Deprecated: The each() function is deprecated. This message will be suppressed on further calls in /home/zhenxiangba/zhenxiangba.com/public_html/phproxy-improved-master/index.php on line 456
JP3339341B2 - Manufacturing method of soft cold rolled steel sheet with small coil end property - Google Patents
[go: Go Back, main page]

JP3339341B2 - Manufacturing method of soft cold rolled steel sheet with small coil end property - Google Patents

Manufacturing method of soft cold rolled steel sheet with small coil end property

Info

Publication number
JP3339341B2
JP3339341B2 JP00145897A JP145897A JP3339341B2 JP 3339341 B2 JP3339341 B2 JP 3339341B2 JP 00145897 A JP00145897 A JP 00145897A JP 145897 A JP145897 A JP 145897A JP 3339341 B2 JP3339341 B2 JP 3339341B2
Authority
JP
Japan
Prior art keywords
temperature
rolling
heating
steel sheet
coil end
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP00145897A
Other languages
Japanese (ja)
Other versions
JPH10195542A (en
Inventor
義正 船川
邦和 冨田
潤 谷合
弘 澤田
康英 石黒
尚志 村山
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JFE Engineering Corp
Original Assignee
JFE Engineering Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JFE Engineering Corp filed Critical JFE Engineering Corp
Priority to JP00145897A priority Critical patent/JP3339341B2/en
Publication of JPH10195542A publication Critical patent/JPH10195542A/en
Application granted granted Critical
Publication of JP3339341B2 publication Critical patent/JP3339341B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Heat Treatment Of Steel (AREA)
  • Heat Treatment Of Sheet Steel (AREA)

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、特に自動車や家電
製品等に用いられ、プレス成形等の加工に適し、コイル
エンド性の小さい軟質冷延鋼板に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a soft cold-rolled steel sheet which is particularly used for automobiles and home electric appliances, is suitable for processing such as press forming, and has a small coil end property.

【0002】[0002]

【従来の技術】自動車や家電製品などに使用される鋼板
には、高い成形性が要求され、軟質、高r値化が精力的
に進められている。連続焼鈍によりこのような鋼板を製
造する場合、r値低下の原因となるC、Nを、熱延の高
温巻取によって析出物として固定する必要がある。しか
し、高温巻取を行うと、常温のマンドレルに巻とられる
コイル先端部と、空気に直接触れるコイル後端部の冷却
速度が速いこと(コイルエンド性)から、中央部に対す
るコイルの先端部、後端部の材質劣化が激しくなる。さ
らには、スケールが厚く生成することにより、酸洗性も
低下する。これに対し、コイル長手方向の両端部を切断
するなどの対応がとられてきた。しかしこれは急激な歩
留まり低下を招き生産性を著しく阻害することから、コ
イル長手方向の両端部の材質を確保する各種の方法が提
案されてきた。従来よりコイルエンド性を生ずる原因は
AlNであると考えられており、AlNの形態を制御す
るものとして、たとえば、特公昭63−72829号公
報には、高温巻取を前提にしたコイルエンド性の低減方
法が開示されており、AlNの微細分散を熱延スラブの
加熱温度低減と高温巻取により抑制することが示されて
いる。しかし、この方法ではAlNを粗大析出させ良好
なr値を得るには700℃〜800℃の超高温巻取が必
須であり、不可避的にコイル両端部とミドル部の冷却速
度に大差が付いてしまい十分な改善がなされないこと
や、酸洗性が著しく劣化するというのが実際である。さ
らには、特公昭55−36051号公報にはストリップ
両端部を無注水で巻取ることによって、両端部を高温巻
取する方法が、特開平5−43946号公報には、両端
部の巻取温度を上げ、タイトに巻き取り、コイル全体の
冷却速度をコントロールする方法が開示されている。し
かし、これらの方法では、巻取温度の制御が難しいこ
と、酸素の供給が容易なコイルの両端部において巻取温
度を高くすることから、その部分の酸洗性が大幅に劣化
するなどという問題がある。また、鋼中のC、Nを極め
て低減した鋼に、Ti等の炭・窒化物形成元素を添加し
た固溶C、Nの存在しないIF鋼を用いることも行われ
ているが、C、Nの低減に要する製鋼コストが大きく、
高価となってしまう。一方、低温巻取を行えばコイルエ
ンド性はある程度低減可能であるが、材質が劣化すると
いう問題がある。そこで、低温巻取を前提に粒成長性を
上げて高r値を得る方法として、特開昭51−1385
16号公報には、B添加低炭素鋼のスラブを低温加熱
し、600〜700℃で巻取ることにより窒化物の大部
分をBNとし、粒成長性を向上させ、材質を良好にする
方法が開示されている。しかし、この方法においても、
コイル中央部の材質は向上するが、コイルエンドにおけ
る材質は従来程度であり、コイルエンド性が大きいのが
現状である。
2. Description of the Related Art High formability is required for steel sheets used for automobiles and home electric appliances, and softness and high r-value are being vigorously promoted. When producing such a steel sheet by continuous annealing, it is necessary to fix C and N, which cause a decrease in the r value, as precipitates by hot rolling of hot rolling. However, when high-temperature winding is performed, since the cooling speed of the coil tip wound around the mandrel at room temperature and the rear end of the coil that is in direct contact with air is fast (coil end property), the tip of the coil with respect to the center, Material deterioration of the rear end becomes severe. Furthermore, when the scale is formed to be thick, the pickling property also decreases. In response to this, measures such as cutting both ends in the coil longitudinal direction have been taken. However, this causes a sharp decrease in yield and significantly impairs productivity, and various methods have been proposed to secure the material at both ends in the coil longitudinal direction. Conventionally, the cause of the coil end property is considered to be AlN. For controlling the form of AlN, for example, Japanese Patent Publication No. Sho 63-72829 discloses a coil end property that presupposes high-temperature winding. A reduction method is disclosed, and it is shown that the fine dispersion of AlN is suppressed by reducing the heating temperature of the hot-rolled slab and winding it at a high temperature. However, in this method, in order to coarsely precipitate AlN and obtain a good r-value, it is necessary to wind an ultra-high temperature of 700 ° C. to 800 ° C., and inevitably there is a large difference between the cooling rates of both ends of the coil and the middle part. In fact, it is in fact that the improvement is not sufficiently made and the pickling property is remarkably deteriorated. Further, Japanese Patent Publication No. 55-36051 discloses a method of winding both ends at a high temperature by winding both ends of the strip without water injection, and Japanese Patent Application Laid-Open No. 5-43946 discloses a method of winding at both ends. A method of controlling the cooling rate of the entire coil by raising the temperature and winding tightly is disclosed. However, in these methods, it is difficult to control the coiling temperature, and since the coiling temperature is increased at both ends of the coil where oxygen can be easily supplied, the pickling property of the coil is greatly deteriorated. There is. Further, an IF steel in which carbon and nitride forming elements such as Ti are added to a steel in which C and N in the steel are extremely reduced, and an IF steel in which no solid solution C and N is present has been used. Steelmaking costs required to reduce
It will be expensive. On the other hand, if low-temperature winding is performed, the coil end property can be reduced to some extent, but there is a problem that the material is deteriorated. Therefore, as a method of obtaining a high r value by increasing the grain growth property on the premise of low-temperature winding, Japanese Patent Application Laid-Open No. 51-1385 discloses a method.
No. 16 discloses a method of heating a slab of B-added low carbon steel at a low temperature and winding the slab at 600 to 700 ° C. to convert most of the nitride to BN, thereby improving the grain growth and improving the material quality. It has been disclosed. However, even in this method,
Although the material at the center of the coil is improved, the material at the coil end is about the same as the conventional one, and at present, the coil end property is large.

【0003】[0003]

【発明が解決しようとする課題】上記したように、コイ
ルエンド性改善についていろいろな発明がなされている
が、未だどの発明においても、材質を維持しながらコイ
ルエンド性を問題にならない程度に小さくするには及ん
でいない。
As described above, various inventions have been made to improve the coil end property. However, in any of the inventions, the coil end property is reduced while maintaining the material so as not to cause a problem. Less than.

【0004】本発明の目的は、コイルエンド性の問題を
根本的に解決するとともに、酸洗などの次工程にも負荷
をかけない、コイルエンド性の小さい軟質冷延鋼板の製
造方法を提供することにある。
An object of the present invention is to provide a method of manufacturing a soft cold-rolled steel sheet having a small coil end property, which fundamentally solves the problem of the coil end property and does not impose a load on a subsequent step such as pickling. It is in.

【0005】[0005]

【課題を解決するための手段】前記課題を解決し目的を
達成するために、本発明は以下に示す手段を用いてい
る。 (1)本発明の冷延鋼板の製造方法は、重量%で、C≦
0.03%と、Mn≦0.5%と、Si≦0.1%と、
P≦0.025%と、S≦0.03%と、Sol.Al
≦0.1%と、N≦0.0035%と、B≦0.003
%とを含有し、かつ原子比でB/N=0.6〜1.5を
満足し、残部がFe及び不可避的不純物からなる鋼板を
製造する方法において、鋼を1150℃以下に加熱し、
粗圧延して粗バーとする工程と、950℃以下の粗バー
を980℃以上に加熱し、Ar3 点以上で仕上げ圧延を
行い、650℃以下で巻き取る工程と、巻き取った熱延
鋼板を冷間圧延し、焼鈍する工程と、を備えたことを特
徴とするコイルエンド性の小さい軟質冷延鋼板の製造方
法である。
In order to solve the above problems and achieve the object, the present invention uses the following means. (1) The method for producing a cold-rolled steel sheet according to the present invention is as follows.
0.03%, Mn ≦ 0.5%, Si ≦ 0.1%,
P ≦ 0.025%, S ≦ 0.03%, Sol. Al
≦ 0.1%, N ≦ 0.0035%, and B ≦ 0.003
%, And the atomic ratio of B / N = 0.6 to 1.5 is satisfied, and the balance is Fe and unavoidable impurities.
A step of roughly rolling to a rough bar, a step of heating a rough bar of 950 ° C. or less to 980 ° C. or more, performing a finish rolling at three or more points of Ar, and winding the same at 650 ° C. or less, And cold rolling and annealing the steel sheet.

【0006】(2)本発明の冷延鋼板の製造方法は、上
記(1)に記載の組成を有する鋼板を製造する方法にお
いて、連続鋳造した鋼を750℃以上で加熱炉に挿入し
て1150℃以下に加熱し、粗圧延して粗バーとする工
程と、950℃以下の粗バーを980℃以上に加熱、A
3 点以上で仕上げ圧延を行い、650℃以下で巻き取
る工程と、巻き取った熱延鋼板を冷間圧延し、焼鈍する
工程と、を備えたことを特徴とするコイルエンド性の小
さい軟質冷延鋼板の製造方法である。
(2) The method for producing a cold-rolled steel sheet according to the present invention is the same as the method for producing a steel sheet having the composition described in (1) above, except that the continuously cast steel is inserted into a heating furnace at a temperature of 750 ° C. or more and 1150. C. or less, and rough rolling to a coarse bar, and heating a coarse bar of 950 ° C. or less to 980 ° C. or more.
r Rolling at a temperature not lower than 3 points and winding at 650 ° C. or lower, and cold rolling and annealing the rolled hot-rolled steel sheet; This is a method for producing a cold-rolled steel sheet.

【0007】[0007]

【発明の実施の形態】本発明者は、コイルエンド性の問
題を根本的に解決するとともに、酸洗などの次工程にも
負荷をかけない、コイルエンド性の小さい軟質冷延鋼板
を得るために、従来のB添加アルミキルド鋼を低温加熱
した場合に生じるコイルエンド性の原因を調査し、仕上
げ圧延時のコイル両端部の粒成長性を阻害する微細析出
物を減少させる製造方法について、鋭意研究を重ねた。
BEST MODE FOR CARRYING OUT THE INVENTION The inventor of the present invention aims to fundamentally solve the problem of the coil end property and to obtain a soft cold-rolled steel sheet having a small coil end property without imposing a load on a subsequent step such as pickling. In addition, we investigated the cause of coil end properties when conventional B-added aluminum-killed steel was heated at low temperature, and conducted intensive research on a manufacturing method that reduces fine precipitates that hinder grain growth at both ends of the coil during finish rolling. Was piled up.

【0008】その結果、本発明者は、以下のようなコイ
ルエンドにおける粒成長阻害因子を発見した。第1に、
いかに低温加熱といえどもある程度のMnSは固溶して
しまうこと。第2に固溶したMnSは高温加熱した場合
よりも固溶量が少ないため、析出駆動力が小さく、熱間
圧延時の粗圧延時に析出を開始し、析出は仕上げ圧延ま
で引き続き微細に析出すること。第3にBNは仕上げ圧
延時に析出するが、その一部は粗圧延時にすでに析出し
たMnSを核に析出するものの仕上げ圧延開始時は微細
MnSの量があまりにも少なくBN単独で微細に析出す
るものが存在すること。第4に、仕上げ圧延時に析出し
たMnSはBNの析出核とならないことである。この仕
上げ圧延時に微細析出したMnSと単独に微細析出した
BNが粒成長を抑制するため、コイル両端部では十分に
粒成長せず、コイルエンド性が発生する。そこで、発明
者らは鋭意研究を重ねた結果、粗圧延後の粗バーを一度
950℃以下にした後、980℃以上に加熱することに
よって微細MnSを仕上げ圧延前に完全に析出させるこ
とが可能であり、それにより仕上げ圧延時に析出する微
細MnSがなくなり、すべての微細MnSがBNの析出
核となって粗大な複合析出物となり無害化できること
と、BNの微細単独析出がなくなることによって、鋼板
全長にわたって良好な粒成長性が確保されるという知見
を得た。以下にその基礎となった実験結果を示す。
As a result, the present inventors have discovered the following grain growth inhibitory factors at the coil end. First,
Even if it is heated at a low temperature, a certain amount of MnS forms a solid solution. Second, since the amount of solid solution MnS is smaller than that when heated at a high temperature, the precipitation driving force is small, precipitation starts at the time of rough rolling at the time of hot rolling, and precipitation is continued finely until finish rolling. thing. Third, BN precipitates at the time of finish rolling. Part of the BN precipitates at the core of MnS already precipitated at the time of rough rolling, but at the start of finish rolling, the amount of fine MnS is too small and BN alone precipitates finely. That there is. Fourth, MnS precipitated at the time of finish rolling does not become BN precipitation nuclei. Since MnS finely precipitated during this finish rolling and BN finely precipitated alone suppress grain growth, grain growth does not occur sufficiently at both ends of the coil, and coil end properties occur. Therefore, the inventors have conducted intensive studies and found that once the coarse bar after the rough rolling is once reduced to 950 ° C. or less, the fine bar can be completely precipitated before the finish rolling by heating to 980 ° C. or more. Accordingly, fine MnS precipitated at the time of finish rolling is eliminated, and all fine MnS become nuclei of BN to become coarse composite precipitates and can be rendered harmless. That good grain growth was ensured over a long period of time. The experimental results on which this is based are shown below.

【0009】重量%で、C:約0.02%、Si:約
0.02%、Mn:約0.16%、P:約0.012
%、S:約0.008%、Sol.Al:約0.015
%、N:約0.0017%、B:約0.0012%を含
む鋼を溶解し、加熱温度1100℃、粗圧延後粗バーが
900℃となったところで、誘導加熱により粗バー加熱
を行い、仕上温度880℃、巻取温度600℃を基本条
件として、粗バー加熱条件を変化させて熱間圧延を行っ
た。得られた熱延板を酸洗後、冷圧率75%で冷間圧延
を行い、750℃で焼鈍を行った。さらに調圧率0.8
%で調質圧延を行い、コイル先端部(T部)3m、中央
部(M部)、後端部(B部)3mのr値を測定した。コ
イル両端部で低い方のr値と中央部のr値の差を、粗バ
ー加熱温度に対してプロットしたものを図1に示す。図
1より、粗圧延後粗バーを980℃以上に加熱すること
によりコイルエンド性が著しく低減することがわかる。
この現象の理由は未だ完全には明らかとなっていない
が、粗バーを950℃以下に冷却することによりMnS
の析出駆動力を上げた状態で加熱するため、粗バー加熱
後にMnSが完全に析出するものと考えられる。ここ
で、950℃以下で保持しても温度が低いため、仕上げ
圧延による大きな歪みがない限り微細MnSの析出はほ
とんど起こらない。BNは仕上げ圧延時に粗バー加熱後
に完全に析出した微細MnSを核に析出し、微細MnS
は粗大複合析出物となるため粒成長性に悪影響を及ぼす
ことはなく、また、BNの単独微細析出はない。このよ
うにして得られた良好な粒成長性は冷延・焼鈍後も引き
継がれるため、冷延板も良好な粒成長性を持つ。従っ
て、本発明における低温巻取においても従来と同等の材
質を確保することができる。
By weight%, C: about 0.02%, Si: about 0.02%, Mn: about 0.16%, P: about 0.012
%, S: about 0.008%, Sol. Al: about 0.015
%, N: about 0.0017%, B: about 0.0012%, melted steel, heating temperature was 1100 ° C, and after rough rolling, when the rough bar reached 900 ° C, coarse bar heating was performed by induction heating. The hot rolling was performed by changing the rough bar heating conditions under the basic conditions of a finishing temperature of 880 ° C. and a winding temperature of 600 ° C. After pickling the obtained hot rolled sheet, cold rolling was performed at a cold pressure ratio of 75%, and annealing was performed at 750 ° C. Further pressure regulation ratio 0.8
%, And the r-value of 3 m of the coil tip (T section), the center (M section), and the rear end (B section) 3 m was measured. FIG. 1 shows a plot of the difference between the lower r value at the both ends of the coil and the r value at the center with respect to the rough bar heating temperature. From FIG. 1, it is understood that heating the rough bar to 980 ° C. or more after the rough rolling significantly reduces the coil end property.
Although the reason for this phenomenon has not yet been completely elucidated, MnS can be obtained by cooling the coarse bar to 950 ° C. or lower.
It is considered that MnS is completely precipitated after heating the coarse bar because heating is performed in a state where the precipitation driving force is increased. Here, since the temperature is low even when the temperature is maintained at 950 ° C. or lower, precipitation of fine MnS hardly occurs unless there is a large distortion due to finish rolling. BN precipitates in the nucleus fine MnS completely precipitated after heating the coarse bar during finish rolling,
Does not adversely affect the grain growth because it becomes a coarse composite precipitate, and there is no single fine precipitation of BN. The good grain growth obtained in this way is inherited even after cold rolling and annealing, so that the cold rolled sheet also has good grain growth. Therefore, even in the low-temperature winding in the present invention, it is possible to secure the same material as the conventional one.

【0010】また、B/Nの原子比を一定範囲に制御す
ることにより、Bの過剰添加による鋼の硬質化を抑え
て、従来と同等の材質を確保することができるという知
見も得た。B/N比が1以下の場合AlNが析出する
が、量が少ないため粒成長性に悪影響を及ぼすことはな
い。
It has also been found that by controlling the atomic ratio of B / N to a certain range, it is possible to suppress the hardening of steel due to excessive addition of B and to secure a material equivalent to that of the prior art. When the B / N ratio is 1 or less, AlN precipitates, but since the amount is small, there is no adverse effect on the grain growth.

【0011】さらに、連続鋳造後のスラブ温度が750
℃以上で加熱炉に挿入すれば、スラブ中にAlNが析出
しないまま、すなわち、固溶Nが十分存在する状態で高
温に保たれるため、スラブ中のBNの粗大化が促進さ
れ、より良好な粒成長性を実現できる。スラブ中のBN
の粗大化はスラブ加熱時間を長くすれば同様な効果が期
待できるが、スラブ加熱時間を長くするとスラブ表面の
粒界酸化による表面品質の低下やエネルギーコストがか
かるという問題点がある。このように、連続鋳造後のス
ラブ温度が750℃以上で加熱炉に挿入すれば、本発明
の効果をさらに増加させることができる。
Further, the slab temperature after continuous casting is 750.
When inserted into a heating furnace at a temperature of not less than ℃, the slab is kept at a high temperature without precipitation of AlN, that is, in a state where there is a sufficient amount of solute N. It can realize a good grain growth. BN in slab
The same effect can be expected by increasing the slab heating time, but there is a problem that if the slab heating time is increased, the surface quality is reduced due to grain boundary oxidation of the slab surface and energy cost is required. Thus, if the slab temperature after continuous casting is inserted into the heating furnace at a temperature of 750 ° C. or higher, the effect of the present invention can be further increased.

【0012】以上のような知見に基づき、本発明者は、
B添加低炭素鋼のB/Nの原子比を一定範囲に制御し、
仕上げ圧延時のコイル両端部の粒成長性を阻害する微細
析出物を減少させるために、鋼(スラブ)の加熱温度、
粗圧延後の粗バーの加熱温度、仕上げ圧延温度及び巻取
り温度を制御するようにして、本発明のコイルエンド性
の小さい軟質冷延鋼板の製造方法を見出し、本発明を完
成した。
[0012] Based on the above findings, the present inventor:
The B / N atomic ratio of the B-added low carbon steel is controlled within a certain range,
In order to reduce fine precipitates that hinder grain growth at both ends of the coil during finish rolling, the steel (slab) heating temperature,
By controlling the heating temperature, the finish rolling temperature, and the winding temperature of the rough bar after the rough rolling, a method for producing a soft cold-rolled steel sheet having a small coil end property of the present invention was found, and the present invention was completed.

【0013】すなわち、本発明は、鋼組成及び製造条件
を下記範囲に限定することにより、コイルエンド性の問
題を根本的に解決するとともに、酸洗などの次工程にも
負荷をかけない、コイルエンド性の小さい軟質冷延鋼板
を得ることができる。以下に本発明の成分添加理由、成
分限定理由、及び製造条件の限定理由について説明す
る。
That is, according to the present invention, the steel composition and the production conditions are limited to the following ranges, thereby fundamentally solving the problem of the coil end property, and also providing no load to the next step such as pickling. A soft cold-rolled steel sheet having a small end property can be obtained. The reasons for adding the components, the reasons for limiting the components, and the reasons for limiting the production conditions of the present invention are described below.

【0014】(1)成分組成範囲 C≦0.03% Cはあまり多いと炭化物が多量に析出し、r値や伸び
(EL)を低下させ、成形性を阻害することから、0.
03%以下である。
(1) Component composition range C ≦ 0.03% If C is too large, a large amount of carbides precipitates out, lowering the r value and elongation (EL) and impairing the formability.
03% or less.

【0015】Mn≦0.5% MnはSをMnSの形で固定し、熱間延性を向上させる
働きがあることから0.05%以上は添加することが望
ましいが、過剰な添加は鋼の硬質化をもたらし、成形性
を劣化させるため、上限は0.5%である。
Mn ≦ 0.5% Mn fixes S in the form of MnS and has a function of improving hot ductility. Therefore, it is desirable to add 0.05% or more of Mn. The upper limit is 0.5% in order to bring about hardening and to deteriorate the formability.

【0016】S≦0.03% Sは熱間延性や成形性を阻害する元素であることからM
nSとして固定される。それゆえ、低い方が望ましい。
また、MnS量があまり多くなるとELの低下を招くこ
とから、上限は0.03%である。
S ≦ 0.03% Since S is an element that inhibits hot ductility and moldability, M
Fixed as nS. Therefore, lower is desirable.
Further, if the amount of MnS is too large, the EL is lowered, so the upper limit is 0.03%.

【0017】Si≦0.1% Siは過剰に添加すると強度が上がり成形性を劣化させ
ることから、0.1%以下である。
Si ≦ 0.1% Since excessive addition of Si increases the strength and deteriorates the formability, the content of Si is 0.1% or less.

【0018】P≦0.025% Pは固溶強化元素であり、過剰な添加は鋼の硬質化をも
たらすことから上限は0.025%である。
P ≦ 0.025% P is a solid solution strengthening element, and the upper limit is 0.025% since excessive addition causes hardening of steel.

【0019】Sol.Al≦0.1% Alは脱酸剤として使用されることから、ある程度は含
まれる。本発明においては、B添加によりNのかなりの
量がBNとして固定されることから、AlNの析出量は
少ないが、過剰に添加されると冷延後の焼鈍時にAlN
が過剰に微細析出して粒成長性を阻害するため、上限は
0.1%である。
Sol. Al ≦ 0.1% Since Al is used as a deoxidizing agent, Al is included to some extent. In the present invention, a considerable amount of N is fixed as BN by the addition of B, so the amount of AlN precipitated is small, but if added excessively, AlN precipitates during annealing after cold rolling.
Is excessively finely precipitated and hinders grain growth, so the upper limit is 0.1%.

【0020】N≦0.0035% NはAlNとして微細に析出するとコイルエンド性増加
の原因となる。本発明においてはBNとして固定される
が、BN量が多いと加工性が低下することから、上限は
0.0035%である。
N ≦ 0.0035% If N is finely precipitated as AlN, it causes an increase in the coil end property. In the present invention, it is fixed as BN. However, if the amount of BN is large, the workability is reduced. Therefore, the upper limit is 0.0035%.

【0021】B≦0.003% Bは本発明において重要な役割を演じる元素である。B
が添加されないとたとえ低温加熱であってもある程度は
MnSやAlNが溶解してしまい、微細なMnSやAl
Nが析出してしまう。Bは微細MnSを核としてBNと
して析出し、粗大複合析出物となるとともにNを固定し
て微細AlNの析出を抑制する。その結果、本発明にお
いては従来にない粒成長性が実現される。しかし、BN
が過剰に存在すると加工性が低下することから、添加量
の上限は0.003%である。
B ≦ 0.003% B is an element that plays an important role in the present invention. B
If MnS or AlN is not added, MnS or AlN will be dissolved to some extent even at low temperature heating, and fine MnS or AlN
N precipitates. B precipitates as BN with fine MnS as a nucleus, becomes a coarse composite precipitate, and fixes N to suppress the precipitation of fine AlN. As a result, in the present invention, unprecedented grain growth is realized. But BN
Is excessively present, the workability is reduced. Therefore, the upper limit of the addition amount is 0.003%.

【0022】B/N(原子比)=0.6〜1.5 Bは、Nに対し過剰に添加されると固溶B量が多くなり
鋼が硬質化するため、BとNの原子%の比は0.6〜
1.5である。これ以外の原子比では良好な加工性(r
値)が得られない。これは以下に示す本発明の実験によ
り明らかとなった。
B / N (atomic ratio) = 0.6 to 1.5 When B is excessively added to N, the amount of solid solution B increases and the steel becomes harder. Is 0.6 ~
1.5. At other atomic ratios, good workability (r
Value) cannot be obtained. This has been clarified by the following experiments of the present invention.

【0023】重量%で、C:約0.02%、Si:約
0.01%、Mn:約0.15%、P:約0.01%、
S:約0.008%、Sol.Al:約0.015%、
N:約0.002%、Bの添加量を各種変化させた材料
を用いて、熱間圧延を行った。スラブ加熱温度を112
0℃とし、粗圧延後940℃の粗バーを1050℃に加
熱し、巻取温度は600℃とした。得られた熱延板を酸
洗し、冷圧率80%で冷間圧延を行った後、720℃で
連続焼鈍を行った。得られた材料のr値を測定した。サ
ンプリング位置は、冷延コイルでT部(熱延時の圧延方
向を基準として、先端部)3mの位置とM部(コイル長
手方向中央部)、B部(熱延時の圧延方向を基準とし
て、後端部)3mとした。結果を図2に示す。M部につ
いては測定値を、T、B部についてはM部との差を示
す。B/N比が0.6以上で、M部とT、B部の差は
0.2以下になった。これより、B/N比が0.6以上
で本発明の効果が現れコイルエンド性が低減されるこ
と、B/N比1.5超えで過剰Bにより著しく材質が劣
化することがわかる。さらに、B/Nは0.8〜1.2
で効果が大きいことから、この範囲が好ましい。
By weight%, C: about 0.02%, Si: about 0.01%, Mn: about 0.15%, P: about 0.01%,
S: about 0.008%, Sol. Al: about 0.015%,
N: about 0.002%, hot rolling was performed using a material in which the addition amount of B was variously changed. Slab heating temperature 112
After the rough rolling, the coarse bar at 940 ° C. was heated to 1050 ° C., and the winding temperature was 600 ° C. The obtained hot rolled sheet was pickled, cold rolled at a cold pressure ratio of 80%, and then continuously annealed at 720 ° C. The r value of the obtained material was measured. Sampling positions are as follows: 3 m at the T section (the leading end, based on the rolling direction during hot rolling), M section (the center in the longitudinal direction of the coil), and B section (based on the rolling direction at the time of hot rolling). (End) 3 m. The results are shown in FIG. The measured value is shown for the M part, and the difference from the M part is shown for the T and B parts. When the B / N ratio was 0.6 or more, the difference between the M part and the T and B parts became 0.2 or less. From this, it is understood that the effect of the present invention is exhibited when the B / N ratio is 0.6 or more, and the coil end property is reduced, and that when the B / N ratio exceeds 1.5, the material is significantly deteriorated due to excess B. Further, B / N is 0.8 to 1.2.
This range is preferable because the effect is large.

【0024】本発明の対象とする鋼には、種々の目的に
応じてCu、Ni、Cr、Sn、Mo、Pb等を添加し
ても本発明の効果が失われることはない。ただし、T
i、V、Nb、Zrなど、微細な窒化物を形成する元素
を添加するとこれらの微細析出物が粒成長性を阻害する
ことから、これらの元素の添加又は混入は0.01%以
下とするのが望ましい。
The effect of the present invention is not lost even if Cu, Ni, Cr, Sn, Mo, Pb or the like is added to the steel to be used in the present invention for various purposes. Where T
When elements that form fine nitrides such as i, V, Nb, and Zr are added, these fine precipitates impair the grain growth. Therefore, the addition or mixing of these elements is 0.01% or less. It is desirable.

【0025】上記の成分範囲に調整することにより、コ
イルエンド性の問題を根本的に解決するとともに、酸洗
などの次工程にも負荷をかけない、コイルエンド性の小
さい軟質冷延鋼板を得ることが可能となる。
By adjusting to the above component range, the problem of the coil end property is fundamentally solved, and a soft cold-rolled steel sheet with a small coil end property is obtained without applying a load to the next step such as pickling. It becomes possible.

【0026】このような特性の鋼板は以下の製造方法に
より製造することができる。 (2)鋼板製造工程 (2−1)態様1の製造条件 (製造方法)上記の成分組成範囲に調整した鋼を転炉に
て溶製した後、連続鋳造によりスラブにし、1150℃
以下に加熱し、粗圧延して粗バーとし、その後950℃
以下の粗バーを980℃以上に加熱し、Ar3 点以上で
仕上げ圧延を行い、650℃以下で巻き取る。次に、巻
き取った熱延鋼板を冷間圧延し、焼鈍する。 a.スラブ加熱温度 スラブを1150℃以下に加熱し、粗圧延して粗バーと
する。本発明においては、スラブの加熱温度は重要な役
割を演ずる。本発明ではMnSを粗大化してコイルエン
ド性を解消している。そこで、スラブ中に粗大析出した
MnSについては、可能な限り粗大なままとするため低
温加熱を指向している。加熱温度があまり高いと、加熱
時にMnSが多量に固溶してしまい、微細MnSが過剰
に析出するため、BNによる粗大化効果が低下してしま
うことから、加熱温度は1150℃以下である。また、
あまり低いと圧延負荷が過剰となることから、1050
℃以上が好ましい。
The steel sheet having such characteristics can be manufactured by the following manufacturing method. (2) Steel plate manufacturing process (2-1) Manufacturing conditions of mode 1 (Manufacturing method) After the steel adjusted to the above-described composition range is melted in a converter, it is slab-formed by continuous casting, and 1150 ° C.
Heated below, rough rolled to rough bar, then 950 ° C
The following coarse bar is heated to 980 ° C. or more, finish-rolled at three or more Ar points, and wound at 650 ° C. or less. Next, the rolled hot-rolled steel sheet is cold-rolled and annealed. a. Slab heating temperature The slab is heated to 1150 ° C. or lower and roughly rolled to form a rough bar. In the present invention, the heating temperature of the slab plays an important role. In the present invention, MnS is coarsened to eliminate the coil end property. Therefore, for MnS coarsely precipitated in the slab, low-temperature heating is intended to keep the coarseness as much as possible. If the heating temperature is too high, a large amount of MnS forms a solid solution at the time of heating and fine MnS precipitates excessively, so that the effect of coarsening by BN is reduced. Therefore, the heating temperature is 1150 ° C. or lower. Also,
If the rolling load is too low, the rolling load becomes excessive.
C. or higher is preferred.

【0027】b.粗バー加熱温度 粗圧延した粗バーを950℃以下とした後、980℃以
上に加熱する。粗バー加熱はMnSの析出を促進し、粗
バー両端の温度差やスキッドマークを解消するなど、本
発明の中核をなすものである。MnSを微細析出させる
ため、粗バー加熱前温度の上限は950℃以下である。
また、粗バー加熱前温度については、仕上げ圧延前にA
lNが析出すると、再結晶を遅延させるとともに再結晶
核となることで結晶粒を細かくすることから750℃以
上が望ましい。さらに好ましくは、粗バー加熱前温度が
Ar3 点以下になるとγ/α変態により粗バー加熱後の
γ粒径が、Ar3 以下に冷却しない場合と比べて若干微
細となり、結果的に熱延板粒径が若干小さくなることか
ら、粗バー加熱前温度はAr3 以上がよい。
B. Coarse Bar Heating Temperature The coarsely rolled coarse bar is heated to 980 ° C. or higher after the temperature of the coarse bar is reduced to 950 ° C. or lower. Coarse bar heating is the core of the present invention, such as promoting the precipitation of MnS and eliminating the temperature difference and skid marks at both ends of the coarse bar. In order to finely precipitate MnS, the upper limit of the temperature before heating the coarse bar is 950 ° C. or less.
As for the temperature before heating the coarse bar, A
When 1N is precipitated, the temperature is preferably 750 ° C. or more because recrystallization is delayed and the crystal grains become fine by becoming recrystallization nuclei. More preferably, when the temperature before heating the coarse bar is lower than the Ar 3 point, the γ particle size after the heating of the coarse bar becomes slightly smaller due to the γ / α transformation than when the temperature is not cooled below Ar 3 , resulting in hot rolling. The temperature before heating the coarse bar is preferably Ar 3 or more because the plate grain size becomes slightly smaller.

【0028】また、粗バー加熱温度を980℃未満とし
た場合には、微細MnSを仕上げ圧延前に完全に析出さ
せることができず、本発明の効果が得られない。従っ
て、加熱温度の下限は980℃以上である。一方、粗バ
ー加熱温度が高いと微細析出したMnSが再び固溶し、
本発明の効果が失われることから、粗バー加熱温度はス
ラブ加熱温度以下が望ましく、さらに1050℃以下が
好ましい。
If the heating temperature of the coarse bar is lower than 980 ° C., fine MnS cannot be completely precipitated before the finish rolling, and the effect of the present invention cannot be obtained. Therefore, the lower limit of the heating temperature is 980 ° C. or higher. On the other hand, if the coarse bar heating temperature is high, MnS precipitated finely dissolves again,
Since the effect of the present invention is lost, the heating temperature of the rough bar is desirably equal to or lower than the slab heating temperature, and more desirably 1050 ° C. or lower.

【0029】加熱方法については特に限定しないが、M
nSの析出駆動力を保持したまま急速に、かつ均一に加
熱できる誘導加熱や電気抵抗加熱などが望ましい。ま
た、粗バー加熱前の粗バーをコイル状に一度巻取り、巻
き戻してから粗バー加熱を行うと、MnSの析出駆動力
が向上することから粗バー加熱前にコイルボックスを使
用しても良い。
The heating method is not particularly limited.
Induction heating, electric resistance heating, or the like that can rapidly and uniformly heat while maintaining the nS precipitation driving force is desirable. Also, if the coarse bar before the coarse bar heating is wound once into a coil shape and then rewound and then coarse bar heating is performed, the driving force for precipitation of MnS is improved. good.

【0030】c.仕上圧延温度 本発明においては、仕上圧延温度はAr3 点以上であ
る。仕上圧延温度がAr3 点未満となると、r値を低下
させる集合組織が発達してしまうため、下限はAr3
以上である。
C. Finish Rolling Temperature In the present invention, the finish rolling temperature is at least Ar 3 points. When the finish rolling temperature is less than 3 points Ar, since the texture to reduce the r value will developed, the lower limit is at least 3 points Ar.

【0031】d.巻取温度 仕上げ圧延を行った熱延鋼板を650℃以下で巻き取
る。巻取温度は本発明において重要である。コイルエン
ド性を解消するにはコイルの中央部と両端部の冷却速度
の差を可能な限り小さくする必要がある。従って、巻取
温度の上限は650℃である。ただし、300℃未満で
は巻取後に十分粒成長しなくなり、軟質化効果が飽和す
ることから、300℃以上が望ましい。
D. Winding temperature The hot-rolled steel sheet subjected to finish rolling is wound at 650 ° C. or lower. The winding temperature is important in the present invention. In order to eliminate the coil end property, it is necessary to make the difference in cooling rate between the center and both ends of the coil as small as possible. Therefore, the upper limit of the winding temperature is 650 ° C. However, if the temperature is lower than 300 ° C., the grains do not grow sufficiently after winding, and the softening effect is saturated.

【0032】(2−2)態様2の製造条件 (製造方法)上記の成分組成範囲に調整した鋼を転炉に
て溶製した後、連続鋳造によりスラブにし、750℃以
上のスラブを加熱炉に挿入して1150℃以下に加熱
し、粗圧延して粗バーとし、その後950℃以下の粗バ
ーを980℃以上に加熱し、Ar3 点以上で仕上げ圧延
を行い、650℃以下で巻き取る。次に、巻き取った熱
延鋼板を冷間圧延し、焼鈍する。 a.スラブの加熱炉挿入温度 連続鋳造後のスラブ温度が750℃以上で加熱炉に挿入
する。
(2-2) Manufacturing conditions of embodiment 2 (Manufacturing method) After smelting the steel adjusted to the above-mentioned component composition range in the converter, it is made into a slab by continuous casting, and the slab having a temperature of 750 ° C. or more is heated in a heating furnace. And heated to 1150 ° C or lower, and rough-rolled to form a coarse bar. Thereafter, the coarse bar at 950 ° C or lower is heated to 980 ° C or higher, finish-rolled at three or more points of Ar, and wound at 650 ° C or lower. . Next, the rolled hot-rolled steel sheet is cold-rolled and annealed. a. Slab heating furnace insertion temperature When the slab temperature after continuous casting is 750 ° C or higher, the slab is inserted into the heating furnace.

【0033】連続鋳造後、スラブ温度が750℃未満に
なるとスラブ中にAlNが析出する。AlNが析出する
とスラブ中のNが消費され、BNの粗大化が促進されな
くなることから、AlNの析出を抑制しBNの粗大析出
を促進するために、連続鋳造後スラブの加熱炉挿入温度
の下限はAlNが析出を開始する750℃以上である。
また、特定するものではないが、1000℃以下に冷却
しないとMnSやBNの粗大析出が逆に遅延することか
ら、1000℃以下で加熱炉に挿入することが望まし
い。このように、連続鋳造後のスラブ温度が750℃以
上で加熱炉に挿入すれば、本発明の効果をさらに増加さ
せることができる。
After the continuous casting, when the slab temperature becomes lower than 750 ° C., AlN precipitates in the slab. When AlN precipitates, N in the slab is consumed and coarsening of BN is not promoted. Therefore, in order to suppress the precipitation of AlN and promote the coarse precipitation of BN, the lower limit of the heating furnace insertion temperature of the slab after continuous casting. Is 750 ° C. or higher at which AlN starts to precipitate.
Although not particularly specified, coarse cooling of MnS and BN is delayed unless cooled to 1000 ° C. or lower. Therefore, it is preferable to insert the heating furnace at 1000 ° C. or lower. Thus, if the slab temperature after continuous casting is inserted into the heating furnace at a temperature of 750 ° C. or higher, the effect of the present invention can be further increased.

【0034】b.スラブ加熱温度 態様1の製造条件と同様。 c.粗バー加熱温度 態様1の製造条件と同様。B. Slab heating temperature Same as the manufacturing condition of the first embodiment. c. Coarse bar heating temperature Same as the manufacturing condition of the first embodiment.

【0035】d.仕上圧延温度 態様1の製造条件と同様。 e.巻取温度 態様1の製造条件と同様。D. Finishing rolling temperature Same as the manufacturing conditions of aspect 1. e. Winding temperature Same as the manufacturing conditions of aspect 1.

【0036】以上、本発明において、態様1及び2の各
工程の温度は重要な意味を持っており、このどれか一つ
でもかけた場合、本発明の効果は得られない。なお、酸
洗後の冷間圧延については、加工性、特に深絞り性から
圧延率は30〜90%が好ましい。焼鈍についても軟質
化のため600℃以上、粗大粒抑制のため900℃以下
とする。焼鈍方法は連続焼鈍である。ただし、箱焼鈍を
行ってもなんら問題は生じない。調質圧延の条件につい
ての制限はないが、あまり高いとELの低下が激しいこ
とから、2%以下が望ましい。また、本発明鋼の成分調
整には、転炉と電気炉のどちらも使用可能である。以下
に本発明の実施例を挙げ、本発明の効果を立証する。
As described above, in the present invention, the temperatures in the respective steps of Embodiments 1 and 2 have an important meaning, and if any one of them is applied, the effect of the present invention cannot be obtained. The cold rolling after pickling is preferably performed at a rolling ratio of 30 to 90% from the viewpoint of workability, particularly deep drawing. Annealing is also performed at 600 ° C. or more for softening and 900 ° C. or less for suppressing coarse grains. The annealing method is continuous annealing. However, there is no problem even if the box annealing is performed. There are no restrictions on the conditions of the temper rolling, but if it is too high, the EL will be drastically reduced. For adjusting the composition of the steel of the present invention, both a converter and an electric furnace can be used. Hereinafter, examples of the present invention will be described to demonstrate the effects of the present invention.

【0037】[0037]

【実施例】【Example】

(実施例1)表1に示す成分の鋼を溶解し、同表に示す
製造条件(本発明例:No.1〜19、比較例:No.
20〜25)にて熱延を行った。粗バーの加熱について
は誘導加熱で行い、昇温に要した時間は5秒以内であ
る。さらに得られた熱延板を冷圧率75%で冷間圧延を
行い、750℃で連続焼鈍熱サイクルにより焼鈍を行っ
た。板厚は0.75mmである。製造したコイルの熱延
時の長手方向先端部(T部)3mと中央部(M部)さら
には後端部(B部)3mからJIS5号引張試験片を採
取し、引張試験による引張強度(TS)、伸び(EL)
と平均のr値を測定した。
(Example 1) Steels having the components shown in Table 1 were melted and manufactured under the manufacturing conditions (Examples of the present invention: Nos. 1 to 19, Comparative Examples: No. 1) shown in the table.
20 to 25). The heating of the coarse bar is performed by induction heating, and the time required for raising the temperature is within 5 seconds. Further, the obtained hot-rolled sheet was cold-rolled at a cold-pressure ratio of 75%, and annealed at 750 ° C. by a continuous annealing heat cycle. The plate thickness is 0.75 mm. A JIS No. 5 tensile test piece was sampled from the front end portion (T portion) 3 m, the center portion (M portion), and the rear end portion (B portion) 3 m of the manufactured coil at the time of hot rolling and the tensile strength (TS ), Elongation (EL)
And the average r value were measured.

【0038】なお、平均のr値は、JIS5号引張試験
片を鋼板の圧延方向、圧延直角方向及び圧延45°方向
に採取し、15%歪みを引張りにより付与した時のr
値、r0 、r90、r45から、mean-r=(r0 +2r45
90)/4により算出された値である。
The average r value was determined by taking a JIS No. 5 tensile test specimen in the rolling direction, the direction perpendicular to the rolling direction, and the 45 ° direction of the rolling of the steel sheet, and applying 15% strain by tension.
From the values, r 0 , r 90 , and r 45 , mean-r = (r 0 + 2r 45 +
r 90 ) / 4.

【0039】以上の測定結果を表2に示す。M部につい
ては測定値を、T、B部についてはM部との差を示し
た。ELについては、本発明例No.1〜19において
は、M部は40%以上であり、かつM部とT、B部の差
は3%以下に、またr値については、M部は1.4以上
であり、かつM部とT、B部の差は0.2以下になっ
た。
Table 2 shows the above measurement results. The measured value is shown for the M part, and the difference from the M part is shown for the T and B parts. As for EL, the present invention example No. In Nos. 1 to 19, the M part is 40% or more, and the difference between the M part and the T and B parts is 3% or less, and the r value of the M part is 1.4 or more and the M part is And the difference between the T and B parts was 0.2 or less.

【0040】一方、比較例No.20〜25において
は、加熱温度、粗バー加熱温度、巻取温度及びB量のい
ずれか一つの条件でもかけた場合であり、ELもしくは
r値の少なくとも一方のコイルエンド性の低減が認めら
れないか、値が低い。比較例No.24についてはBが
過剰に添加されたものであり、コイルエンド性は低減し
ているが、EL、r値とも値が低く、本発明例No.1
〜19よりも劣ることがわかる。以上より、本発明によ
り製造された冷延鋼板のT、B部の材質はM部と同等で
ある。
On the other hand, in Comparative Example No. In the case of 20 to 25, any one of the heating temperature, the rough bar heating temperature, the winding temperature and the B amount was applied, and no reduction in the coil end property of at least one of EL and r value was observed. Or the value is low. Comparative Example No. In the case of Example No. 24 of the present invention, B was excessively added, and although the coil end property was reduced, the values of EL and r were low. 1
It can be seen that it is inferior to # 19. From the above, the materials of the T and B portions of the cold-rolled steel sheet manufactured according to the present invention are equivalent to the M portion.

【0041】[0041]

【表1】 [Table 1]

【0042】[0042]

【表2】 [Table 2]

【0043】(実施例2)表3に示す成分の鋼を溶解
し、同表に示す温度で加熱炉に挿入し、同表に示す製造
条件(本発明例:No.1〜19、比較例:No.20
〜25)にて熱延を行った。さらに得られた熱延板を冷
圧率60%で冷間圧延を行い、680℃で連続焼鈍熱サ
イクルにより焼鈍を行った。板厚は1mmとした。製造
したコイルの熱延時の長手方向先端部(T部)3mと中
央部(M部)さらには後端部(B部)3mのTS、EL
と平均のr値を実施例1と同様に測定した。
(Example 2) Steels having the components shown in Table 3 were melted and inserted into a heating furnace at the temperature shown in the table, and the production conditions shown in the table (Examples of the present invention: Nos. 1 to 19, comparative examples) : No. 20
2525). Further, the obtained hot-rolled sheet was cold-rolled at a cold pressure rate of 60%, and annealed at 680 ° C. by a continuous annealing heat cycle. The plate thickness was 1 mm. TS and EL at the longitudinal end (T section) 3 m, the center (M section) and the rear end (B section) 3 m of the manufactured coil at the time of hot rolling.
And the average r value were measured in the same manner as in Example 1.

【0044】測定結果を表4にまとめて示す。M部につ
いてはTS、EL、r値の測定値を、T、Bについては
ELとr値におけるM部との差を示した。ELについて
は、本発明例No.1〜19においては、M部は40%
以上であり、かつM部とT、Bの差は2%以下に、また
r値については、M部は1.4以上であり、かつM部と
T、B部の差は0.1以下になった。
Table 4 summarizes the measurement results. For the M part, the measured values of the TS, EL, and r values are shown, and for T and B, the difference between the EL and the M part in the r value is shown. As for EL, the present invention example No. In 1 to 19, M part is 40%
The difference between the M part and the T and B parts is 2% or less, and the r value of the M part is 1.4 or more and the difference between the M part and the T and B parts is 0.1 or less. Became.

【0045】一方、比較例No.20〜25において
は、加熱温度、粗バー加熱温度、巻取温度、B量のいず
れか一つの条件でもかけた場合であり、ELもしくはr
値の少なくとも一方のコイルエンド性の低減が認められ
ないか、値が低い。比較例No.24についてはBが過
剰に添加されたものであり、コイルエンド性は低減して
いるが、EL、r値とも値が低く、本発明例No.1〜
19よりも劣ることがわかる。以上より、本発明により
製造された冷延鋼板のT、B部の材質はM部と同等であ
る。
On the other hand, Comparative Example No. In the case of 20 to 25, any one of the heating temperature, the rough bar heating temperature, the winding temperature, and the B amount is applied.
No reduction or low value of the coil end property of at least one of the values is observed. Comparative Example No. In the case of Example No. 24 of the present invention, B was excessively added, and although the coil end property was reduced, the values of EL and r were low. 1 to
It turns out that it is inferior to 19. From the above, the materials of the T and B portions of the cold-rolled steel sheet manufactured according to the present invention are equivalent to the M portion.

【0046】[0046]

【表3】 [Table 3]

【0047】[0047]

【表4】 [Table 4]

【0048】[0048]

【発明の効果】本発明によれば、鋼組成及び製造条件を
特定することにより、コイル長手方向の両端の切断など
を行わなくとも長手方向の材質が均一である、加工性に
優れた軟質冷延鋼板を安価に製造することが可能であ
る。
According to the present invention, by specifying the steel composition and the manufacturing conditions, the material in the longitudinal direction is uniform without cutting the both ends in the longitudinal direction of the coil, and the soft chill with excellent workability is obtained. It is possible to manufacture a rolled steel sheet at low cost.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の実施の形態に係る粗バー加熱温度とM
部とT、B部のr値の差との関係を示す図。
FIG. 1 is a graph showing a relationship between a rough bar heating temperature and M according to an embodiment of the present invention.
The figure which shows the relationship between a part and the difference of r value of T, B part.

【図2】本発明の実施の形態に係るB/N比とM部のr
値及びM部とT、B部のr値の差との関係を示す図。
FIG. 2 shows the B / N ratio and r of the M part according to the embodiment of the present invention.
The figure which shows the relationship between a value and the difference of r value of M part and T, B part.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 澤田 弘 東京都千代田区丸の内一丁目1番2号 日本鋼管株式会社内 (72)発明者 石黒 康英 東京都千代田区丸の内一丁目1番2号 日本鋼管株式会社内 (72)発明者 村山 尚志 東京都千代田区丸の内一丁目1番2号 日本鋼管株式会社内 (58)調査した分野(Int.Cl.7,DB名) C21D 9/46 - 9/48 C21D 8/00 - 8/10 C22C 38/00 - 38/60 ──────────────────────────────────────────────────続 き Continuing on the front page (72) Inventor Hiroshi Sawada 1-1-2 Marunouchi, Chiyoda-ku, Tokyo Nippon Kokan Co., Ltd. (72) Inventor Yasuhide Ishiguro 1-1-2 Marunouchi, Chiyoda-ku, Tokyo Nippon Kokan Co., Ltd. (72) Inventor Naoshi Murayama 1-2-1, Marunouchi, Chiyoda-ku, Tokyo Nippon Kokan Co., Ltd. (58) Field surveyed (Int. Cl. 7 , DB name) C21D 9/46-9/48 C21D 8/00-8/10 C22C 38/00-38/60

Claims (2)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 重量%で、C≦0.03%と、Mn≦
0.5%と、Si≦0.1%と、P≦0.025%と、
S≦0.03%と、Sol.Al≦0.1%と、N≦
0.0035%と、B≦0.003%とを含有し、かつ
原子比でB/N=0.6〜1.5を満足し、残部がFe
及び不可避的不純物からなる鋼板を製造する方法におい
て、 鋼を1150℃以下に加熱し、粗圧延して粗バーとする
工程と、 950℃以下の粗バーを980℃以上に加熱し、Ar3
点以上で仕上げ圧延を行い、650℃以下で巻き取る工
程と、 巻き取った熱延鋼板を冷間圧延し、焼鈍する工程と、 を備えたことを特徴とするコイルエンド性の小さい軟質
冷延鋼板の製造方法。
1. The method according to claim 1, wherein C ≦ 0.03% and Mn ≦
0.5%, Si ≦ 0.1%, P ≦ 0.025%,
S ≦ 0.03%, Sol. Al ≦ 0.1%, N ≦
0.0035% and B ≦ 0.003%, and the atomic ratio of B / N = 0.6 to 1.5 is satisfied, and the balance is Fe
And a process for preparing steel consisting of unavoidable impurities, the steel was heated to 1150 ° C. or less, a step of the rough rolling to a crude bar, heated 950 ° C. or less coarse bar above 980 ° C., Ar 3
Soft rolling with a small coil end property, comprising: a step of performing finish rolling at a temperature of not less than 650 ° C. and winding at 650 ° C. or less; and a step of cold rolling and annealing the rolled hot rolled steel sheet. Steel plate manufacturing method.
【請求項2】 請求項1に記載の組成を有する鋼板を製
造する方法において、 連続鋳造した鋼を750℃以上で加熱炉に挿入して11
50℃以下に加熱し、粗圧延して粗バーとする工程と、 950℃以下の粗バーを980℃以上に加熱、Ar3
以上で仕上げ圧延を行い、650℃以下で巻き取る工程
と、 巻き取った熱延鋼板を冷間圧延し、焼鈍する工程と、 を備えたことを特徴とするコイルエンド性の小さい軟質
冷延鋼板の製造方法。
2. The method for producing a steel sheet having the composition according to claim 1, wherein the continuously cast steel is inserted into a heating furnace at 750 ° C. or higher.
A step of heating to 50 ° C or lower and rough rolling to form a rough bar; a step of heating a coarse bar of 950 ° C or lower to 980 ° C or higher, performing finish rolling at three or more Ar points, and winding at 650 ° C or lower; Cold rolling and annealing the rolled hot-rolled steel sheet; and a method for producing a soft cold-rolled steel sheet having low coil end properties.
JP00145897A 1997-01-08 1997-01-08 Manufacturing method of soft cold rolled steel sheet with small coil end property Expired - Fee Related JP3339341B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP00145897A JP3339341B2 (en) 1997-01-08 1997-01-08 Manufacturing method of soft cold rolled steel sheet with small coil end property

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP00145897A JP3339341B2 (en) 1997-01-08 1997-01-08 Manufacturing method of soft cold rolled steel sheet with small coil end property

Publications (2)

Publication Number Publication Date
JPH10195542A JPH10195542A (en) 1998-07-28
JP3339341B2 true JP3339341B2 (en) 2002-10-28

Family

ID=11502020

Family Applications (1)

Application Number Title Priority Date Filing Date
JP00145897A Expired - Fee Related JP3339341B2 (en) 1997-01-08 1997-01-08 Manufacturing method of soft cold rolled steel sheet with small coil end property

Country Status (1)

Country Link
JP (1) JP3339341B2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100530072B1 (en) * 2001-12-20 2005-11-22 주식회사 포스코 Hot-rolled Low Carbon Steel Sheets having high ductility and low mechanical properties deviation in coil length direction, and its production method

Also Published As

Publication number Publication date
JPH10195542A (en) 1998-07-28

Similar Documents

Publication Publication Date Title
JPH0635619B2 (en) Manufacturing method of high strength steel sheet with good ductility
EP0905267B1 (en) Soft cold-rolled steel sheet and method for making the same
JP4644075B2 (en) High-strength steel sheet with excellent hole expansibility and manufacturing method thereof
JP2007239097A (en) Manufacturing method of hot-rolled steel sheet for high-strength cold-rolled steel sheet
CN109023038B (en) Phase-change induced plasticity steel and preparation method thereof
JP3339340B2 (en) Manufacturing method of high workability soft cold rolled steel sheet
JP3339341B2 (en) Manufacturing method of soft cold rolled steel sheet with small coil end property
JP4010131B2 (en) Composite structure type high-tensile cold-rolled steel sheet excellent in deep drawability and manufacturing method thereof
EP4435133A1 (en) Hot-rolled steel for enameling having enameling and firing strengthening property, and manufacturing method therefor
JP3379404B2 (en) Method for manufacturing soft cold-rolled steel sheet excellent in shape in coil longitudinal direction
JP3339342B2 (en) Manufacturing method of soft hot rolled steel sheet with small coil end property
JP3339343B2 (en) Manufacturing method of high workability soft hot rolled steel sheet
JPH0570836A (en) Manufacturing method of high strength cold rolled steel sheet for deep drawing
JPH09249936A (en) Cold rolled steel sheet excellent in balance between bake hardenability and ductility and room temperature aging, and method for producing the same
JP2975087B2 (en) Manufacturing method of high toughness and high tensile strength hot rolled steel sheet with excellent uniformity
JPH0559970B2 (en)
JP3925063B2 (en) Cold-rolled steel sheet excellent in press formability and strain age hardening characteristics and method for producing the same
JP3508491B2 (en) Soft cold rolled steel sheet excellent in microstructure stability and method for producing the same
JP2669188B2 (en) Manufacturing method of high strength cold rolled steel sheet for deep drawing
JP2000212690A (en) High-strength hot-rolled steel sheet excellent in formability and surface properties and method for producing the same
JP3271655B2 (en) Method for producing silicon steel sheet and silicon steel sheet
JP3704790B2 (en) Cold-rolled steel sheet with good aging resistance
JP2000119804A (en) Hot rolled steel sheet excellent in deep drawability and method for producing the same
JP3551105B2 (en) Cold rolled steel sheet with less material variation in coil and method of manufacturing the same
JPH11350037A (en) Manufacturing method of cold rolled steel sheet material for processing

Legal Events

Date Code Title Description
FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20070816

Year of fee payment: 5

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20080816

Year of fee payment: 6

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20080816

Year of fee payment: 6

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090816

Year of fee payment: 7

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090816

Year of fee payment: 7

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100816

Year of fee payment: 8

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110816

Year of fee payment: 9

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20120816

Year of fee payment: 10

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20120816

Year of fee payment: 10

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130816

Year of fee payment: 11

LAPS Cancellation because of no payment of annual fees