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JP3602375B2 - Dehydration cake hardness meter and hardness measurement method using the same - Google Patents
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JP3602375B2 - Dehydration cake hardness meter and hardness measurement method using the same - Google Patents

Dehydration cake hardness meter and hardness measurement method using the same Download PDF

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Publication number
JP3602375B2
JP3602375B2 JP19300899A JP19300899A JP3602375B2 JP 3602375 B2 JP3602375 B2 JP 3602375B2 JP 19300899 A JP19300899 A JP 19300899A JP 19300899 A JP19300899 A JP 19300899A JP 3602375 B2 JP3602375 B2 JP 3602375B2
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JP
Japan
Prior art keywords
hardness
cake
dewatered
compression spring
compression
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JP19300899A
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JP2001021473A (en
Inventor
隆 石川
隆三 木村
眞司 東
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NGK Insulators Ltd
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NGK Insulators Ltd
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Priority to JP19300899A priority Critical patent/JP3602375B2/en
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Description

【0001】
【発明の属する技術分野】
本発明は、碍子等の窯業製品の原料となる脱水ケーキの硬度測定計及びこれを用いた硬度測定方法に関するものである。
【0002】
【従来の技術】
碍子等の製造工程では、原料スラリーをフィルタープレスにより脱水して平板状の脱水ケーキとし、この脱水ケーキを土練機に投入して所定形状に押し出す方法が採用されている。ところがこの脱水ケーキは微妙な含水率の差等によって硬度がばらつくので、そのまま土練機に投入すると土練機からの押出し速度が不安定となる等のトラブルの原因となる。
【0003】
このため例えば35枚程度の脱水ケーキをパレット上に積載し、縦方向に切断しながら土練機に投入することにより各脱水ケーキ間の硬度のばらつきを平均化する工夫がなされており、これによって同一パレット上に積載された多数枚の脱水ケーキ間の硬度のばらつきは解消できる。しかし異なるパレット間における硬度差は残ることとなる。
【0004】
従ってパレット上に積載された多数枚の脱水ケーキの平均的な硬度を測定する必要がある。そこで本出願人は実開昭63−109639号に示されるように、パレット上に積載された多数枚の脱水ケーキをアムスラー式の加圧機により圧縮し、この加圧機が受ける最大耐力(最大圧力)の値によって脱水ケーキの平均的な硬度を測定する装置を開発した。この装置は多くの場合に正確な硬度を示すため、現在まで工場で用いられている。
【0005】
しかし、この装置には次のような問題があることが判明した。
1) パレット上に積載された多数枚の脱水ケーキの途中に高含水率の脱水ケーキが介在していると、その脱水ケーキが座屈することにより加圧機が受ける最大耐力が著しく低下し、平均的な硬度を測定できない。
2) 同様に、パレット自体が変形してしまうと脱水ケーキの平均的な硬度を測定できない。
3) 一度測定すると脱水ケーキが割れるため、同一品を繰り返して測定できない。従って軟質の脱水ケーキを自然乾燥させ、後日再度硬度を測定することができない。
【0006】
【発明が解決しようとする課題】
本発明は上記した従来の問題点を解決し、パレット上に積載された多数枚の脱水ケーキの平均的な硬度を正確に測定することができ、しかも繰り返し測定が可能で、脱水ケーキを測定装置まで搬送する必要もない、脱水ケーキの硬度測定計及びこれを用いた硬度測定方法を提供するためになされたものである。
【0007】
【課題を解決するための手段】
上記の課題を解決するためになされた請求項1の発明の脱水ケーキの硬度測定計は、基部にハンドルを備えた筒体の内部に圧縮バネを収納するとともに、この筒体の先端部に前記圧縮バネにより常に前方に弾発状態に保持されたスライダを設け、このスライダに複数枚の脱水ケーキを所定深さまで貫通できる長さの長尺棒を取付け、また筒体には長尺棒を脱水ケーキに貫通させたときの圧縮バネの圧縮量を表示する目盛りを設けるとともに、前記長尺棒を前記脱水ケーキに所定深さまで押し込んだときの圧縮バネの圧縮量と脱水ケーキの硬度との相関係数Rが0.900以上になるようにしたことを特徴とするものである。
また請求項2の発明の脱水ケーキの硬度測定方法は、積層された多数枚の脱水ケーキに、請求項1記載の脱水ケーキの硬度測定計の長尺棒を所定深さまで押し込み複数枚の脱水ケーキを貫通させ、そのときの圧縮バネの圧縮量を読み取ることにより、脱水ケーキの平均的な硬度を測定することを特徴とするものである。なお、この硬度測定計を自動測定装置化することも可能である。
【0008】
本発明によれば、パレット上に積載された多数枚の脱水ケーキの平均的な硬度を比較的正確に測定することができる。また長尺棒の押し込み位置をずらすことにより繰り返し測定が可能である。またこの硬度測定計は持ち運びが可能であるから、いつでもどこでも脱水ケーキの硬度測定を行うことができる利点がある。
【0009】
【発明の実施の形態】
以下に本発明の好ましい実施形態を示す。
図1は本発明の脱水ケーキの硬度測定計を示す断面図であり、1は円筒状の筒体、2はその基部に溶接等によって強固に固定されたハンドルである。この筒体1の内部には圧縮バネ3とスライダ4とが収納されている。スライダ4は圧縮バネ3により常に前方に弾発されているが、スライダ4の側方に突設されたピン5が筒体1の長孔6に嵌まっているため、図1の位置よりも前方には移動することはできない。従って、このスライダ4は圧縮バネにより常に前方に弾発状態に保持されている。
【0010】
スライダ4の先端には、やや太いロッド7を介してアダプタ8が固定されており、このアダプタ8にステンレス等の金属よりなる細長い長尺棒9が取り付けられている。この長尺棒9は複数枚の脱水ケーキを貫通できる長さを備えたものであり、この実施形態では直径が6mm、長さが約300mmの丸棒である。長尺棒9の先端をR形状とし、好ましくは半径3mm程度のR形状としておく。また、スライダ4のピン5には指針10が取り付けられているとともに、筒体1の長孔6の側方には、図2に示すように目盛り11が設けられている。この目盛11は、長尺棒9を脱水ケーキに押し込んだときの抵抗による圧縮バネ3の圧縮量を表示するためのものである。
【0011】
この硬度測定計を用いて脱水ケーキの硬度測定を行うには、図3に示すように測定者がハンドル2を握り、パレット12上に積層された多数枚の脱水ケーキに斜めに長尺棒9を押し込む。これに連れて長尺棒9は、図4に示すように複数枚の脱水ケーキを貫通しながら、長尺棒9の押し込み量に対応する体積の脱水ケーキを側方に移動させながら進行するが、このとき長尺棒9の先端に脱水ケーキから物理的な抵抗が作用するとともに、長尺棒9の側面にも脱水ケーキからの抵抗が作用する。しかも、長尺棒9は複数枚の脱水ケーキを貫通できる長さを持つので、複数枚の脱水ケーキが長尺棒9に及ぼす抵抗のトータル値が圧縮バネ3に作用し、圧縮バネ3を圧縮する。測定者は長尺棒9を所定深さ(アダプタ8の位置)まで押し込んで、そのときの圧縮バネ3の圧縮量を目盛り11により読み取る。
【0012】
この圧縮量の読み取り値は、以下の実施例のデータに示す通り、脱水ケーキの硬度の真値との間に高い相関を持つものである。すなわち、本発明では、図5〜から8についての後記説明のように前記長尺棒9を脱水ケーキに所定深さまで押し込んだときの圧縮バネ3の圧縮量と脱水ケーキの硬度との相関係数Rが0.900以上の高い相関を持つのである。
また、この脱水ケーキの硬度の真値は、土練機からの押出し速度から逆算した値である。なお圧縮量の読み取り値は、長尺棒9の押し込み速度や、押し込み力にはほとんど影響されず、長尺棒9を所定深さまで押し込めばほぼ一定となることを確認した。
【0013】
【実施例】
図1に示した構造の硬度測定計であって、圧縮バネ3を直径3mm、巻数14、コイル径50mm、自然長100mmの圧縮コイルバネとし、長尺棒9を直径6mm、長さ340mmとしたものを用いて、脱水ケーキの硬度の測定を行った。脱水ケーキはフィルタープレスにより脱水された直径700mm、厚さ20mmのもので、パレット上に36枚が積層されており、図3に示すようにその端面から斜め方向に長尺棒9を差し込んだ。
【0014】
図5は、36枚中の中央高さで脱水ケーキの硬度を測定した場合の目盛り11の読み取り値を横軸とし、土練機からの押出し速度から逆算された真値を縦軸としたグラフであり、測定対象を変えて約20回測定した。この場合の相関係数は0.903であり、本発明の方法によって脱水ケーキの硬度を精度よく測定できることが確認された。図6は、36枚中の上から約1/4の高さで脱水ケーキの硬度を測定した場合の同様のグラフであり、この場合の相関係数は0.913であった。
【0015】
また、図7と図8は原料系の異なる別の脱水ケーキの硬度を測定した場合の同様のグラフであり、図7は36枚中の中央高さにおける測定結果を、また図8は36枚中の上から約1/4の高さにおける測定結果を示す。図7における相関係数は0.909であり、図8における相関係数は0.914である。このように、本発明によれば真値との相関係数が0.9を上回る測定が可能である。これに対して、従来技術に記したアムスラー式の加圧機を用いた測定値は、例えば図9に示すようにばらつきが大きく、その相関係数は0.686であって本発明の優位性が明らかである。
【0016】
【発明の効果】
以上に説明したように、本発明の硬度測定計及び硬度測定方法によれば、多数枚の脱水ケーキの平均的な硬度を正確に測定することができる。また細い長尺棒を差し込むだけであるために同一サンプルについて繰り返し測定が可能であるため、最初の測定時に硬度が低すぎる場合には、脱水ケーキを自然乾燥させ、後日再度硬度を測定することもできる。更に本発明の硬度測定計はどこへでも携帯可能であるため、従来のように脱水ケーキを測定装置まで搬送する必要もない等の多くの利点がある。
【図面の簡単な説明】
【図1】本発明の脱水ケーキの硬度測定計を示す断面図である。
【図2】目盛り部分の外観図である。
【図3】本発明の脱水ケーキの硬度測定方法の説明図である。
【図4】長尺棒の装入状態を示す断面図である。
【図5】実施例のデータ(測定位置、中央部)を示すグラフである。
【図6】実施例のデータ(測定位置、上方部)を示すグラフである。
【図7】実施例のデータ(測定位置、中央部)を示すグラフである。
【図8】実施例のデータ(測定位置、上方部)を示すグラフである。
【図9】アムスラー式の加圧機を用いた測定データを示すグラフである。
【符号の説明】
1 筒体、2 ハンドル、3 圧縮バネ、4 スライダ、5 ピン、6 長孔7 ロッド、8 アダプタ、9 長尺棒、10 指針、11 目盛り、12 パレット
[0001]
TECHNICAL FIELD OF THE INVENTION
The present invention relates to a hardness meter for a dewatered cake used as a raw material for ceramic products such as insulators and a hardness measuring method using the same.
[0002]
[Prior art]
In the manufacturing process of insulators and the like, a method is employed in which a raw material slurry is dehydrated by a filter press to form a flat dewatered cake, and the dewatered cake is put into a clay kneader and extruded into a predetermined shape. However, since the hardness of the dewatered cake varies due to a slight difference in moisture content and the like, if the dewatered cake is directly put into a clay kneader, it causes troubles such as an unstable extrusion speed from the clay kneader.
[0003]
For this reason, for example, about 35 sheets of dewatered cakes are stacked on a pallet, and cut into a vertical direction while being put into a kneading machine, thereby devising a method of averaging the variation in hardness among the dewatered cakes. Variations in hardness among a number of dewatered cakes stacked on the same pallet can be eliminated. However, the hardness difference between different pallets will remain.
[0004]
Therefore, it is necessary to measure the average hardness of a large number of dewatered cakes stacked on a pallet. Therefore, as shown in Japanese Utility Model Application Laid-Open No. 63-109639, the present applicant compresses a large number of dewatered cakes stacked on a pallet with an Amsler-type press, and the maximum proof stress (maximum pressure) received by the press. A device for measuring the average hardness of the dewatered cake based on the value of was developed. This device has been used in factories to date to show accurate hardness in many cases.
[0005]
However, it has been found that this device has the following problems.
1) If a high moisture content dewatered cake is interposed in the middle of a large number of dewatered cakes stacked on a pallet, the dewatered cake will buckle and the maximum proof stress received by the pressing machine will be significantly reduced. Hardness cannot be measured.
2) Similarly, if the pallet itself is deformed, the average hardness of the dewatered cake cannot be measured.
3) Once measured, the same product cannot be measured repeatedly because the dehydrated cake breaks. Therefore, the soft dehydrated cake is naturally dried, and the hardness cannot be measured again later.
[0006]
[Problems to be solved by the invention]
The present invention solves the above-described conventional problems, and can accurately measure the average hardness of a large number of dewatered cakes stacked on a pallet, and can repeatedly perform the measurement. The purpose of the present invention is to provide a hardness meter for a dehydrated cake and a hardness measuring method using the same, which do not need to be transported to the same.
[0007]
[Means for Solving the Problems]
In order to solve the above-mentioned problems, a dehydration cake hardness meter according to claim 1 of the present invention has a compression spring housed inside a cylindrical body having a handle at a base portion, and the distal end of the cylindrical body has the compression spring. A slider always held forward by a compression spring is provided in a resilient state, and a long rod that can penetrate a plurality of dewatered cakes to a predetermined depth is attached to the slider. Rutotomoni provided a scale for displaying the amount of compression of the compression spring when passed through the cake, the phase of compression of the compression springs and the hardness of the dehydrated cake when pushed in the elongated rod to a predetermined depth in the dehydrated cake The relationship number R is set to 0.900 or more .
The method for measuring the hardness of a dewatered cake according to the second aspect of the present invention is a method for measuring the hardness of a plurality of dehydrated cakes by pushing a long bar of the dehydrated cake hardness meter according to the first aspect of the present invention to a predetermined depth. And the average hardness of the dewatered cake is measured by reading the compression amount of the compression spring at that time. In addition, it is also possible to make this hardness tester an automatic measuring device.
[0008]
According to the present invention, it is possible to relatively accurately measure the average hardness of a large number of dewatered cakes stacked on a pallet. In addition, the measurement can be repeated by shifting the pushing position of the long bar. Further, since the hardness meter is portable, there is an advantage that the hardness of the dehydrated cake can be measured anytime and anywhere.
[0009]
BEST MODE FOR CARRYING OUT THE INVENTION
Hereinafter, preferred embodiments of the present invention will be described.
FIG. 1 is a cross-sectional view showing a hardness meter for a dewatered cake of the present invention. Reference numeral 1 denotes a cylindrical cylinder, and 2 denotes a handle firmly fixed to a base portion thereof by welding or the like. A compression spring 3 and a slider 4 are housed inside the cylindrical body 1. The slider 4 is always repelled forward by the compression spring 3, but since the pin 5 protruding from the side of the slider 4 is fitted in the long hole 6 of the cylindrical body 1, the position of FIG. You cannot move forward. Therefore, the slider 4 is always held forward by the compression spring .
[0010]
An adapter 8 is fixed to the tip of the slider 4 via a slightly thick rod 7, and an elongated rod 9 made of metal such as stainless steel is attached to the adapter 8. The long bar 9 has a length capable of penetrating a plurality of dehydrated cakes, and in this embodiment, is a round bar having a diameter of 6 mm and a length of about 300 mm. The distal end of the long rod 9 has an R shape, preferably an R shape having a radius of about 3 mm. A pointer 10 is attached to the pin 5 of the slider 4, and a scale 11 is provided beside the long hole 6 of the cylindrical body 1 as shown in FIG. 2. The scale 11 is for displaying the compression amount of the compression spring 3 due to the resistance when the long rod 9 is pushed into the dewatering cake.
[0011]
In order to measure the hardness of the dehydrated cake using this hardness meter, the measurer grasps the handle 2 and, as shown in FIG. Press. Accordingly, the long bar 9 moves through the plurality of dewatered cakes as shown in FIG. 4 while moving the dewatered cake having a volume corresponding to the pushing amount of the long bar 9 to the side. At this time, physical resistance from the dehydrated cake acts on the tip of the long bar 9 and resistance from the dehydrated cake also acts on the side surface of the long bar 9. Moreover, since the long bar 9 has a length that can penetrate a plurality of dewatered cakes, the total value of the resistance exerted on the long bar 9 by the plurality of dewatered cakes acts on the compression spring 3 and compresses the compression spring 3. I do. The measurer pushes the long rod 9 to a predetermined depth (the position of the adapter 8), and reads the amount of compression of the compression spring 3 at that time by the scale 11.
[0012]
As shown in the data of the following examples, the read value of the compression amount has a high correlation with the true value of the hardness of the dewatered cake. That is, in the present invention, the correlation coefficient between the compression amount of the compression spring 3 and the hardness of the dewatered cake when the long rod 9 is pushed into the dewatered cake to a predetermined depth as described below with reference to FIGS. R has a high correlation of 0.900 or more.
Moreover, the true value of the hardness of the dehydrated cake is back-calculated values from extrusion rate from clay extruder. In addition, it was confirmed that the read value of the compression amount was hardly affected by the pushing speed and pushing force of the long rod 9 and was almost constant when the long rod 9 was pushed to a predetermined depth.
[0013]
【Example】
A hardness tester having the structure shown in FIG. 1, wherein the compression spring 3 is a compression coil spring having a diameter of 3 mm, a number of turns of 14, a coil diameter of 50 mm, and a natural length of 100 mm, and the long rod 9 has a diameter of 6 mm and a length of 340 mm. Was used to measure the hardness of the dewatered cake. The dewatered cake had a diameter of 700 mm and a thickness of 20 mm and was dehydrated by a filter press, and 36 sheets were stacked on a pallet. As shown in FIG. 3, a long rod 9 was inserted obliquely from its end face.
[0014]
FIG. 5 is a graph in which the read value of the scale 11 when the hardness of the dehydrated cake is measured at the center height of 36 sheets is set on the horizontal axis, and the true value calculated backward from the extrusion speed from the clay kneader is set on the vertical axis. The measurement was performed about 20 times while changing the measurement object. The correlation coefficient in this case was 0.903, and it was confirmed that the hardness of the dehydrated cake can be accurately measured by the method of the present invention. FIG. 6 is a similar graph when the hardness of the dehydrated cake is measured at a height of about 1/4 from the top of 36 sheets, and the correlation coefficient in this case was 0.913.
[0015]
7 and 8 are similar graphs when the hardness of another dewatered cake having a different raw material system is measured. FIG. 7 shows the measurement result at the center height of 36 sheets, and FIG. The measurement results at a height of about 1/4 from the top in the middle are shown. The correlation coefficient in FIG. 7 is 0.909, and the correlation coefficient in FIG. 8 is 0.914. As described above, according to the present invention, it is possible to perform a measurement in which the correlation coefficient with the true value exceeds 0.9. On the other hand, the measured value using the Amsler pressurized machine described in the prior art has a large variation as shown in FIG. 9, for example, and the correlation coefficient is 0.686, which indicates that the advantage of the present invention is high. it is obvious.
[0016]
【The invention's effect】
As described above, according to the hardness meter and the hardness measurement method of the present invention, the average hardness of a large number of dehydrated cakes can be accurately measured. In addition, since the same sample can be repeatedly measured because only a thin long rod is inserted, if the hardness is too low at the first measurement, the dehydrated cake is naturally dried, and the hardness may be measured again at a later date. it can. Further, since the hardness measuring instrument of the present invention can be carried anywhere, there are many advantages such as the need to transport the dehydrated cake to the measuring device unlike the related art.
[Brief description of the drawings]
FIG. 1 is a sectional view showing a hardness meter for a dehydrated cake of the present invention.
FIG. 2 is an external view of a scale portion.
FIG. 3 is an explanatory diagram of a method for measuring the hardness of a dehydrated cake of the present invention.
FIG. 4 is a cross-sectional view showing a state where a long bar is inserted.
FIG. 5 is a graph showing data (measurement position, central portion) of the example.
FIG. 6 is a graph showing data (measurement position, upper part) of the example.
FIG. 7 is a graph showing data (measurement position, central portion) of the example.
FIG. 8 is a graph showing data (measurement position, upper part) of the example.
FIG. 9 is a graph showing measurement data using an Amsler-type press.
[Explanation of symbols]
1 cylindrical body, 2 handles, 3 compression springs, 4 sliders, 5 pins, 6 long holes 7 rods, 8 adapters, 9 long rods, 10 pointers, 11 scales, 12 pallets

Claims (2)

基部にハンドルを備えた筒体の内部に圧縮バネを収納するとともに、この筒体の先端部に前記圧縮バネにより常に前方に弾発状態に保持されたスライダを設け、このスライダに複数枚の脱水ケーキを貫通できる長さの長尺棒を取付け、また筒体には長尺棒を脱水ケーキに所定深さまで貫通させたときの圧縮バネの圧縮量を表示する目盛りを設けるとともに、前記長尺棒を前記脱水ケーキに所定深さまで押し込んだときの圧縮バネの圧縮量と脱水ケーキの硬度との相関係数Rが0.900以上になるようにしたことを特徴とする脱水ケーキの硬度測定計。A compression spring is housed inside a cylinder having a handle at the base, and a slider which is always held forward by the compression spring at the tip of the cylinder is provided. Attach the long length of the length that can penetrate the cake, also the tubular member provided with a scale for displaying the amount of compression of the compression spring when passed through to a predetermined depth a long rod into dehydrated cake Rutotomoni, the long A hardness meter for a dewatered cake, wherein a correlation coefficient R between a compression amount of a compression spring and a hardness of the dewatered cake when the rod is pushed into the dewatered cake to a predetermined depth is 0.900 or more. . 積層された多数枚の脱水ケーキに、請求項1記載の脱水ケーキの硬度測定計の長尺棒を所定深さまで押し込み複数枚の脱水ケーキを貫通させ、そのときの圧縮バネの圧縮量を読み取ることにより、脱水ケーキの平均的な硬度を測定することを特徴とする脱水ケーキの硬度測定方法。The long bar of the hardness meter of the dewatering cake according to claim 1 is pushed to a predetermined depth into a plurality of the dewatering cakes stacked, and the plurality of dewatering cakes penetrate, and the compression amount of the compression spring at that time is read. A method for measuring the hardness of a dewatered cake, comprising: measuring the average hardness of the dewatered cake.
JP19300899A 1999-07-07 1999-07-07 Dehydration cake hardness meter and hardness measurement method using the same Expired - Lifetime JP3602375B2 (en)

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