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JP4134690B2 - Hardening heat treatment method for cast iron member and hardened heat treated cast iron member - Google Patents
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JP4134690B2 - Hardening heat treatment method for cast iron member and hardened heat treated cast iron member - Google Patents

Hardening heat treatment method for cast iron member and hardened heat treated cast iron member Download PDF

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JP4134690B2
JP4134690B2 JP2002332204A JP2002332204A JP4134690B2 JP 4134690 B2 JP4134690 B2 JP 4134690B2 JP 2002332204 A JP2002332204 A JP 2002332204A JP 2002332204 A JP2002332204 A JP 2002332204A JP 4134690 B2 JP4134690 B2 JP 4134690B2
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cast iron
iron member
temperature
hardness
reheating
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JP2004162152A (en
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和幸 織田
稔夫 川上
幸夫 有見
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Mazda Motor Corp
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Mazda Motor Corp
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Description

【0001】
【発明の属する技術分野】
この発明は、例えば高面圧下で繰り返し荷重などを受けるような鋳鉄部材の硬化熱処理方法および硬化熱処理された鋳鉄部材に関する。
【0002】
【従来の技術】
一般に鋳鉄は安価な材料であって、しかも黒鉛の存在により機械加工性にも優れているため自動車用部品その他として多用されている。
しかし、近年においては小型軽量化、出力向上などにより鋳鉄材料にも高強度化が必要になっている。この強度が必要とされる部分は摺動部や応力中集中部などの局部が主である。
【0003】
鋳鉄部材の上述の如き所定部を高強度化するには一般に高周波加熱やレーザ加熱などの局部加熱処理の可能な方法が採用されている。つまり、炉加熱などの部材全体の熱処理ではエネルギ効率の面で不利となるばかりでなく、必要でない部分までもが強化されて、後加工が困難となるので、上述の局部加熱処理が採用されている。
【0004】
上述の高周波加熱などの局部加熱では、加熱後の冷却速度は加熱範囲の大小に依存し、一定ではないため、硬さも冷却速度に依存し、目標とする硬さを安定して得ることが困難である。
【0005】
従来、鋳放し、あるいは焼鈍状態の鋳鉄部材の硬さを向上させて、強度を上げる方法としては一般的に焼準処理(900℃〜950℃に加熱後常温まで放冷する焼ならし処理)が行なわれる。
【0006】
しかしながら、鋳鉄部材の必要部分のみを高周波加熱やレーザ加熱などの局部加熱手段により焼ならしする場合、オーステナイト化温度から常温までの放冷中の冷却速度により、得られる硬さが大きく変化する。
【0007】
すなわち、オーステナイト化温度からの冷却速度が早い場合には、マルテンサイトやベイナイト組織などの硬質組織の生成により、鋳鉄部材の硬さが高くなり過ぎて、後加工における被削性が劣化するという問題点が生じる。
【0008】
逆に、オーステナイト化温度からの冷却速度が遅いと、冷却中にパーライト組織が粗大化して、鋳鉄部材の硬さが低くなり過ぎて、所定の強度が得られないという問題点が生じる。
要するに従来方法においては、所定硬さを有し、均一なパーライト組織を得ることが困難であった。
【0009】
一方、球状黒鉛鋳鉄部材の熱処理方法としては次のような方法がある。
つまり、球状黒鉛鋳鉄製部品を、1173〜1323K(900〜1050℃)に高周波加熱した後に急冷することによって焼入れし、573〜823K(300〜550℃)で0.5〜2.0時間焼戻しする。また基地内に球状黒鉛が分散した形態を有する球状黒鉛鋳鉄を熱処理して得られる部品において、基地の主要組織を焼入れによるマルテンサイト組織とし、球状黒鉛の周囲をソルバイト組織によって囲んだものである(例えば特許文献1参照)。
【0010】
【特許文献1】
特開2000−265210号公報。
【0011】
【発明が解決しようとする課題】
この従来公報による熱処理方法では、あくまでも主要組織が焼入れによるマルテンサイトの組織を得るものであって、所定の硬さを有し、かつ均一なパーライト組織を得るものではない。
【0012】
この発明は、所定の硬さを有し、均一なパーライト組織を得ることができ、被削性を確保しながら耐疲労性、耐摩耗性、耐ヘタリ性を向上でき、また高周波加熱により連続的に処理することができて、短時間で必要とする処理部のみを効率よく熱処理することができる鋳鉄部材の硬化熱処理方法および硬化熱処理された鋳鉄部材の提供を目的とする。
【0013】
【課題を解決するための手段】
この発明による鋳鉄部材の硬化熱処理方法は、黒鉛を有する鋳鉄部材を高周波加熱により950〜1050℃のオーステナイト化温度に加熱した後、20℃/sec以上の冷却速度で500℃以下の温度まで冷却し、引き続き高周波加熱により550〜700℃の温度に再加熱後冷却し、処理部の硬さをビッカース硬度200〜500℃の範囲の均一なパーライト組織を得るものである。
【0014】
上記構成の黒鉛を有する鋳鉄としては、球状黒鉛鋳鉄、ねずみ鋳鉄または片状黒鉛鋳鉄の何れであってもよい。
上記構成によれば、まず黒鉛を有する鋳鉄部材の処理部(強化必要部分)が高周波加熱により950℃〜1050℃のオーステナイト化温度(通常の鋼のA、変態点726℃より比較的高い温度であり、これは炭素を拡散するために必要な温度と時間との一方の条件であって、部分加熱の場合には時間を長く設定できないので、温度により炭素の拡散を図るための値である)に加熱され、この加熱によって鋳鉄中の黒鉛から基地組織へ炭素の固溶を促進させる。
【0015】
このオーステナイト化温度への加熱後、20℃/sec以上の冷却速度で500℃以下の温度まで冷却する。この冷却によりマルテンサイト、パーライト、フェライトの混在組織になる。また500℃以下の温度まで冷却することで、粗大なパーライト組織の生成がなくなる。
【0016】
引き続き高周波加熱により550℃〜700℃の温度に再加熱冷却する。この再加熱により上述の冷却後の前組織がパーライト組織、ベイナイト組織、マルテンサイト組織の単層または、これらの混在組織であっても、基地組織を均一で微細なパーライト組織とし、処理部の硬さをHv200〜500のばらつきの僅少な安定した硬さを確保することができる。
なお、再加熱後の冷却は得られる組織や硬さに変化がなく、水冷のような速い冷却でも、または空冷のような遅い冷却でもよい。
【0017】
ここで、上述のオーステナイト化温度が950℃未満の場合には、黒鉛からの炭素固溶が不足し、その後の冷却中にフェライトが生成し始め、硬さ低下を招く。逆に、オーステナイト化温度が1050℃を超過する場合には、黒鉛からの炭素固溶が過剰となって、冷却中にセメンタイトが析出し始め、硬さが高くなり過ぎる。このため上記オーステナイト化温度を950〜1050℃の範囲とする。
【0018】
また冷却速度が20℃/secよりも遅くなると、冷却中にパーライト組織が粗大化して、硬さが低くなり過ぎ、逆に冷却速度が速くなり過ぎると、冷却後に生成される組織はパーライト組織からベイナイト組織、マルテンサイト組織へと順次変化するので、この冷却速度はマルテンサイト組織へと変化しない所定の冷却速度(50℃/sec程度まで)が望ましい。
【0019】
さらに冷却する温度を500℃以下とするのは、500℃まで冷却すると、粗大なパーライト組織の生成がなく、最終的に得られる硬さに変動がなくなるためである。
【0020】
さらにまた、上述の再加熱は均一なパーライト組織を得るものであって、混在組織を均等な硬さにする処理であり、再加熱温度が550℃未満では硬さが高くなり過ぎ、再加熱温度が700℃を超過する場合には、硬さが低くなり過ぎる。したがってHv200〜500の所定範囲の硬さを得るために再加熱温度を550℃〜700℃の範囲とするものである。
【0021】
またビッカース硬度を200〜500とするのは、Hv200未満では耐へタリ性が確保できず、逆にHv500以上では硬さが高すぎて例えば仕上げ加工時の工具劣化が顕著となるので、上記範囲内とするものである。
【0022】
このように上記構成によれば、所定の硬さを有し、均一なパーライト組織を得ることができ、被削性を確保しつつ耐疲労性、耐摩耗性、耐ヘタリ性を向上させることができ、また高周波加熱により必要とする処理部のみを連続的に処理することができて、短時間で必要とする処理部のみを効率よく熱処理することができる。
【0023】
この発明の一実施態様においては、上記再加熱の温度が600〜650℃の範囲に設定されたものである。
上記構成によれば、再加熱温度を550〜700℃の中間の値としての600〜650℃としたので、鋳造された鋳鉄部材それ自体に多少のばらつきがあっても、ビッカース硬度をHv200〜500の範囲内の中間の望ましい値と成すことができる。
【0024】
この発明の硬化熱処理された鋳鉄部材は、黒鉛を有する鋳鉄部材を高周波加熱により950〜1050℃のオーステナイト化温度に加熱した後、20℃/sec以上の冷却速度で500℃以下の温度まで冷却し、引き続き高周波加熱により550〜700℃の温度に再加熱後冷却し、処理部の硬さをビッカース硬度200〜500℃の範囲の均一なパーライト組織にしたものである。
【0025】
上記構成によれば、所定の硬さ(Hv200〜500)を有し、均一なパーライト組織を得ることができ、被削性を確保しつつ耐疲労性、耐摩耗性、耐ヘタリ性を向上させることができ、また高周波加熱により短時間で、かつ必要とする処理部のみを連続的に効率よく熱処理することができる。
【0026】
この発明の一実施態様においては、上記鋳鉄部材は球状黒鉛鋳鉄部材に設定されたものである。
上記構成によれば、オーステナイト化温度とへの加熱時に球状黒鉛が均一に固溶するので、より一層均一なパーライト組織を得ることができる。
【0027】
この発明の一実施態様においては、上記鋳鉄部材はロータリエンジンのロータに設定されたものである。
上記構成によれば、ロータの頂点にはアペックスシールを配設するアペックスシール溝部が設けられるが、このアペックスシール溝部を上記処理部に設定すると、アペックスシールとの摺動により該アペックスシール溝部が摩耗するのを防止できて、ロータの耐久性向上を図ることができる。
【0028】
【実施例】
この発明の一実施例を以下図面に基づいて詳述する。
図面は鋳鉄部材の硬化熱処理方法および硬化熱処理された鋳鉄部材を示す。この実施例では鋳鉄部材としてのロータリエンジンのロータを例示しているので、まず図1〜図3を参照して、ロータの構成およびその処理部について説明する。
【0029】
図1に示すようにロータリエンジンのロータ1は三葉の内方包絡面2…を有し、ロータ頂点部にはアペックスシール溝部3が設けられると共に、ロータ1の中心部にはトロコイド位相歯車(内歯歯車)4が形成されている。
【0030】
そして、この実施例の硬化熱処理方法により熱処理される処理部5は図2、図3に図示の便宜上ハッチングを施して示すように、アペックスシール溝部3の頂点からの深さWが2mmで、溝縁からロータ側面方向への幅L1が2mmで、アペックスシール溝の端部からエキセントリックシャフトの軸芯線方向への長さL2が4mmの溝部3のコーナ部分に設定されている。
【0031】
ここで、上述のアペックスシール溝部3には図4に示す如きアペックスシール6がスプリング(図示せず)を介して配設される。
このアペックスシール6はメインピース7と、セカンドピース8と、サイドピース9との3ピース構造のシール部材で、ロータハウジングとロータとの間に形成される作動室相互間の気密性向上を図るものである。
【0032】
また上述のロータ1の材質はFCD450の球状黒鉛鋳鉄に設定されている。
このFCD450F(球状黒鉛鋳鉄)の化学組成は、C:3.63wt%、Si:2.54wt%、Mn:0.32wt%、Mg:0.04wt%、P:0.06wt%、S:0.02wt%と残部Feおよび他の不可避の不純物が微量である。
【0033】
上述のロータ1の処理部5を高周波加熱装置(出力80KW、周波数200KHz)を用いると共に、図5に示す加熱パターンに従って硬化熱処理した。
すなわち、上述の処理部5を高周波加熱装置の加熱コイル(図示せず)によりt1=10秒間かけてオーステナイト化温度T1=950〜1050℃に加熱し、その後、冷却速度V=20℃/sec以上でt2=10〜25秒間かけて500℃以下の温度(再加熱開始温度T2参照)まで自然冷却し、引き続き高周波加熱装置の加熱コイル(図示せず)によりt3=5秒間かけて再加熱温度T3=550〜700℃の温度に再加熱した後に、水冷または空冷により冷却処理した。
【0034】
ここで、オーステナイト化温度T1、冷却速度V、再加熱開始温度T2、再加熱温度T3を上述の範囲内において若干異ならせた実施例1〜7の鋳鉄部材(ロータ1参照)と、何れかの条件を上述の範囲外と成した比較例8〜14の鋳鉄部材とのビッカース硬さを実測した結果を各種の熱処理条件と共に次の[表1]に示す。
なお、上述の硬さは処理部5の断面をビッカース硬さ(荷重5kgf)にて測定したものである。
【0035】
【表1】

Figure 0004134690
【0036】
実施例1のものは全ての熱処理条件を上下限内に設定し、実施例2のものはオーステナイト化温度T1および再加熱温度T3を下限に設定し、実施例3のものはオーステナイト化温度T1を下限に設定する一方、再加熱温度T3を上限に設定し、実施例4のものはオーステナイト化温度T1を上限に設定する一方、再加熱温度T3を下限に設定し、実施例5のものはオーステナイト化離温度T1および再加熱温度T3を上限に設定し、実施例6のものは他の実施例1〜5,7のものよりも冷却速度V=50℃/secの速い値に設定し、実施例7のものは再加熱開始温度T2を上限に設定したものである。
【0037】
上記[表1]から明らかなように、オーステナイト化温度T1、冷却速度V、再加熱開始温度T2、再加熱温度T3が上述の所定範囲の実施例1〜7のものは、ビッカース硬さが、Hv200〜500の範囲内となった。
【0038】
これに対して比較例8のものは、オーステナイト化温度がT1=900℃と低いため、炭素の固溶不足により硬さHv=195と低い値になった。
また比較例9のものは、オーステナイト化温度がT1=1100℃と高いため、炭素の固溶過剰により硬さHv=506と高い値になった。
【0039】
さらに比較例10のものは冷却速度がV=10℃/secと遅いため、パーライト組織が粗大化し、これにより硬さHv=191と低い値になった。
比較例11のものは、再加熱開始温度T2が600℃と高く、500℃以下の冷却されない時点で再加熱を開始したので、オーステナイト組織の残留と、パーライト組織の粗大化に起因して、硬さHv=193と低い値になった。
【0040】
また比較例12のものは、再加熱温度T3が500℃と低いため、マルテンサイト組織およびベイナイト組織のパーライト変態が不足し、硬さHv=513と高い値になった。
さらに比較例13のものは、再加熱温度T3が800℃と高いため、パーライト組織の凝集、粗大化により、硬さHv=172と低い値になった。
【0041】
さらにまた比較例14のものは、再加熱処理を実行しないものであって、このように再加熱を施さないものは、冷却速度が速いことに起因して、マルテンサイト組織およびベイナイト組織の生成により、硬さHv=567と高い値になった。
【0042】
すなわち、比較例8〜14のものは何れかの条件が上記範囲外となるので、硬さはHv200〜500の範囲内に収まることがなく、硬さが過小または過大となった。
【0043】
図6はロータ1のアペックスシール溝部3のヘタリ量とビッカース硬さHvとの関係を示す特性図で、Hv200〜500の範囲においてヘタリ量が望ましい値となることを示している。
【0044】
このように上記実施例の鋳鉄部材の硬化熱処理方法は、図5のその加熱パターンに示すように、黒鉛を有する鋳鉄部材(ロータ1参照)を高周波加熱により950〜1050℃のオーステナイト化温度T1に加熱した後、20℃/sec以上の冷却速度Vで500℃以下の温度T2まで冷却し、引き続き高周波加熱により550〜700℃の温度T3に再加熱後冷却し、処理部5の硬さをビッカース硬度200〜500℃の範囲の均一なパーライト組織を得るものである。
【0045】
上記構成によれば、まず黒鉛を有する鋳鉄部材(ロータ1参照)の処理部5(強化必要部分)が高周波加熱により950℃〜1050℃のオーステナイト化温度T1に加熱され、この加熱によって鋳鉄中の黒鉛から基地組織へ炭素の固溶を促進させる。
【0046】
このオーステナイト化温度T1への加熱後、20℃/sec以上の冷却速度Vで500℃以下の温度T2まで冷却する。この冷却によりマルテンサイト、パーライト、フェライトの混在組織になる。また500℃以下の温度T2まで冷却することで、粗大なパーライト組織の生成がなくなる。
【0047】
引き続き高周波加熱により550℃〜700℃の温度T3に再加熱冷却する。この再加熱により上述の冷却後の前組織がパーライト組織、ベイナイト組織、マルテンサイト組織の単層または、これらの混在組織であっても、基地組織を均一で微細なパーライト組織とし、処理部5の硬さをHv200〜500のばらつきの僅少な安定した硬さを確保することができる(表1の実施例1〜7参照)。
なお、再加熱後の冷却は得られる組織や硬さに変化がなく、水冷のような速い冷却でも、または空冷のような遅い冷却でもよい。
【0048】
ここで、上述のオーステナイト化温度T1が950℃未満の場合には、比較例8で示したように黒鉛からの炭素固溶が不足し、その後の冷却中にフェライトが生成し始め、硬さ低下を招く。逆に、オーステナイト化温度が1050℃を超過する場合には、比較例9で示したように黒鉛からの炭素固溶が過剰となって、冷却中にセメンタイトが析出し始め、硬さが高くなり過ぎる。このため上記オーステナイト化温度を950〜1050℃の範囲とする。
【0049】
また冷却速度が20℃/secよりも遅くなると、比較例10で示したように冷却中にパーライト組織が粗大化して、硬さが低くなり過ぎ、逆に冷却速度が速くなり過ぎると、比較例14で示したように冷却後に生成される組織はパーライト組織からベイナイト組織、マルテンサイト組織へと順次変化するので、この冷却速度Vはマルテンサイト組織へと変化しない所定の冷却速度が望ましい。
【0050】
さらに冷却する温度を500℃以下とするのは、500℃まで冷却すると、粗大なパーライト組織の生成がなく、最終的に得られる硬さに変動がなくなるためである。
【0051】
さらにまた、上述の再加熱は均一なパーライト組織を得るものであって、混在組織、特にマルテンサイトをパーライトに変態させて均等な硬さにする処理であり、再加熱温度が550℃未満では比較例12で示したように、硬さが高くなり過ぎ、再加熱温度が700℃を超過する場合には、比較例13で示したように硬さが低くなり過ぎる。したがってHv200〜500の所定範囲の硬さを得るために再加熱温度を550℃〜700℃の範囲とするものである。
【0052】
またビッカース硬度を200〜500とするのは、図6の特性図にも示すようにHv200未満では耐へタリ性が確保できず、逆にHv500以上では硬さが高すぎて例えば仕上げ加工時の工具劣化が顕著となるので、上記範囲内とするものである。
【0053】
このように上記構成によれば、所定の硬さ(Hv200〜500)を有し、均一なパーライト組織を得ることができ、被削性を確保しつつ耐疲労性、耐摩耗性、耐ヘタリ性を向上させることができ、また高周波加熱により必要とする処理部のみを連続的に処理することができて、短時間で必要とする処理部のみを効率よく熱処理することができる。
【0054】
さらに、上記再加熱の温度を600〜650℃の範囲に設定すると、鋳造された鋳鉄部材それ自体に多少のばらつきがあっても、ビッカース硬度をHv200〜500の範囲内の中間の望ましい値と成すことができる。
【0055】
一方、上記実施例の硬化熱処理された鋳鉄部材(ロータ1参照)は、黒鉛を有する鋳鉄部材を高周波加熱により950〜1050℃のオーステナイト化温度T1に加熱した後、20℃/sec以上の冷却速度Vで500℃以下の温度T2まで冷却し、引き続き高周波加熱により550〜700℃の温度T3に再加熱後冷却し、処理部5の硬さをビッカース硬度200〜500℃の範囲の均一なパーライト組織にしたものである。
【0056】
この構成によれば、所定の硬さ(Hv200〜500)を有し、均一なパーライト組織を得ることができ、被削性を確保しつつ耐疲労性、耐摩耗性、耐ヘタリ性を向上させることができ、また高周波加熱により短時間で、かつ必要とする処理部のみを連続的に効率よく熱処理することができる。
【0057】
しかも、上記鋳鉄部材は球状黒鉛鋳鉄部材(FCD450F参照)に設定されたものであるから、オーステナイト化温度T1とへの加熱時に球状黒鉛が均一に固溶するので、より一層均一なパーライト組織を得ることができる。
【0058】
さらに、上記鋳鉄部材はロータリエンジンのロータ1に設定されたものである。
この構成によれば、ロータ1の頂点にはアペックスシール6を配設するアペックスシール溝部3が設けられるが、このアペックスシール溝部3を上記処理部5に設定すると、アペックスシール6との摺動により該アペックスシール溝部3が摩耗するのを防止できて、ロータ1の耐久性向上を図ることができる。
【0059】
この発明の構成と、上述の実施例との対応において、
この発明の黒鉛を有する鋳鉄は、実施例の球状黒鉛鋳鉄に対応し、
以下同様に、
鋳鉄部材は、ロータリエンジンのロータ1に対応するも、
この発明は、上述の実施例の構成のみに限定されるものではない。
【0060】
例えば、黒鉛を有する鋳鉄としては上述の球状黒鉛鋳鉄の他にねずみ鋳鉄や片状黒鉛鋳鉄であってもよく、鋳鉄部材としてはロータリエンジンのロータの他に高面圧下で繰り返し荷重などを受ける他の鋳鉄部材であってもよい。
【0061】
【発明の効果】
この発明によれば、所定の硬さを有し、均一なパーライト組織を得ることができ、被削性を確保しながら耐疲労性、耐摩耗性、耐ヘタリ性を向上でき、また高周波過熱により連続的に処理することができて、短時間で必要とする処理部のみを効率よく熱処理することができる効果がある。
【0062】
【図面の簡単な説明】
【図1】 鋳鉄部材の一例としてのロータリエンジンのロータを示す斜視図。
【図2】 処理部の説明図。
【図3】 図2のA−A線矢視図。
【図4】 アペックスシールの説明図。
【図5】 鋳鉄部材の硬化熱処理方法を示す加熱パターンの説明図。
【図6】 ビッカース硬さとヘタリ量との関係を示す特性図。
【符号の説明】
1…ロータ
5…処理部[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a hardening heat treatment method for a cast iron member that receives, for example, repeated loads under high surface pressure, and a hardening iron heat-treated cast iron member.
[0002]
[Prior art]
In general, cast iron is an inexpensive material, and because of its excellent machinability due to the presence of graphite, it is frequently used as an automotive part or the like.
However, in recent years, cast iron materials have been required to have higher strength due to the reduction in size and weight and the improvement in output. The parts where this strength is required are mainly local parts such as sliding parts and stress-concentrating parts.
[0003]
In order to increase the strength of the predetermined portion of the cast iron member as described above, a method capable of local heating treatment such as high-frequency heating or laser heating is generally employed. In other words, heat treatment of the entire member such as furnace heating is not only disadvantageous in terms of energy efficiency, but also strengthens parts that are not necessary, making post-processing difficult, so the above-mentioned local heat treatment is adopted. Yes.
[0004]
In local heating such as the above-mentioned high-frequency heating, the cooling rate after heating depends on the size of the heating range and is not constant, so the hardness also depends on the cooling rate and it is difficult to stably obtain the target hardness. It is.
[0005]
Conventionally, as a method for improving the hardness by raising the hardness of an as-cast or annealed cast iron member, generally normalizing treatment (normalizing treatment in which it is heated to 900 ° C. to 950 ° C. and then allowed to cool to room temperature) Is done.
[0006]
However, when only a necessary part of the cast iron member is normalized by local heating means such as high-frequency heating or laser heating, the hardness obtained varies greatly depending on the cooling rate during cooling from the austenitizing temperature to room temperature.
[0007]
That is, when the cooling rate from the austenitizing temperature is fast, the hard iron cast becomes too hard due to the formation of hard structures such as martensite and bainite structures, and the machinability in post-processing deteriorates. A point is created.
[0008]
Conversely, when the cooling rate from the austenitizing temperature is slow, the pearlite structure becomes coarse during cooling, and the hardness of the cast iron member becomes too low, and a predetermined strength cannot be obtained.
In short, in the conventional method, it is difficult to obtain a uniform pearlite structure having a predetermined hardness.
[0009]
On the other hand, there are the following methods as a heat treatment method for the spheroidal graphite cast iron member.
That is, spheroidal graphite cast iron parts are quenched by high-frequency heating to 1173 to 1323K (900 to 1050 ° C) and then quenched, and tempered at 573 to 823K (300 to 550 ° C) for 0.5 to 2.0 hours. . Also, in a part obtained by heat treating spheroidal graphite cast iron having a form in which spheroidal graphite is dispersed in the base, the main structure of the base is a martensite structure by quenching, and the periphery of the spheroidal graphite is surrounded by a sorbite structure ( For example, see Patent Document 1).
[0010]
[Patent Document 1]
JP 2000-265210 A.
[0011]
[Problems to be solved by the invention]
In the heat treatment method according to this conventional publication, the main structure is to obtain a martensite structure by quenching, and does not have a predetermined hardness and a uniform pearlite structure.
[0012]
This invention has a predetermined hardness, can obtain a uniform pearlite structure, can improve the fatigue resistance, wear resistance, and sag resistance while ensuring machinability, and can be continuously applied by high-frequency heating. It is an object of the present invention to provide a method for hardening and heat-treating a cast iron member capable of efficiently heat-treating only a processing portion required in a short time and a cast iron member subjected to hardening and heat treatment.
[0013]
[Means for Solving the Problems]
According to the method for heat-treating a cast iron member according to the present invention, a cast iron member having graphite is heated to an austenitizing temperature of 950 to 1050 ° C. by high frequency heating, and then cooled to a temperature of 500 ° C. or less at a cooling rate of 20 ° C./sec or more. Then, it is reheated to a temperature of 550 to 700 ° C. by high-frequency heating and then cooled to obtain a uniform pearlite structure having a Vickers hardness of 200 to 500 ° C. in the treated portion.
[0014]
The cast iron having graphite having the above-described configuration may be spheroidal graphite cast iron, gray cast iron, or flake graphite cast iron.
According to the above-described configuration, first, the processing portion (required portion) of the cast iron member having graphite is subjected to high-frequency heating at an austenitizing temperature of 950 ° C. to 1050 ° C. (normal steel A, at a temperature relatively higher than the transformation point 726 ° C. Yes, this is one of the conditions of temperature and time necessary for diffusing carbon, and in the case of partial heating, the time cannot be set long, so it is a value for diffusing carbon by temperature) This heating promotes solid solution of carbon from the graphite in the cast iron to the base structure.
[0015]
After heating to this austenitizing temperature, it is cooled to a temperature of 500 ° C. or lower at a cooling rate of 20 ° C./sec or higher. This cooling results in a mixed structure of martensite, pearlite, and ferrite. Further, by cooling to a temperature of 500 ° C. or lower, generation of a coarse pearlite structure is eliminated.
[0016]
Subsequently, it is reheated and cooled to a temperature of 550 ° C. to 700 ° C. by high frequency heating. Even if the previous structure after cooling is a single layer of a pearlite structure, a bainite structure, a martensite structure, or a mixed structure thereof by this reheating, the base structure becomes a uniform and fine pearlite structure, and the hardened portion of the processing section is hardened. It is possible to secure a stable hardness with a slight variation of Hv 200 to 500.
In addition, the cooling after reheating does not change in the structure | tissue and hardness which are obtained, Fast cooling like water cooling or slow cooling like air cooling may be sufficient.
[0017]
Here, when the austenitizing temperature is less than 950 ° C., carbon solid solution from graphite is insufficient, and ferrite starts to form during the subsequent cooling, leading to a decrease in hardness. Conversely, when the austenitizing temperature exceeds 1050 ° C., carbon solid solution from graphite becomes excessive, cementite starts to precipitate during cooling, and the hardness becomes too high. For this reason, the said austenitizing temperature shall be the range of 950-1050 degreeC.
[0018]
When the cooling rate is slower than 20 ° C./sec, the pearlite structure becomes coarse during cooling, and the hardness becomes too low. Conversely, when the cooling rate becomes too fast, the structure generated after cooling is from the pearlite structure. Since the bainite structure and the martensite structure are sequentially changed, the cooling rate is preferably a predetermined cooling rate (up to about 50 ° C./sec) that does not change to the martensite structure.
[0019]
The reason why the cooling temperature is set to 500 ° C. or less is that when cooling to 500 ° C., there is no generation of coarse pearlite structure, and there is no fluctuation in the finally obtained hardness.
[0020]
Furthermore, the above-mentioned reheating is a process for obtaining a uniform pearlite structure and making the mixed structure uniform hardness. If the reheating temperature is less than 550 ° C., the hardness becomes too high, and the reheating temperature. When the temperature exceeds 700 ° C., the hardness becomes too low. Therefore, in order to obtain a hardness in a predetermined range of Hv 200 to 500, the reheating temperature is set to a range of 550 ° C to 700 ° C.
[0021]
Also, the Vickers hardness of 200 to 500 is that if the hardness is less than Hv200, the resistance to sag cannot be secured, and conversely if the hardness is Hv500 or more, the hardness is too high and, for example, tool deterioration during finishing is remarkable. It is intended to be inside.
[0022]
Thus, according to the above configuration, it is possible to obtain a uniform pearlite structure having a predetermined hardness, and improve fatigue resistance, wear resistance, and sag resistance while ensuring machinability. In addition, only the necessary processing unit can be continuously processed by high-frequency heating, and only the necessary processing unit can be efficiently heat-treated in a short time.
[0023]
In one embodiment of the present invention, the reheating temperature is set in a range of 600 to 650 ° C.
According to the above configuration, since the reheating temperature is 600 to 650 ° C. as an intermediate value of 550 to 700 ° C., even if there is some variation in the cast iron member itself, the Vickers hardness is Hv 200 to 500 The desired value can be in the middle of the range.
[0024]
The cast iron member subjected to hardening heat treatment according to the present invention is obtained by heating a cast iron member having graphite to an austenitizing temperature of 950 to 1050 ° C. by high frequency heating, and then cooling to a temperature of 500 ° C. or less at a cooling rate of 20 ° C./sec or more. Subsequently, it is cooled again after being reheated to a temperature of 550 to 700 ° C. by high-frequency heating, and the hardness of the treated portion is made into a uniform pearlite structure in the range of Vickers hardness 200 to 500 ° C.
[0025]
According to the said structure, it has predetermined hardness (Hv200-500), can obtain a uniform pearlite structure | tissue, and improves fatigue resistance, abrasion resistance, and sag resistance, ensuring machinability. In addition, it is possible to perform heat treatment continuously and efficiently only in a short time by using high-frequency heating.
[0026]
In one embodiment of the present invention, the cast iron member is a spheroidal graphite cast iron member.
According to the above configuration, since the spherical graphite is uniformly dissolved when heated to the austenitizing temperature, a more uniform pearlite structure can be obtained.
[0027]
In one embodiment of the present invention, the cast iron member is set to a rotor of a rotary engine.
According to the above configuration, the apex seal groove portion in which the apex seal is disposed is provided at the apex of the rotor. When the apex seal groove portion is set as the processing portion, the apex seal groove portion is worn by sliding with the apex seal. The durability of the rotor can be improved.
[0028]
【Example】
An embodiment of the present invention will be described below in detail with reference to the drawings.
The drawings show a method for hardening heat treatment of a cast iron member and a cast iron member subjected to hardening heat treatment. In this embodiment, a rotor of a rotary engine as a cast iron member is illustrated. First, the configuration of the rotor and its processing unit will be described with reference to FIGS.
[0029]
As shown in FIG. 1, the rotor 1 of the rotary engine has a three-leaf inner envelope surface 2..., Apex seal grooves 3 are provided at the top of the rotor, and a trochoid phase gear ( An internal gear) 4 is formed.
[0030]
The processing portion 5 to be heat-treated by the curing heat-treatment method of this embodiment has a depth W of 2 mm from the apex of the apex seal groove portion 3 as shown in FIG. 2 and FIG. The width L1 from the edge to the rotor side surface is 2 mm, and the length L2 from the end of the apex seal groove to the axial axis direction of the eccentric shaft is set to the corner portion of the groove 3.
[0031]
Here, an apex seal 6 as shown in FIG. 4 is disposed in the above-described apex seal groove 3 via a spring (not shown).
This apex seal 6 is a three-piece seal member consisting of a main piece 7, a second piece 8, and a side piece 9, which improves the airtightness between the working chambers formed between the rotor housing and the rotor. It is.
[0032]
The material of the rotor 1 is set to FCD450 spheroidal graphite cast iron.
The chemical composition of this FCD450F (spheroidal graphite cast iron) is as follows: C: 3.63 wt%, Si: 2.54 wt%, Mn: 0.32 wt%, Mg: 0.04 wt%, P: 0.06 wt%, S: 0 0.02 wt% and the balance Fe and other inevitable impurities are very small.
[0033]
The processing section 5 of the rotor 1 described above was subjected to curing heat treatment according to the heating pattern shown in FIG.
That is, the above-described processing unit 5 is heated to an austenitizing temperature T1 = 950 to 1050 ° C. over t1 = 10 seconds by a heating coil (not shown) of a high-frequency heating apparatus, and then a cooling rate V = 20 ° C./sec or more. Then, it is naturally cooled to a temperature of 500 ° C. or lower (see reheating start temperature T2) over t2 = 10 to 25 seconds, and then reheated temperature T3 over t3 = 5 seconds by a heating coil (not shown) of the high frequency heating device. After reheating to a temperature of 550 to 700 ° C., cooling treatment was performed by water cooling or air cooling.
[0034]
Here, any one of the cast iron members (see rotor 1) of Examples 1 to 7 in which the austenitizing temperature T1, the cooling rate V, the reheating start temperature T2, and the reheating temperature T3 are slightly different within the above-described range. The following [Table 1] shows the results of actual measurement of Vickers hardness with the cast iron members of Comparative Examples 8 to 14 whose conditions are out of the above range, together with various heat treatment conditions.
The above-mentioned hardness is obtained by measuring the cross section of the processing section 5 with Vickers hardness (load 5 kgf).
[0035]
[Table 1]
Figure 0004134690
[0036]
In Example 1, all heat treatment conditions are set within the upper and lower limits, in Example 2, the austenitizing temperature T1 and reheating temperature T3 are set to the lower limits, and in Example 3, the austenitizing temperature T1 is set. While the lower limit is set, the reheating temperature T3 is set to the upper limit, and in Example 4, the austenitizing temperature T1 is set to the upper limit, while the reheating temperature T3 is set to the lower limit, and in Example 5, the austenite is set. The upper limit is set at the separation temperature T1 and the reheating temperature T3, and the example 6 is set to a faster cooling rate V = 50 ° C./sec than those of the other examples 1 to 5 and 7. In Example 7, the reheating start temperature T2 is set to the upper limit.
[0037]
As is clear from the above [Table 1], the austenitizing temperature T1, the cooling rate V, the reheating start temperature T2, and the reheating temperature T3 in Examples 1 to 7 in the above-described predetermined ranges have Vickers hardness. It became in the range of Hv200-500.
[0038]
On the other hand, since the austenitizing temperature of the comparative example 8 is as low as T1 = 900 ° C., the hardness Hv = 195 is low due to insufficient solid solution of carbon.
In Comparative Example 9, since the austenitizing temperature was as high as T1 = 1100 ° C., the hardness Hv = 506 was high due to excessive solid solution of carbon.
[0039]
Furthermore, since the cooling rate of Comparative Example 10 was as low as V = 10 ° C./sec, the pearlite structure was coarsened, and thus the hardness Hv = 191 was low.
In Comparative Example 11, since the reheating start temperature T2 was as high as 600 ° C. and reheating was started when the temperature was not cooled below 500 ° C., the hardness of the austenite structure remained and the pearlite structure became coarse. Hv = 193, which is a low value.
[0040]
Moreover, since the reheating temperature T3 was as low as 500 degreeC, the thing of the comparative example 12 lacked the pearlite transformation of a martensite structure and a bainite structure, and became hardness Hv = 513 and a high value.
Furthermore, since the reheating temperature T3 of the comparative example 13 is as high as 800 ° C., the hardness Hv = 172 is low due to the aggregation and coarsening of the pearlite structure.
[0041]
Furthermore, the thing of the comparative example 14 is what does not perform a reheating process, and what does not give a reheating in this way originates in the production | generation of a martensite structure | tissue and a bainite structure | tissue due to a high cooling rate. The hardness Hv = 567 was a high value.
[0042]
That is, since any of the conditions of Comparative Examples 8 to 14 was outside the above range, the hardness did not fall within the range of Hv 200 to 500, and the hardness was too small or too large.
[0043]
FIG. 6 is a characteristic diagram showing the relationship between the amount of stickiness of the apex seal groove 3 of the rotor 1 and the Vickers hardness Hv, and shows that the amount of stickiness is a desirable value in the range of Hv 200 to 500.
[0044]
Thus, the hardening heat treatment method of the cast iron member of the above-described embodiment is, as shown in the heating pattern of FIG. 5, the cast iron member having graphite (see rotor 1) is heated to an austenitizing temperature T1 of 950 to 1050 ° C. by high frequency heating. After heating, it is cooled to a temperature T2 of 500 ° C. or less at a cooling rate V of 20 ° C./sec or more, then reheated to a temperature T3 of 550 to 700 ° C. by high frequency heating and then cooled, and the hardness of the processing unit 5 is reduced to Vickers A uniform pearlite structure having a hardness in the range of 200 to 500 ° C. is obtained.
[0045]
According to the said structure, the process part 5 (strengthening required part) of the cast iron member (refer rotor 1) which has graphite is first heated by the high frequency heating to the austenitizing temperature T1 of 950 degreeC-1050 degreeC, and this heating WHEREIN: Promotes solid solution of carbon from graphite to the matrix structure.
[0046]
After heating to this austenitizing temperature T1, it is cooled to a temperature T2 of 500 ° C. or lower at a cooling rate V of 20 ° C./sec or higher. This cooling results in a mixed structure of martensite, pearlite, and ferrite. Further, by cooling to a temperature T2 of 500 ° C. or less, generation of a coarse pearlite structure is eliminated.
[0047]
Subsequently, it is reheated and cooled to a temperature T3 of 550 ° C. to 700 ° C. by high frequency heating. Even if the previous structure after cooling is a single layer of a pearlite structure, a bainite structure, a martensite structure, or a mixed structure thereof by this reheating, the base structure is a uniform and fine pearlite structure, It is possible to ensure a stable hardness with a slight variation of Hv 200 to 500 (see Examples 1 to 7 in Table 1).
In addition, the cooling after reheating does not change in the structure | tissue and hardness which are obtained, Fast cooling like water cooling or slow cooling like air cooling may be sufficient.
[0048]
Here, when the austenitizing temperature T1 is less than 950 ° C., the carbon solid solution from graphite is insufficient as shown in Comparative Example 8, and ferrite starts to form during the subsequent cooling, resulting in a decrease in hardness. Invite. Conversely, when the austenitizing temperature exceeds 1050 ° C., the carbon solid solution from graphite becomes excessive as shown in Comparative Example 9, and cementite begins to precipitate during cooling, resulting in an increase in hardness. Pass. For this reason, the said austenitizing temperature shall be the range of 950-1050 degreeC.
[0049]
When the cooling rate is slower than 20 ° C./sec, the pearlite structure becomes coarse during cooling as shown in Comparative Example 10 and the hardness becomes too low. On the contrary, when the cooling rate becomes too high, the comparative example Since the structure generated after cooling sequentially changes from a pearlite structure to a bainite structure and a martensite structure as indicated by 14, this cooling rate V is preferably a predetermined cooling rate that does not change to a martensite structure.
[0050]
The reason why the cooling temperature is set to 500 ° C. or less is that when cooling to 500 ° C., there is no generation of coarse pearlite structure, and there is no fluctuation in the finally obtained hardness.
[0051]
Furthermore, the above-mentioned reheating is to obtain a uniform pearlite structure, and is a process of transforming the mixed structure, particularly martensite, to pearlite to obtain a uniform hardness. When the reheating temperature is less than 550 ° C., the comparison is made. As shown in Example 12, when the hardness becomes too high and the reheating temperature exceeds 700 ° C., the hardness becomes too low as shown in Comparative Example 13. Therefore, in order to obtain a hardness in a predetermined range of Hv 200 to 500, the reheating temperature is set to a range of 550 ° C to 700 ° C.
[0052]
Further, the Vickers hardness of 200 to 500 is that, as shown in the characteristic diagram of FIG. 6, the hardness resistance is not secured when it is less than Hv200, and conversely the hardness is too high at Hv500 or more. Since tool deterioration becomes remarkable, it is within the above range.
[0053]
As described above, according to the above-described configuration, a uniform pearlite structure can be obtained with a predetermined hardness (Hv 200 to 500), and fatigue resistance, wear resistance, and sag resistance are ensured while ensuring machinability. In addition, it is possible to continuously process only the processing unit required by high-frequency heating, and it is possible to efficiently heat-treat only the processing unit required in a short time.
[0054]
Further, when the reheating temperature is set in the range of 600 to 650 ° C., the Vickers hardness is set to an intermediate desired value in the range of Hv 200 to 500 even if there is some variation in the cast iron member itself. be able to.
[0055]
On the other hand, the hardened and heat-treated cast iron member of the above example (see rotor 1) is obtained by heating a cast iron member having graphite to an austenitizing temperature T1 of 950 to 1050 ° C. by high frequency heating, and then a cooling rate of 20 ° C./sec or more. V is cooled to a temperature T2 of 500 ° C. or less, and then reheated to a temperature T3 of 550 to 700 ° C. by high-frequency heating and then cooled, and the hardness of the processing unit 5 is a uniform pearlite structure having a Vickers hardness of 200 to 500 ° C. It is a thing.
[0056]
According to this structure, it has predetermined hardness (Hv200-500), can obtain a uniform pearlite structure, and improves fatigue resistance, wear resistance, and settling resistance while ensuring machinability. In addition, it is possible to perform heat treatment continuously and efficiently only in a short time by using high-frequency heating.
[0057]
Moreover, since the cast iron member is set to be a spheroidal graphite cast iron member (see FCD450F), since the spheroidal graphite is uniformly dissolved when heated to the austenitizing temperature T1, a more uniform pearlite structure is obtained. be able to.
[0058]
Further, the cast iron member is set to the rotor 1 of the rotary engine.
According to this configuration, the apex seal groove portion 3 in which the apex seal 6 is disposed is provided at the apex of the rotor 1. When the apex seal groove portion 3 is set as the processing portion 5, the apex seal groove portion 3 is slid with the apex seal 6. The wear of the apex seal groove 3 can be prevented, and the durability of the rotor 1 can be improved.
[0059]
In the correspondence between the configuration of the present invention and the above-described embodiment,
The cast iron having graphite of the present invention corresponds to the spheroidal graphite cast iron of the example,
Similarly,
The cast iron member corresponds to the rotor 1 of the rotary engine,
The present invention is not limited to the configuration of the above-described embodiment.
[0060]
For example, the cast iron having graphite may be gray cast iron or flake graphite cast iron in addition to the above-mentioned spheroidal graphite cast iron, and the cast iron member may be subjected to repeated load under high surface pressure in addition to the rotor of a rotary engine. The cast iron member may be used.
[0061]
【The invention's effect】
According to the present invention, a uniform pearlite structure having a predetermined hardness can be obtained, fatigue resistance, wear resistance, and sag resistance can be improved while securing machinability. Since it can process continuously, only the process part required in a short time can be heat-processed efficiently.
[0062]
[Brief description of the drawings]
FIG. 1 is a perspective view showing a rotor of a rotary engine as an example of a cast iron member.
FIG. 2 is an explanatory diagram of a processing unit.
FIG. 3 is a view taken along the line AA in FIG. 2;
FIG. 4 is an explanatory diagram of an apex seal.
FIG. 5 is an explanatory diagram of a heating pattern showing a hardening heat treatment method for a cast iron member.
FIG. 6 is a characteristic diagram showing the relationship between Vickers hardness and amount of settling.
[Explanation of symbols]
1 ... Rotor 5 ... Processing section

Claims (5)

黒鉛を有する鋳鉄部材を高周波加熱により950〜1050℃のオーステナイト化温度に加熱した後、20℃/sec以上の冷却速度で500℃以下の温度まで冷却し、
引き続き高周波加熱により550〜700℃の温度に再加熱後冷却し、
処理部の硬さをビッカース硬度200〜500℃の範囲の均一なパーライト組織を得る
鋳鉄部材の硬化熱処理方法。
After heating the cast iron member having graphite to an austenitizing temperature of 950 to 1050 ° C. by high frequency heating, the cast iron member is cooled to a temperature of 500 ° C. or less at a cooling rate of 20 ° C./sec or more,
Subsequently, it is cooled after reheating to a temperature of 550 to 700 ° C. by high frequency heating,
A hardening heat treatment method for a cast iron member that obtains a uniform pearlite structure having a Vickers hardness of 200 to 500 ° C. in the hardness of the processing portion.
上記再加熱の温度が600〜650℃の範囲に設定された
請求項1記載の鋳鉄部材の硬化熱処理方法。
The method of hardening heat treatment of a cast iron member according to claim 1, wherein the reheating temperature is set in a range of 600 to 650 ° C.
黒鉛を有する鋳鉄部材を高周波加熱により950〜1050℃のオーステナイト化温度に加熱した後、20℃/sec以上の冷却速度で500℃以下の温度まで冷却し、
引き続き高周波加熱により550〜700℃の温度に再加熱後冷却し、
処理部の硬さをビッカース硬度200〜500℃の範囲の均一なパーライト組織にした
硬化熱処理された鋳鉄部材。
After heating the cast iron member having graphite to an austenitizing temperature of 950 to 1050 ° C. by high frequency heating, the cast iron member is cooled to a temperature of 500 ° C. or less at a cooling rate of 20 ° C./sec or more,
Subsequently, it is cooled after reheating to a temperature of 550 to 700 ° C. by high frequency heating,
A hardened and heat-treated cast iron member having a uniform pearlite structure with a Vickers hardness in the range of 200 to 500 ° C. in the processing portion.
上記鋳鉄部材は球状黒鉛鋳鉄部材に設定された
請求項3記載の硬化熱処理された鋳鉄部材。
The hardened and heat-treated cast iron member according to claim 3, wherein the cast iron member is a spheroidal graphite cast iron member.
上記鋳鉄部材はロータリエンジンのロータに設定された
請求項3または4記載の硬化熱処理された鋳鉄部材。
The hardened and heat-treated cast iron member according to claim 3 or 4, wherein the cast iron member is set in a rotor of a rotary engine.
JP2002332204A 2002-11-15 2002-11-15 Hardening heat treatment method for cast iron member and hardened heat treated cast iron member Expired - Fee Related JP4134690B2 (en)

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