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JP3633165B2 - Attachment for spray particle measurement. - Google Patents
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JP3633165B2 - Attachment for spray particle measurement. - Google Patents

Attachment for spray particle measurement. Download PDF

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Publication number
JP3633165B2
JP3633165B2 JP34734496A JP34734496A JP3633165B2 JP 3633165 B2 JP3633165 B2 JP 3633165B2 JP 34734496 A JP34734496 A JP 34734496A JP 34734496 A JP34734496 A JP 34734496A JP 3633165 B2 JP3633165 B2 JP 3633165B2
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Japan
Prior art keywords
cylinder
spray
inner cylinder
attachment
space
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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JP34734496A
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Japanese (ja)
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JPH10185794A (en
Inventor
猛 丹羽
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Shimadzu Corp
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Shimadzu Corp
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Priority to JP34734496A priority Critical patent/JP3633165B2/en
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Description

【0001】
【発明の属する技術分野】
この発明は、例えば化粧品用や清掃用として使用する各種スプレ−粒子の粒度分布を測定するためのスプレ−粒子測定用アタッチメントに関する。
【0002】
【従来の技術】
図4は、各種スプレ−粒子の粒度分布測定に際して使用されるレ−ザ−回折/散乱法を用いる粒度分布測定装置の原理図である。レ−ザ光源10より測定対照となる粒子群21にコリメ−タレンズ22を通したレ−ザ−光を照射すると、空間的に回折/散乱光の強度分布パタ−ンが生ずる。このうち前方散乱光の強度分布パタ−ンは、集光レンズ11によって集光され、焦点距離の位置にある検出面にリング状の回折/散乱像を結ぶ。これをリング状フォトダイオ−ドアレイ20で検出する。また、側方散乱光や後方散乱光は、側方散乱センサ23や後方散乱センサ24で検出する。前記リング状フォトダイオ−ドアレイ20で検出する粒度分布パタ−ンは、粒子の大きさによって変化する。実際のサンプルには大きさの異なる粒子が混在しているため、粒子群から生ずる光強度分布パタ−ンは、それぞれの粒子からの回折/散乱光の重ね合わせとなり、この重なり合った光強度分布パタ−ンから、サンプル粒子群の中にどのような大きさの粒子がどのような割合で含まれているかを計算によって求めることができる。
【0003】
従来の粒度分布測定装置では、光源10と集光レンズ11間を長くして、測定空間を開放、または開放に近い構造にしてスプレ−粒子を測定する場合、スプレ−を直接レ−ザ−ビ−ムに吹き付けている。このため集光レンズとスプレ−吹きつけ位置とは離れている。
【0004】
【発明が解決しようとする課題】
レ−ザ回折式粒度分布測定装置の原理上、集光レンズと測定位置、即ち、スプレ−吹き付け位置を離すと、測定範囲は粒子域が大きいほうへシフトする。微小粒子も正確に測定するためには測定位置(スプレ−吹き付け位置)をレンズに近づけた方が好ましい。しかし、そのままで近づけても拡散するスプレ−粒子がレンズに付着して汚染したり、或いは損傷し、その都度清掃、修理しなければならなくなる。また、微小粒子測定に際しては、種々の大きさの粒子を造粒して試験しなければならないが、微小粒子がある程度以上小さくなると健康上悪影響があるといわれているため安全衛生上にも問題がある。
【0005】
この発明は上記する課題に対処するためなされたものであり、集光レンズを汚染させることなく、また微小粒子測定精度もよくなり、且つ労働安全上の問題も解決することのできるスプレ−粒子測定用アタッチメントを提供することを目的としている。
【0006】
【課題を解決するための手段】
即ち、この発明は、上記する課題を解決するために、請求項1に記載のスプレ−粒子測定用アタッチメントが、径の大きな外側の筒体(2)に、所定の空間(4)を形成できるよう該筒体(2)内径よりも外径の小さな内側の筒体(3)を嵌め入れ、これら外側の筒体(2)と内側の筒体(3)との間の空間(4)の一方の端部を密封封止し、前記外側の筒体(2)と内側の筒体(3)との間の空間(4)の他方の端部には、小さなエア排出口(7)となるすき間を周設するとともに、該内側の筒体(3)の内径面には液垂れ防止フィルタ(8)を貼り付け、前記外側の筒体(2)には、エア導入口(9)を設けたことを特徴とする。
【0007】
また、請求項2に記載の発明は、前記径の大きな外側の筒体と外径の小さな内側の筒体との間のエア排出口のすき間を、これら外側の筒体と外径の小さな内側の筒体との間の内部空間より狭く周設したことを特徴とする。
【0008】
【発明の実施の形態】
以下、この発明の具体的実施の形態について図面を参照して説明する。
図1は、スプレ−用粒度分布測定装置に使用するこの発明のスプレ−粒子測定用アタッチメントの縦断面図であり、図2は図1のA−A矢視断面図である。
このスプレ−粒子測定用アタッチメント1は、径の大きな外側の筒体2に、所定の空間(筒状空間)4を形成できるよう該筒体2の内径よりも外径の小さな筒体3を嵌め入れ、これら外側の筒体2と内側の筒体3との間の空間4の一方の端部(図1の左端)に、短い筒状のスペ−サ5を圧入等により密封嵌合して封止し、これらこれら外側の筒体2と内側の筒体3とを固定している。また、内側の筒体3の内径面には液垂れ防止フィルタ8が貼り付けてある。
【0009】
前記外側の筒体2と内側の筒体3との間の空間4の他方の端部(図1の右端)には、内側の筒体3の外周に密着するよう、外径が外側の筒体2の内径よりも小さな別の短い筒状のスペ−サ6を圧入嵌合してある。これにより外側の筒体2と内側の筒体3との間に小さなすき間7が周設されることになる。このスペ−サ6は、内径が内側の筒対3の外形より大きな径の短い筒対として外側の筒対2の内径部に圧入するようにしてもよい。このすき間7は、後述するように、エアの排出口(以下、すき間7をエア排出口7とする)となるものである。また、前記外側の筒体2の一方の端部(図1の左端)近傍には、エア導入口9が取り付けてある。なお、図1において、このスプレ−粒子測定用アタッチメント1の右側近傍には平行光源10が配置されるが、この平行光源は紙面垂直上方に投射している。11は集光レンズである。
【0010】
このスプレ−粒子測定用アタッチメント1は、以上のような構成から成り、外側の筒体2と内側の筒体3との間のエア排出口7を、例えば0.5mm程度にして、エア導入口9より3〜4kgf/cm2 程度の圧縮空気を供給すれば、リング状のエアカ−テン12を形成することができる。このようなエアカ−テン12が形成された状態で、このスプレ−粒子測定用アタッチメント1の左側に配置したスプレ−13からスプレ−粒子を導入すれば、図3に示すように、スプレ−粒子はスプレ−粒子測定用アタッチメント1内の空間1aを通過した後もエア−カ−テン12内を流通し、外側には飛散しない。
【0011】
次に、内側の筒体2内に貼り付けた液垂れ防止フィルタ8は、スプレーが液滴となった場合のこの液滴の落下を防止するためのものである。すなわち、導入されたスプレ−粒子が内側の筒体3の内壁に当たって液滴となり、スプレ−粒子測定用アタッチメント1の右端から、エアカ−テン12が形成されていれば大粒子として吹き飛ばされる。しかし、この液垂れ防止フィルタ8は、エアカ−テン12が形成されていない場合、そのまま測定室に落下するのを防止する。この液垂れ防止フィルタ8としては、例えば試験管形濾紙の円筒部分を利用することができる。
【0012】
この発明のスプレ−粒子測定用アタッチメント1の一実施の形態は以上のようであり、外側の筒体2と内側の筒体3との間の空間4を密封するに際してはスペ−サ5を圧入嵌合するようにしたが、かかるスペ−サ5を用いずに、治具等を使用して外側の筒体2と内側の筒体3のいずれかを曲げて溶接して密封するようにしても良い。また、外側の筒体2と内側の筒体3との間のエア排出口7を小さくするに際しても、スペ−サ6を内側の筒体3外表面に圧入嵌合せずに、治具等を使用して外側の筒体2と内側の筒体3のいずれかを曲げてエア排出口7を周設するようにしてもよい。
【0013】
【発明の効果】
以上詳述したように、この発明のスプレ−粒子測定用アタッチメントによれば、エア−カ−テンによりスプレ−粒子はエアカ−テンの外側には飛散しないので集光レンズの近くへ測定用粒子を供給することができる。したがって、微小粒子測定の精度を向上させることができる。また、測定空間でスプレ−粒子は拡散しないので試験者が細かい粒子を吸引する恐れもなくなり、労働安全上の問題も解決することができる。
【図面の簡単な説明】
【図1】スプレ−用粒度分布測定装置に使用するこの発明のスプレ−粒子測定用アタッチメントの縦断面図である。
【図2】図1のA−A矢視断面図である。
【図3】図1のP矢視図である。
【図4】レ−ザ−回折/散乱法を用いる粒度分布測定装置の原理図である。
【符号の説明】
1 スプレ−粒子測定用アタッチメント
2 外側の筒体
3 内側の筒
4 内部空間
5 スペ−サ
6 スペ−サ
7 エア排出口
8 液垂れ防止フィルタ
9 エア導入口
10 平行光源
11 集光レンズ
12 エアカ−テン
13 スプレ−
[0001]
BACKGROUND OF THE INVENTION
The present invention relates to an attachment for measuring spray particles for measuring the particle size distribution of various spray particles used for cosmetics and cleaning, for example.
[0002]
[Prior art]
FIG. 4 is a principle diagram of a particle size distribution measuring apparatus using a laser diffraction / scattering method used for measuring the particle size distribution of various spray particles. When the laser light passing through the collimator lens 22 is irradiated from the laser light source 10 to the particle group 21 to be measured, the intensity distribution pattern of diffracted / scattered light is generated spatially. Among these, the intensity distribution pattern of the forward scattered light is condensed by the condensing lens 11 and forms a ring-shaped diffraction / scattered image on the detection surface at the position of the focal length. This is detected by the ring-shaped photodiode array 20. Further, the side scattered light and the back scattered light are detected by the side scattered sensor 23 and the back scattered sensor 24. The particle size distribution pattern detected by the ring-shaped photodiode array 20 varies depending on the size of the particles. Since particles of different sizes are mixed in an actual sample, the light intensity distribution pattern generated from the particle group is an overlap of diffracted / scattered light from each particle, and this overlapped light intensity distribution pattern. Therefore, it is possible to obtain by calculation what size particles and what proportion are included in the sample particle group.
[0003]
In the conventional particle size distribution measuring apparatus, when measuring the spray particles by making the space between the light source 10 and the condenser lens 11 long and the measurement space open or close to the open structure, the spray is directly connected to the laser. -Spraying For this reason, the condensing lens and the spray spray position are separated.
[0004]
[Problems to be solved by the invention]
Due to the principle of the laser diffraction type particle size distribution measuring apparatus, when the condensing lens is separated from the measurement position, that is, the spray spraying position, the measurement range shifts toward the larger particle area. In order to accurately measure fine particles, it is preferable to bring the measurement position (spray spray position) closer to the lens. However, even if it approaches as it is, the spray particles that diffuse will adhere to the lens and become contaminated or damaged, and must be cleaned and repaired each time. In addition, when measuring fine particles, particles of various sizes must be granulated and tested, but it is said that if the microparticles are reduced to a certain extent, there are adverse health effects. is there.
[0005]
The present invention has been made in order to cope with the above-mentioned problems, and spray particle measurement that does not contaminate the condensing lens, improves fine particle measurement accuracy, and can solve problems in occupational safety. The purpose is to provide an attachment.
[0006]
[Means for Solving the Problems]
That is, in order to solve the above-mentioned problems, the present invention can provide the spray particle measurement attachment according to claim 1 so that a predetermined space (4) can be formed in the outer cylindrical body (2) having a large diameter. An inner cylinder (3) having an outer diameter smaller than the inner diameter of the cylinder (2) is fitted, and the space (4) between the outer cylinder (2) and the inner cylinder (3) is inserted. One end is hermetically sealed, and the other end of the space (4) between the outer cylinder (2) and the inner cylinder (3) has a small air discharge port (7) A gap is formed around the inner cylinder (3), a liquid dripping prevention filter (8) is attached to the inner surface of the inner cylinder (3) , and an air inlet (9) is provided in the outer cylinder (2). It is provided.
[0007]
In the invention according to claim 2, the clearance of the air discharge port between the outer cylindrical body having a large diameter and the inner cylindrical body having a small outer diameter is set between the outer cylindrical body and the inner diameter having a small outer diameter. It is characterized in that it is arranged narrower than the internal space between the cylindrical body.
[0008]
DETAILED DESCRIPTION OF THE INVENTION
Hereinafter, specific embodiments of the present invention will be described with reference to the drawings.
FIG. 1 is a longitudinal sectional view of the spray particle measuring attachment of the present invention used in a spray particle size distribution measuring apparatus, and FIG. 2 is a sectional view taken along the line AA in FIG.
In this spray particle measurement attachment 1, a cylindrical body 3 having an outer diameter smaller than the inner diameter of the cylindrical body 2 is fitted in an outer cylindrical body 2 having a large diameter so that a predetermined space (cylindrical space) 4 can be formed. Then, a short cylindrical spacer 5 is hermetically fitted into one end (left end in FIG. 1) of the space 4 between the outer cylinder 2 and the inner cylinder 3 by press fitting or the like. These outer cylinders 2 and the inner cylinder 3 are fixed. A liquid dripping prevention filter 8 is attached to the inner diameter surface of the inner cylinder 3.
[0009]
An outer cylinder having an outer diameter so as to be in close contact with the outer periphery of the inner cylinder 3 at the other end (right end in FIG. 1) of the space 4 between the outer cylinder 2 and the inner cylinder 3. Another short cylindrical spacer 6 smaller than the inner diameter of the body 2 is press-fitted. As a result, a small gap 7 is provided between the outer cylinder 2 and the inner cylinder 3. The spacer 6 may be press-fitted into the inner diameter portion of the outer cylinder pair 2 as a short cylinder pair whose inner diameter is larger than the outer diameter of the inner cylinder pair 3. As will be described later, the gap 7 serves as an air discharge port (hereinafter, the gap 7 is referred to as an air discharge port 7). An air inlet 9 is attached in the vicinity of one end (left end in FIG. 1) of the outer cylinder 2. In FIG. 1, a parallel light source 10 is disposed in the vicinity of the right side of the spray particle measurement attachment 1, and the parallel light source is projected vertically upward on the paper surface. Reference numeral 11 denotes a condenser lens.
[0010]
The spray particle measurement attachment 1 is configured as described above, and the air discharge port 7 between the outer cylinder 2 and the inner cylinder 3 is set to about 0.5 mm, for example, to introduce air. If compressed air of about 3 to 4 kgf / cm 2 is supplied from the port 9, a ring-shaped air curtain 12 can be formed. When the spray particles are introduced from the spray 13 disposed on the left side of the spray particle measurement attachment 1 in the state in which such an air curtain 12 is formed, the spray particles are obtained as shown in FIG. Even after passing through the space 1a in the spray particle measuring attachment 1, it circulates in the air curtain 12 and does not scatter outside.
[0011]
Next, the dripping prevention filter 8 affixed in the inner cylinder 2 is for preventing the drop of the droplet when the spray becomes a droplet. That is, the introduced spray particles hit the inner wall of the inner cylinder 3 to form droplets, and if the air curtain 12 is formed from the right end of the spray particle measurement attachment 1, it is blown off as large particles. However , the dripping prevention filter 8 prevents the liquid curtain 12 from dropping into the measurement chamber as it is when the air curtain 12 is not formed. As the liquid dripping prevention filter 8, for example, a cylindrical portion of a test tube type filter paper can be used.
[0012]
Spray of the invention - an embodiment of the particle measuring attachment 1 Ri der way, space is when sealing the space 4 between the outer cylindrical member 2 and the inner cylindrical body 3 - a support 5 Although press-fitting is performed, the outer cylinder 2 and the inner cylinder 3 are bent and welded using a jig or the like without using the spacer 5 and sealed. May be. Further, when reducing the air discharge port 7 between the outer cylinder 2 and the inner cylinder 3, a jig or the like is used without press-fitting the spacer 6 to the outer surface of the inner cylinder 3. The air discharge port 7 may be provided by bending either the outer cylinder 2 or the inner cylinder 3 in use.
[0013]
【The invention's effect】
As described above in detail, according to the spray particle measurement attachment of the present invention, since the spray particles are not scattered outside the air curtain by the air curtain, the measurement particles are placed near the condenser lens. Can be supplied. Therefore, the precision of microparticle measurement can be improved. Further, since the spray particles do not diffuse in the measurement space, there is no possibility that the examiner sucks fine particles, and the problem of occupational safety can be solved.
[Brief description of the drawings]
FIG. 1 is a longitudinal sectional view of a spray particle measuring attachment of the present invention used in a spray particle size distribution measuring apparatus.
FIG. 2 is a cross-sectional view taken along the line AA in FIG.
FIG. 3 is a view taken in the direction of arrow P in FIG. 1;
FIG. 4 is a principle diagram of a particle size distribution measuring apparatus using a laser diffraction / scattering method.
[Explanation of symbols]
1 spray - particle measuring attachment 2 outside of the cylindrical body 3 inside of the cylindrical body 4 inner space 5 space - Sa 6 space - Sa 7 Air outlet 8 liquid sagging filter 9 air inlet 10 parallel light source 11 a condenser lens 12 Eaka -Ten 13 spray

Claims (2)

径の大きな外側の筒体に、所定の空間を形成できるよう該外側の筒体内径よりも外径の小さな内側の筒体を嵌め入れ、これら外側の筒体と内側の筒体との間の空間の一方の端部を密封封止し、前記外側筒体と内側筒体との間の空間の他方の端部には、小さなエア排出口となるすき間を周設するとともに、該内側の筒体の内径面には液垂れ防止フィルタを貼り付け、前記外側の筒体には、エア導入口を設けたことを特徴とするスプレ−粒子測定用アタッチメント。An inner cylinder having an outer diameter smaller than the inner diameter of the outer cylinder is fitted into the outer cylinder having a large diameter so that a predetermined space can be formed, and the gap between the outer cylinder and the inner cylinder is set. One end of the space is hermetically sealed, and a gap serving as a small air discharge port is provided around the other end of the space between the outer cylinder and the inner cylinder, and the inner cylinder A spray particle measurement attachment , wherein a liquid dripping prevention filter is attached to an inner diameter surface of a body, and an air introduction port is provided in the outer cylinder. 前記径の大きな外側の筒体と外径の小さな内側の筒体との間のエア排出口のすき間を、これら外側の筒体と外径の小さな内側の筒体との間の内部空間より狭く周設したことを特徴とする請求項1に記載のスプレ−粒子測定用アタッチメント。The clearance of the air discharge port between the outer cylinder having a large diameter and the inner cylinder having a small outer diameter is narrower than the internal space between the outer cylinder and the inner cylinder having a small outer diameter. The spray particle measurement attachment according to claim 1, wherein the attachment is arranged around.
JP34734496A 1996-12-26 1996-12-26 Attachment for spray particle measurement. Expired - Fee Related JP3633165B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP34734496A JP3633165B2 (en) 1996-12-26 1996-12-26 Attachment for spray particle measurement.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP34734496A JP3633165B2 (en) 1996-12-26 1996-12-26 Attachment for spray particle measurement.

Publications (2)

Publication Number Publication Date
JPH10185794A JPH10185794A (en) 1998-07-14
JP3633165B2 true JP3633165B2 (en) 2005-03-30

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JP5172798B2 (en) * 2009-09-02 2013-03-27 東洋エアゾール工業株式会社 Jig for measuring oxygen concentration in aerosol container

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