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JP3557712B2 - Method and apparatus for detecting defect position of hollow fiber membrane module - Google Patents
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JP3557712B2 - Method and apparatus for detecting defect position of hollow fiber membrane module - Google Patents

Method and apparatus for detecting defect position of hollow fiber membrane module Download PDF

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JP3557712B2
JP3557712B2 JP09182195A JP9182195A JP3557712B2 JP 3557712 B2 JP3557712 B2 JP 3557712B2 JP 09182195 A JP09182195 A JP 09182195A JP 9182195 A JP9182195 A JP 9182195A JP 3557712 B2 JP3557712 B2 JP 3557712B2
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Prior art keywords
hollow fiber
fiber membrane
face
membrane module
case
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JPH08257375A (en
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信男 金山
茂 出茂
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Nok Corp
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Nok Corp
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • G01N21/88Investigating the presence of flaws or contamination
    • G01N21/95Investigating the presence of flaws or contamination characterised by the material or shape of the object to be examined
    • G01N21/956Inspecting patterns on the surface of objects
    • G01N21/95692Patterns showing hole parts, e.g. honeycomb filtering structures

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
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  • Pathology (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Description

【0001】
【産業上の利用分野】
本発明は、中空糸膜の束をケース内に装填し、ケース端部において封止した後に、中空糸膜モジュールの欠陥部(封止不良、中空糸膜の破損等)の封止部端面における位置を検出する方法とその装置に関する。
【0002】
【従来の技術】
中空糸膜の束をケース内に装填し、ケース端部において封止した後で、中空糸膜モジュールの欠陥部の封止部端面における位置を検出する方法として、出願人が先に発明を行い特願平4ー316480号で発表したものがある。
【0003】
この特願平4ー316480号の中空糸膜モジュールの欠陥位置検出方法は図3に示すものであって、その概略を以下に説明する。
【0004】
101が中空糸膜モジュールであって、多数本の中空糸膜102を束ねてU字状として、その中空糸膜束103を両端を開口するケース104内に挿入し、ケース104の一方の開口端部にて各中空糸膜102間の透き間及び中空糸膜102とケース104間の透き間を封止材105で封止固定し、その封止固定された各中空糸膜102の端末と硬化した封止材105とを共に切断し、各中空糸膜102の端末を開口して、封止部端面としての中空糸膜開口端面106を形成して成り、ケース104内部の各種気体や液体を、中空糸膜102を通過させてろ過し、中空糸膜開口端面106から流出させるものである。
【0005】
欠陥位置検出装置110は、上向きになっている中空糸膜開口端面106の面方向にレーザビーム111を横から走査させるための光学部112と、中空糸膜開口端面106上に設けられてレーザビーム111により発生する散乱光113を見やすくし又空気吸引する穴114を有する暗室115と、暗室115の上部に設けられ散乱光113を検出するためのCCDカメラ116と、散乱光113の位置から欠陥位置を求める位置解析パソコン117とから成る。
【0006】
封止後の中空糸膜モジュールの欠陥検出方法は、先ず暗室115内を負圧にすることにより、中空糸膜開口端面106より上に向かって流れる空気の気流を作る。中空糸膜102に封止不良や中空糸膜の破損等の欠陥があれば、空気内にある塵などの微粒子が中空糸膜102にろ過されずに破損個所等を通過してそのまま空気流に含まれて流出してくる。そこに横からレーザビーム111を当てると、レーザビーム111が塵などの微粒子に当たった時に散乱して、CCDカメラ116で確認することができるから、欠陥の存在を知ることができるし、散乱光の位置から欠陥のある中空糸膜の位置(封止部端面における開口した位置)を知ることができる。
【0007】
また、欠陥のあることが分かった中空糸膜の開口端面に封止材を滴下することにより、欠陥のある中空糸膜をその端面でふさいで、中空糸膜モジュールの欠陥を修復する。
【0008】
【発明が解決しようとする課題】
この方法では、図4に示すように、欠陥を有する中空糸膜102aがケース104の端部で斜めに傾いて封止固定されている場合、その欠陥を有する中空糸膜102aから流出する空気流130aもまた、中空糸膜102aに沿って斜めに傾いたものとなる。また、レーザビーム111は中空糸膜開口端面106から所定の距離だけ離れて通過する。このために、レーザビーム111と傾いて流れる空気流の中の微粒子とが衝突して散乱光を出す位置131をCCDカメラで見た場合、中空糸膜開口端面106上では位置102cにあるように見えて、欠陥を有する中空糸膜102aの開口端面における位置102bとずれてしまう。
【0009】
このことは、欠陥のある中空糸膜があるということは確認することができるが、欠陥のある中空糸膜の開口端面における位置を特定する場合に、誤差を生じてしまうと言うことである。これでは、封止材を滴下することによる欠陥の修復を高精度に行うことができない。
【0010】
本発明は上記従来技術の問題を解決するためになされたもので、その目的とするところは、特願平4ー316480号で発表した中空糸膜モジュールの欠陥検出方法を改良し、中空糸膜の開口端面における欠陥位置の検出精度を向上させることである。
【0011】
【課題を解決するための手段】
上記目的を達成するために本発明にあっては、中空糸膜の束をケース内に装填し、ケース端部において中空糸膜の束の端末を開口した状態で封止した封止部を形成し、この封止部でケース内部と外部とを隔離した中空糸膜モジュールに関して、前記ケースの内部から外部に向けて各中空糸膜を通り封止部端面から流れる気流を形成し、この気流の中の中空糸膜の欠陥部を通り抜けた塵等の微粒子を光学的に検出することによって、封止部端面における中空糸膜モジュールの欠陥部の位置を検出する方法において、前記封止部端面の外側に近接させて整流子を設け、前記気流についてその整流子を通らせた後に光学的な検出を行うことを特徴とする。
【0012】
中空糸膜の束をケース内に装填し、ケース端部において中空糸膜の束の端末を開口した状態で封止した封止部を形成し、この封止部でケース内部と外部とを隔離した中空糸膜モジュールに関して、前記ケースの内部から外部に向けて各中空糸膜を通り封止部端面から流れる気流を形成し、この気流の中の中空糸膜の欠陥部を通り抜けた塵等の微粒子を光学的に検出する検出手段により、封止部端面における中空糸膜モジュールの欠陥部の位置を検出する装置において、多数の整流管を集合させた整流子を前記封止部端面の外側に近接させて設けたことを特徴とする。
【0013】
また、前記整流管は少なくとも3つの壁により形成されていることが好適である。
【0014】
【作用】
上記のように構成された本発明においては、中空糸膜モジュールの封止部端面の外側に近接させて整流子を設けることにより、封止部端面即ち中空糸膜開口端面から流出した後に、傾いた中空糸膜に沿ってそのまま傾いて流れようとする気流を、整流子を通過させて封止部端面に垂直な方向、即ち検出手段の構成要素としてのCCDカメラの方向へ矯正するので、散乱光の発生位置と欠陥のある中空糸膜の封止部端面位置とをずれなく重ね合わせて確認することができる。
【0015】
また、整流子は多数の整流管を集合させたものであることから、封止部端面から流出する気流が整流管を通ることで拡散させることなく安定した状態で流出させることができる。
【0016】
さらに、整流管を少なくとも3つの壁により形成するものとし、その整流管を形成する各壁間のピッチを小さくすることで、各整流管を極めて小さいものに製作できるので、散乱光の発生位置の特定を高精度に行える。
【0017】
さらにまた、中空糸膜の封止部端面上に整流子を設置すると、非検出部即ち封止部端面を暗くし、発生する散乱光とのコントラストをはっきりさせ、CCDカメラによる検出の信頼性を向上させる。
【0018】
【実施例】
以下に本発明による中空糸膜モジュールの欠陥位置検出方法及びその装置を図示の実施例に基づいて説明する。
【0019】
図1において1は中空糸膜モジュールであって、図示省略したが多数本の中空糸膜を束ねてU字状として、その中空糸膜束を両端を開口するケース4内に挿入し、ケース4の一方の開口端部にて各中空糸膜間の透き間及び中空糸膜とケース4間の透き間を封止材で封止固定し、その封止固定された各中空糸膜の端末と硬化した封止材とを共に切断し、各中空糸膜の端末を開口して、封止部端面としての中空糸膜開口端面6を形成して成り、ケース4内部の各種気体や液体を、中空糸膜を通過させてろ過し、中空糸膜開口端面6から流出させるものである。
【0020】
前述の中空糸膜モジュール1を欠陥検出のために、この実施例では開口端面6側を欠陥位置検出手段10と対向するように配置させている。2aは多数本の中空糸膜の中の1本であって、これが欠陥を有する中空糸膜とする。
【0021】
40が本発明の要部となる整流子であって、中空糸膜モジュール1の開口端面6のすぐ上に設けられて、それぞれの中空糸膜の開口端面から流出してくる気流の向きを真っ直ぐ上に向けて揃える働きをするものである。
【0022】
整流子40は、複数の整流管41を集合させたという上位概念から得られるもので、様々の具体的な実施例が展開されるが、個々の整流管41の直径は、次に示す値が望ましい。即ち、径が大きく過ぎると、欠陥の無い中空糸膜まで欠陥補修のための封止材が滴下される場合があり、これにより中空糸膜モジュール1の通水量に影響を及ぼすことになるので、実際上最大でも5mm以下、好ましくは1mmであることが望ましい。
【0023】
また、管の長さは、気流の流れを矯正するためには、実際上最小で直径の3倍以上、好ましくは5倍以上であることが望ましい。
【0024】
整流子40の平面上の大きさは最小でも検出する中空糸膜モジュール1の被検出部の大きさ(中空糸膜の束を封止材で埋設している面の大きさ)と同じでなければならないが、実際は、中空糸膜モジュール1の開口端面6から整流子40を通過してくる気流がその外周部において整然と整った流れ状態を実現するためには、整流子40の外周部は中空糸膜モジュール1の被検出部の外周部よりも半径方向に(外側方向に)10mm程度大きいことが望ましい。
【0025】
次に、欠陥の位置を検出する検出手段10は、図示省略したが(従来例の図3と同様の構成)、横から整流子40の上面の方向にその上面から少し離してレーザビーム11を走査させるための光学部と、中空糸膜モジュール1、整流子40の上部に設けられ散乱光13を検出するためのCCDカメラ16と、散乱光13の位置から中空糸膜モジュール1の開口端面6上の欠陥位置を求める位置解析パソコン17とから成るものである。
【0026】
また、このほかに、ケース4の内側から中空糸膜を通って図1において上方に向かって流れる気流を起こす装置が必要であり、そのためには、整流子40の上に暗室を設け上部において空気を吸引する方法や、ケース4に圧力を加えて空気を押し出す方法を採用することも可能である。
【0027】
封止後の中空糸膜モジュールの欠陥検出方法は、先ず上記の吸入または押出により、中空糸膜開口端面6より整流子40を通過し上方に向かって流れる空気流を作る。例えば欠陥中空糸膜2aのように中空糸膜に封止不良や中空糸膜の破損等の欠陥があれば、空気内にある塵などの微粒子が中空糸膜にろ過されずにそのまま空気流に含まれて流出してくる。
【0028】
そこに横からレーザビーム11を当てると、レーザビーム11が塵などの微粒子に当たった時に散乱して、CCDカメラ16で確認することができるから、欠陥の存在を知ることができる。
【0029】
さらに、図1のように、欠陥のある中空糸膜2Aが封止部で傾いて封止固定されていて、その中空糸膜2Aの開口端から傾いて空気を送り出しても、すぐ上にある整流子40が真っ直ぐ上下方向を向いている整流管41により空気流を上方向に矯正してくれるから、空気流は真っ直ぐ上に立ち上がり、拡散を減少することができる。
【0030】
そして、濾過を免れてその空気流の中に含まれる塵等の微粒子とレーザビーム11とが衝突することにより生じる散乱光13の発生位置14と、その塵等を含んだ気流が飛び出した中空糸膜の端部の位置15とは、上部のCCDカメラで見た場合には精度よく一致することになる。
【0031】
その位置をパソコン17で解析し、記憶して、後でその位置に封止材を滴下することにより、破損した中空糸膜の端部をふさぎ、中空糸膜モジュールの欠陥補修を行うことができる。
【0032】
また、二次的な効果として、散乱光13が整流子40に照射されても、各整流管の内部に反射吸収されてしまうのでCCDカメラ16に反射する反射光がなくなり、散乱光13の発生位置とその他の部分との間が高いコントラストとなり、画像処理的にも高い精度とすることができる。
【0033】
図2は整流子40を図1のS1−S1面から見た図である。図2(a)の整流子40aのものは、波板51を平板52に貼設した整流板53を複数枚重ねたもので、気流を通過させる各整流管の形状は3つの壁から形成される山形をしており、また図2(b)の整流子40bは各整流管54の形状は6つの壁から形成されるハニカム状を成している。
【0034】
これら、山形,ハニカム状の整流管を形成する各壁間のピッチを小さくすることで、各整流管を極めて小さいものに製作できるので、散乱光の発生位置の特定を高精度に行える。
【0035】
尚、整流管を丸や四角等のパイプとし、そのパイプを複数透き間無く束ねた整流子としても良い。この場合、多少、各パイプの壁の厚みで散乱光の発生位置を特定する精度が悪くなる可能性があるが、壁を薄くすることで、精度を高めることができる。
【0036】
さらに、具体的な実施例として、整流子の材料はアルミ薄板で、ピッチ(各整流管の直径)は1mm,厚さ(1つ1つの管の長さ)は10mm,アルミ薄板の壁の厚さは加工能力の制約から0. 2 mmのものを使用したが、実施例の寸法や形状に限定されるものではない。
【0037】
【発明の効果】
本発明によれば、ケースの内部から外部に向けて各中空糸膜を通って流れる気流を形成し、その気流の中に中空糸膜の欠陥部を通って来た塵等の微粒子を光学的に検出することによって、封止部端面外側から中空糸膜モジュールの欠陥部を検出する方法において、封止部端面の外側に近接して整流子を設け、前記気流についてその整流子を通らせた後に光学的な検出を行うようにしたので欠陥の存在する中空糸膜の封止部端面における欠陥位置の検出を精度よく行うことができるようになった。
【0038】
そして、中空糸膜モジュールの欠陥部を検出する装置においては、検出手段により検出された位置と欠陥中空糸膜の封止部端面の位置とのズレがない。
【0039】
また、整流子は多数の整流管を集合させたものであるので、封止部端面から流出する気流が整流管を通ることで拡散させることなく安定した状態で流出させることができる。
【0040】
さらに、整流管を少なくとも3つの壁により形成するものとし、その整流管を形成する各壁間のピッチを小さくすることで、各整流管を極めて小さいものに製作できるので、散乱光の発生位置の特定を高精度に行うことができる。
【0041】
さらにまた、中空糸膜の封止部端面上に整流子を設置すると、非検出部即ち封止部端面を暗くし、発生する散乱光とのコントラストをはっきりさせ、CCDカメラによる検出の信頼性を向上させることができる。
【図面の簡単な説明】
【図1】図1は本発明の実施例であって、中空糸膜モジュールの欠陥検出方法の概略説明図である。
【図2】図2は、整流子を流体通過方向からみた図。
【図3】図3は従来の中空糸膜モジュールの欠陥検出方法の構成説明図。
【図4】図4は従来の中空糸膜モジュールの欠陥検出方法の欠陥位置検出に誤差が生じることを説明する説明図。
【符号の説明】
1 中空糸膜モジュール
2a 欠陥のある中空糸膜
4 ケース
6 封止部端面(中空糸膜開口端面)
11 レーザビーム
13 錯乱光
40,40a,40b 整流子
51 波板
52 平板
[0001]
[Industrial applications]
According to the present invention, after a bundle of hollow fiber membranes is loaded in a case and sealed at an end of the case, a defective portion of the hollow fiber membrane module (poor sealing, breakage of the hollow fiber membrane, etc.) at the sealing portion end face. The present invention relates to a method and an apparatus for detecting a position.
[0002]
[Prior art]
After loading the bundle of hollow fiber membranes into the case and sealing the case at the end, the applicant first made the invention as a method of detecting the position of the defective portion of the hollow fiber membrane module at the end face of the sealing portion. There is one announced in Japanese Patent Application No. 4-316480.
[0003]
The method of detecting a defect position of a hollow fiber membrane module disclosed in Japanese Patent Application No. 4-316480 is shown in FIG. 3, and its outline will be described below.
[0004]
Reference numeral 101 denotes a hollow fiber membrane module, in which a large number of hollow fiber membranes 102 are bundled into a U shape, and the hollow fiber membrane bundle 103 is inserted into a case 104 having both ends opened. The gap between the hollow fiber membranes 102 and the gap between the hollow fiber membranes 102 and the case 104 are sealed and fixed with the sealing material 105 at the portions, and the ends of the sealed and fixed hollow fiber membranes 102 and the hardened seals. The end member of each hollow fiber membrane 102 is opened by cutting the stopper material 105 together, and a hollow fiber membrane opening end face 106 as a sealing end face is formed. Filtration is performed by passing through the fiber membrane 102 and flowing out from the opening end face 106 of the hollow fiber membrane opening.
[0005]
The defect position detection device 110 includes an optical unit 112 for scanning the laser beam 111 from the side in the plane direction of the hollow fiber membrane opening end face 106 facing upward, and a laser beam provided on the hollow fiber membrane opening end face 106. A dark room 115 having holes 114 for facilitating viewing of the scattered light 113 generated by the air 111 and sucking air; a CCD camera 116 provided above the dark room 115 for detecting the scattered light 113; And a position analysis personal computer 117 for obtaining
[0006]
In the method for detecting a defect of the hollow fiber membrane module after sealing, first, a negative pressure is applied to the inside of the dark chamber 115 to create an airflow of air flowing upward from the hollow fiber membrane opening end face 106. If the hollow fiber membrane 102 has a defect such as poor sealing or breakage of the hollow fiber membrane, fine particles such as dust in the air pass through the broken point or the like without being filtered by the hollow fiber membrane 102 and are directly converted into an air flow. Includes and leaks. When the laser beam 111 is applied from the side, the laser beam 111 is scattered when it hits fine particles such as dust, and can be confirmed by the CCD camera 116. The position of the defective hollow fiber membrane (the open position on the end face of the sealing portion) can be known from the position.
[0007]
In addition, a sealing material is dropped on the opening end face of the hollow fiber membrane that has been found to have a defect, thereby covering the defective hollow fiber membrane with the end face, thereby repairing the defect of the hollow fiber membrane module.
[0008]
[Problems to be solved by the invention]
In this method, as shown in FIG. 4, when the hollow fiber membrane 102a having a defect is sealed and fixed at an end of the case 104 at an angle, the air flow flowing out of the hollow fiber membrane 102a having the defect 130a is also inclined obliquely along the hollow fiber membrane 102a. Further, the laser beam 111 passes away from the hollow fiber membrane opening end face 106 by a predetermined distance. For this reason, when the position 131 where the laser beam 111 collides with the fine particles in the airflow that flows obliquely and emits scattered light is viewed with a CCD camera, as shown in the position 102 c on the hollow fiber membrane opening end surface 106. It looks and shifts from the position 102b on the opening end face of the hollow fiber membrane 102a having the defect.
[0009]
This means that it is possible to confirm that there is a defective hollow fiber membrane, but that an error occurs when specifying the position of the defective hollow fiber membrane on the open end face. In this case, the defect cannot be repaired with high accuracy by dropping the sealing material.
[0010]
SUMMARY OF THE INVENTION The present invention has been made to solve the above-mentioned problems of the prior art. It is an object of the present invention to improve the method of detecting a defect in a hollow fiber membrane module disclosed in Japanese Patent Application No. 4-316480. Is to improve the accuracy of detecting a defect position on the end face of the opening.
[0011]
[Means for Solving the Problems]
In order to achieve the above object, according to the present invention, a bundle of hollow fiber membranes is loaded into a case, and a sealed portion is formed in a state where the ends of the bundle of hollow fiber membranes are opened at the ends of the case. Then, with respect to the hollow fiber membrane module in which the inside and the outside of the case are separated by the sealing portion, an airflow flowing from the end surface of the sealing portion through each hollow fiber membrane from the inside of the case to the outside is formed, and A method for detecting the position of a defective portion of a hollow fiber membrane module on an end face of a sealing portion by optically detecting fine particles such as dust passing through a defective portion of a hollow fiber membrane therein, wherein: A commutator is provided close to the outside, and optical detection is performed after the airflow passes through the commutator.
[0012]
A bundle of hollow fiber membranes is loaded into a case, and a sealed portion is formed at the end of the case with the ends of the bundles of hollow fiber membranes opened, and the inside and outside of the case are separated by the sealed portion. With respect to the hollow fiber membrane module thus formed, an airflow flowing from the inside of the case to the outside through each hollow fiber membrane and from the end face of the sealing portion is formed, and dust or the like passing through a defective portion of the hollow fiber membrane in the airflow is formed. In a device for detecting the position of a defective portion of a hollow fiber membrane module on an end face of a sealing portion by a detecting means for optically detecting fine particles, a commutator in which a large number of flow straightening tubes are assembled is provided outside the end face of the sealing portion. It is characterized by being provided close to.
[0013]
Further, it is preferable that the straightening tube is formed by at least three walls.
[0014]
[Action]
In the present invention configured as described above, the commutator is provided close to the outside of the end face of the sealing portion of the hollow fiber membrane module. The airflow which is inclined and flows along the hollow fiber membrane as it is is corrected by passing through a commutator in a direction perpendicular to the end face of the sealing portion, that is, in the direction of the CCD camera as a component of the detection means, so that scattering is performed. The position where light is generated and the position of the end face of the sealing portion of the defective hollow fiber membrane can be overlapped and checked without any deviation.
[0015]
Further, since the commutator is formed by assembling a large number of flow straightening tubes, the airflow flowing out of the end face of the sealing portion can flow out in a stable state without being diffused by passing through the flow straightening tubes.
[0016]
Furthermore, since the rectifying tube is formed by at least three walls, and the pitch between the walls forming the rectifying tube is reduced, each rectifying tube can be manufactured to be extremely small. Identification can be performed with high accuracy.
[0017]
Furthermore, when a commutator is installed on the end face of the sealing portion of the hollow fiber membrane, the non-detection portion, that is, the end face of the sealing portion is darkened, the contrast with the generated scattered light is made clear, and the reliability of detection by the CCD camera is improved. Improve.
[0018]
【Example】
Hereinafter, a method and an apparatus for detecting a defect position of a hollow fiber membrane module according to the present invention will be described based on the illustrated embodiment.
[0019]
In FIG. 1, reference numeral 1 denotes a hollow fiber membrane module. Although not shown, a number of hollow fiber membranes are bundled into a U-shape, and the hollow fiber membrane bundle is inserted into a case 4 having both ends opened. The gap between the hollow fiber membranes and the gap between the hollow fiber membrane and the case 4 were sealed and fixed with a sealing material at one open end, and the ends of the sealed and fixed hollow fiber membranes were cured. The sealing material is cut together, the ends of the hollow fiber membranes are opened, and a hollow fiber membrane opening end face 6 is formed as an end face of the sealing portion. Filtration is performed by passing through the membrane and flowing out from the opening end face 6 of the hollow fiber membrane.
[0020]
In this embodiment, the above-mentioned hollow fiber membrane module 1 is disposed so that the opening end face 6 side faces the defect position detecting means 10 for defect detection. 2a is one of many hollow fiber membranes, which is a hollow fiber membrane having a defect.
[0021]
Reference numeral 40 denotes a commutator which is a main part of the present invention, which is provided immediately above the open end face 6 of the hollow fiber membrane module 1 and straightens the direction of the airflow flowing out from the open end face of each hollow fiber membrane. It serves to align upwards.
[0022]
The commutator 40 is obtained from the general concept that a plurality of rectifier tubes 41 are assembled, and various specific embodiments are developed. The diameter of each rectifier tube 41 has the following value. desirable. That is, if the diameter is too large, the sealing material for repairing the defect may be dripped to the hollow fiber membrane having no defect, thereby affecting the water flow rate of the hollow fiber membrane module 1. In practice, it is desirable that the maximum is 5 mm or less, preferably 1 mm.
[0023]
Further, in order to correct the flow of the airflow, the length of the tube is practically minimum and is desirably at least three times the diameter, preferably at least five times the diameter.
[0024]
The size of the commutator 40 on the plane must be at least the same as the size of the portion to be detected of the hollow fiber membrane module 1 to be detected (the size of the surface in which the bundle of hollow fiber membranes is embedded with the sealing material). In practice, however, in order for the airflow passing through the commutator 40 from the opening end face 6 of the hollow fiber membrane module 1 to achieve a neat flow state at the outer periphery thereof, the outer periphery of the commutator 40 is hollow. It is desirable that the outer diameter of the detection target portion of the thread membrane module 1 be larger by about 10 mm in the radial direction (outward).
[0025]
Next, the detection means 10 for detecting the position of the defect, which is not shown (same configuration as in FIG. 3 of the conventional example), slightly separates the laser beam 11 from the side in the direction of the upper surface of the commutator 40 from the side. An optical unit for scanning, a hollow fiber membrane module 1, a CCD camera 16 provided above the commutator 40 for detecting the scattered light 13, and an opening end face 6 of the hollow fiber membrane module 1 from the position of the scattered light 13. And a position analysis personal computer 17 for determining the position of the defect above.
[0026]
In addition, it is necessary to provide a device for generating an airflow that flows upward in FIG. 1 from the inside of the case 4 through the hollow fiber membrane, and for this purpose, a dark room is provided on the commutator 40 and air is provided in the upper part. , Or a method of applying pressure to the case 4 to push out air.
[0027]
In the method of detecting a defect of the hollow fiber membrane module after sealing, first, an air flow that flows upward through the commutator 40 from the hollow fiber membrane opening end face 6 is created by the above-described suction or extrusion. For example, if the hollow fiber membrane has a defect such as defective sealing or breakage of the hollow fiber membrane as in the case of the defective hollow fiber membrane 2a, fine particles such as dust in the air are not filtered by the hollow fiber membrane and are directly passed through the air flow. Includes and leaks.
[0028]
When the laser beam 11 is applied from the side, the laser beam 11 is scattered when hitting fine particles such as dust, and can be confirmed by the CCD camera 16, so that the presence of a defect can be known.
[0029]
Furthermore, as shown in FIG. 1, the defective hollow fiber membrane 2A is sealed and fixed at the sealing portion while being inclined, and even if air is sent out from the opening end of the hollow fiber membrane 2A, it is immediately above. Since the commutator 40 straightens the air flow upward by the straightening tube 41 which faces straight up and down, the air flow rises straight up and the diffusion can be reduced.
[0030]
Then, a generation position 14 of the scattered light 13 generated by the collision of the laser beam 11 with fine particles such as dust contained in the air flow, which escapes from the filtration, and the hollow fiber from which the air flow containing the dust etc. has flown out. The position 15 at the end of the film is accurately coincident with the position when viewed with the upper CCD camera.
[0031]
The position is analyzed and stored by the personal computer 17, and the end of the damaged hollow fiber membrane can be closed by dropping the sealing material at the position later to repair the defect of the hollow fiber membrane module. .
[0032]
As a secondary effect, even if the scattered light 13 is irradiated on the commutator 40, the reflected light is reflected and absorbed inside each rectifier tube, so that there is no reflected light reflected on the CCD camera 16 and the generation of the scattered light 13 is generated. High contrast is obtained between the position and other parts, and high accuracy can be achieved also in image processing.
[0033]
FIG. 2 is a view of the commutator 40 viewed from the S1-S1 plane in FIG. The commutator 40a shown in FIG. 2A is obtained by stacking a plurality of rectifying plates 53 in which a corrugated plate 51 is attached to a flat plate 52, and the shape of each rectifying tube through which an air flow passes is formed by three walls. In the commutator 40b shown in FIG. 2B, the shape of each flow straightening tube 54 has a honeycomb shape formed by six walls.
[0034]
By reducing the pitch between the walls forming the mountain-shaped or honeycomb-shaped rectifying tubes, each rectifying tube can be made extremely small, so that the position where scattered light is generated can be specified with high accuracy.
[0035]
The rectifying tube may be a round or square pipe or the like, and a plurality of such pipes may be bundled without any transparency. In this case, the accuracy of specifying the position where the scattered light is generated may be slightly deteriorated by the thickness of the wall of each pipe, but the accuracy can be improved by making the wall thinner.
[0036]
Further, as a specific example, the material of the commutator is a thin aluminum plate, the pitch (diameter of each straightening tube) is 1 mm, the thickness (length of each tube) is 10 mm, and the thickness of the thin aluminum plate wall is The height is 0. Although a 2 mm one was used, it is not limited to the dimensions and shape of the embodiment.
[0037]
【The invention's effect】
According to the present invention, an airflow that flows from the inside of the case to the outside through each hollow fiber membrane is formed, and fine particles such as dust that have passed through a defective portion of the hollow fiber membrane are optically formed in the airflow. In the method of detecting a defective portion of the hollow fiber membrane module from the outside of the sealing portion end face, a commutator is provided close to the outside of the sealing portion end face, and the commutator is passed through the airflow. Since the optical detection is performed later, it is possible to accurately detect the defect position on the end face of the sealing portion of the hollow fiber membrane having the defect.
[0038]
In the device for detecting a defective portion of the hollow fiber membrane module, there is no deviation between the position detected by the detecting means and the position of the end face of the sealing portion of the defective hollow fiber membrane.
[0039]
Further, since the commutator is formed by assembling a large number of flow straightening tubes, the airflow flowing out from the end face of the sealing portion can flow out in a stable state without being diffused by passing through the flow straightening tubes.
[0040]
Furthermore, since the rectifying tube is formed by at least three walls, and the pitch between the walls forming the rectifying tube is reduced, each rectifying tube can be manufactured to be extremely small. Identification can be performed with high accuracy.
[0041]
Furthermore, when a commutator is installed on the end face of the sealing portion of the hollow fiber membrane, the non-detection portion, that is, the end face of the sealing portion is darkened, the contrast with the generated scattered light is made clear, and the reliability of detection by the CCD camera is improved. Can be improved.
[Brief description of the drawings]
FIG. 1 is a schematic explanatory view of a method for detecting a defect of a hollow fiber membrane module according to an embodiment of the present invention.
FIG. 2 is a diagram of a commutator viewed from a fluid passage direction.
FIG. 3 is an explanatory view of a configuration of a conventional method for detecting a defect of a hollow fiber membrane module.
FIG. 4 is an explanatory view for explaining that an error occurs in defect position detection in a conventional method for detecting a defect in a hollow fiber membrane module.
[Explanation of symbols]
DESCRIPTION OF SYMBOLS 1 Hollow fiber membrane module 2a Defective hollow fiber membrane 4 Case 6 Sealing part end face (hollow fiber membrane opening end face)
11 laser beam 13 confusion light 40, 40a, 40b commutator 51 corrugated plate 52 flat plate

Claims (3)

中空糸膜の束をケース内に装填し、ケース端部において中空糸膜の束の端末を開口した状態で封止した封止部を形成し、この封止部でケース内部と外部とを隔離した中空糸膜モジュールに関して、前記ケースの内部から外部に向けて各中空糸膜を通り封止部端面から流れる気流を形成し、この気流の中の中空糸膜の欠陥部を通り抜けた塵等の微粒子を光学的に検出することによって、封止部端面における中空糸膜モジュールの欠陥部の位置を検出する方法において、
真っ直ぐな複数の整流管を集合させた整流子を前記封止部端面の外側に近接させて設け、前記気流についてその整流子を通らせた後に光学的な検出を行うことを特徴とする中空糸膜モジュールの欠陥位置検出方法。
A bundle of hollow fiber membranes is loaded into a case, and a sealed portion is formed at the end of the case with the ends of the bundles of hollow fiber membranes opened, and the inside and outside of the case are separated by the sealed portion. With respect to the hollow fiber membrane module thus formed, an airflow flowing from the inside of the case to the outside through each hollow fiber membrane and from the end face of the sealing portion is formed, and dust or the like passing through a defective portion of the hollow fiber membrane in the airflow is formed. In a method for detecting the position of a defective portion of a hollow fiber membrane module on an end face of a sealing portion by optically detecting fine particles,
A hollow fiber, wherein a straightener is formed by assembling a plurality of straight straightening tubes close to an end face of the sealing portion, and optical detection is performed after passing the straightener through the commutator. Defect position detection method for membrane modules.
中空糸膜の束をケース内に装填し、ケース端部において中空糸膜の束の端末を開口した状態で封止した封止部を形成し、この封止部でケース内部と外部とを隔離した中空糸膜モジュールに関して、前記ケースの内部から外部に向けて各中空糸膜を通り封止部端面から流れる気流を形成し、この気流の中の中空糸膜の欠陥部を通り抜けた塵等の微粒子を光学的に検出する検出手段により、封止部端面における中空糸膜モジュールの欠陥部の位置を検出する装置において、
多数の整流管を集合させた整流子を前記封止部端面の外側に近接させて設けたことを特徴とする中空糸膜モジュールの欠陥位置検出装置。
A bundle of hollow fiber membranes is loaded into a case, and a sealed portion is formed at the end of the case with the ends of the bundles of hollow fiber membranes opened, and the inside and outside of the case are separated by the sealed portion. With respect to the hollow fiber membrane module thus formed, an airflow flowing from the inside of the case to the outside through each hollow fiber membrane and from the end face of the sealing portion is formed, and dust or the like passing through a defective portion of the hollow fiber membrane in the airflow is formed. In a device for detecting the position of a defective portion of the hollow fiber membrane module on the end face of the sealing portion by a detecting means for optically detecting the fine particles,
A defect position detecting device for a hollow fiber membrane module, wherein a commutator in which a number of flow straightening tubes are assembled is provided close to the outside of the end face of the sealing portion.
前記整流管は少なくとも3つの壁により形成されていることを特徴とする請求項2に記載の中空糸膜モジュールの欠陥位置検出装置。The defect position detecting device for a hollow fiber membrane module according to claim 2, wherein the straightening tube is formed by at least three walls.
JP09182195A 1995-03-24 1995-03-24 Method and apparatus for detecting defect position of hollow fiber membrane module Expired - Fee Related JP3557712B2 (en)

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