Deprecated: The each() function is deprecated. This message will be suppressed on further calls in /home/zhenxiangba/zhenxiangba.com/public_html/phproxy-improved-master/index.php on line 456
JP3201842B2 - Manufacturing method of potatoes packed in pouches - Google Patents
[go: Go Back, main page]

JP3201842B2 - Manufacturing method of potatoes packed in pouches - Google Patents

Manufacturing method of potatoes packed in pouches

Info

Publication number
JP3201842B2
JP3201842B2 JP25295692A JP25295692A JP3201842B2 JP 3201842 B2 JP3201842 B2 JP 3201842B2 JP 25295692 A JP25295692 A JP 25295692A JP 25295692 A JP25295692 A JP 25295692A JP 3201842 B2 JP3201842 B2 JP 3201842B2
Authority
JP
Japan
Prior art keywords
pouch
potatoes
potato
pouches
packed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP25295692A
Other languages
Japanese (ja)
Other versions
JPH0698672A (en
Inventor
潤一 黒木
克伸 伊藤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dai Nippon Printing Co Ltd
Original Assignee
Dai Nippon Printing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dai Nippon Printing Co Ltd filed Critical Dai Nippon Printing Co Ltd
Priority to JP25295692A priority Critical patent/JP3201842B2/en
Publication of JPH0698672A publication Critical patent/JPH0698672A/en
Application granted granted Critical
Publication of JP3201842B2 publication Critical patent/JP3201842B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Storage Of Fruits Or Vegetables (AREA)

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】本発明は、パウチ詰め馬鈴薯の製
造方法および該製造方法で得られるパウチ詰め馬鈴薯に
関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a potato stuffed with pouches and to a potato stuffed potato obtained by the method.

【0002】[0002]

【従来の技術】従来、パウチ詰め馬鈴薯の製造方法とし
ては、剥皮・カッティング後の馬鈴薯を、必要に応じて
ブランチング処理を施した後、酸素バリアー性を付与し
た透明パウチ、またはアルミ箔を使用した不透明パウチ
に真空包装し、加圧加熱殺菌するのが一般的である。こ
の方法により製造された馬鈴薯製品は、外食産業の素
材、一般小売用として広く使用されている。
2. Description of the Related Art Conventionally, potatoes packed in pouches have been prepared by using peeled and cut potatoes, blanching if necessary, and then using transparent pouches or oxygen foils provided with oxygen barrier properties. It is common to vacuum package in a opaque pouch and sterilize it under pressure and heat. Potato products produced by this method are widely used as materials for the restaurant industry and for general retail use.

【0003】[0003]

【発明が解決しようとする課題】上記製造方法で製造さ
れた馬鈴薯製品は、酸素バリアー性を有するパウチによ
り包装されているが、加圧加熱殺菌時にパウチ内の酸素
による酸化褐変が起こったり、流通・保存時にパウチ内
に透過してくる酸素により褐変が起こったりしてその商
品価値を損なう場合があった。
The potato product produced by the above production method is packaged in a pouch having an oxygen barrier property. However, during sterilization under pressure and heat, browning due to oxygen in the pouch occurs, and -Oxygen permeating into the pouch during storage may cause browning or impair the commercial value of the pouch.

【0004】そこで、褐変を防止するために酸化防止剤
として亜硫酸塩が使用されるが、異臭の問題および消費
者の添加物に対する消費者の抵抗意識により、その使用
が困難である場合が多い。また、真空包装しているた
め、加圧加熱殺菌時にブロキングが発生し、取り出し難
いという問題もあった。
Therefore, sulfite is used as an antioxidant to prevent browning, but its use is often difficult due to the problem of unpleasant odor and the consumer's resistance to additives. In addition, there is also a problem that since the package is vacuum-packed, blocking occurs during sterilization under pressure and heat, and it is difficult to take out the product.

【0005】[0005]

【課題を解決するための手段】上記問題点を解決するた
め、本発明者らは鋭意研究を重ねた結果、脱酸素剤包装
体とともに脱気包装することがきわめて効果的であるこ
とを知見し、本発明を完成するに至った。すなわち、本
発明は、馬鈴薯を剥皮後、これを脱酸素剤包装体ととも
に酸素バリアー性を有するパウチ内に脱気包装し、加圧
加熱殺菌することを特徴とするパウチ詰め馬鈴薯の製造
方法にある。
Means for Solving the Problems In order to solve the above problems, the present inventors have conducted intensive studies and found that it is extremely effective to perform deaeration packaging together with an oxygen scavenger package. Thus, the present invention has been completed. That is, the present invention resides in a method for producing potatoes packed with pouches, comprising peeling potatoes, degassing and packaging them in a pouch having an oxygen barrier property together with a deoxidizer package, and sterilizing under pressure and heat. .

【0006】上記方法において、剥皮した馬鈴薯をパウ
チ内に脱気包装する前に、該馬鈴薯を任意の形状にカッ
トし、ブランチング処理を施してもよい。さらに、本発
明は、上記製造方法により得られたパウチ詰め馬鈴薯に
ある。以下、本発明の構成と作用を説明する。本発明に
おいては、酸素バリアー性を有するパウチが使用され
る。このパウチに使用されるフィルムの構成としては、
PET/ON/CPP, PET/PVDC/CPP, PET/EVOH/CPP, PET/SiO2
蒸着フィルム/CPP, PET/アルミ蒸着フィルム/CPP, PET/
ON/Al/CPP 等を挙げることができる (ここでPET:ポリエ
チレンテレフタレート、ON:延伸ナイロン、CPP:未延伸
ポリプロピレン、PVDC:ポリ塩化ビニリデン、EVOH: エ
チレンビニルアルコール共重合体、Al:アルミ箔であ
る) 。
[0006] In the above method, before peeling the peeled potato into a pouch, the potato may be cut into an arbitrary shape and blanched. Furthermore, the present invention resides in a potato stuffed potato obtained by the above-mentioned production method. Hereinafter, the configuration and operation of the present invention will be described. In the present invention, a pouch having an oxygen barrier property is used. As the composition of the film used for this pouch,
PET / ON / CPP, PET / PVDC / CPP, PET / EVOH / CPP, PET / SiO 2
Evaporated film / CPP, PET / Aluminum evaporated film / CPP, PET /
ON / Al / CPP etc. (where PET: polyethylene terephthalate, ON: stretched nylon, CPP: unstretched polypropylene, PVDC: polyvinylidene chloride, EVOH: ethylene vinyl alcohol copolymer, Al: aluminum foil is there) .

【0007】馬鈴薯の形態は、任意の形態が使用可能
で、例えば剥皮しただけのホール形態、それをスライス
した形態、またダイス状の形態等が選択できる。脱気包
装は、馬鈴薯の取り出しを容易に行えるように、パウチ
内の残存空気量が、馬鈴薯体積の1%以上、80%未満と
なるように行うのが好ましい。残存空気量が馬鈴薯体積
の1%未満の場合には、開封後の馬鈴薯の取り出しが困
難になり、また残存空気量が馬鈴薯体積の80%以上にな
ると、馬鈴薯がパウチ内で固定されないため、輸送時の
振動等により、馬鈴薯の形が崩れる場合がある。
[0007] The potato can be in any form, for example, a peeled hole form, a sliced form thereof, or a dice-like form. The deaerated packaging is preferably performed so that the amount of residual air in the pouch is 1% or more and less than 80% of the potato volume so that the potato can be easily taken out. When the residual air content is less than 1% of the potato volume, it is difficult to take out the potato after opening, and when the residual air content is 80% or more of the potato volume, the potato is not fixed in the pouch, and is transported. The shape of the potato may be lost due to vibration at the time.

【0008】本発明に用いられる脱酸素剤包装体におけ
る包装材料としては、耐水性、耐破損性、安全衛生性等
を有するものが好ましく、例えば、プラスチック繊維か
らなる通気性シートとプラスチックフィルムに多数の細
孔を設けてなる有孔フィルムとを貼り合わせたものをそ
の一部または全部に使用したものが用いられる。本発明
において脱酸素剤包装体内に封入される脱酸素剤として
は、酸素を吸収する作用を有するものであれば特に限定
されないが、亜硫酸塩、亜硫酸水素塩、亜二チオン酸
塩、第一鉄塩、ヒドロキノン、カテコール、レゾルシ
ン、ピロガロール、没食子酸、ロンガット、アスコルビ
ン酸および/またはその塩、ソルボース、グルコース、
リグリン、ジブチルヒドロキシトルエン、またはブチル
ヒドロキシアニソール等を含有する脱酸素剤、または鉄
粉等の金属粉を含有する脱酸素剤が用いられ、アスコル
ビン酸および/またはその塩、イソアスコルビン酸およ
び/またはその塩、もしくは、鉄粉を含有する脱酸素剤
が好適に用いられる。これらのうち鉄粉を含有する脱酸
素剤が特に好ましく用いられる。そして、脱酸素剤の使
用量は、パウチ内の残存空気量により適宜決定される。
As the packaging material for the oxygen scavenger package used in the present invention, those having water resistance, breakage resistance, safety and hygiene, etc. are preferable. And a perforated film provided with pores of the above is used for part or all of the perforated film. The oxygen scavenger enclosed in the oxygen scavenger package in the present invention is not particularly limited as long as it has an action of absorbing oxygen, but sulfite, bisulfite, dithionite, ferrous iron Salts, hydroquinone, catechol, resorcinol, pyrogallol, gallic acid, longat, ascorbic acid and / or its salts, sorbose, glucose,
A deoxidizer containing ligulin, dibutylhydroxytoluene, or butylhydroxyanisole, or a deoxidizer containing metal powder such as iron powder is used, and ascorbic acid and / or a salt thereof, isoascorbic acid and / or A deoxidizer containing salt or iron powder is preferably used. Of these, oxygen absorbers containing iron powder are particularly preferably used. The amount of the oxygen absorber used is appropriately determined based on the amount of residual air in the pouch.

【0009】加圧加熱殺菌は、100 ℃以上で行う。ま
た、加圧加熱殺菌の条件は、馬鈴薯の形態製品の流通の
条件にもよるが、常温流通を前提とした場合には、中心
部が120 ℃、4分相当以上(F0値が3.1以上)が好ま
しい。
The pressurized heat sterilization is performed at 100 ° C. or higher. The conditions of pressurized heat sterilization also depend on the conditions of distribution of the potato-shaped product, but assuming normal temperature distribution, the central part is at 120 ° C. for 4 minutes or more (F 0 value of 3. 1 or more).

【0010】[0010]

【実施例】【Example】

(実施例1)繊維長0.9〜1.3mm、平均幅0.01mmを有す
るポリエチレン繊維の1重量%懸濁液を抄紙機に導入
し、繊維層を形成させた後、脱水・乾燥し、坪量90g/m2
を有する通気性シート材料を得た。このシート材料 100
重量部に対して、撥水撥油剤 (旭硝子 (株) 社製、アサ
ヒガードAG530) の希釈水溶液 (弗素樹脂濃度2重
量%) を50重量部含浸させた後、乾燥し、通気性シート
を得た。
(Example 1) A 1% by weight suspension of polyethylene fiber having a fiber length of 0.9 to 1.3 mm and an average width of 0.01 mm was introduced into a paper machine to form a fiber layer, and then dewatered and dried. 90g / m 2
Was obtained. This sheet material 100
50 parts by weight of a diluted aqueous solution (fluorine resin concentration: 2% by weight) of a water / oil repellent (Asahigard AG530, manufactured by Asahi Glass Co., Ltd.) was impregnated with the resulting mixture, followed by drying to obtain a breathable sheet. Was.

【0011】上記通気性シートをPET/LDPEからなる有孔
複合フィルム (平均孔計:0.15mm、孔数:1,000,000ヶ/
m2) のLDPE面と合わせて、熱ロール間を通過させ、通気
性シートと有孔複合フィルムの貼合体を作成した。上記
貼合体で作成したパウチ内に、鉄粉を主剤とし、酸素吸
収能力が 100mlの脱酸素剤を内部に封入し、脱酸素剤包
装体を作成した。
The above-mentioned air-permeable sheet is made of a perforated composite film of PET / LDPE (average porosity: 0.15 mm, number of holes: 1,000,000 /
The sheet was passed between hot rolls together with the m 2 ) LDPE surface to prepare a bonded body of a breathable sheet and a perforated composite film. An oxygen scavenger containing iron powder as a main ingredient and an oxygen absorption capacity of 100 ml was enclosed inside the pouch created by the above-mentioned bonded body to prepare an oxygen scavenger package.

【0012】馬鈴薯 (メークイーン) を剥皮後、ダイス
状 (約2cm角) にカット後、90℃の熱水10L中に5kg投
入し、5分間ブランチング処理を行った。該馬鈴薯800g
をPET/PVDC/CPP (23℃における酸素透過度:1.6cc/m2
24hrs・atm ) からなるパウチ (200mm×300mm) に入
れ、上記脱酸素剤包装体を封入した後、真空包装機を用
いて、一旦200mmHg まで減圧後、空気を導入して脱気包
装をおこなった。パウチ内の残存空気量は、馬鈴薯の密
度を1.0とした場合に、約80mlであった。該包装済馬鈴
薯を熱水式レトルト殺菌機を用いて 120℃、2.1kg/cm2
×50分の条件で殺菌処理を行った。中心部のF0値は、
4.2であった。
[0012] After peeling the potato (Mayqueen), the potato was cut into a dice (about 2 cm square), 5 kg was put into 10 L of hot water at 90 ° C, and a blanching treatment was performed for 5 minutes. 800 g of the potato
To PET / PVDC / CPP (oxygen permeability at 23 ° C: 1.6 cc / m 2
24hrs ・ atm), put in a pouch (200mm × 300mm), sealed the oxygen scavenger package, and then, using a vacuum packaging machine, once decompressed to 200mmHg, introduced air, and performed deaeration packaging. . The amount of residual air in the pouch was about 80 ml when the potato density was 1.0. The packaged potatoes were heated at 120 ° C. and 2.1 kg / cm 2 using a hot water retort sterilizer.
A sterilization treatment was performed under the conditions of × 50 minutes. The F 0 value at the center is
4.2.

【0013】(比較例1)実施例1と同様に馬鈴薯を処
理し、脱酸素剤包装体を用いずに包装した後、実施例1
と同条件で殺菌処理を行った。 (比較例2)実施例1と同様に馬鈴薯を処理し、脱酸素
剤包装体を用いずに真空包装した後、実施例1と同条件
で殺菌条件を行った。
Comparative Example 1 Potatoes were treated in the same manner as in Example 1 and packaged without using an oxygen scavenger package.
A sterilization treatment was performed under the same conditions as described above. (Comparative Example 2) Potatoes were treated in the same manner as in Example 1, packaged in a vacuum without using a package of oxygen scavenger, and sterilized under the same conditions as in Example 1.

【0014】(実験)殺菌後のパウチ詰め馬鈴薯を37℃
で90日間保存し、カラーコンピューター (スガ試験機社
製 SMカラーコンピューターSM 5) を用いて、色
差を経時的に測定した。未変色の基準としては、比較例
2のものを脱酸素剤包装体 (三菱瓦斯化学社製エージレ
スS) とともにアルミパウチ (PET/Al/ON/CPP)で包装
し、0℃で保存したものを用いた (測定時には、双方と
も常温にした後、判定) 。
(Experiment) The potatoes packed in a pouch after sterilization were heated at 37 ° C.
For 90 days, and the color difference was measured over time using a color computer (SM Color Computer SM5 manufactured by Suga Test Instruments Co., Ltd.). As a reference for the undiscolored color, the one obtained in Comparative Example 2 was packaged in an aluminum pouch (PET / Al / ON / CPP) together with an oxygen absorber package (Ageless S manufactured by Mitsubishi Gas Chemical Company) and stored at 0 ° C. It was used (at the time of measurement, both were brought to room temperature and then judged).

【0015】結果を表1に示す。The results are shown in Table 1.

【0016】[0016]

【表1】 [Table 1]

【0017】[0017]

【発明の効果】以上記述してきたように、本発明のパウ
チ詰め馬鈴薯の製造方法によれば、酸化防止剤を使用す
ることなしに、流通・保存時の褐変を防止できることは
勿論のこと、従来の真空包装の欠点であった開封時の馬
鈴薯の取り出しが容易にできる画期的なものである。
As described above, according to the method for producing pouched potatoes of the present invention, browning during distribution and storage can be prevented without using an antioxidant. This is an epoch-making thing that can easily take out potatoes at the time of opening, which is a drawback of vacuum packaging.

【図面の簡単な説明】[Brief description of the drawings]

【図1】パウチ詰め馬鈴薯の1実施例を示す断面図であ
る。
FIG. 1 is a cross-sectional view showing one embodiment of a potato stuffed with pouches.

【図2】パウチ詰め馬鈴薯に使用できる包装材料の1実
施例を示す断面図である。
FIG. 2 is a sectional view showing one embodiment of a packaging material that can be used for potatoes packed with pouches.

【図3】パウチ詰め馬鈴薯に使用できる脱酸素剤包装体
の包装材料の1例の断面図である。
FIG. 3 is a cross-sectional view of an example of a packaging material for an oxygen scavenger package that can be used for potatoes packed with pouches.

【符号の説明】[Explanation of symbols]

1 酸素バリアー性を有するパウチ 2 馬鈴薯 3 脱酸素剤包装体 4 空隙部 5 ポリエチレンテレフタレート 6 ポリ塩化ビニリデン 7 未延伸ポリプロピレン 8 通気性シート 9 有孔複合フィルム 10 脱酸素剤 11 開孔部 DESCRIPTION OF SYMBOLS 1 Pouch which has an oxygen barrier property 2 Potato 3 Oxygen-absorbing agent package 4 Void 5 Polyethylene terephthalate 6 Polyvinylidene chloride 7 Unstretched polypropylene 8 Air-permeable sheet 9 Perforated composite film 10 Oxygen-absorbing agent 11 Opening part

フロントページの続き (58)調査した分野(Int.Cl.7,DB名) A23B 7/00 - 7/152 JICSTファイル(JOIS) JAFICファイル(JOIS)Continuation of the front page (58) Fields surveyed (Int. Cl. 7 , DB name) A23B 7/ 00-7/152 JICST file (JOIS) JAFIC file (JOIS)

Claims (5)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 馬鈴薯を剥皮後、これを脱酸素剤包装体
とともに酸素バリアー性を有するパウチ内に脱気包装
し、加圧加熱殺菌することを特徴とするパウチ詰め馬鈴
薯の製造方法。
1. A process for producing potatoes packed with pouches, comprising peeling potatoes, degassing and packaging them in a pouch having an oxygen barrier property together with a package of oxygen absorbers, and sterilizing under pressure.
【請求項2】 剥皮した馬鈴薯をパウチ内に脱気包装す
る前に、該馬鈴薯を任意の形状にカットし、ブランチン
グ処理を施すことを特徴とする請求項1記載のパウチ詰
め馬鈴薯の製造方法。
2. A method for producing potatoes packed in pouches according to claim 1, wherein the peeled potatoes are cut into an arbitrary shape and blanched before degassing and packaging in a pouch. .
【請求項3】 脱気包装時のパウチ内の残存空気量が、
馬鈴薯体積の1%以上、80%未満であることを特徴とす
る請求項1記載のパウチ詰めの製造方法。
3. The amount of air remaining in the pouch at the time of degassing packaging is as follows:
2. The method according to claim 1, wherein the potato volume is 1% or more and less than 80%.
【請求項4】 脱酸素剤包装体における包装材料の一部
または全部が、通気性シートと有孔複合フィルムを貼り
合わせた包装材料からなることを特徴とする請求項1乃
至3のいづれか記載のパウチ詰め馬鈴薯の製造方法。
4. The method according to claim 1, wherein a part or all of the packaging material in the oxygen absorber package is made of a packaging material in which a breathable sheet and a perforated composite film are bonded. A method for producing potatoes packed in pouches.
【請求項5】 請求項1乃至4のいづれか記載の製造方
法で得られるパウチ詰め馬鈴薯。
5. A pouch-packed potato obtained by the method according to any one of claims 1 to 4.
JP25295692A 1992-09-22 1992-09-22 Manufacturing method of potatoes packed in pouches Expired - Fee Related JP3201842B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP25295692A JP3201842B2 (en) 1992-09-22 1992-09-22 Manufacturing method of potatoes packed in pouches

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP25295692A JP3201842B2 (en) 1992-09-22 1992-09-22 Manufacturing method of potatoes packed in pouches

Publications (2)

Publication Number Publication Date
JPH0698672A JPH0698672A (en) 1994-04-12
JP3201842B2 true JP3201842B2 (en) 2001-08-27

Family

ID=17244504

Family Applications (1)

Application Number Title Priority Date Filing Date
JP25295692A Expired - Fee Related JP3201842B2 (en) 1992-09-22 1992-09-22 Manufacturing method of potatoes packed in pouches

Country Status (1)

Country Link
JP (1) JP3201842B2 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006059610A1 (en) * 2004-11-30 2006-06-08 Q.P. Corporation Processed potato and process for producing the same
EP2991497A4 (en) * 2013-02-26 2016-09-07 Smart Spuds Inc Chemical and preservative free peeled potatoes
KR102355755B1 (en) 2017-12-14 2022-02-08 코카 크롬 인더스트리 컴퍼니 리미티드 Cooling roll and method for producing thermoplastic resin sheet using same

Also Published As

Publication number Publication date
JPH0698672A (en) 1994-04-12

Similar Documents

Publication Publication Date Title
JP3230853B2 (en) Fruit and Vegetable Freshness Packaging Film
WO1998058842A1 (en) Method for sterilizing packages of medical supplies
JP2010089280A (en) Oxygen-absorbing laminated film, flavor of dried food using the same, and method for keeping aroma
JP2876320B2 (en) Radiation sterilization method for medical equipment
JP3201842B2 (en) Manufacturing method of potatoes packed in pouches
JP4534781B2 (en) Package for maintaining freshness
JP4917896B2 (en) Blood purifier package and method for producing the same
JP4553148B2 (en) Method for producing freshness-maintaining packaging
JPH0889561A (en) Method for sterilizing articles containing plastic by irradiation with radiation or electron beams
JP4095625B2 (en) Freshness-maintaining packaging bag and freshness-maintaining package
JPH0852841A (en) Hygroscopic packaging material and freshness-keeping packaging bag using the material
JP2002080647A (en) Deoxidizing agent resin composition and sheet
JP4141606B2 (en) Packaging for maintaining freshness of fruits and vegetables
JP2010057426A (en) Method for maintaining freshness of fruit
JP2901669B2 (en) Manufacturing method of radiation sterilized medical device
JP4061448B2 (en) How to store goods
JP2001169722A (en) Package for retaining vegetable and fruit freshness
JP3195667B2 (en) Heat sterilization method of fungi
JP4586945B2 (en) How to preserve fermented pickles
JP3765659B2 (en) Cut burdock packaging
JP3898270B2 (en) Cereal freshness preservation method
JP3797794B2 (en) Apple freshness preservation package
JP3154443B2 (en) Package with sliced onion
JP2524549Y2 (en) Fruit and vegetable freshness preserving paper
JPS6241062B2 (en)

Legal Events

Date Code Title Description
FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20080622

Year of fee payment: 7

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20080622

Year of fee payment: 7

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090622

Year of fee payment: 8

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090622

Year of fee payment: 8

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100622

Year of fee payment: 9

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110622

Year of fee payment: 10

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110622

Year of fee payment: 10

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20120622

Year of fee payment: 11

LAPS Cancellation because of no payment of annual fees