesium stearate, silica and the like can be used.
At this time, the size difference between the selected granules and the size of the granules should be selected and used as the molding material for incense. That is, it is related to the color pattern. In other words, if the particle size is close, the color distinction will not show a noticeable appearance, and if the particle size is far away, the color distinction will have a locally apparent appearance. . In addition, when mixing granules having the same particle size and different colors, if there is a difference in the density of the granules, the incense obtained by molding the molding material for incense is applied to the front and back surfaces. The result is a different color pattern. According to the study of the present inventors, the difference in density was 0.2 g.
/ Ml or more, the particles are unevenly distributed or separated when the particles move from the hopper to the molding die, and further, are unevenly distributed in the mold due to mechanical vibration during the compression molding, resulting in fragrance or colored particles. Has been found to be extremely unevenly distributed, which is not preferable for obtaining a suitably dispersed molded product. Therefore, the incense obtained by molding the incense molding material obtained by mixing the granules having a difference of more than 0.2 g / ml in density exhibits, for example, different color patterns on the front surface and the back surface.

[0008] Further, the Chinese herb flavoring powder used in one granulated material and the other granulated material of the incense flavoring material is different from each other in flavor, so that the Chinese herbal flavoring material in the incense is different. The distribution of the powder can be changed, realizing the change of the scent during burning.

The molding material for incense according to the present invention is formed into incense of various shapes by a compression molding method. The obtained incense can be made into various arbitrary shapes as long as the shape can make the mold. For example, cones, cylinders, prisms, polygons, geometric patterns, sectors, flowers, birds,
It can be shaped into animals and plants such as fish, incense sticks, etc.
Further, the incense shaped into these shapes can be arbitrarily processed according to the purpose such as patterning, engraving of characters and the like, embossing. For the compression molding, for example, a rotary molding device or a hydraulic molding device can be used, and the mold can be used by changing the mold of a known tableting machine into a desired shape.

In order to help the understanding of the present invention, some examples of incense made using the incense molding material of the present invention are shown in FIGS. 1 to 3, which limit the present invention. Not something. 1 to 3 are perspective views of the formed incense. The incense shown in FIG. 1 is obtained by mixing two types of granules having different colors in equal amounts and compression-molding, and is a perfume in which a marble-like color pattern is drawn. The incense shown in FIGS. 2 and 3 is a mixture of three types of granules having different types of Chinese herbal fragrance fine powder and different colors, and compression-molded by mixing equal amounts.
When it is fired, it is a perfume that creates a marble-like color pattern as well as changes in the scent. The incense shown in the figure is a two-color or three-color molding, but a plurality of four or more colors can be formed by the same method. The incense shown in Fig. 2 is an image of a snow crystal, and is a granulated product obtained by granulating three types of fine powder of Chinese herbal fragrances according to the image of snow, each separately adding an excipient and a different pigment. Are mixed in equal amounts and compression molded. You can enjoy a dreamy snowy world from the change of shape, color and fragrance. Needless to say, this snow crystal-shaped incense can also be formed by a granulated material containing many colors and several kinds of fine Chinese herbs. The incense shown in FIG. 3 is substantially in the shape of a stick, and is obtained by mixing and compressing granules obtained by coloring and granulating three types of fine powders of Chinese herb spice separately and compressing them. You can enjoy the change. Similarly, it is possible to infinitely widen the change in fragrance depending on the combination, amount, shape, color, and the like of the granules.

An example of the composition of a granulated material containing fine powder of Chinese herb in the practice of the present invention is as follows, but the composition of the granulated material according to the present invention is not limited to the following. .

Composition% by weight Chinese herb spice fine powder 40-60 Crystalline cellulose 10-20 Aluminum silicate 5-20 Potato starch 5-20 Light anhydrous silicic acid 5-10 Tub powder 5-10 Paste 2-10 Oxidizing agent 1-5 Dyes 0.1 to 1 The incense obtained by compression-molding the incense molding material provided by the present invention has a color appearance, that is, a color pattern, in appearance. Is caused.

Hereinafter, the present invention will be described more specifically based on examples. ○ Example 1 5 parts of agarwood, 3 parts of cinnamon, 2 parts of cloves, 500 g of mixed powder, 80 g of crystalline cellulose, 100 g of aluminum silicate, 80 g of potato starch, 60 g of light anhydrous silicic acid, and 50 g of tub powder were placed in a fluidized bed granulating dryer. Blow and mix. While maintaining the intake air temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C., the mixture is colored and dried while intermittently spraying 500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 10 g of Food Red No. 102 in distilled water in advance. Then, add hydroxypropylcellulose 3 to distilled water.
700 g of the solution in which 0 g is dissolved is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product A.
Next, 5 parts of agarwood, 3 parts of cinnamon bark, 2 parts of incense powder 500 mixed powder
g, crystalline cellulose 80 g, aluminum silicate 100
g, potato starch (80 g), light anhydrous silicic acid (60 g), and tub powder (50 g) are put into a fluidized bed granulation dryer, blown, and mixed. While maintaining the intake air temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C., 30 g of the oxidizing agent and edible yellow No. 1 were added to distilled water in advance.
While intermittently spraying 500 g of a liquid in which 0 g is dissolved, coloring and drying are performed. Subsequently, 700 g of a solution prepared by dissolving 30 g of hydroxypropylcellulose in distilled water was added at 10 ml / mi.
granulated and dried while intermittently spraying at intervals of n.
Get. The obtained granules A and B have openings of 850 μm.
The particles are classified using a sieve of m and 180 μm to remove particles larger than 850 μm and particles smaller than 180 μm. Each density is 0.28 g / ml for A and 0.29 g / ml for B
Met. Each of the sized granules A and B 500 each
5 g each of magnesium stearate as lubricant
And mix. The resulting mixture is passed through a 35 m longest part.
m and a 2.5 mm-thick chevron were filled into a mold and compression-molded. Colored particles were not unevenly distributed on both the front and back surfaces, and a fragrance in which red and yellow were mixed, reminiscent of autumn mountains, was obtained (see FIG. 1).

Example 2 500 g of mixed powder of agarwood, clove, and cinnamon were mixed, 80 g of crystalline cellulose, 100 g of aluminum silicate, 80 g of potato starch, 60 g of light anhydrous silicic acid, and 50 g of tub powder were placed in a fluidized bed granulating dryer. Blow and mix. While maintaining the intake air temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C., the mixture is colored and dried while intermittently spraying 500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 10 g of methylene blue in distilled water in advance. Subsequently, 700 g of a liquid in which 30 g of hydroxypropylcellulose is dissolved is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product C. Next, 500 g of a mixed powder of equal amounts of Ryuen, Toji and Kanmatsu, 90% crystalline cellulose
g, aluminum silicate 80 g, potato starch 100
g, 50 g of light anhydrous silicic acid, and 50 g of tub powder are put into a fluidized bed granulation dryer, blown, and mixed. Intake air temperature in the fluidized bed 7
500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 5 g of methylene blue in distilled water in advance while maintaining the temperature at 0 ° C. and the product temperature at 40 ° C.
While drying intermittently. Subsequently, 700 g of a liquid obtained by dissolving 20 g of hydroxypropyl cellulose in distilled water is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product D. Similarly, a mixed powder of white powder, benzoic acid, and licorice in an equal amount of 500 g, crystalline cellulose 110
g, aluminum silicate 50 g, potato starch 80 g,
60 g of light anhydrous silicic acid and 40 g of tub powder are put into a fluidized bed granulator, blown, and mixed. Intake temperature 70 in the fluidized bed
While maintaining the temperature at 40 ° C. and the product temperature at 40 ° C., color drying is performed while intermittently spraying in advance 500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 1 g of methylene blue in distilled water. Subsequently, a solution 7 in which 20 g of hydroxypropyl cellulose was dissolved in distilled water
00g is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product E. Obtained granules C and D
And E were classified using a sieve having openings of 850 μm and 180 μm, and particles having a size larger than 850 μm were removed.
Also excludes smaller particles. Each density is 0.28 g / C
ml, D was 0.28 g / ml, and E was 0.25 g / ml. Granules C, D and E thus sized 50 each
0 g each, magnesium stearate 5 as a lubricant
Add g and mix. The resulting mixture was added to the longest part 20.2
mm and a thickness of 2.5 mm were filled in a mold for forming a snow crystal and compression-molded. A beautiful incense was obtained, reminiscent of a falling snow world in which colored particles are not unevenly distributed on both the front and back surfaces (see FIG. 2).

Example 3 500 g of mixed powder of agarwood, clove, and cinnamon were mixed, 80 g of crystalline cellulose, 100 g of aluminum silicate, 80 g of potato starch, 60 g of light anhydrous silicic acid, and 50 g of tub powder were placed in a fluidized bed granulating dryer. Blow and mix. Liquid 5 prepared by previously dissolving 30 g of oxidizing agent and 10 g of Food Blue No. 1 in distilled water while maintaining the intake temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C.
Coloring and drying is performed while intermittently spraying 00 g. Subsequently, 700 g of a liquid obtained by dissolving 30 g of hydroxypropylcellulose in distilled water is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product F. Next, 500 g of mixed powder of equal volume of Ry 脳 n, T 字 ji, and Kanmatsu, 90 g of crystalline cellulose, 80 g of aluminum silicate, and 10 g of potato starch.
0 g, light anhydrous silicic acid 50 g, and tub powder 50 g are put into a fluidized bed granulation dryer, blown, and mixed. 500 g of a liquid obtained by previously dissolving 30 g of the oxidizing agent and 5 g of Food Blue No. 1 in distilled water while maintaining the intake temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C.
While drying intermittently. Subsequently, a liquid 7 obtained by dissolving 20 g of hydroxypropylcellulose in distilled water 7
00g is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product G. Similarly, a mixed powder of white powder, benzoic acid, and licorice in an equal amount of 500 g, crystalline cellulose 110
g, aluminum silicate 50 g, potato starch 80 g,
60 g of light anhydrous silicic acid and 40 g of tub powder are put into a fluidized bed granulator, blown, and mixed. Intake temperature 70 in the fluidized bed
While maintaining the temperature at 40 ° C. and the product temperature at 40 ° C., the mixture is colored and dried while intermittently spraying 500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 1 g of Food Blue No. 1 in distilled water in advance. Subsequently, a liquid 70 prepared by dissolving 20 g of hydroxypropylcellulose in distilled water was used.
0 g is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product H. The obtained granules F, G, and H were classified using a sieve having openings of 850 μm and 180 μm, and particles having a size larger than 850 μm were excluded, and particles having a size smaller than 180 μm were also excluded. Each density is F 0.30 g / m
1, G was 0.28 g / ml and H was 0.26 g / ml. Granules F, G and H thus sized 900 each
g, 500 g, and 100 g, and 5 g of magnesium stearate as a lubricant is added and mixed. The obtained mixture was filled into a linear mold having a longest part of 40.5 mm and a thickness of 2.5 mm and compression-molded. A beautiful incense was obtained, reminiscent of a falling snow world in which colored particles are not unevenly distributed on both the front and back sides, and the scent changes with time (see FIG. 3).

Reference Example 5 parts of agarwood, 3 parts of cinnamon, 2 parts of incense, 500 g of mixed powder, 80 g of crystalline cellulose, 100 g of aluminum silicate, 80 g of potato starch, 60 g of light anhydrous silicic acid, and 50 g of tub powder were placed in a fluidized bed granulating dryer. Put, blow, mix. While maintaining the intake air temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C., the mixture is colored and dried while intermittently spraying 500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 10 g of the red pigment in distilled water in advance. Subsequently, 700 g of a solution obtained by dissolving 30 g of hydroxypropyl cellulose in distilled water is granulated and dried while intermittently spraying at an interval of 10 ml / min to obtain a granulated product A ′. Next, 5 parts of agarwood, 3 parts of cinnamon bark, 2 parts of cloves, 500 g of mixed powder,
80 g of crystalline cellulose, 100 g of aluminum silicate, 80 g of potato starch, 60 g of heavy silicic anhydride, 50 g of tub powder
g into a fluidized bed granulator, blow and mix. While maintaining the intake air temperature in the fluidized bed at 70 ° C. and the product temperature at 40 ° C., it is colored and dried while intermittently spraying 500 g of a solution prepared by dissolving 30 g of the oxidizing agent and 10 g of the yellow pigment in distilled water in advance.
Subsequently, 30 g of hydroxypropyl cellulose was added to distilled water.
Is granulated and dried intermittently at an interval of 10 ml / min to obtain a granulated product B ′. The obtained granules A ′ and B ′ had openings of 850 μm and 1
Classify using an 80 μm sieve to remove particles larger than 850 μm and smaller than 180 μm. The density of each of A 'was 0.27 g / ml and that of B' was 0.49 g / ml. The granules A 'and B', each of which is thus sized, are 50
0 g each, magnesium stearate 5 as a lubricant
Add g and mix. The resulting mixture is passed through a 35 m longest part.
When filled into a mold for forming a chevron having a thickness of 2.5 mm and a thickness of 2.5 mm, the particles were compression-molded.

The following table lists the components and amounts used in the examples and comparative examples.

[0018]

[Table 1]

[0019]

As described above, according to the present invention,
By using different coloring materials for one granulated material and another granulated material for the incense molding material, it is possible to obtain an incense having a beautiful appearance with a color pattern. At this time, by setting the density difference of the granules within a predetermined value, uneven distribution of the granules can be eliminated. In addition, the distribution of the Chinese herb fragrance fine powder in the fragrance can be achieved by making the Chinese herbal fragrance fine powder used for one granulated material and the other granulated material different in incense. To change the scent during the burning of the incense.

[Brief description of the drawings]

FIG. 1 is a perspective view showing a specific example of a perfume produced using the perfume molding material of the present invention.

FIG. 2 is a perspective view showing another example of incense produced using the incense molding material of the present invention.

FIG. 3 is a perspective view showing another example of an incense produced using the incense molding material of the present invention.

Claims (5)

(57) [Claims] 1. An incense molding material comprising a mixture of at least two types of granules containing fine powder of Chinese herbs and fragrances having different colors and / or fragrances. 2. The granulated product has a particle size of 150 to 1300.
The molding material for incense according to claim 1, wherein the thickness is μm. 3. A molding material for incense, comprising a fine powder of Chinese herbs and a mixture of at least two types of granules having different colors and / or fragrances, wherein the difference in density between the granules is 0-0.
A molding material for incense, which is in the range of 2 g / ml. 4. A molding material for incense, comprising a fine powder of a Chinese herb and a mixture of at least two types of granules having different colors and / or fragrances, wherein the difference in density between the granules is 0-0.
A molding material for incense, which is in the range of 2 g / ml and has the same average particle size or distribution range of particle size. 5. An incense, wherein the incense molding material according to any one of claims 1 to 4 is placed in a molding die and compression molded.