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JP4866095B2 - Production method of flame-retardant tobacco - Google Patents
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JP4866095B2 - Production method of flame-retardant tobacco - Google Patents

Production method of flame-retardant tobacco Download PDF

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JP4866095B2
JP4866095B2 JP2006035300A JP2006035300A JP4866095B2 JP 4866095 B2 JP4866095 B2 JP 4866095B2 JP 2006035300 A JP2006035300 A JP 2006035300A JP 2006035300 A JP2006035300 A JP 2006035300A JP 4866095 B2 JP4866095 B2 JP 4866095B2
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tobacco
flame
retardant
cut
tobacco cut
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JP2007209302A (en
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和幸 鈴木
勝秀 横田
康信 井上
信康 遠藤
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Japan Tobacco Inc
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Description

本発明は、難燃性であることにより軽い喫味を呈するタバコ刻の製造方法に関する。   The present invention relates to a method for producing a tobacco cut that exhibits a light taste by being flame retardant.

近年、軽い(マイルドな)喫味を呈するシガレットを好む傾向が強まっている。軽い喫味を呈するシガレットは、主に、膨化させたタバコ刻を用いて製造されている。   In recent years, there is an increasing tendency to prefer cigarettes that exhibit a light (mild) taste. Cigarettes with a light taste are mainly produced using expanded tobacco cuts.

例えば、特許文献1には、液体二酸化炭素にタバコ材料を浸漬してタバコ材料に液体二酸化炭素を含浸させ、含浸した液体二酸化炭素を固体二酸化炭素に変換させた後、高温下で固体二酸化炭素を蒸発させてタバコ組織を膨化させる方法が開示されている。また、特許文献2には、二酸化炭素をガス状でタバコ材料に含浸させた後、これを急速加熱することによってタバコ材料を膨化させる方法が開示されている。   For example, in Patent Document 1, a tobacco material is immersed in liquid carbon dioxide to impregnate the tobacco material with liquid carbon dioxide, the impregnated liquid carbon dioxide is converted into solid carbon dioxide, and then solid carbon dioxide is converted at a high temperature. A method of evaporating to expand tobacco tissue is disclosed. Patent Document 2 discloses a method of expanding tobacco material by impregnating tobacco material in gaseous form with carbon dioxide and then rapidly heating it.

しかしながら、このような手法を用いる膨化タバコ刻は、コスト高となり、また柔らかいため堅牢性に劣り、シガレットに巻き上げる際に支障をきたすおそれがある。
特公昭56−50830号公報 特公昭56−50952号公報
However, a puffed tobacco using such a method is costly and soft, so it is inferior in robustness and may cause trouble when it is wound up on a cigarette.
Japanese Patent Publication No. 56-50830 Japanese Patent Publication No.56-50952

したがって、本発明は、軽い喫味を呈しながら、十分な堅牢性を有する難燃性タバコ刻の製造方法を提供することを目的とする。   Accordingly, an object of the present invention is to provide a method for producing a flame-retardant cigarette having sufficient fastness while exhibiting a light taste.

本発明者らは、軽い喫味を呈するタバコ刻について鋭意検討する中で、タバコ刻を難燃性とすることにより、喫味が緩和されることに着目した。難燃性であれば、燃焼量が低減し、結果喫味が軽いものとなる。さらに研究を進めた結果、通常のタバコ刻をより高密度化するか、厚さをより厚くすることにより難燃化が図られると同時に堅牢性も十分なタバコ刻が得られることを見いだした。本発明は、かかる知見に基づく。   The inventors focused on the fact that the taste is alleviated by making the tobacco incombustible while intensively studying the tobacco inscription that exhibits a light taste. If it is flame retardant, the amount of combustion is reduced and the result is light. As a result of further research, we have found that by increasing the density of ordinary cigarettes or increasing the thickness of the cigarettes, flame retardancy can be achieved and at the same time sufficient cigarettes can be obtained. The present invention is based on such knowledge.

本発明によると、原料タバコ刻を、製茶揉捻機による揉捻処理に供した後、再乾処理もしくは精揉処理または水乾処理に供することを特徴とする難燃性タバコ刻の製造方法が提供される。
According to the present invention, there is provided a method for producing a flame-retardant tobacco cut, characterized in that the raw tobacco cut is subjected to a twisting process by a tea making machine and then subjected to a re-drying process, a koji process or a water-drying process. The

本発明によれば、難燃性であることにより軽い喫味を呈するとともに堅牢性に優れたタバコ刻を製造することができる。   According to the present invention, it is possible to produce a tobacco cut that has a light taste due to its flame retardancy and is excellent in fastness.

本発明では、タバコ刻をより高密度化するか、厚さをより厚くするために、製茶で用いられている技術を利用する。すなわち、原料タバコ刻を、揉捻処理した後、再乾処理もしくは精揉処理または水乾処理に供する。   In the present invention, a technique used in tea making is used to increase the density of the tobacco cut or to increase the thickness. That is, the raw tobacco cut is subjected to a twisting process and then subjected to a re-drying process, a koji process or a water drying process.

原料タバコ刻は、常法に従い、ラミナタバコを状態調整(コンディショニング)により、水分を18重量%(湿基準)に調整し、蔵置し、水蒸気により水分を18%〜20重量%(湿基準)に調湿した後、裁刻することによって得られる。このようにして得られる原料タバコ刻は、0.1〜0.2mm程度の厚さと、0.8mm〜1mmの幅を有する。また、原料タバコ刻は、通常、0.40〜1.0g/cm3の密度を有する。 In accordance with the conventional method, the raw tobacco is adjusted to 18% by weight (humidity standard) by laminating tobacco (conditioning), stored, and adjusted to 18-20% by weight (humidity standard) with water vapor. It is obtained by slicing after wetting. The raw tobacco cut thus obtained has a thickness of about 0.1 to 0.2 mm and a width of 0.8 mm to 1 mm. Moreover, the raw material tobacco cut usually has a density of 0.40 to 1.0 g / cm 3 .

本発明では、上記のように裁刻して得られる0.2mm程度の厚さと、0.8mm〜1mmの幅を有するタバコ刻(原料タバコ刻)を所定の処理に供するが、その前にまず、原料タバコ刻を水蒸気で加湿することが好ましい。この加湿は、原料タバコ刻の水分が22〜26重量%(湿基準)となるように行うことが好ましい。   In the present invention, a cigarette carved (raw material cigarette carved) having a thickness of about 0.2 mm obtained by cutting as described above and a width of 0.8 mm to 1 mm is subjected to a predetermined treatment. It is preferable to humidify the raw tobacco with steam. This humidification is preferably performed so that the moisture of the raw tobacco is 22 to 26% by weight (humid basis).

次に加湿した原料タバコ刻を揉捻処理に供する。揉捻処理は、製茶の分野で周知のものであり、揉捻機を用いて行われる。揉捻機は、基本的に、揉盤と、揉盤上を回動可能に設けられた揉捻鉢と、揉圧盤とを備え、揉圧盤に揉圧を印加するものである。そのような揉捻機は、例えば、特開平11−346655号公報、特開2001−29013号公報、特開2001−45972号公報、特開2001−231449号公報、特開2002−119208号公報等多数の特許文献に開示されており、また市販もされている。本発明では、この製茶用の揉捻機をそのまま使用することができる。すなわち、上記加湿した原料タバコ刻を鉢体に入れ、揉盤に受け、揉圧盤を設置して揉圧を印加する。揉捻処理では、製茶での揉捻処理と同様、原料タバコ刻を加熱しない。   Next, the humidified raw material tobacco is subjected to a twisting process. The twisting process is well known in the field of tea making and is performed using a twisting machine. The scissor is basically provided with a scissors, a scissor bowl provided so as to be rotatable on the scissors, and a scissors, and applies a scissors pressure to the scissors. Such a twisting machine includes, for example, JP-A-11-346655, JP-A-2001-29013, JP-A-2001-45972, JP-A-2001-231449, and JP-A-2002-119208. In the patent literature, and is also commercially available. In the present invention, this tea making machine can be used as it is. That is, the humidified raw material tobacco cut is put into a pot body, received by a chopping board, and a heel pressure board is installed to apply a heel pressure. In the twisting process, as in the twisting process in tea making, the raw tobacco cut is not heated.

次に、揉捻処理した原料タバコ刻を再乾処理もしくは精揉処理または水乾処理に供する。   Next, the raw tobacco cut subjected to the twisting process is subjected to a re-drying process, a refinement process, or a water-drying process.

再乾処理もしくは精揉処理は、製茶の分野で周知の技術であり、再乾機もしくは精揉機を用いて行われる。再乾機は、熱風による回転乾燥機の一種であり、精揉機は、揉捻処理した原料タバコ刻を伸直な形状に整形しつつ乾燥させるものである。再乾処理もしくは精揉処理により原料タバコ刻の厚さは有意に変化しないものの、タバコ刻の密度が大きくなる。再乾処理もしくは精揉処理により得られるタバコ刻は、密度が0.9〜1.5g/cm3まで増加し得る。再乾処理もしくは精揉処理は、60〜100℃の温度で行うことができる。処理時間は、20〜60分程度である。 The re-drying process or the koji process is a well-known technique in the field of tea making and is performed using a re-drying machine or a koji machine. The redrying machine is a kind of rotary drier using hot air, and the precision milling machine dries the twisted raw tobacco cut into a straight shape while drying it. Although the thickness of the raw tobacco cut does not change significantly due to the re-drying process or the milling process, the density of the tobacco cut increases. Tobacco chops obtained by re-drying or milling can increase in density to 0.9-1.5 g / cm 3 . The re-drying process or the koji process can be performed at a temperature of 60 to 100 ° C. The processing time is about 20 to 60 minutes.

水乾処理は、回転乾燥機の一種であり、揉捻処理した原料タバコ刻同士を互いに絡ませ合わせ、球状に整形するものである。水乾処理により原料タバコ刻の密度は、有意に変化しないものの、タバコ刻の厚さが増大する。水乾処理により得られるタバコ刻は、厚さが0.5mm〜8mmまで増加し得る。ここで、タバコ刻の厚さは、各試料の裁刻されていない面と面との間の長さである。水乾処理は、100〜250℃の温度で行うことができる。処理時間は、20〜60分程度である。   The water-drying process is a kind of rotary drier, in which twisted raw tobacco pieces are entangled with each other and shaped into a spherical shape. Although the density of the raw tobacco cut does not change significantly by the water drying process, the thickness of the tobacco cut increases. The tobacco cut obtained by the water-drying process can increase in thickness from 0.5 mm to 8 mm. Here, the thickness of the tobacco cut is the length between the uncut surfaces of each sample. The water drying treatment can be performed at a temperature of 100 to 250 ° C. The processing time is about 20 to 60 minutes.

上に述べたように、本発明により原料タバコ刻を揉捻処理する前に、原料タバコを加湿することが好ましいが、揉捻処理後に再乾処理または精揉処理を行う場合には、原料タバコを加湿した後、グリセリンを添加することが好ましい。グリセリンを添加することにより再乾処理または精揉処理がより一層円滑に行われ、密度の増大が図られる。グリセリンは、0.1〜20.0重量%(湿基準)の割合で原料タバコ刻に含まれるように添加することが好ましい。また、揉捻処理後に水乾処理を行う場合には、原料タバコを加湿した後、グリセリンを添加するとともにさらに水を添加することが好ましい。グリセリンと水を添加することにより、水乾処理がより一層円滑に行われ、球状整形による厚さの増大が図られる。グリセリンおよび追加の水は、それぞれ、0.1〜20重量%(湿基準)および0.1〜20重量%(湿基準)の割合で原料タバコ刻に含まれるように添加することが好ましい。   As described above, it is preferable to humidify the raw material tobacco before twisting the raw tobacco according to the present invention. However, when the re-drying process or the sperm treatment is performed after the twisting process, the raw tobacco is humidified. After that, it is preferable to add glycerin. By adding glycerin, the re-drying process or the koji process is performed more smoothly, and the density is increased. It is preferable to add glycerin at a ratio of 0.1 to 20.0% by weight (wet basis) so as to be included in the raw tobacco. Moreover, when performing a water-drying process after a twisting process, after humidifying raw material tobacco, it is preferable to add water while adding glycerol. By adding glycerin and water, the water-drying process is performed more smoothly, and the thickness is increased by spherical shaping. Glycerin and the additional water are preferably added so as to be included in the raw tobacco cut at a ratio of 0.1 to 20% by weight (wet basis) and 0.1 to 20% by weight (wet basis), respectively.

本発明の方法により得られるタバコ刻は、密度が増大し、あるいは厚さが増加しているので、タバコ刻の体積当たりの表面積が減少し、それによりシガレット吸煙時のタバコ刻の燃焼量が減少し、すなわち元の原料タバコ刻よりも難燃性となる。難燃性であるから、喫味も軽くなり、併せてCOの発生量も減少する。しかも、本発明により得られるタバコ刻は、密度または厚さが増大しているので、シガレット巻き上げも支障なく行うことができる。   Since the tobacco cut obtained by the method of the present invention has an increased density or increased thickness, the surface area per volume of tobacco cut is reduced, thereby reducing the amount of tobacco burned when smoking cigarettes. In other words, it is more flame retardant than the original raw tobacco. Since it is flame retardant, the taste is lightened and the amount of CO generated is also reduced. In addition, since the density or thickness of the tobacco cut obtained according to the present invention is increased, the cigarette can be wound up without any trouble.

次に、本発明を実施例により説明するが、本発明はこれら実施例に限定されるものではない。   EXAMPLES Next, although an Example demonstrates this invention, this invention is not limited to these Examples.

なお、以下の実施例で用いた揉捻機、精揉機、再乾機および水乾機は、それぞれ(株)寺田製作所製のものであり、揉捻機は、型式EJ−200型であり、精揉機は、型式EH−2000型であり、再乾機は、型式EC−2000型であり、水乾機は、型式IR−10相当型であった。また、タバコ刻の密度は、水銀法見かけ密度測定器を用いて各試料について3点測定し、平均した。タバコ刻の厚さは、マイクロメータを用いて各試料について10点測定し、平均した。   In addition, the twisting machine, the scouring machine, the re-drying machine, and the water drying machine used in the following examples are manufactured by Terada Manufacturing Co., Ltd., and the twisting machine is a model EJ-200 type. Was model EH-2000, the re-dryer was model EC-2000, and the water dryer was model IR-10 equivalent. Further, the density of tobacco cuts was measured by averaging three points for each sample using a mercury method apparent density measuring device. The thickness of the tobacco cut was measured by averaging 10 points for each sample using a micrometer.

実施例1
原料タバコ刻(厚さ:0.14mm、密度:0.8g/cm3)500gを水分が23重量%(湿基準)となるまで、恒温恒湿槽で蔵置した後、グリセリンを10重量%(湿基準)となるように添加した後、揉捻機に入れ、50分間揉捻処理した。この揉捻処理した原料タバコ刻を温度65℃に設定した再乾機に入れ、25分間再乾処理して、所望のタバコ刻(処理タバコ刻A)を得た。
Example 1
After storing 500 g of raw material tobacco cut (thickness: 0.14 mm, density: 0.8 g / cm 3 ) in a thermo-hygrostat until the water content becomes 23% by weight (humid basis), 10% by weight of glycerin ( After being added so as to satisfy the wet standard), it was put into a twisting machine and subjected to twisting for 50 minutes. This twisted raw material tobacco cut was put into a re-dryer set at a temperature of 65 ° C. and re-dried for 25 minutes to obtain a desired tobacco cut (processed tobacco cut A).

実施例2
実施例1で用いた原料タバコ刻に水およびグリセリンをそれぞれ10重量%(湿基準)となるように添加した後、揉捻機に入れ、50分間揉捻処理した。この揉捻処理した原料タバコ刻を温度150℃に設定した水乾機で20分間水乾処理して、所望のタバコ刻(処理タバコ刻B)を得た。
Example 2
Water and glycerin were added to the raw tobacco cut used in Example 1 so that each would be 10% by weight (humid basis), and then placed in a twisting machine and twisted for 50 minutes. This twisted raw material tobacco cut was water-dried for 20 minutes with a water dryer set at a temperature of 150 ° C. to obtain a desired tobacco cut (processed tobacco cut B).

実施例3
再乾処理の代わりに、90℃に設定した精揉機による30分間の精揉処理を行った以外は、実施例1の手法を繰り返し、所望のタバコ刻(処理タバコ刻C)を得た。
Example 3
Instead of the re-drying process, the method of Example 1 was repeated except that a 30 minute scouring process was performed with a scouring machine set to 90 ° C. to obtain a desired tobacco cut (processed tobacco cut C).

実施例1〜3で得た処理タバコ刻と未処理の原料タバコ刻(対照タバコ刻)の密度および厚さをそれぞれ表1および表2に示す。なお、表1には、処理タバコ刻の密度を対照タバコ刻の密度で除した値を密度変化として示し、表2には、処理タバコ刻の厚さを対照タバコ刻の厚さで除した値を厚さ変化として示してある。

Figure 0004866095
Tables 1 and 2 show the densities and thicknesses of the treated tobacco cuts and the untreated raw tobacco cuts (control tobacco cuts) obtained in Examples 1 to 3, respectively. Table 1 shows the value obtained by dividing the density of the treated tobacco by the density of the control tobacco as a density change, and Table 2 shows the value obtained by dividing the thickness of the treated tobacco by the thickness of the control tobacco. Is shown as a change in thickness.
Figure 0004866095

Figure 0004866095
Figure 0004866095

表1および表2に示すように、処理タバコ刻AおよびCは、対照タバコ刻に対し、密度がおよそ20%増加したが、厚さはほとんど変わらなかった。揉捻処理後の再乾処理により、厚さは変化しないものの、タバコ刻に存在する細孔が埋まり、タバコ刻の密度が大きくなるものと考えられる。他方、処理タバコ刻Bは、対照タバコ刻に対する密度増加はほとんど認められなかったが、厚さが大幅に増大している。揉捻処理後の水乾処理により、タバコ刻の細孔は埋まらないものの、タバコ刻同士が絡み合い、球状に整形されるため、見かけの厚さが増大したものと考えられる。   As shown in Tables 1 and 2, the treated tobacco cuts A and C increased in density by approximately 20% over the control tobacco cut, but the thickness was almost unchanged. Although the thickness is not changed by the re-drying process after the twisting process, it is considered that the pores existing in the tobacco are filled and the density of the tobacco is increased. On the other hand, the treated tobacco cut B showed little increase in density over the control tobacco cut, but the thickness increased significantly. The water-drying treatment after the twisting process does not fill the tobacco pores, but the tobacco thicknesses are intertwined and shaped into a spherical shape, which is thought to increase the apparent thickness.

実施例4
実施例1〜2で得た処理タバコ刻および対照タバコ刻を用い、小型タバコ巻き上げ機(RIZLA UK社製)により、長さ59mm、巻周25mmのシガレットを作製した。
Example 4
A cigarette having a length of 59 mm and a winding circumference of 25 mm was prepared by using a small tobacco winding machine (manufactured by RIZLA UK) using the treated tobacco stamp and the control tobacco stamp obtained in Examples 1 and 2.

各シガレットをボルグワルド社製喫煙器にセットし、点火後先端から15mmまで自然燃焼させたところで、喫煙容量35mLで1回吸煙(パフ)した。この吸煙により発生した主流煙をテフロン(登録商標)製のガスパックに捕集し、Aglient社製ガスクロマトグラフMicroGC(M200H)により、カラムとして分子ふるいカラム(Agilent MolSieve 5A 10M)を用いて酸素ガスの定量分析を行った。この定量分析は、各タバコ刻について3回行い、平均値を算出した。図1に、各シガレットの1回の吸煙当たりの酸素消費量を示す。この結果から、処理タバコ刻Aおよび処理タバコ刻Bを用いたシガレットは、対照タバコ刻を用いたシガレットに対し、酸素消費量がそれぞれ20%および50%減少したことがわかる。   Each cigarette was set in a smoker manufactured by Borgwald, and after ignition, when it was spontaneously combusted from the tip to 15 mm, it smoked (puffed) once with a smoking capacity of 35 mL. Mainstream smoke generated by the smoke absorption is collected in a gas pack made of Teflon (registered trademark), and a gas chromatograph MicroGC (M200H) manufactured by Agilent is used as a column with a molecular sieve column (Agilent MolSieve 5A 10M). Quantitative analysis was performed. This quantitative analysis was performed three times for each tobacco cut, and the average value was calculated. FIG. 1 shows the oxygen consumption per smoke of each cigarette. From this result, it can be seen that the cigarettes using the processed tobacco cut A and the processed tobacco cut B had a 20% and 50% reduction in oxygen consumption compared to the cigarette using the control tobacco cut, respectively.

シガレットの1回の吸煙で消費される酸素量を示すグラフ。The graph which shows the amount of oxygen consumed by one smoke absorption of a cigarette.

Claims (7)

原料タバコ刻を、製茶揉捻機による揉捻処理に供した後、再乾処理もしくは精揉処理または水乾処理に供することを特徴とする難燃性タバコ刻の製造方法。 A method for producing a flame-retardant tobacco cut, characterized in that the raw tobacco cut is subjected to a twisting process using a tea making machine and then subjected to a re-drying process, a koji process or a water-drying process. 前記揉捻処理前に、前記タバコ刻にグリセリンを添加することを特徴とする請求項1に記載の難燃性タバコ刻の製造方法。   The method for producing a flame-retardant tobacco stamp according to claim 1, wherein glycerin is added to the tobacco stamp before the twisting process. 前記揉捻処理後、前記原料タバコ刻を再乾処理または精揉処理に供することを特徴とする請求項2に記載の難燃性タバコ刻の製造方法。   3. The method for producing a flame-retardant tobacco cut according to claim 2, wherein after the twisting process, the raw tobacco cut is subjected to a re-drying process or a refinement treatment. 前記難燃性タバコ刻が、0.9〜1.5g/cm3の密度を有することを特徴とする請求項3に記載の難燃性タバコ刻の製造方法。 The method for producing a flame-retardant tobacco stamp according to claim 3, wherein the flame-retardant tobacco stamp has a density of 0.9 to 1.5 g / cm 3 . 前記揉捻処理前に、前記タバコ刻に水およびグリセリンを添加することを特徴とする請求項1に記載の難燃性タバコ刻の製造方法。   The method for producing a flame-retardant tobacco cut according to claim 1, wherein water and glycerin are added to the tobacco cut before the twisting process. 前記揉捻処理後、前記原料タバコ刻を水乾処理に供することを特徴とする請求項4に記載の難燃性タバコ刻の製造方法。   The method for producing a flame-retardant tobacco stamp according to claim 4, wherein after the twisting treatment, the raw tobacco cut is subjected to a water-drying treatment. 前記難燃性タバコ刻が、0.5〜8mmの厚さを有することを特徴とする請求項6に記載の難燃性タバコ刻の製造方法。   The method for producing a flame-retardant tobacco stamp according to claim 6, wherein the flame-retardant tobacco stamp has a thickness of 0.5 to 8 mm.
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CN103383541A (en) * 2013-06-27 2013-11-06 红云红河烟草(集团)有限责任公司 Moisture regain feed-forward control method based on incoming material moisture content difference
WO2017130347A1 (en) * 2016-01-28 2017-08-03 日本たばこ産業株式会社 Tobacco material for smoking tool having pipe bowl
WO2018034004A1 (en) * 2016-08-19 2018-02-22 日本たばこ産業株式会社 Method for manufacturing shredded tobacco to be used in smoking article
CN108523198B (en) * 2018-05-07 2020-09-29 中国烟草总公司郑州烟草研究院 Pretreatment process of threshed and re-cured tobacco leaves based on characteristics of tobacco raw materials

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JP2000106861A (en) * 1998-10-01 2000-04-18 Harunori Shimamura Production of tobacco substitute

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