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JP4020459B2 - Filling confirmation method of foam-cured foam - Google Patents
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JP4020459B2 - Filling confirmation method of foam-cured foam - Google Patents

Filling confirmation method of foam-cured foam Download PDF

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Publication number
JP4020459B2
JP4020459B2 JP18822697A JP18822697A JP4020459B2 JP 4020459 B2 JP4020459 B2 JP 4020459B2 JP 18822697 A JP18822697 A JP 18822697A JP 18822697 A JP18822697 A JP 18822697A JP 4020459 B2 JP4020459 B2 JP 4020459B2
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JP
Japan
Prior art keywords
foam
filling
closed cross
confirmation method
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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JP18822697A
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Japanese (ja)
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JPH1134082A (en
Inventor
喜市 山下
達也 若森
正仁 森
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sunstar Giken KK
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Sunstar Giken KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Priority to JP18822697A priority Critical patent/JP4020459B2/en
Application filed by Sunstar Giken KK filed Critical Sunstar Giken KK
Priority to EP20080158466 priority patent/EP1970184A3/en
Priority to KR1019997006676A priority patent/KR20000070441A/en
Priority to EP98900998A priority patent/EP1020273B2/en
Priority to DE69840213T priority patent/DE69840213D1/en
Priority to US09/355,035 priority patent/US6337355B1/en
Priority to CA 2278683 priority patent/CA2278683C/en
Priority to PCT/JP1998/000269 priority patent/WO1998032580A1/en
Publication of JPH1134082A publication Critical patent/JPH1134082A/en
Priority to US09/986,675 priority patent/US6866804B2/en
Priority to US11/025,152 priority patent/US7459107B2/en
Application granted granted Critical
Publication of JP4020459B2 publication Critical patent/JP4020459B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Description

【0001】
【発明の属する技術分野】
本発明は、発泡硬化フォームの充填確認方法、更に詳しくは、閉断面構造を有する車体部材の閉断面内部に二液型発泡性材料を注入し、発泡硬化によって発泡硬化フォームを充填するに際し、上記閉断面内部の容積に見合った充填容量の適正を確認するため、充填部位と未充填部位の温度差を外部から非接触で測定検出する方法に関する。
【0002】
【従来の技術と発明が解決しようとする課題】
我国の自動車業界では、車の衝突安全性向上を目的として、車体全体の剛性や強度の向上が検討されている。このように、我国での自動車の衝突安全性の要求はますます厳しくなり、より安全度の高い車の生産が要求されつつある。
【0003】
ところで、かかる衝突安全性向上の対策として、各自動車メーカーでは鋼板での補強構造が検討され、独自の車体構造が開発されているが、車1台当りの重量増(一般に30〜50kg)は避けられない。
また、かかる構造補強とは別に、衝撃など多くの負荷が加わる車体部材、たとえばシートベルト装置のベルトアンカーが装着され、閉断面構造を有するセンターピラーや、その他前部車体の閉断面構造を有するフロントピラー等に対し、それらの閉断面部分(通常、区画の仕切板を設置して閉断面を形成)に二液型発泡性材料を注入し、発泡硬化によって、補強材として機能する発泡硬化フォームを充填することが検討されている。
【0004】
この発泡硬化フォームの充填技術は、二液型発泡性材料の発泡倍率やその他発泡条件を考慮した上で、充填すべき閉断面内部の容積に見合う量で定量注入することにより、所望範囲で発泡硬化フォームを充填した、上記センターピラーやフロントピラー等の閉断面構造を有する車体部材を得ることができるようになっている。
しかしながら、不測の事態として注入装置等に故障が起った場合、発泡硬化フォームの充填容量が所望範囲より不足すると空洞部が生じ、設計通りの強度が得られなくなることが予測される。また、閉断面部分に設けた仕切板の不意の欠損によっても、充填容量の不足を来すことが考えられる。
実際には、このような充填容量の不足を未然に防止するすべはなく、生産ライン後に衝突試験や実車の剛性測定あるいは振動解析を行うことにより、初めて充填容量の適否を判断できるのが現状で、生産ライン途中で、車の設計強度や剛性を保証することは困難であった。
【0005】
【課題を解決するための手段】
本発明者らは、かかる充填容量の不足による問題点を未然に防止せしめ、発泡硬化フォームを適正に充填して補強するため鋭意検討を進めたところ、閉断面構造を有する車体部材の閉断面内部に二液型発泡性材料を注入すると、反応によって発泡と同時に発熱を起し、この発熱が該車体部材の充填部位のパネル温度を上昇せしめることに着目した。すなわち、車体部材側面の発泡硬化フォームが最終的に到達する限界位置付近の箇所を外部から非接触で温度測定すれば、その温度差によって充填部位と未充填部位を区別できることから、閉断面内部の容積に見合った充填容量の適正を確認しうることを見出し、本発明を完成させるに至った。
【0006】
すなわち、本発明は、閉断面構造を有する車体部材の閉断面内部に二液型発泡性材料を注入し、発泡硬化によって発泡硬化フォームを充填するに際し、上記閉断面内部の容積に見合った充填容量の適正を確認するため、該車体部材の側面に対し外部から非接触で温度測定を行い、充填部位と未充填部位の温度差によって充填容量の適正を確認することを特徴とする発泡硬化フォームの充填確認方法を提供するものである。
【0007】
本発明において閉断面構造を有する車体部材としては、たとえば図1に示される、フロントルーフ1(ルーフレールインナーとルーフレールアウターで構成)とフロントサイドルーフレール2(フロントサイドアウターパネルとサイドルーフレールインナーで構成)とフロントピラー3(フロントサイドアウターパネルとフロントピラーインナーで構成)とを連結した構造部材が挙げられ、フロントサイドルーフレール2およびフロントピラー3のそれぞれの内部に、仕切板4および5が設置され、かつフロントサイドルーフレール2には注入穴6が開設されている。
【0008】
本発明において上記注入穴6に注入される二液型発泡性材料としては、常温下で発泡硬化しうるものであれば特にその種類に制限はなく、たとえばポリオール主剤[多価アルコール,ビスフェノール類,各種アミンなどの活性水素含有化合物に、アルキレンオキシドを付加反応させて得られるポリエーテルポリオールが好ましい]と、ポリイソシアネート硬化剤[芳香族ポリイソシアネート、脂肪族または脂環式ポリイソシアネート、芳香脂肪族ポリイソシアネート、これらの各種変性物、ポリオール類と過剰のポリイソシアネート化合物との反応で得られる末端NCO基含有ウレタンプレポリマーなど]からなり、該主剤側に発泡剤[水、熱分解型化学発泡剤(アゾジカルボジアミド、p,p'−オキシビスベンゼンスルホニルヒドラジドなど)、熱分解型無機発泡剤(炭酸水素ナトリウムなど)、熱膨張型マイクロバルーン(ポリマーカプセルにペンタン、ヘプタンなどの低沸点溶剤を包み込んだもの)等]を配合し、さらに必要に応じて反応触媒、鎖延長剤、整泡剤、着色剤、可塑剤、充填剤、難燃剤、老化防止剤、抗酸化剤などを加えた二液型発泡性ウレタン材料の使用が好適である。
【0009】
【発明の実施の形態】
本発明に係る発泡硬化フォームの充填確認方法は、上記図1に示されるような車体部材の側面に対し外部から非接触で温度測定を行い、充填部位と未充填部位の温度差を求めるものである。たとえば図1において、注入穴6から二液型発泡材料を注入すると、該発泡材料は最初にフロントピラー3の方へ発泡硬化(同時に発熱)しながら進み、次いでフロントサイドルーフレール2へと広がり、その間上端部やコーナー部を回って、最終的にフロントルーフ1の上方へと進み、図示の限界位置Pに到達する。ここで、車体部材における充填箇所のパネル温度は、充填材(発泡硬化フォーム)の発熱温度(一般に170℃付近)により上昇する。パネルの板厚や2重構造になっているかどうかによって、温度の上昇速度は異なるが、目安として1〜5分(板厚が必要以上に厚い場合は、2〜5分程度)の経時で、パネル温度の上昇を確認でき、一般に50〜100℃に達する(これに対し、未充填部位のパネル温度は、周囲温度を少し越える、40℃以下にある)。従って、二液型発泡性材料の注入、発泡硬化後、上記経時範囲内で、充填側面箇所のパネル温度を非接触で測定すれば、その温度差(通常、10℃以上、好ましくは20℃以上)により、充填部位と未充填部位を区別でき、これによって充填容量の適正を確認することができ、同時に設計上の強度や剛性の保証が可能となり、充填不足の予測される車のむやみの生産を未然に回避できる。
【0010】
なお、充填不足が発覚した場合、未充填部位に別途注入穴を設けて、二液型発泡性材料の補充注入を行えばよい。
上記非接触での温度測定には、「物体が自然に放射する赤外線をとらえ、非接触で物体の表面の温度を多点表示し、または温度分布を熱画像データとして提供する」、一般に赤外線熱画像装置または赤外放射温度計と称せられているものを使用すればよい。
また、計測対象物が監視設定温度範囲を超えた場合に、適正信号を出力して正常を知らせる機能を備えた装置を用いることにより、充填部位と未充填部位の温度を同時に測定し、その温度差を検知し、10℃以上の温度差にならない場合に警告信号を発生する装置を導入することもできる。
【0011】
【実施例】
次に実施例を挙げて、本発明をより具体的に説明する。
実施例1
図1に示す車体部材(閉断面内部容積:1250cc)の注入穴6(口径20mm)から、二液型発泡性ウレタン材料(発泡後の密度350kg/m3)を高圧発泡機にて5kg/分の速度で438g注入し、発泡硬化後、2分経過してから、赤外線熱画像装置(日本アビオニクス社製、TVS−110)を用いて、図1に示す部位(A〜F点)のパネル温度を測定したところ、A点=58℃、B点=54℃、C点=63℃、D点=22℃、E点=20℃、F点=25℃であった。
また、A〜F点を含む全体のパネル温度分布を同装置で観察した。
さらに、各2点(AとD、BとE、CとF)間の温度差が10℃未満であると、警告信号を発し、ブザーが鳴るように設定したアラーム機能付の同装置でも測定したが、ブザーが鳴らないことを確認した。
【0012】
【発明の効果】
以上の構成からなる本発明は、二液型発泡性材料の注入、発泡硬化後に所定の経時範囲内に、非接触でのパネル温度の測定を行うことにより、所望範囲の全てに充填できたかを確認でき、このような充填補強材の適用を前提とした設計上の強度や剛性を保証するものであり、しかも、軽量かつ車体強度剛性向上の社会ニーズを満たす発泡充填材の適用工法を実用化させる有効な手段となり得る。
【図面の簡単な説明】
【図1】 本発明における閉断面構造を有する車体部材の一例を示す概要図である。
【符号の説明】
1:フロントルーフ
2:フロントサイドルーフレール
3:フロントピラー
6:注入穴
[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a method for confirming filling of foam-cured foam, more specifically, when a two-component foamable material is injected into a closed cross section of a vehicle body member having a closed cross-section structure, and the foam cured foam is filled by foam curing. The present invention relates to a method for measuring and detecting the temperature difference between a filled part and an unfilled part from the outside in a non-contact manner in order to confirm the appropriate filling capacity corresponding to the volume inside the closed section.
[0002]
[Prior art and problems to be solved by the invention]
In the automobile industry in Japan, improvement of the rigidity and strength of the entire vehicle body is being studied for the purpose of improving the collision safety of vehicles. In this way, the demand for automobile crash safety in Japan has become increasingly severe, and production of vehicles with higher safety is being demanded.
[0003]
By the way, as a measure to improve the collision safety, each automobile manufacturer has studied the reinforcement structure with steel plate and developed its own body structure, but avoid the weight increase per car (generally 30-50kg). I can't.
In addition to such structural reinforcement, a vehicle body member to which a lot of loads such as impacts are applied, for example, a center pillar having a closed cross-section structure and a front pillar having a closed cross-section structure of a front vehicle body, which is mounted with a belt anchor of a seat belt device. A foam-cured foam that functions as a reinforcing material by injecting a two-component foamable material into pillars, etc., into their closed section (usually installing partition partitions to form a closed section) Filling is being considered.
[0004]
This foam-cured foam filling technology takes into account the foaming ratio and other foaming conditions of a two-part foamable material, and injects in a desired range by quantitatively injecting it in an amount commensurate with the volume inside the closed section to be filled. A vehicle body member having a closed cross-sectional structure such as the center pillar or the front pillar filled with the hardened foam can be obtained.
However, when a failure occurs in the injection device or the like as an unexpected situation, it is predicted that if the filling capacity of the foam-cured foam is insufficient below the desired range, a hollow portion is generated and the strength as designed cannot be obtained. Further, it is conceivable that the filling capacity is insufficient due to an unexpected loss of the partition plate provided in the closed cross section.
Actually, there is no way to prevent such a shortage of filling capacity, and it is currently possible to determine the suitability of the filling capacity for the first time by performing a crash test, measuring the rigidity of the actual vehicle, or analyzing the vibration after the production line. During the production line, it was difficult to guarantee the design strength and rigidity of the car.
[0005]
[Means for Solving the Problems]
The present inventors have made extensive studies to prevent such problems due to insufficient filling capacity and to properly fill and reinforce the foam-cured foam. It was noted that when a two-component foaming material was injected into the body, heat was generated simultaneously with foaming due to the reaction, and this heat generation increased the panel temperature at the filling portion of the vehicle body member. That is, if the temperature near the limit position where the foam-cured foam finally arrives on the side of the vehicle body member is measured from the outside without contact, the filled portion and the unfilled portion can be distinguished from each other by the temperature difference. The present inventors have found that it is possible to confirm the appropriateness of the filling capacity corresponding to the volume, and have completed the present invention.
[0006]
That is, according to the present invention, when a two-component foamable material is injected into a closed cross-section of a vehicle body member having a closed cross-sectional structure, and a foam-cured foam is filled by foam hardening, a filling capacity corresponding to the volume inside the closed cross-section is provided. In order to confirm the suitability of the foam-cured foam, the temperature of the body member is measured from the outside in a non-contact manner, and the suitability of the filling capacity is confirmed by the temperature difference between the filled portion and the unfilled portion. A filling confirmation method is provided.
[0007]
As a vehicle body member having a closed cross-sectional structure in the present invention, for example, as shown in FIG. 1, a front roof 1 (configured by a roof rail inner and a roof rail outer) and a front side roof rail 2 (configured by a front side outer panel and a side roof rail inner) are shown. Examples include a structural member in which a front pillar 3 (consisting of a front side outer panel and a front pillar inner) is connected, and partition plates 4 and 5 are installed inside the front side roof rail 2 and the front pillar 3, respectively. An injection hole 6 is formed in the side roof rail 2.
[0008]
In the present invention, the two-pack type foamable material injected into the injection hole 6 is not particularly limited as long as it can be foam-cured at room temperature. For example, a polyol main agent [polyhydric alcohol, bisphenols, A polyether polyol obtained by addition reaction of an alkylene oxide with an active hydrogen-containing compound such as various amines is preferable] and a polyisocyanate curing agent [aromatic polyisocyanate, aliphatic or alicyclic polyisocyanate, aromatic aliphatic polyisocyanate]. Isocyanate, various modified products thereof, terminal NCO group-containing urethane prepolymer obtained by reaction of polyols with excess polyisocyanate compound, etc.], and a foaming agent [water, pyrolytic chemical foaming agent ( Azodicarbodiamide, p, p'-oxybisbenzenesulfonyl hydrazide, etc.), no thermal decomposition Machine foaming agent (such as sodium bicarbonate), thermal expansion type microballoon (in which polymer capsules are encapsulated with a low boiling point solvent such as pentane, heptane, etc.), and further, if necessary, reaction catalyst, chain extender, It is preferable to use a two-component foamable urethane material to which a foam stabilizer, a colorant, a plasticizer, a filler, a flame retardant, an anti-aging agent, an antioxidant, and the like are added.
[0009]
DETAILED DESCRIPTION OF THE INVENTION
The method for confirming the filling of foam-cured foam according to the present invention is a method for measuring the temperature difference between the filled part and the unfilled part by measuring the temperature from the outside in a non-contact manner on the side surface of the vehicle body member as shown in FIG. is there. For example, in FIG. 1, when a two-component foam material is injected from the injection hole 6, the foam material first proceeds while being foam-cured (simultaneously generated heat) toward the front pillar 3, and then spreads to the front side roof rail 2. It goes around the upper end and the corner, and finally proceeds upward of the front roof 1 to reach the limit position P shown in the figure. Here, the panel temperature of the filling portion in the vehicle body member rises due to the heat generation temperature (generally around 170 ° C.) of the filler (foamed and cured foam). The rate of temperature rise varies depending on whether the panel is thick or has a double structure, but as a guideline, it takes 1-5 minutes (2-5 minutes if the board is thicker than necessary) over time, An increase in the panel temperature can be confirmed, and generally reaches 50 to 100 ° C. (in contrast, the panel temperature at the unfilled site is slightly higher than the ambient temperature, being 40 ° C. or less). Therefore, if the panel temperature at the filling side surface is measured in a non-contact manner within the above-mentioned time range after injection of the two-component foamable material and foam curing, the temperature difference (usually 10 ° C or higher, preferably 20 ° C or higher) ) Makes it possible to distinguish between filled and unfilled parts, which allows you to check the appropriateness of the filling capacity, and at the same time guarantees the strength and rigidity of the design. Can be avoided in advance.
[0010]
In addition, when insufficient filling is detected, a separate injection hole may be provided in the unfilled portion, and replenishment injection of the two-pack type foamable material may be performed.
In the non-contact temperature measurement, “infrared rays naturally emitted from an object are captured, the surface temperature of the object is displayed in multiple points without contact, or the temperature distribution is provided as thermal image data”. What is called an image device or an infrared radiation thermometer may be used.
In addition, when the measurement object exceeds the monitoring set temperature range, the temperature of the filled part and the unfilled part is measured at the same time by using a device with a function to output a proper signal and notify normality. It is also possible to introduce a device that detects the difference and generates a warning signal when the temperature difference does not reach 10 ° C. or more.
[0011]
【Example】
Next, an Example is given and this invention is demonstrated more concretely.
Example 1
From the injection hole 6 (diameter 20 mm) of the vehicle body member (closed cross-section internal volume: 1250 cc) shown in FIG. 1, a two-pack foaming urethane material (density after foaming 350 kg / m 3 ) is 5 kg / min with a high-pressure foaming machine. After injecting 438 g at a rate of 2 minutes, after 2 minutes of foaming, the panel temperature of the part (points A to F) shown in FIG. 1 using an infrared thermal imager (Japan Avionics, TVS-110). As a result, A point = 58 ° C., B point = 54 ° C., C point = 63 ° C., D point = 22 ° C., E point = 20 ° C., and F point = 25 ° C.
Further, the entire panel temperature distribution including the points A to F was observed with the same apparatus.
Furthermore, if the temperature difference between each of the two points (A and D, B and E, C and F) is less than 10 ° C, a warning signal is issued and the same device with an alarm function set to sound a buzzer is also measured. However, it was confirmed that the buzzer did not sound.
[0012]
【The invention's effect】
In the present invention having the above-described configuration, whether or not the desired range can be filled by measuring the panel temperature in a non-contact manner within a predetermined time range after the injection of the two-component foamable material and the foam curing is confirmed. We can confirm the strength and rigidity of the design based on the premise that such filler reinforcement is applied, and we have put to practical use a foam filler application method that meets the social needs of light weight and improved body strength and rigidity. It can be an effective means.
[Brief description of the drawings]
FIG. 1 is a schematic view showing an example of a vehicle body member having a closed cross-sectional structure in the present invention.
[Explanation of symbols]
1: Front roof 2: Front side roof rail 3: Front pillar 6: Injection hole

Claims (3)

自動車生産ラインにおいて、閉断面構造を有する車体部材の閉断面内部に二液型発泡性材料を注入し、発泡硬化によって発泡硬化フォームを充填するに際し、上記閉断面内部の容積に見合った充填容量の適正を確認するため、該材料の注入後1〜5分の範囲内で、該車体部材の側面に対し外部から非接触で温度測定を行い、該材料の発泡硬化時の発熱に基づく充填部位と未充填部位の温度差によって充填容量の適正を確認することを特徴とする自動車生産ラインにおける発泡硬化フォームの充填確認方法。In an automobile production line, when a two-component foamable material is injected into a closed cross-section of a body member having a closed cross-sectional structure, and a foam-cured foam is filled by foam curing, a filling capacity corresponding to the volume inside the closed cross-section is obtained. In order to confirm appropriateness, within 1 to 5 minutes after the injection of the material, temperature measurement is performed from the outside in a non-contact manner with respect to the side surface of the vehicle body member, The filling confirmation method of the foaming hardening foam in the automobile production line characterized by confirming the appropriate filling capacity by the temperature difference of the unfilled part. 温度差が10℃以上である請求項1に記載の充填確認方法。  The filling confirmation method according to claim 1, wherein the temperature difference is 10 ° C. or more. 温度測定に赤外線熱画像装置または赤外放射温度計を用いる請求項1または2に記載の充填確認方法。  The filling confirmation method according to claim 1, wherein an infrared thermal image device or an infrared radiation thermometer is used for temperature measurement.
JP18822697A 1997-01-23 1997-07-14 Filling confirmation method of foam-cured foam Expired - Lifetime JP4020459B2 (en)

Priority Applications (10)

Application Number Priority Date Filing Date Title
JP18822697A JP4020459B2 (en) 1997-07-14 1997-07-14 Filling confirmation method of foam-cured foam
PCT/JP1998/000269 WO1998032580A1 (en) 1997-01-23 1998-01-23 Two-pack urethane foam composition, and two-pack urethane foam composition packing apparatus and method
EP98900998A EP1020273B2 (en) 1997-01-23 1998-01-23 Urethane foam formed from a two-pack urethan foam composition
DE69840213T DE69840213D1 (en) 1997-01-23 1998-01-23 TWO COMPONENT URETHANSCHAUMZUSAMMENSTELLUNG
US09/355,035 US6337355B1 (en) 1997-01-23 1998-01-23 Two-pack urethane foam composition
CA 2278683 CA2278683C (en) 1997-01-23 1998-01-23 Two-pack urethane foam composition, and two-pack urethane foam composition injecting apparatus and method
EP20080158466 EP1970184A3 (en) 1997-01-23 1998-01-23 Two-pack urethane foam composition and two-pack urethane foam composition injecting apparatus and method
KR1019997006676A KR20000070441A (en) 1997-01-23 1998-01-23 Two-pack urethane foam composition, and two-pack urethane foam composition packing apparatus and method
US09/986,675 US6866804B2 (en) 1997-01-23 2001-11-09 Two-pack urethane foam composition, and two-pack urethane foam composition injecting apparatus and method
US11/025,152 US7459107B2 (en) 1997-01-23 2004-12-30 Two-pack urethane foam composition, and two-pack urethane foam composition injecting apparatus and method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP18822697A JP4020459B2 (en) 1997-07-14 1997-07-14 Filling confirmation method of foam-cured foam

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JP4020459B2 true JP4020459B2 (en) 2007-12-12

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JP4119237B2 (en) * 2002-12-17 2008-07-16 サンスター技研株式会社 One-component moisture-curable urethane composition that can be thermoplasticized

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