JP3100142B2 - Production method of muddy shochu - Google Patents
Production method of muddy shochuInfo
- Publication number
- JP3100142B2 JP3100142B2 JP01243436A JP24343689A JP3100142B2 JP 3100142 B2 JP3100142 B2 JP 3100142B2 JP 01243436 A JP01243436 A JP 01243436A JP 24343689 A JP24343689 A JP 24343689A JP 3100142 B2 JP3100142 B2 JP 3100142B2
- Authority
- JP
- Japan
- Prior art keywords
- shochu
- muddy
- production method
- ultrasonic treatment
- oily
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000020083 shōchū Nutrition 0.000 title claims description 42
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 238000009210 therapy by ultrasound Methods 0.000 claims description 9
- 235000014113 dietary fatty acids Nutrition 0.000 description 6
- 229930195729 fatty acid Natural products 0.000 description 6
- 239000000194 fatty acid Substances 0.000 description 6
- -1 fatty acid ester Chemical class 0.000 description 5
- 235000019640 taste Nutrition 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- XIRNKXNNONJFQO-UHFFFAOYSA-N ethyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC XIRNKXNNONJFQO-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 238000001944 continuous distillation Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- FMMOOAYVCKXGMF-MURFETPASA-N ethyl linoleate Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCC FMMOOAYVCKXGMF-MURFETPASA-N 0.000 description 1
- 229940031016 ethyl linoleate Drugs 0.000 description 1
- 229940067592 ethyl palmitate Drugs 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- FMMOOAYVCKXGMF-UHFFFAOYSA-N linoleic acid ethyl ester Natural products CCCCCC=CCC=CCCCCCCCC(=O)OCC FMMOOAYVCKXGMF-UHFFFAOYSA-N 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
- 238000000527 sonication Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Landscapes
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Description
【発明の詳細な説明】 [産業上の利用分野] 本発明は乙類焼酎の製造法に関し、より具体的には、
焼酎中の呈味成分である高級脂肪酸エステルを高濃度で
焼酎中に混濁させた状態において、安定性のある濁り焼
酎の製造法に係わる。[Detailed description of the invention] [Industrial application field] The present invention relates to a method for producing a second class shochu, more specifically,
The present invention relates to a method for producing a stable turbid shochu in a state where a higher fatty acid ester as a taste component in the shochu is turbidized in the shochu at a high concentration.
[従来の技術] 本格焼酎とも呼ばれる乙類焼酎は、単式蒸留法によっ
て得られる焼酎であり、連続蒸留法による甲類焼酎と異
なり、原料に由来する固有の香味を有している。近年、
製法の改良により、その独特の香味を柔げ、広く一般の
嗜好に合うように改良されてきているが、焼酎の多様化
が進む中で、昔ながらの濁り焼酎を希望する声も多くな
っている。[Prior Art] Class B shochu, also called full-scale shochu, is shochu obtained by a simple distillation method, and has a unique flavor derived from raw materials, unlike shochu shochu by a continuous distillation method. recent years,
By improving the manufacturing method, its unique flavor has been softened, and it has been improved to meet general tastes.However, with the diversification of shochu, many people are hoping for a traditional muddy shochu. .
乙類焼酎中には、呈味成分として、パルミチン酸エチ
ル,リノール酸エチルといった高級脂肪酸エステルが含
まれており、これらの成分が、焼酎に濃醇さを付与して
いるが、これらが多過ぎると、浮上して空気酸化され、
分解して油様の異臭を発生し、また気温が低下すると、
溶解度が落ちてオリとなって析出し、商品価値を著しく
損なうことになる。そのため、広く普及している透明な
乙類焼酎は、一度ろ過して上記成分を除去して出荷して
いるが、濃醇さを特徴とする濁り焼酎は、一般に原酒を
ろ過せずにそのまま割水して製品としている。The second class shochu contains higher fatty acid esters such as ethyl palmitate and ethyl linoleate as taste components, and these components impart richness to the shochu, but these are too much. And it floats up and is oxidized in the air,
Decomposes to produce an oily off-flavor and when the temperature drops,
Solubility drops and deposits as drips, significantly impairing commercial value. For this reason, transparent Otsu Shochu, which is widely used, is filtered once to remove the above components before shipping. However, muddy Shochu, which is characterized by its richness, is generally split without filtering the original sake. The product is watered.
[発明が解決しようとする課題] 然しながら、従来の濁り焼酎の製造法では、高級脂肪
酸エステルによる前述の問題があるため、焼酎の濁度
は、せいぜい35(▲OD10 660▼)前後までしか濁らせる
ことはできない。また、これ以下であっても、時間経過
に伴なって浮上分離が生じたり、気温の低下に伴なっ
て、オリを発生する虞れが高い。[Problems to be Solved by the Invention] However, in the conventional method for producing turbid shochu, the turbidity of shochu is reduced to about 35 (▲ OD 10 660 ▼) at most because of the above-mentioned problem caused by the higher fatty acid ester. I can't do that. Even below this, there is a high risk that flotation will occur with the passage of time, and that ori will occur as the temperature drops.
そこで、本発明は上記従来製法による濁り焼酎の欠点
を解消し、呈味成分でもある油性成分を高濃度で安定さ
せた濁り焼酎を製造する方法を提供するものである。Accordingly, the present invention is to provide a method for producing a cloudy shochu in which the disadvantages of the cloudy shochu produced by the above-mentioned conventional production method are solved and an oily component which is also a taste component is stabilized at a high concentration.
[課題を解決するための手段] 本発明は、蒸留後の乙類焼酎を5〜10分間かけて超音
波処理することを特徴とする。[Means for Solving the Problems] The present invention is characterized in that the distilled shochu after the distillation is subjected to ultrasonic treatment for 5 to 10 minutes.
超音波処理は、蒸留後直ぐに行なってもよいし、貯蔵
して、油性成分が浮上した後に行なって、均一分散させ
てもよい。The ultrasonic treatment may be performed immediately after the distillation, or may be performed after the oil component has been stored and floated, and may be uniformly dispersed.
また、一般的に透明乙類焼酎製造のろ過工程で得られ
る油性成分や、貯蔵中に浮上した油性成分など、一旦焼
酎から分離した油性成分を超音波処理して、これを焼酎
に添加し、高濃度の濁り焼酎とすることもできる。この
方法によれば、濁度と香味を、目的に応じて広範囲に設
定し得るので、多様且つ酒質的に安定した濁り焼酎を製
造することが可能となる。In addition, generally, the oily components obtained in the filtration step of the production of transparent shochu, and the oily components that floated during storage, such as the oily components once separated from the shochu, were subjected to ultrasonic treatment and added to the shochu. It can also be a high concentration turbid shochu. According to this method, the turbidity and the flavor can be set in a wide range according to the purpose, so that it is possible to produce various and liquor stable turbid shochu.
超音波処理の条件は、乙類焼酎の種類、含有する油性
成分の量によって適宜選択するが、通常、波長20〜50KH
z、処理時間は5〜10分である。The conditions of the ultrasonic treatment are appropriately selected depending on the type of the second kind shochu and the amount of the oil component contained, but usually, the wavelength is 20 to 50 KH.
z, processing time is 5-10 minutes.
[作用] 焼酎中に含まれている高級脂肪酸、或いは高級脂肪酸
エステルは、Cu,Fe等の金属イオンを核にしてイオン的
な結合を形成し、これが、オリとして凝集沈澱すること
が知られているが、後述する通り、超音波処理は、これ
を単に一時的に破壊して分散性を高めるにとどまらず、
長期間に亘って、その分散性及び安定性が維持されるこ
とが判明した。従来では全く不可能であった高濃度の濁
り焼酎を油性成分の浮上またはオリの沈澱を伴なうこと
なく、長期間に亘って安定に維持し得ることは、乙類焼
酎の中の他の各種成分との相互関係において、超音波処
理後に極めて安定なコロイド状態が形成されたものと考
えることができる。[Action] It is known that higher fatty acids or higher fatty acid esters contained in shochu form ionic bonds with metal ions such as Cu and Fe as nuclei, and these coagulate and precipitate as drips. However, as will be described later, sonication not only breaks this temporarily to improve dispersibility,
It has been found that its dispersibility and stability are maintained over a long period of time. The ability to maintain high-concentration turbid shochu, which was impossible at all in the past, over a long period of time without the floating of oily components or sedimentation of slime, is another type of liquor in the class B shochu. In relation to the various components, it can be considered that a very stable colloidal state was formed after the ultrasonic treatment.
[実施例] 以下に本発明の実施例を示す。[Example] An example of the present invention will be described below.
常法に従って芋焼酎を製造し、貯蔵中に、表面に分離
浮上した油性成分を焼酎の一部と共に掬い取った。この
分別分(アルコール度25%、油性成分0.1%以上)を、
超音波発生装置の処理槽に入れるか、または振動子を容
器の中に入れて、20〜50KHzで5〜10分間超音波処理を
行ない、この処理物を、濁度5(▲OD10 660▼)の通常
の乙類焼酎に適量添加して、表1に示す各濁度の焼酎を
造った。また、対照として、超音波処理しない上記分別
分を同量添加して対照焼酎を造り、それぞれ1ケ月後の
濁度、性状、口利酒の結果を表1に示した。A potato shochu was produced according to a conventional method, and during storage, oily components separated and floated on the surface were scooped together with a part of the shochu. This fraction (alcohol 25%, oily component 0.1% or more)
Put in the treatment tank of the ultrasonic generator or put the vibrator in the container and perform ultrasonic treatment at 20 to 50 KHz for 5 to 10 minutes. The treated product is turbidity 5 (▲ OD 10 660 ▼) ) Was added in an appropriate amount to the ordinary type B shochu to produce shochu having each turbidity shown in Table 1. As a control, the same amount of the above fractions without ultrasonic treatment was added to produce a control shochu, and the results of turbidity, properties and liquor after one month are shown in Table 1.
超音波処理しない上記分別分は、添加直後に分離して
しまい、安定した懸濁状態とすることはできなかった。The fractions not subjected to ultrasonic treatment were separated immediately after the addition and could not be brought into a stable suspension state.
これに対して、本発明に従って超音波処理した濁り焼
酎は、何れの濁度においても、油性成分が分離せず、1
ケ月後においても安定で、酒質の劣化も見られなかっ
た。On the other hand, the muddy shochu ultrasonically treated according to the present invention does not separate oily components at any turbidity, and
Even after a month, it was stable and no deterioration of the sake quality was observed.
[発明の効果] 以上説明した通り、本発明の方法によれば、濁り焼酎
中の油性成分を長期間に亘って極めて安定な状態とする
ことができ、従来では困難であった濁度100以上の濁り
焼酎の製造も可能となる。このため、呈味成分である高
級脂肪酸エステルを高濃度に焼酎中に採り込むことがで
き、より濃醇で、而も安定した酒質の濁り焼酎を提供す
ることができる。 [Effects of the Invention] As described above, according to the method of the present invention, the oily component in muddy shochu can be made to be in an extremely stable state for a long period of time. Shochu can be produced. For this reason, the higher fatty acid ester as a taste component can be incorporated into shochu at a high concentration, and it is possible to provide a richer and more stable alcoholic turbid shochu.
Claims (1)
音波処理することを特徴とする濁り焼酎の製造法。1. A method for producing turbid shochu, comprising subjecting a distilled shochu to an ultrasonic treatment for 5 to 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP01243436A JP3100142B2 (en) | 1989-09-21 | 1989-09-21 | Production method of muddy shochu |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP01243436A JP3100142B2 (en) | 1989-09-21 | 1989-09-21 | Production method of muddy shochu |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP31251398A Division JP3285831B2 (en) | 1989-09-21 | 1998-11-02 | Production method of muddy shochu |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH03108473A JPH03108473A (en) | 1991-05-08 |
| JP3100142B2 true JP3100142B2 (en) | 2000-10-16 |
Family
ID=17103844
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP01243436A Expired - Fee Related JP3100142B2 (en) | 1989-09-21 | 1989-09-21 | Production method of muddy shochu |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP3100142B2 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6660105B1 (en) | 1997-07-22 | 2003-12-09 | Nippon Steel Corporation | Case hardened steel excellent in the prevention of coarsening of particles during carburizing thereof, method of manufacturing the same, and raw shaped material for carburized parts |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100830733B1 (en) * | 2006-01-17 | 2008-05-20 | 임경아 | How to prepare distilled Chinese medicine |
| WO2012165272A1 (en) | 2011-06-03 | 2012-12-06 | サントリーホールディングス株式会社 | Mixed distilled liquor and method for producing same |
| JP6969037B2 (en) * | 2019-08-05 | 2021-11-24 | 霧島ホールディングス株式会社 | Alcohol-containing O / W emulsion and its manufacturing method |
-
1989
- 1989-09-21 JP JP01243436A patent/JP3100142B2/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6660105B1 (en) | 1997-07-22 | 2003-12-09 | Nippon Steel Corporation | Case hardened steel excellent in the prevention of coarsening of particles during carburizing thereof, method of manufacturing the same, and raw shaped material for carburized parts |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH03108473A (en) | 1991-05-08 |
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