JP4831407B2 - Estimation method of permeability of porous objects using renormalization - Google Patents
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本発明は、様々なサイズの空隙を内包する不均一な多孔質物体、例えば地層のシステム全体としての実効的な浸透率を、くりこみ(renormalization)という手法を用いて、空隙サイズ分布データから推定する発明に関するものである。 The present invention estimates the effective permeability of a heterogeneous porous object, for example, a formation as a whole, containing voids of various sizes from the void size distribution data using a technique called renormalization. It relates to the invention.
地下水や石油などの地下流体は、多孔質地層の空隙に存在し、地層に井戸を掘って吸引すると、流体は圧力勾配に駆動されて空隙内部を流れて井戸に向かって移動する。多孔質地層の浸透率(単位はm2)は、一定の圧力勾配をかけたときの単位面積当たりの流速を決める量であり、井戸の生産速度を規定する経済的に重要な水理学的特性である。多孔質地層の空隙サイズデータは、浸透率を計算するために必要な量であり、核磁気共鳴法(NMR)法や、回収したコアの水銀ポロシメーター室内分析法などで計測している。 Underground fluids such as groundwater and petroleum exist in the voids of the porous formation, and when a well is dug and sucked into the formation, the fluid is driven by a pressure gradient and flows inside the void and moves toward the well. Permeability of porous formation (unit: m 2 ) is a quantity that determines the flow rate per unit area when a certain pressure gradient is applied, and is an economically important hydraulic characteristic that defines the production rate of wells. It is. The pore size data of the porous formation is an amount necessary for calculating the permeability, and is measured by a nuclear magnetic resonance (NMR) method, a mercury porosimeter indoor analysis method of the collected core, or the like.
この場合、問題となるのは天然の岩石の空隙サイズの著しい不均一性である(例えば、図3参照。)。図3は、天然の秩父産多孔質砂岩の2次元X線CT画像で、直径4mmの円柱形試料の断面図を示しており、黒い部分が空隙、灰色・白色部分が造岩鉱物である。わずか4mmの中に大小さまざまなサイズの空隙が混在しているのがわかる。
一般に、数nmサイズの空隙から数mmオーダーの空隙が、一見均一に見える数グラムの岩石試料の中に混在している。カルマン・コゼニーモデル(円柱パイプモデル)によれば、浸透率は空隙サイズの2乗できいてくる(たとえば、非特許文献1参照。)。したがって、たとえば10nmの空隙サイズから計算する浸透率と、10mmの空隙サイズから計算するそれとでは、サイズが100万倍異なるので、浸透率では1兆倍ものひらきがある。井戸の生産速度を支配する浸透率を正しく評価するためには、図3のように微視的に桁違いに広い空隙サイズをもつ多孔質岩石から、たとえば数cm〜数100mサイズでの巨視的な(実効的な)地層の浸透率を求める方法が要求される。
In general, a gap of several nanometers to a few millimeters is mixed in a rock sample of several grams that looks uniform at first glance. According to the Kalman-Cozeny model (cylindrical pipe model), the permeability is the square of the void size (see, for example, Non-Patent Document 1). Therefore, for example, the permeability calculated from the 10 nm gap size is different from that calculated from the 10 mm gap size by 1 million times, so there is a trillion times increase in the permeability. In order to correctly evaluate the permeability that governs the production rate of wells, macroscopically, for example, several centimeters to several hundred meters in size from porous rocks with microscopically wide pore sizes as shown in FIG. There is a need for a method to determine the penetration rate of the effective (effective) formation.
頻繁に使われている従来技術の一つとして、図10に示すように、核磁気共鳴センサーを井戸に降ろして坑壁を連続スキャンして、水や石油で満たされた多孔質地層のプロトン横緩和時間分布データ(空隙サイズ分布データと等価)を原位置で得て、それから地層の浸透率を推定する物理探査方法がある(たとえばK.-J. Dunn, D.J. Bergman, G.A. Latorraca著、 Nuclear Magnetic Resonance Petrophysical and Logging Applications, Pergamon, Amsterdam, 2002年)。
図10は、NMR検層の模式図であり、NMRゾンデ中に、プロトンを歳差運動させる永久磁石と、スピンを励起・検出するためのコイルが搭載されている。ゾンデを坑壁に押しつけて、ワイヤーを引き上げながら、地下水や石油で満たされた多孔質地層の坑壁表面から1.9cm奥にある感度領域(斜線部、概形は直径1.3cm, 長さ12cmの円柱)の間隙流体のプロトン横緩和時間をスキャンするものである。
As one of the conventional technologies frequently used, as shown in FIG. 10, the nuclear magnetic resonance sensor is lowered into the well and the wall of the well is continuously scanned, so that the proton profile of the porous formation filled with water or oil is obtained. There is a geophysical exploration method that obtains relaxation time distribution data (equivalent to void size distribution data) in-situ and then estimates the permeability of the formation (eg by K.-J. Dunn, DJ Bergman, GA Latorraca, Nuclear Magnetic Resonance Petrophysical and Logging Applications, Pergamon, Amsterdam, 2002).
FIG. 10 is a schematic diagram of NMR logging, in which a permanent magnet that precesses protons and a coil for exciting and detecting spin are mounted in an NMR sonde. Sensitivity area 1.9cm deep from the surface of the porous wall of the porous formation filled with groundwater or oil while pushing the sonde against the pit wall and pulling up the wire (hatched area, outline is 1.3cm in diameter and 12cm in length) The proton transverse relaxation time of the interstitial fluid is scanned.
この、いわゆる核磁気共鳴検層では、下記の(1)式または(2)式で地層の巨視的な浸透率kを推定している。
〔Schlumberger-Doll-Research法〕
〔Timur-Coates法〕
[Schlumberger-Doll-Research method]
[Timur-Coates method]
上記の両方式に共通する点は、数桁にわたって広く連続的に分布している空隙サイズの分布から、分布の面積総和(空隙率φ)と平均値(対数平均値あるいは、FFV/BFV比)という2つの統計量だけを使って地層の浸透率を推定している点である。この方式は計算量が少ないので、プロトン横緩和時間分布から浸透率を迅速に知りたい場合は役にたつ。しかし、2つの統計量だけではサイズ分布の形状をユニークに決めることはできない。図11は、2つの仮想的な空隙サイズ分布を斜線と黒で示したものである。斜線はバイモーダル分布で2つのピーク間隔が狭い。黒もバイモーダルだが、ピーク間隔は広い。斜線と黒の分布は、ともに総面積(φ)と対数平均値(T2LM)は同じであるが、あきらかに分布の形状はことなる。したがって、巨視的な浸透率が同じ値を示す保証はない。
このように、2つの統計量だけを使った(1)(2)式は、原油を貯留する砂岩や石灰岩などの特殊な地層には使えるかもしれないが、いかなる形状のサイズ分布(横緩和時間分布)にも適用できるかといえば、それは間違いである。石油の貯留岩以外の、様々な空隙構造特性を持つ自然界の地層のすべてに適用できる保証はない。実際、仮想的なデータについてではあるが、幾何平均値(対数平均値と同義)を使うと真の浸透率値を正しく計算できない例が既に報告されている(Transport in Porous Media, 4, 37-58, 1989)。
The point common to both of the above formulas is from the distribution of void sizes widely distributed over several digits, the total area of the distribution (void ratio φ) and the average value (logarithmic average value or FFV / BFV ratio) It is the point that the penetration rate of the formation is estimated using only these two statistics. Since this method requires a small amount of calculation, it is useful if you want to know the permeability quickly from the proton transverse relaxation time distribution. However, the shape of the size distribution cannot be determined uniquely using only two statistics. FIG. 11 shows two hypothetical gap size distributions with diagonal lines and black. The diagonal line is bimodal and the distance between the two peaks is narrow. Black is also bimodal, but the peak interval is wide. Both the diagonal and black distributions have the same total area (φ) and logarithmic mean (T 2LM ), but the shape of the distribution is clearly different. Therefore, there is no guarantee that the macroscopic penetration rate will show the same value.
In this way, equations (1) and (2) using only two statistics may be used for special formations such as sandstone and limestone that store crude oil, but any shape size distribution (lateral relaxation time) If it can be applied to (distribution), it is wrong. There is no guarantee that it can be applied to all natural formations with various void structure characteristics other than oil reservoirs. In fact, although it is about hypothetical data, there are already reports of cases where the true penetration value cannot be calculated correctly using the geometric mean (synonymous with logarithmic mean) (Transport in Porous Media, 4, 37- 58, 1989).
本発明は、統計物理学で使われているくりこみ(renormalization)理論を空隙構造モデルに適用し、図3のような様々なサイズの空隙を内包する不均一な多孔質物体、たとえば地層の、システム全体としての実効的な浸透率(「透水係数」ともいう。)を推定するものであって、空隙サイズ分布のすべてのデータポイントを使うことにより、面積総和と平均値の2つしか使わない従来の方法にくらべて精度良く浸透率を推定可能とすることを目的とする。 The present invention applies a renormalization theory used in statistical physics to a void structure model, and a system of heterogeneous porous objects, such as formations, including voids of various sizes as shown in FIG. The total effective permeability (also called “permeability coefficient”) is estimated. By using all the data points of the void size distribution, only the total area and the average value are used. The purpose is to make it possible to estimate the penetration rate with higher accuracy than the above method.
「くりこみ」とは,もともとは多体系の統計力学において粗視化の概念を定式化して巨視的な性質を導くための方法で、とくに臨界現象に適用されて成功をおさめている。くりこみを地下水理学における巨視的な浸透率の計算に初めて応用したのは、P.R. Kingである(Transport in Porous Media, 4, 37-58, 1989年)。 “Renormalization” was originally a method for formulating the concept of coarse-graining in the statistical mechanics of many-body systems and deriving macroscopic properties, and was especially successful when applied to critical phenomena. The first application of renormalization to the calculation of macroscopic permeability in groundwater science was P.R. King (Transport in Porous Media, 4, 37-58, 1989).
図1は、「くりこみ」の基本概念を示したもので、本発明は3次元くりこみであるが、わかりやすいように2次元の場合を示している。
今、4x4のセルからなる不均一な多孔質物体である多孔質の岩石があるとする。これが、オリジナルの岩石組織である。16個のセルの空隙サイズは異なっている。その結果、浸透率もある分布K1に従い、セルごとに異なる値(K1A, K1B,,,,,,K1P)をとる。くりこみの第1ステップは、4個のセルをサブシステムとして仮想的に考え、その4個の系の全体的な浸透率(いわば電気回路網の合成抵抗)をキルヒホッフとオームの法則を用いて厳密に解くことである。その操作を4回くりかえすと、サブシステム4個の浸透率組み合わせを得る。その結果、浸透率分布として、K2を得る(成分はK2A, K2B, K2C, K2D)。
くりこみの第2ステップでは、さらに上位の2x2スーパーサブシステムを想定して、4個のサブシステム(成分はK2A, K2B, K2C, K2D)を統合した全体的な浸透率K3を、キルヒホッフとオームの法則を用いて厳密にとく。このようなセルの粗視化による、システム全体の浸透率の推定がくりこみ操作である。実際の岩石は4x4ではなく無数のセルから構成されているので、くりこみ操作も多数回行うのが通常であり、得られた浸透率分布の列K2,K3、K4、、、が十分小さい標準偏差の分布に収束していくことを確認して、収束したその平均値をシステム全体の実効的な浸透率とみなすものである。
FIG. 1 shows the basic concept of “renormalization”. Although the present invention is a three-dimensional renormalization, a two-dimensional case is shown for easy understanding.
Suppose now that there is a porous rock that is a non-uniform porous object consisting of 4 × 4 cells. This is the original rock texture. The 16 cells have different void sizes. As a result, the permeation rate also takes a different value (K1 A , K1 B ,,,,,, K1 P ) for each cell according to a certain distribution K1. In the first step of renormalization, four cells are virtually considered as subsystems, and the total penetration rate (so-called combined resistance of the electric network) of the four systems is strictly calculated using Kirchhoff and Ohm's law. It is to solve. If the operation is repeated four times, a penetration rate combination of four subsystems is obtained. As a result, as a penetration index, obtain K2 (component K2 A, K2 B, K2 C , K2 D).
In the second step of renormalization, assuming an upper 2 × 2 super subsystem, the overall penetration rate K3, which integrates four subsystems (components are K2 A , K2 B , K2 C , K2 D ), Strictly using Kirchhoff and Ohm's law. The estimation of the permeability of the entire system by such coarse-grained cell is a renormalization operation. Since the actual rock is composed of an infinite number of cells instead of 4x4, the renormalization operation is usually carried out many times, and the columns K2, K3, K4, etc. of the obtained permeability distribution are sufficiently small in standard deviation. Is confirmed to converge to the distribution, and the average value converged is regarded as the effective penetration rate of the entire system.
図2に基づいて、くりこみによる具体的な浸透率の計算方法を説明する。
図1の4x4の2次元のオリジナルシステムを例にとると、2x2=4個のセルごとにくりこみ操作を行う。たとえば、K1A, K1B, K1E, K1Fの浸透率をもつ4個のセルについていえば、各セルを抵抗値1/K1A, 1/K1B, 1/K1E, 1/K1Fの電気抵抗値をもつ素子と見なす。なお、抵抗値は流れにくさの指標であり、浸透率は流れやすさの指標なのでお互いに逆数の関係にある点に注意する。さらに、セル間の接続を可能にするため、たとえばK1Aのセルは、抵抗値1/2K1Aの素子4個に細分し、図2(b)のように組み上げて、4種類の電気抵抗値をもつ合計16個の抵抗素子からなる電気回路ネットワークを形成する。図2(c)のように、この回路に仮想的に電流を流すことを考え、回路全体の合成抵抗値, 1/K2A, をキルヒホッフとオームの法則を用いて厳密に解く。その結果、
Taking the 4 × 4 two-dimensional original system of FIG. 1 as an example, a renormalization operation is performed every 2 × 2 = 4 cells. For example, in the case of four cells having permeability of K1 A , K1 B , K1 E , K1 F , each cell has a resistance value 1 / K1 A , 1 / K1 B , 1 / K1 E , 1 / K1 F It is regarded as an element having an electrical resistance value of. Note that the resistance value is an index of difficulty in flowing, and the permeability is an index of ease of flowing, so they are in a reciprocal relationship with each other. Further, for enabling connections between cells, for example cells of K1 A is subdivided into four elements in the resistance 1 / 2K1 A, and assembled as shown in FIG. 2 (b), 4 types of electrical resistance To form an electric circuit network consisting of a total of 16 resistive elements. As shown in FIG. 2C, considering that a current is virtually passed through this circuit, the combined resistance value of the entire circuit, 1 / K2 A , is solved exactly using Kirchhoff and Ohm's law. as a result,
上記した精度良く浸透率を推定可能とすることを達成するため、本発明のくりこみを用いた様々なサイズの空隙を内包する不均一な多孔質物体の浸透率の推定方法において、推定対象となる前記多孔質物体の空隙率φと空隙サイズdの分布データを計測し、空隙サイズdの分布からランダムにデータを多数選び、以下の(4)式から浸透率kを計算してオリジナルの浸透率分布K1を作成し、該オリジナルの浸透率分布K1をくりこみ操作によって次第に小さな標準偏差の分布に収束させ、その平均値を推定対象となる前記多孔質物体全体の浸透率とすることを特徴としている。
本発明は、上記の手段を採用することにより、以下のような優れた効果を奏する。
(1)数桁にわたって広く分布している空隙サイズの分布から、たった2つの統計量(面積と平均値)しか抽出していない従来の核磁気共鳴法では石油の貯留岩(砂岩及び石灰岩など)の特殊な地層にしか使えないのに比較して、本発明は、様々な空隙構造をもつ自然界の多孔質物体のすべてに適用可能である。
(2)従来の核磁気共鳴法に比べて、格段に真の浸透率の値(実測値)に近い値を得ることができる。
By adopting the above-mentioned means, the present invention has the following excellent effects.
(1) In the conventional nuclear magnetic resonance method, which extracts only two statistics (area and average value) from the distribution of pore sizes widely distributed over several digits, oil storage rocks (sandstone, limestone, etc.) The present invention is applicable to all of the natural porous objects having various void structures, as compared to that which can only be used for a specific formation.
(2) Compared to the conventional nuclear magnetic resonance method, it is possible to obtain a value that is much closer to the true permeability value (actually measured value).
本発明に係るくりこみを用いた多孔質物体の浸透率の推定方法を実施するための最良の形態を実施例に基づいて図面を参照して以下に説明する。 The best mode for carrying out the method for estimating the permeability of a porous object using renormalization according to the present invention will be described below with reference to the drawings based on the embodiments.
くりこみ理論を使うために、まず、図4に示すようにくりこみのための空隙構造モデル(パイプモデル)を作った。多孔質セル1は、一辺の長さがLの立方体とし、これが、図1の4x4個のオリジナルセルの一個一個に相当する。各セル1には、この図のように3方向に直交して走るまっすぐなパイプ2の群が埋め込まれている。各方向に走っているパイプ2の数は同じとする。パイプ2の中を流体が低いレイノルズ数で流れる。パイプ2の直径dは、セル1ごとには異なるが一つのセル内では共通な値をとる。セル1の空隙率φはdによらずすべてのセルで共通である。すなわち、セルとして十分大きなL値のモデルを想定した場合、すべてのセルで空隙率が共通な値φ(中心極限定理で収束した値)をとることができる。 In order to use the renormalization theory, a void structure model (pipe model) for renormalization was first created as shown in FIG. The porous cell 1 is a cube with a side length of L, which corresponds to each of the 4 × 4 original cells in FIG. Each cell 1 is embedded with a group of straight pipes 2 that run orthogonal to three directions as shown in this figure. The number of pipes 2 running in each direction is the same. The fluid flows through the pipe 2 at a low Reynolds number. The diameter d of the pipe 2 is different for each cell 1, but takes a common value in one cell. The porosity φ of the cell 1 is common to all the cells regardless of d. That is, assuming a sufficiently large L value model as a cell, the value φ (a value converged by the central limit theorem) having a common porosity in all cells can be taken.
ちなみに、K. Xu, J-F Daian, and D. Quenard の提出した空隙構造モデル(Transport in Porous Media, 26, 51-73, 1997年)は、数学的な処理の効率性を追求するあまり、現実的でない空隙構造モデルを採用したので不自然である。たとえば、彼らはセルサイズLの分布がべき乗であることを仮定し、さらにLとdの比率が一定であるという前提条件を設けている。しかし、これは、現実の多孔質岩石の3次元空隙構造に関する最近の研究(Lindquist他、Journal of Geophysical Research, 105, 21509-21527, 2000年)から明らかなように、現実とは矛盾する内容である。一方当該特許は、このような非現実的な仮定は設けていないので、より現実に則したモデルといえる。 By the way, the void structure model submitted by K. Xu, JF Daian, and D. Quenard (Transport in Porous Media, 26, 51-73, 1997) is too realistic to pursue the efficiency of mathematical processing. It is unnatural because a void structure model is used. For example, they assume that the distribution of cell size L is a power, and further make the precondition that the ratio of L and d is constant. However, this is inconsistent with reality, as is clear from recent research on the three-dimensional void structure of real porous rocks (Lindquist et al., Journal of Geophysical Research, 105, 21509-21527, 2000). is there. On the other hand, the patent does not make such an unrealistic assumption, so it can be said that the model is more realistic.
くりこみ法による浸透率の推定の手順は以下のとおりである。 The procedure for estimating permeability by the renormalization method is as follows.
手順(1):
空隙率と空隙サイズ分布データを計測する。たとえば回収したコアを水銀ポロシメーターで分析する。あるいは、NMR検層を行って横緩和時間の分布を得る。ただしNMR検層の生データは横緩和時間分布であってサイズ分布ではないので、たとえばコア試料を使って岩石のプロトン表面緩和率 (surface relaxivity),ρ2, を計測して横緩和時間, T2, をサイズ分布に換算する必要がある(たとえばK.-J. Dunn, D.J. Bergman, G.A. Latorraca著、 Nuclear Magnetic Resonance Petrophysical and Logging Applications, Pergamon, Amsterdam, 2002年)。ここでは、図4に示す円柱パイプを仮定しているので、d = 4T2ρ2という式で換算した。
Procedure (1):
Measure porosity and void size distribution data. For example, the collected core is analyzed with a mercury porosimeter. Alternatively, NMR logging is performed to obtain a transverse relaxation time distribution. However, since the raw data of the NMR logging is a transverse relaxation time distribution and not a size distribution, for example, using a core sample, the proton surface relaxation rate (ρ 2 ) of rock is measured to measure the transverse relaxation time, T2 , Must be converted to a size distribution (eg, K.-J. Dunn, DJ Bergman, GA Latorraca, Nuclear Magnetic Resonance Petrophysical and Logging Applications, Pergamon, Amsterdam, 2002). Here, since it is assumed the cylindrical pipe shown in FIG. 4, converted by the expression d = 4T2ρ 2.
手順(2):
空隙サイズdの分布からランダムにデータを多数選び、(4)式で与えられる浸透率kを計算し、浸透率の分布をつくる。これが、図1のオリジナル浸透率データセットK1に相当する。
Procedure (2):
A large number of data are selected at random from the distribution of the gap size d, and the permeability k given by the equation (4) is calculated to create a permeability distribution. This corresponds to the original permeability data set K1 in FIG.
手順(3):
図1の概念で、3次元セルのくりこみシミュレーションを行う。2x2x2個からなる3次元立方体サブシステムについて、この8個からなる系の全体的な浸透率(いわば電気回路網の合成抵抗)をキルヒホッフとオームの法則を用いて厳密に解く。詳細な計算方法は、Transport in Porous Media, 4, 37-58, 1989年)に従う。広い標準偏差を持つオリジナルの浸透率分布K1がくりこみ操作によって次第に小さな標準偏差の分布に収束していく様子を計算機上でモニタリングしながら、十分な精度まで収束したと判断したらそこでくりこみ操作を終了して、その平均値をシステム全体の実効的な浸透率とみなす。
Procedure (3):
A renormalization simulation of a three-dimensional cell is performed with the concept of FIG. For a 2 × 2 × 2 three-dimensional cubic subsystem, the overall permeability of the eight system (the combined resistance of the electrical network) is solved exactly using Kirchhoff and Ohm's law. Detailed calculation method follows Transport in Porous Media, 4, 37-58, 1989). While monitoring on the computer how the original permeability distribution K1 with a wide standard deviation gradually converges to a small standard deviation distribution by the renormalization operation, if it is determined that it has converged to a sufficient accuracy, the renormalization operation is terminated. The average value is regarded as the effective penetration rate of the entire system.
〔実験例〕
2つの多孔質砂岩と1つの多孔質溶岩について、水銀ポロシメーターによる空隙サイズ分布データから本発明のくりこみ手法で浸透率を推定した。また比較のため、従来の核磁気共鳴法、つまり(1)式および(2)式、による浸透率推定も行った。結果は表1に示す。
(1)埼玉県秩父産の砂岩(図3)は、空隙率φ=0.14であり、プロトン表面緩和率(ρ2= 5.6x10-5 m/s)や浸透率の実測値などのデータは「Y. Nakashima, T. Nakano, K. Nakamura, K. Uesugi, A. Tsuchiyama, and S. Ikeda 著(2004年) Journal of Contaminant Hydrology, 74, 253-264」で開示されている。水銀ポロシメーター実験による空隙サイズdの分布データを図6にしめす。縦軸は岩石試料1gあたりの空隙体積である。図6のdをd = 4T2ρ2という式で換算した横緩和時間分布について解析した結果、FFV = 0.0155, BFV = 0.1245, T2LM = 2.61 msであった。
(2)秋田県澄川産の安山岩質溶岩は、澄川地熱発電所の構内でボーリングして地下57.3mから採取したコア由来のものである。空隙率φ=0.0286であり、コアの透水試験の実測値は3x10-19 m2である。水銀ポロシメーター実験による空隙サイズdの分布データを図7にしめす。縦軸は岩石試料1gあたりの空隙体積である。水銀ポロシメーターで計測した空隙サイズ分布をNMR横緩和時間に換算する時に必要なプロトン表面緩和率ρ2は9.5x10-4 m/sである。その結果、図7のdをd = 4T2ρ2という式で換算した横緩和時間分布について解析した結果、FFV = 0, BFV = 0.0286, T2LM = 0.0143 msであった。
[Experimental example]
For two porous sandstones and one porous lava, the permeability was estimated by the renormalization technique of the present invention from the void size distribution data by a mercury porosimeter. For comparison, the permeability was estimated by the conventional nuclear magnetic resonance method, that is, the equations (1) and (2). The results are shown in Table 1.
(1) Sandstone produced in Chichibu, Saitama Prefecture (Fig. 3) has a porosity of φ = 0.14. Data such as proton surface relaxation rate (ρ 2 = 5.6x10 -5 m / s) and measured values of permeability are “ Y. Nakashima, T. Nakano, K. Nakamura, K. Uesugi, A. Tsuchiyama, and S. Ikeda (2004) Journal of Contaminant Hydrology, 74, 253-264. The distribution data of the void size d by the mercury porosimeter experiment is shown in FIG. The vertical axis represents the void volume per gram of rock sample. The d in FIG. 6 d = 4T2ρ 2 results of analysis for the transverse relaxation time distribution converted by the expression, FFV = 0.0155, BFV = 0.1245 , was T 2LM = 2.61 ms.
(2) Andesitic lava from Sumikawa, Akita Prefecture, is derived from the core taken from 57.3m underground by drilling on the premises of the Sumikawa geothermal power plant. The porosity is φ = 0.0286, and the measured value of the core permeability test is 3 × 10 −19 m 2 . FIG. 7 shows distribution data of the gap size d by the mercury porosimeter experiment. The vertical axis represents the void volume per gram of rock sample. The proton surface relaxation rate ρ 2 required when converting the pore size distribution measured by the mercury porosimeter into the NMR transverse relaxation time is 9.5 × 10 −4 m / s. As a result, a result of analysis for the transverse relaxation time distribution converted by the expression to d in FIG. 7 d = 4T2ρ 2, FFV = 0, BFV = 0.0286, was T 2LM = 0.0143 ms.
秩父産砂岩に関するシミュレーション結果を図9の(a)〜(e)にしめす。ヒストグラムの縦軸は浸透率データの数。横軸は、浸透率の値(単位は10-15 m2)。K2,K3、K4,K8の各ヒストグラムのデータ点の総数は7000個。ヒストグラムの算術平均値と標準偏差も書き込んである(単位は10-15 m2)。非常に広いオリジナル浸透率分布(K1)が、くりこみ操作を繰り返すごとに標準偏差が小さくなっていく様子がわかる。この場合では、7回くりこみを行うと十分小さな標準偏差になることがわかり、その分布K8の平均値1.32x10-15 m2 ≒1x10-15 m2をもって浸透率の推定値とした。 The simulation results for Chichibu sandstone are shown in Fig. 9 (a) to (e). The vertical axis of the histogram is the number of penetration data. The horizontal axis is the permeability value (unit: 10 -15 m 2 ). The total number of data points in each histogram of K2, K3, K4, and K8 is 7000. The arithmetic mean and standard deviation of the histogram are also written (unit is 10 -15 m 2 ). It can be seen that the standard deviation of the very wide original permeability distribution (K1) decreases as the renormalization operation is repeated. In this case, notice that becomes sufficiently small standard deviation is performed seven times renormalization, and with a mean 1.32x10 -15 m 2 ≒ 1x10 -15 m 2 of the distribution K8 and the estimated value of the penetration rate.
[実験結果の考察]
上記3つの岩石試料について、本発明のくりこみ手法と従来のNMR法((2)式のSDR法と(3)式のTimur-Coates法)による推定結果の比較を表1に総括した。表1から明らかなように、本発明の推定値は、埼玉県秩父産の砂岩と秋田県澄川産の安山岩質溶岩について、従来の核磁気共鳴法による推定値よりも格段に真の値(実測した浸透率値)に近くでた。NMR法をくりこみ法と比べてみると、ベレア産の砂岩についてはSDR法はくりこみ法とかろうじて同じ推定値を出したものの、それ以外のケースでは、桁違いに推定精度が悪いといえる。秩父産砂岩の推定精度は、真の値(実測値)より1桁食い違っている。しかし、天然の地層は、本来約10-21 m2から約10-10m2まで10桁以上の広い不確定性をもっているものである。したがって、くりこみ法による秩父産砂岩の推定が真の値からのズレをわずか1桁に押さえることができたのは、許容できる誤差といえる。このように、3つの試料をもちいた実例によって、当該特許の有効性が確認された。
[Consideration of experimental results]
Table 1 summarizes the comparison of estimation results for the above three rock samples by the renormalization method of the present invention and the conventional NMR method (SDR method of equation (2) and Timur-Coates method of equation (3)). As is clear from Table 1, the estimated values of the present invention are much more true for sandstones from Chichibu, Saitama and andesitic lava from Sumikawa, Akita than the values estimated by the conventional nuclear magnetic resonance method (actual measurements). Was close to the permeability value). Comparing the NMR method with the renormalization method, the SDR method barely gave the same estimation value as the renormalization method for the sandstones from Bellaire, but in other cases, the estimation accuracy was extremely low. The estimated accuracy of Chichibu sandstone differs by an order of magnitude from the true value (actual measurement). However, natural strata have inherently uncertainties of more than 10 orders of magnitude from about 10 -21 m 2 to about 10 -10 m 2 . Therefore, it can be said that it is an acceptable error that the estimation of the Chichibu sandstone by the renormalization method was able to suppress the deviation from the true value to only one digit. Thus, the effectiveness of the patent was confirmed by an example using three samples.
1 セル
2 パイプ
3 3次元ランダム多孔質物体
1 cell 2 pipe 3 3D random porous object
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