JP3397552B2 - Cosmetics - Google Patents

Description

DETAILED DESCRIPTION OF THE INVENTION [0001] BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to the use of
The present invention relates to a cosmetic that prevents aging and hair fatigue. [0002] 2. Description of the Related Art Rinacanthus nasuta (L.)
Kurz) is Linaca, native to the Deccan Plateau in southern India
It is an evergreen shrub belonging to the sessile fox family
Whole grass (Linacanthus grass) against anthelmintic, anti-inflammatory and skin fungus
It is known to have antibacterial action, mainly in China, Taiwan, etc.
In recent years, it has also been used as a Kampo medicine in Japan.
It has been. However, the makeup of Hakutsuru Reishi is currently
There is no example used in the fee. [0003] Ganoderma lucidum is another name
Mannentake, also known as Mannentake, grows in various parts of Japan
It is a basidiomycete belonging to the genus Monkey. This one
The powder is used for fatigue, insomnia, nervous breakdown, indigestion,
It is said to be effective for bronchial diseases, etc.
And is used as a health food. In addition, Dokudami (Ho
uttuynia cordana Thumberg)
Which is commonly found in Honshu, Shikoku, Kyushu and Okinawa
It is an annual grass. The water immersion liquid has an antihypertensive effect.
And the decoction has diuretic, antibacterial and bacteriostatic effects.
It is said that it is also used for health foods such as medical use and tea.
Used. However Reishi and Dokudami
But at least it is used in cosmetics with Hakutsuru Reishi
No examples are found. [0004] SUMMARY OF THE INVENTION Human skin, especially
Due to age, stress, and the effects of ultraviolet light in sunlight,
Causes the so-called skin aging phenomenon such as pigmentation, wrinkles, dry skin, etc.
You. In addition, hair is moisturizing, elastic,
Causes hair fatigue phenomenon that deteriorates strength and loses luster
Rub Such phenomena that occur on the skin and hair are
Superoxide and arsenic generated in the air by the action of wire
Active oxygen such as droxy radical, especially superoxide
This irritation is caused by skin irritation.
And superoxide dismutase on hair surface
(SOD) or other substance having the ability to scavenge active oxygen
Then, the active oxygen may be eliminated by the action. [0005] The present inventors have found that skin aging and hair fatigue can be reduced.
As a result of intensive research on cosmetic materials that do not occur, Hakutsuru
Reishi solvent extract has excellent ability to scavenge active oxygen
And came to the conclusion that this should be used for cosmetics.
Thus, the present invention has been completed. [0006] SUMMARY OF THE INVENTION The present invention relates to a method for producing water from Hakutsuru Reishi.
And / or an organic solvent extract.
Cosmetics. Furthermore, the present invention provides
Water and / or organic solvent for the mixture of turf and prickle
A cosmetic comprising an extract. [0007] Hakutsuru Reishi used in the present invention is commercially available.
Raw or dry, whole grass (aboveground) or
Can be used alone or in combination with leaves, stems, branches and roots.
What mixed the above suitably may be used. [0008] Such a white cranes Reishi is extracted by solvent extraction
Water and organic solvents.
Media, and these may be used alone or in appropriate proportions.
Used. These water and organic solvents are at room temperature or
Use in a heated or cooled state. use
The organic solvents used include ethanol, methanol, and
Alcohols such as panol and 1,3-butylene glycol
, Dimethyl ether, diethyl ether, methyl ethyl
Ethers such as toluene ether, ketones such as acetone,
Charcoal such as xane, heptane, liquid paraffin, squalane
Hydrides and others, and these may be used alone or in combination.
These can be used in combination. The resulting extract of Hakutsuru Reishi is odorless or slightly odorless.
Kana fragrance, transparent and greenish brown with a unique rich taste
Deep green liquid that can be used as is
But preferably purified by filtration, centrifugation or other methods
These are used after being appropriately concentrated by means such as distillation. Also
The extract is further processed by means of distillation to dryness, freeze drying, etc.
Odorless or slight fragrance, unique rich taste
Greenish brown to deep green fine powder
It is possible. The solvent extraction of Hakutsuru Reishi obtained in this way
The product has excellent active oxygen scavenging ability. In the present invention, the solvent extraction raw material is used.
Not only Hakutsuru Reishi, but also Hakutsuru Reishi as described above.
And a mixture of dokudami may be used. This place
If the mixture ratio of Reishi and Dokudami is 1-
40% by weight, preferably 5 to 30% by weight, more preferably
Or 10 to 20% by weight. Extraction method is Hakutsuru Reishi
What is necessary is just to do it in the case of Germany. Extract of the resulting mixture
Has a slight aroma, a distinctive rich taste,
Clear liquid, which is also the same as Hakutsuru Reishi
Can be used as purified, concentrated or fine powder
Wear. This fine powder has a slight aroma and a unique rich taste
Greenish brown to deep green. Like this
The solvent extract of the resulting mixture is also an excellent cosmetic base
It has suitability as a fee. [0011] Such Hakutsuru Reishi or this and Reishi and
And extract the solvent extract of the mixture
Compounded with various materials commonly used as cosmetic materials
Manufacture cosmetics. Formulation of cosmetics of solvent extract of Hakutsuru Reishi
When the ratio is in the form of an extract, the ratio is 0.1 to the total amount of the cosmetic.
001 to 30.0% by weight, preferably 0.01 to 20.
0% by weight. In the case of fine powder, the whole cosmetic
0.00001 to 10.0% by weight, preferably
0.0001 to 5.0% by weight. Hakutsuru Reishi, Spirit
The compounding ratio of the solvent extract of the mixture of turf and dokudami is
The extract of Hakutsuru Reishi from this solvent extract is
The range may be the same as the case. The solution according to the present invention
The vehicle extract applies to all skin and hair cosmetic formulations.
For example, emulsions, lotions
, Soap, cream, pack, powder, foundation
Skin, essence, other skin cosmetics and shampoos
ー, rinse, hair tonic, hair liquid, hair spray
And other hair cosmetics. Next, extraction examples, test examples, and examples of the present invention will be described in order.
However, these limits the technical scope of the present invention.
It is not specified. 【Example】Extraction example 1 Dried Hakutsuru Reishi (Daikyo Bussan Co., Ltd .; hereinafter, acquisition of Hakutsuru Reishi)
3 g of leaves and branches were put in hot water of 100 ° C. 50
Soak in 0ml for 2 minutes, make up to 500ml and have a unique taste
, A transparent green-brown extract having odor and aroma was obtained. [0013]Extraction example 2 3g of a mixture (whole plant) of dried white crane reishi stalks, branches and leaves
Immerse in 500 ml of water, heat to 100 ° C and hold for 60 minutes
After filtration, the resulting filtrate was made up to a volume of 500 ml.
Obtain a clear, green-brown extract with a unique taste and aroma
Was. [0014]Extraction example 3 Dip 3 g of dried white crane Reishi branch in 500 ml of water and add 100 g
After heating to 90 ° C. and holding for 90 minutes, filtration was performed, and the obtained filtrate was
With a unique taste and aroma
To obtain a green-brown extract. [0015]Extraction example 4 The extraction residue of Extraction Example 1 was immersed in 500 ml of water,
And hold for 60 minutes.
Obtain a clear, green-brown extract with a unique taste and aroma
Was. [0016]Extraction example 5 Table 1 shows the dried mixture of the whole grass and roots of Hakutsuru Reishi.
Put each sample prepared as described in
Inject 600ml of hot water and shake for 1 minute, unique taste and aroma
And a green-brown extract having the formula:Composition of each raw material Sample No. Hakutsuru Reishi (2.0g) Ａ Blend with all raw materials solidB Blend after grinding all raw materials [0017]Extraction example 6 The powder obtained by crushing the whole dried white crane Reishi grass with a crusher
The crushed material is acetone, benzene, 1,3-butylene glycol
1.00g / 50ml each in water, ethanol and ether
For about 24 hours. Then these
Transparent deep green color with unique taste and aroma
Each solvent extract was obtained. [0018]Test example 1 Each extract extracted by the method of Extraction Examples 1 to 4 was 100
% And 10% dilution with distilled water
Used. Superoxide is hypoxanthine-
Xanthine oxidase (hypoxanthin-xanthin oxidas
e) O generated by the system₂ ⁻To 5,5-dimethyl-1
-Pyrroline-1-oxide [5,5-dimethyl-1-pyrroline-
1-oxide (DMPO)]
Radical strength was measured using an ESR (ESR). Control
For this rule, distilled water was used, and the deviation (SD) was determined. test
Table 1 shows the results. High Sue for solvent extract of Hakutsuru Reishi
It is clear that there is peroxide erasing ability. [0019] [Table 1] [0020]Test example 2 Each extract extracted by the method of Extraction Examples 1-4 is freeze-dried,
A sample obtained by appropriately diluting the obtained powder with distilled water
The same treatment as in Test Example 1 was carried out, except that the above was used. Three times
Table 2 shows the average values of the test results. Heat from test results
It was suggested that the extraction method was efficient. [0021] [Table 2] [0022]Test example 3 Using samples A and B extracted by the method of extraction example 5
Was. Superoxide is hypoxanthine-xanthi
Oxidase (hypoxanthin-xanthin oxidase) system
O generated₂ ⁻To 5,5-dimethyl-1-pyrroli
1-oxide [5,5-dimethyl-1-pyrroline-1-oxide
(DMPO)] and an electron spin resonance device (E
SR) was used to measure the radical strength. Also, hydroxy
The sil radical was generated by the Fenton reaction system.
H is adducted with DMPO and radical strength is obtained using ESR.
The degree was measured. The control uses ultrapure water,
Calculate the radical intensity ratio and standard deviation (SD) based on the values
I did. Table 3 shows the test results. Super oxide disappearance
In castration, the difference due to the difference in form is only about 3%.
Since it has a radical scavenging ability of 0% or more,
Can also be said to have a strong erasing ability. [0023] [Table 3] [0024]Test example 4 Acetone, ethanol extracted by the method of Extraction Example 6 and
Each extract of ether was used as 100% stock solution, and these stock solutions were
In addition, samples diluted appropriately with each solvent were used as samples.
-Diphenyl-2-picrylhydrazy
The l (DPPH) radical scavenging ability was measured. The test is DP
Dissolve 0.0012 g of PH in 100 ml of ethanol
0.1 ml of the obtained DPPH solution and 0.1 ml of the sample.
The radical strength is obtained by reacting the product with
Was measured. Note that the control
Use the same solvent used for each extraction.
Was. Table 4 shows the test results. All samples are excellent
It is clear that it has a DPPH radical scavenging ability. [0025] [Table 4] [0026]Test example 5 A test was performed using the benzene extract extracted by the method of Extraction Example 6.
Radical strength of superoxide in the same manner as in Example 1.
Was measured. The benzene used for extraction is water-insoluble
Since it is a solvent, leave it until it is completely removed
After natural evaporation, the mixture was diluted with 20 ml of ethanol.
The extract thus treated was used as a 100% stock solution.
Solution diluted to 10% and 1% with ethanol
Was used as a sample. Table 5 shows the test results.
All samples have superoxide erasing ability
It is clear that. [0027] [Table 5] [0028]Test example 6 1,3-butylene glycol extracted by the method of Extraction Example 6
Using the same method as in Test Example 1
The side radical strength was measured. The test results are shown in Table 6.
You. This extract also has superoxide scavenging ability.
It is clear. [0029] [Table 6] [0030]Example 1 Bar soap After thoroughly kneading the soap material of the following formulation example 1,
The die is put into an extruder maintained at 50 ° C and extruded.
Bar soap was produced using a punching machine.Formulation Example 1 (% By weight; all formulas below are expressed in weight%)
)   Cetanol 10.00   Dibutylhydroxytoluene 0.02   Extract from Extraction Example 1 20.00   Colorant trace   Natural oil soap base (40% tallow, 20% coconut oil,   (NaOH 30%, moisture 10%) After using this soap for 3 months, it improves skin roughness
Keeps your skin moist and moisturized
Was. [0031]Example 2 Bar soap After thoroughly kneading the soap material of the following formulation example 2,
Extrude by inserting the die into an extruder maintained at 45 ° C.
Bar soap was produced using a punching machine.Formulation Example 2   N-lauroyl-L-glutamate monosodium 64.00   N-oleoyl-monosodium L-glutamate 10.00   Myristyl alcohol 5.00   Lauric acid diethanolamide 2.00   Edetate disodium 0.20   Titanium oxide 0.10   Lyophilized powder of the extract of Extraction Example 1 0.10   Purified water balance After using this soap for 2 months, it improves skin roughness
Keeps your skin moist and moisturized
Was. [0032]Example 3 Cream The cream material of the formulation of the following formulation example 3 was heated and dissolved, stirred.
The cream is manufactured by the usual methods such as stirring, emulsification and cooling.
Was.Formulation Example 3   Glycerin monostearate 5.00   Stearic acid 5.00   Polyethylene glycol monostearate 2.00   Behenyl alcohol 1.00   Liquid paraffin 10.00   Glyceryl trioctanoate 10.00   Extract of Extraction Example 2 0.01   1,3-butylene glycol 5.00   Paraoxybenzoate 0.20   Edetate disodium 0.01   Purified water balance After using this cream for 3 months, the skin became rough
Improves and keeps skin moist and moist
Came. [0033]Example 4 Cream Extraction Example 2 Instead of 0.01% by weight of the extract of Extraction Example 2,
Using 0.0001% by weight of freeze-dried powder
Was processed in the same manner as in Example 3 to produce a cream. This
After using the cream for 2 months, the skin became rough
Good, moisturized and moisturized skin
Was. [0034]Example 5 lotion Stir and dissolve the lotion material of the following formula 4
A lotion was prepared by a conventional method such as squeezing.Formulation Example 4   Ethanol 15.00   Polyoxyethylene hydrogenated castor oil 8.00   1,3-butylene glycol 4.00   Coconut oil 1.00   Sodium citrate 0.30   Citric acid 0.10   Paraoxybenzoate 0.10   Sodium citrate 0.30   Edetate disodium 0.01   Extract of Extraction Example 3 10.00   Purified water balance After using this lotion for one month,
Can improve and keep your skin moist and moist
did it. [0035]Example 6 lotion Instead of 10.00% by weight of the extract of Extraction Example 3, an extraction example
Use 0.10% by weight of freeze-dried powder of extract 3
Was treated in the same manner as in Example 5 to produce a lotion.
After using this lotion for 3 months,
Can improve and keep your skin moist and moist
did it. [0036]Example 7 mousse After stirring and dissolving the mousse material of the formulation of the following formulation example 5,
Pressure-fill with dimethyl ether and liquefied petroleum gas
A mousse was produced by sealing in a container equipped with a spraying device.Formulation Example 5   N-methacryloylethyl-N, N-diethyl   Ammonium / α-N-methylcarboxy solid   In-butyl methacrylate copolymer (30%) 4.00   Ethanol 13.00   Polyoxyethylene cetyl ether 3.00   Edetate disodium 0.01   Extract of Extraction Example 4 5.00   Purified liquid balance After using this mousse for two months,
Good, moisturized and moisturized skin
Was. [0037]Example 8 Mousse Instead of 5.00% by weight of the extract of Extraction Example 4,
Except for using 0.05% by weight of freeze-dried powder of the extract,
A mousse was produced in the same manner as in Example 7. This mousse
Has been used for three months,
I was able to keep the skin moist and moist. [0038]Example 9 Emulsion The emulsion material of the formulation of the following formulation example 6 is heated, dissolved, and stirred milk.
The emulsion was processed by conventional methods such as conversion and cooling.Formulation Example 6   Polyoxyethylene sorbitan monostearate 2.00   Stearic acid 0.50   Polyoxyethylene sorbite tetraoleate 0.50   Behenyl alcohol 0.50   Lipophilic glyceryl monostearate 1.00   Glyceryl trioctanoate 4.00   Avocado oil 4.00   Extract of Extraction Example 5A 30.00   1,3-butylene glycol 5.00   Paraoxybenzoate 0.20   Edetate disodium 0.01   Xanthan gum 0.14   Glycerin 0.50   Purified water balance After using this emulsion for 2 months, it improves skin roughness
And keeps your skin moist and moist
Was. [0039]Example 10 Emulsion Extraction Example 5 Instead of 30.0% by weight of the extract of Extraction Example 5A
Aside from using 0.3% by weight of the freeze-dried powder of the extract of A,
An emulsion was prepared in the same manner as in Example 9. This emulsion
After using it for 3 months, the rough skin has been improved and
I was able to keep my skin moist and moist. [0040]Example 11 Emulsion Heating dissolution and stirring milk
The emulsion was processed by conventional methods such as conversion and cooling.Formulation Example 7   Polyoxyethylene sorbitan monostearate 1.00   Stearic acid 0.50   Polyoxyethylene sorbite tetraoleate 0.50   Behenyl alcohol 0.50   Lipophilic glyceryl monostearate 1.00   Glyceryl trioctanoate 4.00   Avocado oil 4.00   Ascorbic acid 0.10   Extract of Extraction Example 5B 0.015   1,3-butylene glycol 5.00   Paraoxybenzoate 0.20   Edetate disodium 0.01   Xanthan gum 0.14   Purified water balance After using this emulsion for 3 months, it improves skin roughness
And keeps your skin moist and moist
Was. [0041]Example 12 Emulsion Extraction was performed in place of 0.015% by weight of the extract of Extraction Example 5B.
Using 0.0002% by weight of freeze-dried powder of the extract of Example 5B
Otherwise, the same processing as in Example 10 was performed to produce an emulsion.
Was. After using this emulsion for one month,
Improves and keeps skin moist and moist
Came. [0042]Example 13 Ointment Instead of using 3g of dried Hakutsuru Reishi branch,
Except for using 3 g of root, the extract was processed in the same manner as in Extraction Example 3
I got Ointment of the formulation of the following formulation example 8 using this extract
The agent material is processed by a conventional method such as heating and dissolving, stirring emulsification, and cooling.
Then, an ointment was produced.Formulation Example 8   Polyethylene glycol monostearate 2.00   Stearic acid 5.00   Polyoxyethylene sorbite tetraoleate 0.50   Behenyl alcohol 1.00   Lipophilic glyceryl monostearate 5.00   Glyceryl trioctanoate 10.00   Liquid paraffin 10.00   Hakutsuru Reishi root extract 1.50   1,3-butylene glycol 5.00   Paraoxybenzoate 0.20   Edetate disodium 0.01   Propylene glycol 1.00   Purified water balance After using this ointment for one month, the rough skin improved.
Good, moisturized and moisturized skin
Was. [0043]Example 14 Ointment Instead of 1.50% by weight of Hakutsuru Reishiba root extract, this Hakutsuru
Use 10.00% by weight of freeze-dried powder of Reishi root extract
Other than that, it processed similarly to Example 13 and manufactured the ointment.
After using this ointment for one month, the rough skin improved.
Good, moisturized and moisturized skin
Was. [0044]Example 15 Emulsion Using the ethanol extract obtained by the method of Extraction Example 6,
A milky lotion is prepared by stirring and mixing the milky lotion material of the formula 9
did.Formulation Example 9   Natural fat (tallow: coconut oil = 7: 3, moisture 15%) 8.00   Ethanol 5.00   Behenyl alcohol 0.50   Citric acid 0.10   Sodium citrate 0.20   Ethanol extract of Extraction Example 6 15.00   1,3-butylene glycol 4.00   Paraoxybenzoate 0.10   Edetate disodium 0.01   Purified water balance After using this emulsion for 3 months, it improves skin roughness
And keeps your skin moist and moist
Was. [0045]Example 16 Emulsion Instead of 15.00% by weight of the ethanol extract of Extraction Example 6
The freeze-dried powder of the ethanol extract of Extraction Example 6 was 0.15
Except for using wt%, the same treatment as in Example 15
A liquid was produced. After using this emulsion for 3 months
To improve moist and moist skin
I was able to keep. [0046]Example 17 Hair cream 3g of raw root of Hakutsuru Reishi was mixed with water: ethanol = 4: 1
After immersion in 500 ml for 120 minutes, this was filtered and extracted.
A liquid was obtained. Formulation of Formulation Example 10 below using this extract
Heating, dissolving, stirring emulsification, cooling, etc.
A hair cream was produced by a conventional treatment.Formulation Example 10   Solid paraffin 3.00   Liquid paraffin 10.00   Squalane 5.00   Jojoba oil 2.00   Polyoxyethylene cetyl ether 1.00   Hakutsuru Reishi lawn root extract 0.50   Sorbitan sesquioleate 1.00   Glycerin 3.00   Ethyl paraben 0.10   Purified water balance After using this hair cream for 3 months,
The hair became supple and elastic. [0047]Example 18 Hair cream Instead of 0.50% by weight of Hakutsuru Reishi turf root extract,
Use 0.005% by weight of freeze-dried powder of lawn root extract
Otherwise, process in the same manner as in Example 17 to produce a hair cream
did. After using this hair cream for 3 months
To make the hair shiny, supple and elastic
Was. [0048]Example 19 Hair Tonic Using the 1,3-butylene glycol extract of Extraction Example 6,
Heating and dissolving the material for hair tonic of the following prescription example 11
To produce a hair tonic.Formulation Example 11   Ethanol 20.00   1% chitosan aqueous solution 20.00   1,3-butylene glycol extract of extraction example 6 0.30   Purified water balance After using this hair tonic for three months,
The hair became supple and elastic. [0049]Example 20 Hair tonic 1,3-butylene glycol extract of extraction example 6 0.30
Instead of weight%, the 1,3-butylene glyco of Extraction Example 6
Use 0.003% by weight of freeze-dried powder
Was processed in the same manner as in Example 19 to produce a hair tonic.
Was. After using this hair tonic for three months,
It became shiny, supple and elastic hair. [0050]Example 21 Bar Soap 3 g of leaves and branches of dried white crane reishi in ethanol for 120 minutes
Immersed for a while, and the obtained liquid was made up to 500 ml to extract the extract.
Obtained. Instead of using 20% by weight of the extract of Extraction Example 1,
Same as Example 1 except for using 20% by weight of the obtained extract
To produce a solid soap. Use this soap for 3 months
Continued use improved skin roughness and moisturized
I was able to keep moist skin. [0051]Example 22 Bar Soap 500 ml of the acetone extract obtained by the method of extraction example 6
Evaporator [N-N type manufactured by Tokyo Rika Co., Ltd., the same applies hereinafter]
The solvent is distilled off using, and the volume is extracted in 500 ml of distilled water.
An aqueous solution was obtained. Example of using 20% by weight of the extract of Extraction Example 1
Instead of using 20% by weight of this aqueous extraction solution,
In the same manner as in Example 1, a solid soap was produced. This soap
After using it for 3 months, the rough skin has been improved,
I was able to keep my skin moist and moist. [0052]Example 23 Bar Soap 500 ml of the aqueous extraction solution obtained by the method of Example 22 was frozen.
Drying to obtain a fine powder. Extract freeze-dried powder of extraction example 1
Instead of using 0.1% by weight of the powder
Example 2 except that 0.1% by weight of the freeze-dried powder was used.
Thus, a solid soap was produced. This soap for 3 months
As you continue to use, the rough skin is improved and moist
I was able to keep moist skin. [0053]Example 24 Lotion Hakutsuru Ganoderma Whole Grass 2g, Ganoderma 0.2g and Dokudami 0.3
g of the dry mixture in ethanol and hold for 60 minutes
After filtration, the obtained liquid is made up to 500 ml and extracted.
I got Instead of using 10% by weight of the extract of Extraction Example 3
10% by weight of the extract thus obtained is used
Except for this, a lotion was produced in the same manner as in Example 5.
After using this lotion for 3 months,
Can improve and keep your skin moist and moist
did it. [0054]Example 25 Lotion The extract obtained in Example 24 was freeze-dried to obtain a fine powder.
Was. Using 0.1% by weight of the freeze-dried powder of the extract of Extraction Example 3
Instead of the lyophilized powder obtained in this way, the lyophilized powder is used.
Except for using 1% by weight, the same treatment as in Example 6
Was manufactured. Use this lotion for 3 months
The glowing improves skin roughness and moisturizes
I was able to keep some skin. [0055]Example 26 Bar Soap 3g of leaves and branches of dried white crane Reishi
Immerse in coal for 120 minutes, make the resulting solution 500 ml
The volume was adjusted to obtain an extract. 20% by weight of the extract of Extraction Example 1
Instead of using 20% by weight of the obtained extract,
Was treated in the same manner as in Example 1 to produce a solid soap. this
After using the soap for 3 months, the rough skin improved
As a result, it was possible to keep the skin moist and moist. [0056]Example 27 Bar soap 500 ml of the ether extract obtained by the method of extraction example 6
The solvent is distilled off using an evaporator, and distilled water is added to 500 ml.
The aqueous solution was extracted to constant volume. 20 weight of extract from Extraction Example 1
% Instead of using 20% by weight of the aqueous extraction solution
Was treated in the same manner as in Example 1 to produce a solid soap. this
After using the soap for 3 months, the rough skin improved
As a result, it was possible to keep the skin moist and moist. [0057]Example 28 Bar soap 500 ml of the aqueous extraction solution obtained by the method of Example 27 was frozen.
Drying to obtain a fine powder. Extract freeze-dried powder of extraction example 1
Instead of using 0.1% by weight of the powder,
Example 2 except that 0.1% by weight of the freeze-dried powder was used.
The same treatment was performed to produce a solid soap. 3 months of this soap
After using it for a while, it improves skin roughness and moisturizes
I was able to keep the hydrated skin. [0058]Example 29 Lotion Hakutsuru Ganoderma whole grass 2g, Ganoderma 0.5g and Dokudami 0.5
g of the mixture in 1,3-butylene glycol,
After holding for 0 minutes, the mixture was filtered, and the obtained filtrate was made up to 500 ml.
The volume was adjusted to obtain an extract. 10% by weight of the extract of Extraction Example 3
Instead of using 10 times the extract thus obtained
Except that the amount% is used, the treatment is performed in the same manner as in Example 5 and the lotion is used.
Was manufactured. I have been using this lotion for 3 months
Roller, rough skin improved, moist and moisturized skin
Was able to keep. [0059]Example 30 Lotion The extract obtained in Example 29 is freeze-dried to obtain a fine powder.
Was. Using 0.1% by weight of the freeze-dried powder of the extract of Extraction Example 3
Instead of the lyophilized powder obtained in this way, the lyophilized powder is used.
Except for using 1% by weight, the same treatment as in Example 6
Was manufactured. Use this lotion for 3 months
The glowing improves skin roughness and moisturizes
I was able to keep some skin. [0060]Example 31 Bar soap 3 g of leaves and branches of dried white crane ganoderma ethanol: water = 1:
1 was immersed in the mixture for 60 minutes,
To obtain an extract. 20% by weight of the extract of Extraction Example 1
Instead of using the extract, the thus obtained extract 20
The same procedure as in Example 1 was carried out except that the weight% was used.
Was manufactured. After using this soap for three months,
Improves rough skin and keeps skin moist and moist
I was able to. [0061]Example 32 Bar soap 500 ml of the benzene extract obtained by the method of extraction example 6
The solvent is distilled off with an evaporator, and the volume is made up to 500 ml with distilled water.
Thus, an aqueous extraction solution was obtained. 20% by weight of the extract of Extraction Example 1
Instead of using it, the aqueous extraction solution 2 thus obtained
Except for using 0% by weight, the solid stone was treated in the same manner as in Example 1.
A soap was produced. After using this soap for three months
To improve moist and moist skin
I was able to keep. [0062]Example 33 Bar soap Ethanol: 1,3-butylene with 3g of dried whole white crane Reishi
It was immersed in a 3: 1 mixture of glycols for 60 minutes and obtained.
After cooling the solution, the volume was adjusted to 500 ml to obtain an extract. Extraction
Instead of using 20 weights of the extract of Example 1,
Same as Example 1 except for using 20 weight of the extract obtained
To produce a solid soap. Use this soap for 3 months
Continued use improved skin roughness and moisturized
I was able to keep moist skin. [0063]Example 34 Bar soap Hakutsuru Reishi 3 g whole grass, Reishi 0.15 g and Dokudami 0.
15 g of the dry mixture was mixed with ethanol: water = 1: 1
Immersed in water for 60 minutes and filtered.
The volume was adjusted to 1 to obtain an extract. 20 weight of extract from Extraction Example 1
Instead of using the extract, the thus obtained extract 20
Except for using the weight, the same treatment as in Example 1 was carried out to obtain a solid soap.
Manufactured. After using this soap for 3 months,
Improves roughness and keeps skin moist and moist
I was able to. [0064] The cosmetic of the present invention has an active oxygen scavenging ability.
Hakutsuru Reishi or a mixture of Hakutsuru Reishi and Reishi and Dokudami
Containing a solvent extract of the product.
Can prevent skin aging and hair fatigue
it can.

Continued on the front page (51) Int.Cl. ⁷ Identification code FI C11D 3/382 C11D 3/382 9/38 9/38

Claims (1)

(57) [Claim 1] A cosmetic composition for preventing skin aging or hair fatigue, comprising a water and / or organic solvent extract of Hakutsuru Reishi.