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JP5266089B2 - Fluid measuring device - Google Patents
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JP5266089B2 - Fluid measuring device - Google Patents

Fluid measuring device Download PDF

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JP5266089B2
JP5266089B2 JP2009037816A JP2009037816A JP5266089B2 JP 5266089 B2 JP5266089 B2 JP 5266089B2 JP 2009037816 A JP2009037816 A JP 2009037816A JP 2009037816 A JP2009037816 A JP 2009037816A JP 5266089 B2 JP5266089 B2 JP 5266089B2
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chamber
flow channel
fluid
gas
introduction member
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JP2010190835A (en
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広行 稲垣
靖江 林
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Azbil Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a measurement apparatus for properly measuringphysical properties of fluid. <P>SOLUTION: The measurement apparatus 1 is provided and arranged in a flow path pipe 10 for flowing the fluid, and includes: a chamber 5 arranged in an exterior of the flow path pipe 10; an introduction member 20 protruded and arranged in an interior of the flow path pipe 10, and introducing the fluid from the interior of the flow path pipe 10 into the chamber 5; and a microchip 8 arranged in the chamber 5, and measuring the physical properties of the fluid. The introduction member 20 is protruded into the interior of the flow path pipe 10, thereby the fluid in the interior of the flow path pipe 10 can be efficiently introduced into the chamber 5. <P>COPYRIGHT: (C)2010,JPO&amp;INPIT

Description

本発明は、計測技術に関し、流体測定装置に関する。   The present invention relates to a measurement technique, and relates to a fluid measurement device.

ガスを効率よく使用するためには、濃度変化等によるガス物性の変化を監視、制御する必要がある。そのため、ガスの物性を測定する測定装置が提案されている(例えば、特許文献1、2参照。)。流路を流れるガス等の流体の物性を測定する測定装置においては、安定的な測定の観点から、流路からチャンバにガスを導き、チャンバ内のセンサで、ガスの物性を測定している。   In order to use gas efficiently, it is necessary to monitor and control changes in gas properties due to changes in concentration. For this reason, measuring devices for measuring the physical properties of gas have been proposed (see, for example, Patent Documents 1 and 2). In a measuring apparatus that measures the physical properties of a fluid such as a gas flowing in a flow path, the gas is guided from the flow path to the chamber from the viewpoint of stable measurement, and the physical properties of the gas are measured by a sensor in the chamber.

特開平11−174010号公報Japanese Patent Laid-Open No. 11-174010 特開2007−248220号公報JP 2007-248220 A

しかし、流体を流路からチャンバに効率的に導かないと、チャンバ内にガスを充填するために必要な時間が長くなり、ガス等の流体の物性の変化を適切に測定できないという問題があった。そこで本発明は、流路から流体を効率的にチャンバに導き、流体の物性変化を適切に測定可能な測定装置を提供することを目的の一つとする。   However, if the fluid is not efficiently guided from the flow path to the chamber, the time required for filling the chamber with gas becomes long, and there is a problem that a change in physical properties of fluid such as gas cannot be measured appropriately. . Therefore, an object of the present invention is to provide a measuring device that can efficiently guide a fluid from a flow path to a chamber and appropriately measure a change in physical properties of the fluid.

本発明の態様は、流体を流す流路管に配置される測定装置であって、流路管の外部に配置されるチャンバと、流路管内部に突出するよう配置される、流路管内部からチャンバに流体を導入する導入部材と、チャンバに配置され、流体の物性を測定するセンサと、を備える測定装置であることを要旨とする。本発明の態様に係る測定装置によれば、導入部材が流路管内部に突出しているため、流路管内部の流体を効率的にチャンバに導入することが可能となる。そのため、センサによって流体の物性を適切に測定することが可能となる。   An aspect of the present invention is a measuring device disposed in a flow channel pipe for flowing a fluid, the chamber disposed outside the flow channel tube, and the flow channel tube disposed so as to protrude inside the flow channel tube The gist of the present invention is a measuring device including an introduction member that introduces a fluid into the chamber and a sensor that is disposed in the chamber and measures a physical property of the fluid. According to the measuring apparatus according to the aspect of the present invention, since the introduction member protrudes into the flow channel tube, the fluid inside the flow channel tube can be efficiently introduced into the chamber. Therefore, it becomes possible to appropriately measure the physical properties of the fluid by the sensor.

本発明によれば、流体の物性を適切に測定可能な測定装置を提供可能である。   ADVANTAGE OF THE INVENTION According to this invention, the measuring apparatus which can measure the physical property of fluid appropriately can be provided.

本発明の第1の実施の形態に係る測定装置の断面図である。It is sectional drawing of the measuring apparatus which concerns on the 1st Embodiment of this invention. 本発明の第1の実施の形態に係るマイクロチップの斜視図である。1 is a perspective view of a microchip according to a first embodiment of the present invention. 本発明の第1の実施の形態に係るマイクロチップの図2のIII−III方向から見た断面図である。It is sectional drawing seen from the III-III direction of FIG. 2 of the microchip which concerns on the 1st Embodiment of this invention. 本発明の第1の実施の形態に係る補助ヒータに関する回路図である。It is a circuit diagram regarding the auxiliary heater which concerns on the 1st Embodiment of this invention. 本発明の第1の実施の形態に係る測定装置の中央演算処理装置の模式図である。It is a schematic diagram of the central processing unit of the measuring apparatus which concerns on the 1st Embodiment of this invention. 本発明の第1の実施の形態に係るガスの放熱係数と熱伝導率との関係を示すグラフである。It is a graph which shows the relationship between the thermal radiation coefficient of gas and thermal conductivity which concern on the 1st Embodiment of this invention. 本発明の第1の実施の形態に係るガスの放熱係数と濃度との関係を示すグラフである。It is a graph which shows the relationship between the thermal radiation coefficient and density | concentration of gas which concern on the 1st Embodiment of this invention. 本発明の第1の実施の形態の比較例に係る測定装置の断面図である。It is sectional drawing of the measuring apparatus which concerns on the comparative example of the 1st Embodiment of this invention. 本発明の第2の実施の形態に係る測定装置の断面図である。It is sectional drawing of the measuring apparatus which concerns on the 2nd Embodiment of this invention. 本発明の第2の実施の形態に係る導入部材の図9のX−X方向から見た断面図である。It is sectional drawing seen from the XX direction of FIG. 9 of the introduction member which concerns on the 2nd Embodiment of this invention. 本発明の第3の実施の形態に係る測定装置の断面図である。It is sectional drawing of the measuring apparatus which concerns on the 3rd Embodiment of this invention. 本発明の第3の実施の形態に係る導入部材の図11のXII−XII方向から見た断面図である。It is sectional drawing seen from the XII-XII direction of FIG. 11 of the introduction member which concerns on the 3rd Embodiment of this invention. 本発明の実施例に係るチャンバ内のガスの置換に要する時間を示すグラフである。It is a graph which shows the time which replacement | exchange of the gas in the chamber based on the Example of this invention requires. 本発明のその他の実施の形態に係る導入部材の模式図である。It is a schematic diagram of the introduction member which concerns on other embodiment of this invention.

以下に本発明の実施の形態を説明する。以下の図面の記載において、同一又は類似の部分には同一又は類似の符号で表している。但し、図面は模式的なものである。したがって、具体的な寸法等は以下の説明を照らし合わせて判断するべきものである。また、図面相互間においても互いの寸法の関係や比率が異なる部分が含まれていることは勿論である。   Embodiments of the present invention will be described below. In the following description of the drawings, the same or similar parts are denoted by the same or similar reference numerals. However, the drawings are schematic. Therefore, specific dimensions and the like should be determined in light of the following description. Moreover, it is a matter of course that portions having different dimensional relationships and ratios are included between the drawings.

(第1の実施の形態)
第1の実施の形態に係る測定装置1は、断面図である図1に示すように、上流側から下流側に気体又は液体等の流体を流す流路管10に配置される。測定装置1は、流路管10の外部に配置されるチャンバ5と、流路管10内部に突出するよう配置される、流路管10内部からチャンバ5に流体を導入する導入部材20と、チャンバ5に配置され、流体の物性を測定するマイクロチップ8を含むセンサと、を備える。以下において、「流体」としてガスが流路管10を流れる例を説明する。
(First embodiment)
As shown in FIG. 1, which is a cross-sectional view, the measuring apparatus 1 according to the first embodiment is disposed in a flow path pipe 10 that flows a fluid such as gas or liquid from the upstream side to the downstream side. The measuring device 1 includes a chamber 5 disposed outside the flow channel tube 10, an introduction member 20 that is disposed so as to protrude into the flow channel tube 10, and introduces a fluid into the chamber 5 from the flow channel tube 10. And a sensor including a microchip 8 that is disposed in the chamber 5 and measures the physical properties of the fluid. Hereinafter, an example in which a gas flows as a “fluid” through the flow channel pipe 10 will be described.

流路管10には、開口11が設けられている。また、流路管10の外壁には、開口11を囲むように、円筒状の雌ねじ12が配置されている。雌ねじ12としては、Rcねじ(ISO規格)等が使用可能である。チャンバ5は、雌ねじ12にはまる雄ねじ13と一体的に成形されている。チャンバ5は、雄ねじ13を雌ねじ12にはめ込むことにより、流路管10の外部に固定される。はめあわされた雄ねじ13と雌ねじ12は、流路管10とチャンバ5の接続部を構成する。雄ねじ13内部には、流路管10内部とチャンバ5内部とを連通させる貫通孔14が設けられている。   The channel tube 10 is provided with an opening 11. A cylindrical female screw 12 is arranged on the outer wall of the flow channel tube 10 so as to surround the opening 11. As the female screw 12, an Rc screw (ISO standard) or the like can be used. The chamber 5 is formed integrally with a male screw 13 that fits into the female screw 12. The chamber 5 is fixed to the outside of the flow channel tube 10 by fitting the male screw 13 into the female screw 12. The fitted male screw 13 and female screw 12 constitute a connection portion between the flow path tube 10 and the chamber 5. A through hole 14 is provided in the male screw 13 to allow communication between the inside of the flow path tube 10 and the inside of the chamber 5.

導入部材20は管状であり、互いに連通された導入口としての開口21と、排出口としての開口22とを有する。開口21は円管状の導入部材20の先端を管の軸線に対して斜めに切り落とした形状に設けられている。導入部材20は、開口21が流路管10の上流に向くように、例えば貫通孔14の内壁に固定される。ここで「開口21が流路管10の上流に向く」とは、開口21全体が完全に上流を向いていることを必ずしも意味しない。流路管10の上流側から導入部材20を見たときに、開口21の一部が見える状態であれば良い。また、導入部材20の外径は貫通孔14の内径よりも小さいので、導入部材20の外側には空間が存在する。   The introduction member 20 is tubular and has an opening 21 as an introduction port and an opening 22 as a discharge port that are communicated with each other. The opening 21 is provided in a shape in which the distal end of a circular tubular introduction member 20 is cut off obliquely with respect to the axis of the tube. The introduction member 20 is fixed to, for example, the inner wall of the through hole 14 so that the opening 21 faces the upstream side of the flow channel pipe 10. Here, “the opening 21 faces the upstream side of the flow channel pipe 10” does not necessarily mean that the entire opening 21 faces completely upstream. When the introduction member 20 is viewed from the upstream side of the flow channel tube 10, it may be in a state where a part of the opening 21 can be seen. Further, since the outer diameter of the introduction member 20 is smaller than the inner diameter of the through hole 14, there is a space outside the introduction member 20.

流路管10内部に突出する管状の導入部材20の導入口としての開口21が流路管10内のガスの進行方向に対して斜めになるよう設けられており、流路管10の上流側に対向しているため、導入部材20の内壁が流路管10の上流側に露出する。したがって、流路管10内部を上流側から流れてきたガスの一部は、導入部材20の開口21に入り、導入部材20の内壁に衝突して、進行方向を変えられる。そのため、導入部材20の上流側と下流側で差圧が発生し、進行方向を変えられたガスの一部が導入部材20内部に流れ込み、排出口としての開口22を介してチャンバ5に導かれる。さらにチャンバ5に導かれたガスの一部は、貫通孔14(導入部材20の外側の空間)を通って、開口11から流路管10の内部に還流する。   An opening 21 as an introduction port of a tubular introduction member 20 protruding into the flow channel tube 10 is provided so as to be inclined with respect to the gas traveling direction in the flow channel tube 10, and upstream of the flow channel tube 10. Therefore, the inner wall of the introduction member 20 is exposed to the upstream side of the flow channel tube 10. Therefore, a part of the gas flowing from the upstream side in the flow channel pipe 10 enters the opening 21 of the introduction member 20 and collides with the inner wall of the introduction member 20 to change the traveling direction. Therefore, a differential pressure is generated between the upstream side and the downstream side of the introduction member 20, and a part of the gas whose traveling direction is changed flows into the introduction member 20 and is guided to the chamber 5 through the opening 22 as the discharge port. . Further, a part of the gas guided to the chamber 5 passes through the through hole 14 (space outside the introduction member 20) and returns to the inside of the flow channel pipe 10 from the opening 11.

なお、開口21を斜めに設けず、ガスの進行方向と平行に設けてもよい。具体的には、開口21を、円管状の導入部材20の先端を管の軸線に対して垂直に切り落とした形状に設けてもよい。導入部材20が流路管10内部に突出するよう配置されているため、開口21をガスの進行方向と平行に設けても、導入部材20の上流側と下流側で差圧が発生し、進行方向を変えられたガスの一部が導入部材20内部に流れ込む。   The opening 21 may not be provided obliquely, but may be provided in parallel with the gas traveling direction. Specifically, the opening 21 may be provided in a shape in which the tip of the circular tubular introduction member 20 is cut off perpendicular to the axis of the tube. Since the introduction member 20 is disposed so as to protrude into the flow channel pipe 10, even if the opening 21 is provided in parallel with the gas traveling direction, a differential pressure is generated between the upstream side and the downstream side of the introduction member 20 and proceeds. A part of the gas whose direction has been changed flows into the introduction member 20.

導入部材20を流れる流量に対してチャンバ5の容積が小さい場合、チャンバ5内の流体の置換が速くなる利点はあるが、マイクロチップ8の測定値が流体の流速の影響を受け易いという欠点が生じる。逆に、導入部材20を流れる流量に対してチャンバ5の容積が大きい場合、チャンバ5内の流体の置換が遅くなる欠点はあるが、マイクロチップ8の測定値が流体の流速の影響を受けにくいという利点が生じる。したがって、導入部材20を流れる流体の流量とチャンバ5の容積との関係については、何回かの試行によって最適な状態に定めることが望ましい。   When the volume of the chamber 5 is small with respect to the flow rate flowing through the introduction member 20, there is an advantage that the replacement of the fluid in the chamber 5 is fast, but the measurement value of the microchip 8 is easily affected by the flow velocity of the fluid. Arise. On the contrary, when the volume of the chamber 5 is large with respect to the flow rate flowing through the introduction member 20, there is a drawback that the replacement of the fluid in the chamber 5 is slow, but the measured value of the microchip 8 is not easily affected by the flow velocity of the fluid. This produces the advantage. Therefore, it is desirable that the relationship between the flow rate of the fluid flowing through the introduction member 20 and the volume of the chamber 5 be determined in an optimum state by several trials.

チャンバ5内に配置されたマイクロチップ8は、斜視図である図2、及びIII−III方向から見た断面図である図3に示すように、キャビティ66が設けられた基板60、及び基板60上にキャビティ66を覆うように配置された絶縁膜65を備える。基板60の厚みは、例えば0.5mmである。また、基板60の縦横の寸法は、例えばそれぞれ1.5mm程度である。絶縁膜65のキャビティ66を覆う部分は、断熱性のダイアフラムをなしている。   As shown in FIG. 2 which is a perspective view and FIG. 3 which is a cross-sectional view seen from the III-III direction, the microchip 8 disposed in the chamber 5 includes a substrate 60 provided with a cavity 66, and a substrate 60. An insulating film 65 is provided on the cavity 66 so as to cover the cavity 66. The thickness of the substrate 60 is, for example, 0.5 mm. The vertical and horizontal dimensions of the substrate 60 are, for example, about 1.5 mm. A portion of the insulating film 65 covering the cavity 66 forms a heat insulating diaphragm.

さらにマイクロチップ8は、絶縁膜65に設けられた発熱抵抗体61と、発熱抵抗体61を挟むように絶縁膜65に設けられた第1の測温抵抗素子62及び第2の測温抵抗素子63と、基板60上に設けられたガス温度センサ64を備える。ガス温度センサ64も電気抵抗素子等からなる。発熱抵抗体61は、キャビティ66を覆う絶縁膜65の中心に配置されている。発熱抵抗体61は、電力を与えられて発熱し、図1に示すチャンバ5内に導入されて発熱抵抗体61に接するガスを加熱する。図2及び図3に示すガス温度センサ64は、絶縁膜65を介して発熱抵抗体61から隔離されて設けられており、図1に示すチャンバ5内に導入されたガスのガス温度を検出する。   Further, the microchip 8 includes a heating resistor 61 provided on the insulating film 65, and a first resistance temperature measuring element 62 and a second temperature measuring resistance element provided on the insulating film 65 so as to sandwich the heating resistor 61 therebetween. 63 and a gas temperature sensor 64 provided on the substrate 60. The gas temperature sensor 64 also includes an electric resistance element or the like. The heating resistor 61 is disposed at the center of the insulating film 65 that covers the cavity 66. The heating resistor 61 generates heat when power is applied, and heats the gas that is introduced into the chamber 5 shown in FIG. 1 and contacts the heating resistor 61. The gas temperature sensor 64 shown in FIGS. 2 and 3 is provided separately from the heating resistor 61 via the insulating film 65, and detects the gas temperature of the gas introduced into the chamber 5 shown in FIG. .

図2及び図3に示す基板60の材料としては、シリコン(Si)等が使用可能である。絶縁膜65の材料としては、酸化ケイ素(SiO2)等が使用可能である。キャビティ66は、異方性エッチング等により形成される。また発熱抵抗体61、第1の測温抵抗素子62、第2の測温抵抗素子63、及びガス温度センサ64のそれぞれの材料には白金(Pt)等が使用可能であり、リソグラフィ法等により形成可能である。 As a material of the substrate 60 shown in FIGS. 2 and 3, silicon (Si) or the like can be used. As a material of the insulating film 65, silicon oxide (SiO 2 ) or the like can be used. The cavity 66 is formed by anisotropic etching or the like. Also, platinum (Pt) or the like can be used as the material of the heating resistor 61, the first temperature measuring resistance element 62, the second temperature measuring resistance element 63, and the gas temperature sensor 64. It can be formed.

ここで、発熱抵抗体61は、温度によって抵抗値が変化する。発熱抵抗体61の発熱温度THと、発熱抵抗体61の抵抗値RHの関係は、下記(1)式で与えられる。
RH = RSTD×[1+α(TH-TSTD) + β(TH-TSTD)2] ・・・(1)
(1)式において、TSTDは標準温度を表し、例えば20℃である。RSTDは標準温度TSTDにおける予め計測された抵抗値を表す。αは1次の抵抗温度係数、βは2次の抵抗温度係数を表す。また、発熱抵抗体61の抵抗値RHは、発熱抵抗体61の駆動電力PHと、発熱抵抗体61の通電電流IHから、下記(2)式で与えられる。
RH = PH / IH 2 ・・・(2)
あるいは発熱抵抗体61の抵抗値RHは、発熱抵抗体61にかかる電圧VHと、発熱抵抗体61の通電電流IHから、下記(3)式で与えられる。
RH = VH / IH ・・・(3)
Here, the resistance value of the heating resistor 61 varies depending on the temperature. The relationship between the heat generation temperature TH of the heat generation resistor 61 and the resistance value R H of the heat generation resistor 61 is given by the following equation (1).
R H = R STD × [1 + α (T H -T STD ) + β (T H -T STD ) 2 ] (1)
In the formula (1), T STD represents a standard temperature, for example, 20 ° C. R STD represents a resistance value measured in advance at the standard temperature T STD . α represents a first-order resistance temperature coefficient, and β represents a second-order resistance temperature coefficient. Further, the resistance value R H of the heating resistor 61 is given by the following equation (2) from the driving power P H of the heating resistor 61 and the energization current I H of the heating resistor 61.
R H = P H / I H 2 (2)
Alternatively, the resistance value R H of the heating resistor 61 is given by the following equation (3) from the voltage V H applied to the heating resistor 61 and the energization current I H of the heating resistor 61.
R H = V H / I H (3)

発熱抵抗体61の発熱温度THは、発熱抵抗体61とガスの間が熱的に平衡になったときに安定する。なお、熱的に平衡な状態とは、発熱抵抗体61の発熱と、発熱抵抗体61からガスへの放熱と、が釣り合っている状態をいう。平衡状態において、下記(4)式に示すように、発熱抵抗体61の駆動電力PHを、発熱抵抗体61の発熱温度THとガスのガス温度TOとの差で割ることにより、ガスの放熱係数MOが得られる。なお、放熱係数MOの単位は、例えばW/℃である。
MO = PH / (TH - TO) ・・・(4)
The heating temperature TH of the heating resistor 61 is stabilized when the heating resistor 61 and the gas are in thermal equilibrium. The thermally balanced state refers to a state in which the heat generation of the heating resistor 61 and the heat dissipation from the heating resistor 61 to the gas are balanced. In equilibrium, as shown in the following equation (4), the driving power P H of the heating resistor 61 is divided by the difference between the gas temperature T O of the heating temperature T H and the gas of the heating resistor 61, the gas radiation coefficient M O is obtained. The unit of the heat dissipation coefficient M O is, for example, W / ° C.
M O = P H / (T H -T O ) (4)

発熱抵抗体61の通電電流IHと、駆動電力PH又は電圧VHは計測可能であるため、上記(1)乃至(3)から発熱抵抗体61の発熱温度THが算出可能である。また、ガスのガス温度TOは、図2に示すガス温度センサ64で測定可能である。したがって、図2及び図3に示すマイクロチップ8を用いて、図1に示すチャンバ5内に導入されたガスの放熱係数MOが算出可能である。 Energizing current I H of the heating resistor 61, since the driving power P H or the voltage V H can be measured, the heat producing temperature T H of the heating resistor 61 from the (1) to (3) can be calculated. The gas temperature T O of the gas can be measured by the gas temperature sensor 64 shown in FIG. Thus, by using the microchip 8 shown in FIGS. 2 and 3, the radiation coefficient M O of the gas introduced into the chamber 5 as shown in FIG. 1 can be calculated.

図2及び図3に示すマイクロチップ8は、熱伝導性の基板60の温度を一定に保つ補助ヒータをさらに備えていてもよい。基板60の温度を一定に保つことにより、マイクロチップ8の近傍のガスの温度が、基板60の一定の温度と近似する。そのため、ガスの温度の変動が抑制され、より高い精度で放熱係数MOを算出することが可能となる。補助ヒータにも電気抵抗素子等が使用可能である。また、ガス温度センサ64が補助ヒータを兼ねていてもよい。 The microchip 8 shown in FIGS. 2 and 3 may further include an auxiliary heater that keeps the temperature of the thermally conductive substrate 60 constant. By keeping the temperature of the substrate 60 constant, the temperature of the gas in the vicinity of the microchip 8 approximates the constant temperature of the substrate 60. Therefore, variations in the temperature of the gas is suppressed, it is possible to calculate the radiation coefficient M O with higher accuracy. An electric resistance element or the like can also be used for the auxiliary heater. The gas temperature sensor 64 may also serve as an auxiliary heater.

図4に示すように、ガス温度センサ64は、抵抗ブリッジ回路の一部をなしている。抵抗ブリッジ回路は、ガス温度センサ64と直列に接続された抵抗素子181と、ガス温度センサ64及び抵抗素子181と並列に接続された抵抗素子182,183を備える。ここで、ガス温度センサ64の抵抗値をRr、抵抗素子181,182,183の固定された抵抗値をそれぞれR181,R182,R183とする。抵抗ブリッジ回路には、オペアンプ171が接続されている。ガス温度センサ64を補助ヒータとして機能させる場合、抵抗素子181とガス温度センサ64の間のブリッジ電圧V2aが、抵抗素子182と抵抗素子183の間のブリッジ電圧V2bと等しくなるよう、ブリッジ駆動電圧V1がフィードバック制御される。これにより、ガス温度センサ64の抵抗値Rrが一定となり、ガス温度センサ64が補助ヒータとして一定の温度で発熱する。 As shown in FIG. 4, the gas temperature sensor 64 forms part of a resistance bridge circuit. The resistance bridge circuit includes a resistance element 181 connected in series with the gas temperature sensor 64, and resistance elements 182 and 183 connected in parallel with the gas temperature sensor 64 and the resistance element 181. Here, the resistance value of the gas temperature sensor 64 is Rr, and the fixed resistance values of the resistance elements 181 , 182 , and 183 are R 181 , R 182 , and R 183 , respectively. An operational amplifier 171 is connected to the resistance bridge circuit. When the gas temperature sensor 64 functions as an auxiliary heater, bridge driving is performed so that the bridge voltage V 2a between the resistance element 181 and the gas temperature sensor 64 is equal to the bridge voltage V 2b between the resistance element 182 and the resistance element 183. The voltage V 1 is feedback controlled. Thereby, the resistance value Rr of the gas temperature sensor 64 becomes constant, and the gas temperature sensor 64 generates heat at a constant temperature as an auxiliary heater.

図1に示すように、マイクロチップ8は、断熱部材18を介してチャンバ5内に配置される。断熱部材18によって、マイクロチップ8の温度が、チャンバ5の内壁の温度変動の影響を受けにくくなる。断熱部材18の熱伝導率は、例えば10W/(m・K)以下である。なお、チャンバ5内に、マイクロチップ8を覆うように、金網等のフィルタを配置してもよい。フィルタを配置することにより、チャンバ5内に導入されるガスに含まれる塵芥等が、マイクロチップ8に衝突することを防止することが可能となる。また、フィルタを配置することにより、マイクロチップ8に向かうガスの流速を緩和することも可能となる。   As shown in FIG. 1, the microchip 8 is disposed in the chamber 5 via a heat insulating member 18. The heat insulating member 18 makes the temperature of the microchip 8 less susceptible to the temperature fluctuation of the inner wall of the chamber 5. The heat conductivity of the heat insulating member 18 is, for example, 10 W / (m · K) or less. A filter such as a wire mesh may be disposed in the chamber 5 so as to cover the microchip 8. By disposing the filter, it is possible to prevent dust or the like contained in the gas introduced into the chamber 5 from colliding with the microchip 8. Further, by arranging the filter, the flow rate of the gas toward the microchip 8 can be reduced.

測定装置1は、マイクロチップ8に電気的に接続された回路基板100を含む計測ユニット30をさらに備える。回路基板100は、図5に模式的に示す中央演算処理装置(CPU)300を備える。CPU300は、放熱係数算出部301を含む。放熱係数算出部301は、上記(4)式に示すように、図2及び図3に示すマイクロチップ8の発熱抵抗体61の駆動電力PHを、発熱抵抗体61の発熱温度THとガス温度センサ64で測定されたガスのガス温度TOとの差で割り、発熱抵抗体61と熱的に平衡なときのガスの放熱係数の値を算出する。 The measurement apparatus 1 further includes a measurement unit 30 including a circuit board 100 electrically connected to the microchip 8. The circuit board 100 includes a central processing unit (CPU) 300 schematically shown in FIG. CPU 300 includes a heat dissipation coefficient calculation unit 301. The radiation coefficient calculating portion 301, the (4) As shown in equation, the driving power P H of the heating resistor 61 of the microchip 8 shown in FIGS. 2 and 3, the heating temperature T H and the gas of the heating resistor 61 Dividing by the difference from the gas temperature T O of the gas measured by the temperature sensor 64, the value of the heat radiation coefficient of the gas when in thermal equilibrium with the heating resistor 61 is calculated.

図5に示すCPU300には、熱伝導率記憶装置352が接続されている。ここで、図6は、ガス温度TOが0℃、20℃、及び40℃のときのプロパンガスの放熱係数と熱伝導率との関係を示す。図6に示すように、ガスの放熱係数と熱伝導率とは、一般に比例関係にある。そこで、図5に示す熱伝導率記憶装置352は、図1に示すチャンバ5に導入されるガスの放熱係数と熱伝導率との対応関係を、近似式あるいはテーブル等で予め保存する。 A thermal conductivity storage device 352 is connected to the CPU 300 shown in FIG. Here, FIG. 6 shows the relationship between the heat dissipation coefficient and the thermal conductivity of propane gas when the gas temperature T O is 0 ° C., 20 ° C., and 40 ° C. As shown in FIG. 6, the heat dissipation coefficient of gas and the thermal conductivity are generally in a proportional relationship. Therefore, the thermal conductivity storage device 352 shown in FIG. 5 stores the correspondence relationship between the heat release coefficient of the gas introduced into the chamber 5 shown in FIG. 1 and the thermal conductivity in advance using an approximate expression or a table.

図5に示すCPU300は、熱伝導率算出部302をさらに含む。熱伝導率算出部302は、放熱係数算出部301からガスの放熱係数の算出された値を受信し、熱伝導率記憶装置352からガスの放熱係数と熱伝導率との対応関係を読み出す。さらに熱伝導率算出部302は、ガスの放熱係数の値と、ガスの放熱係数と熱伝導率との対応関係とに基づいて、図1に示すチャンバ5に導入されたガスの熱伝導率を算出する。   CPU 300 shown in FIG. 5 further includes a thermal conductivity calculator 302. The thermal conductivity calculator 302 receives the calculated value of the gas heat dissipation coefficient from the heat dissipation coefficient calculator 301 and reads the correspondence relationship between the heat dissipation coefficient of gas and the thermal conductivity from the thermal conductivity storage device 352. Furthermore, the thermal conductivity calculation unit 302 calculates the thermal conductivity of the gas introduced into the chamber 5 shown in FIG. 1 based on the value of the heat dissipation coefficient of the gas and the correspondence relationship between the heat dissipation coefficient of the gas and the heat conductivity. calculate.

図5に示すCPU300には、濃度記憶装置353がさらに接続されている。ここで、図7は、ガス温度TOが0℃、20℃、及び40℃のときのプロパンガスの放熱係数と濃度との関係を示す。図7に示すように、ガスの放熱係数とガスの濃度とは、一般に比例関係にある。そこで、図5に示す濃度記憶装置353は、図1に示すチャンバ5に導入されるガスの放熱係数と濃度との対応関係を、近似式あるいはテーブル等で予め保存する。 A density storage device 353 is further connected to the CPU 300 shown in FIG. Here, FIG. 7 shows the relationship between the heat dissipation coefficient and the concentration of propane gas when the gas temperature T O is 0 ° C., 20 ° C., and 40 ° C. As shown in FIG. 7, the gas heat dissipation coefficient and the gas concentration are generally in a proportional relationship. Therefore, the concentration storage device 353 shown in FIG. 5 stores the correspondence relationship between the heat dissipation coefficient and the concentration of the gas introduced into the chamber 5 shown in FIG.

図5に示すCPU300は、濃度算出部303をさらに含む。濃度算出部303は、放熱係数算出部301からガスの放熱係数の算出された値を受信し、濃度記憶装置353からガスの放熱係数と濃度との対応関係を読み出す。さらに濃度算出部303は、ガスの放熱係数の値と、ガスの放熱係数と濃度との対応関係とに基づいて、図1に示すチャンバ5に導入されたガスの濃度を算出する。   CPU 300 shown in FIG. 5 further includes a density calculation unit 303. The concentration calculation unit 303 receives the calculated value of the gas heat dissipation coefficient from the heat dissipation coefficient calculation unit 301, and reads the correspondence between the gas heat dissipation coefficient and the concentration from the concentration storage device 353. Further, the concentration calculation unit 303 calculates the concentration of the gas introduced into the chamber 5 shown in FIG. 1 based on the value of the gas heat dissipation coefficient and the correspondence between the gas heat dissipation coefficient and the concentration.

以上示した第1の実施の形態に係る測定装置1は、流路管10に開口11と雌ねじ12を設けることにより、流路管10の太さに関係なく、流路管10に容易に配置可能である。そのため、流路管10が既設の配管であっても、流路管10に測定装置1を容易に配置可能である。また、流路管10内部を流れるガスの一部をチャンバ5に導入することにより、ガスの物性を測定するため、ガスの総てをチャンバに導入する測定装置と比較して小型化が可能となる。   The measuring apparatus 1 according to the first embodiment described above is easily arranged in the flow channel tube 10 by providing the flow channel tube 10 with the opening 11 and the female screw 12, regardless of the thickness of the flow channel tube 10. Is possible. Therefore, even if the flow channel pipe 10 is an existing pipe, the measuring device 1 can be easily arranged in the flow channel pipe 10. In addition, by introducing a part of the gas flowing inside the flow channel tube 10 into the chamber 5, the physical properties of the gas are measured, so that the size can be reduced as compared with a measuring apparatus that introduces all of the gas into the chamber. Become.

また、測定装置1を小型化するために、雌ねじ12と雄ねじ13の径を細くすると、雌ねじ12の貫通孔14内にマイクロチップ8を配置するのが困難になる。そのため、雄ねじ13と一体的に成形されたチャンバ5内にマイクロチップ8が配置されている。ここで、図8に示すように、導入部材20を設けなかった場合、流路管10からチャンバ5に流入するガスはわずかである。そのため、流路管10を流れるガスと同じガスにチャンバ5内が置換されるのに時間がかかるという問題がある。すなわち、流路管10を流れるガスの組成が変化した場合、その変化をマイクロチップ8が検出するまでに時間がかかり、応答性が悪い。   Further, if the diameters of the female screw 12 and the male screw 13 are reduced in order to reduce the size of the measuring apparatus 1, it is difficult to arrange the microchip 8 in the through hole 14 of the female screw 12. Therefore, the microchip 8 is disposed in the chamber 5 formed integrally with the male screw 13. Here, as shown in FIG. 8, when the introduction member 20 is not provided, the amount of gas flowing from the flow path tube 10 into the chamber 5 is very small. Therefore, there is a problem that it takes time to replace the inside of the chamber 5 with the same gas as the gas flowing through the flow path pipe 10. That is, when the composition of the gas flowing through the flow channel tube 10 changes, it takes time until the microchip 8 detects the change, and the responsiveness is poor.

これに対し、第1の実施の形態によれば、図1に示すように、流路管10内部に突出するよう配置された管状の導入部材20の導入口としての開口21が、流路管10の上流側に対向している。そのため、流路管10を流れるガスが効率的にチャンバ5内に導入される。したがって、流路管10を流れるガスと同じガスでチャンバ5内が置換されるのに必要な時間を短縮することが可能となり、応答性が良い。また、従来、計測装置が取り付けられる流路管10に設けられていたオリフィスを省略することも可能となる。   On the other hand, according to the first embodiment, as shown in FIG. 1, the opening 21 serving as the introduction port of the tubular introduction member 20 disposed so as to protrude into the flow channel tube 10 is formed by the flow channel tube. It faces 10 upstream. Therefore, the gas flowing through the flow channel pipe 10 is efficiently introduced into the chamber 5. Therefore, it is possible to reduce the time required for replacing the inside of the chamber 5 with the same gas as the gas flowing in the flow channel tube 10, and the responsiveness is good. Further, it is possible to omit an orifice conventionally provided in the flow channel pipe 10 to which the measuring device is attached.

(第2の実施の形態)
図9及びX−X方向から見た断面図である図10に示すように、第2の実施の形態に係る測定装置1の導入部材220には、複数の貫通孔25,26a,26b,26c,26d,26e,26fが平行に設けられている。円柱状の導入部材220の断面において、複数の貫通孔26a,26b,26c,26d,26e,26fは円周上に一定の間隔をおいて設けられており、貫通孔25は、円周の中心に設けられている。
(Second Embodiment)
As shown in FIG. 9 and FIG. 10 which is a cross-sectional view seen from the XX direction, the introduction member 220 of the measuring apparatus 1 according to the second embodiment has a plurality of through holes 25, 26a, 26b, 26c. , 26d, 26e, and 26f are provided in parallel. In the cross section of the cylindrical introduction member 220, the plurality of through holes 26a, 26b, 26c, 26d, 26e, and 26f are provided at regular intervals on the circumference, and the through hole 25 is the center of the circumference. Is provided.

図9に示すように、流路管10内に突出するように位置する、導入部材220の端部は、略円錐状である。貫通孔26aは、導入部材220の略円錐状の端部の側面に設けられた開口221aと、チャンバ5側の端部に設けられた開口222aとを連通する。貫通孔26dは、導入部材220の略円錐状の端部の側面に設けられた開口221dと、チャンバ5側の端部に設けられた開口222dとを連通する。図10に示す貫通孔26b,26c,26e,26fのそれぞれも、略円錐状の端部の側面に設けられた開口と他端に設けられた開口とを連通する。また、図9に示す貫通孔25は、略円錐状の端部の頂点に設けられた開口223と他端の開口224を連通する。   As shown in FIG. 9, the end portion of the introduction member 220 located so as to protrude into the flow channel tube 10 has a substantially conical shape. The through hole 26a communicates the opening 221a provided on the side surface of the substantially conical end portion of the introduction member 220 and the opening 222a provided on the end portion on the chamber 5 side. The through hole 26d communicates the opening 221d provided on the side surface of the substantially conical end portion of the introduction member 220 and the opening 222d provided on the end portion on the chamber 5 side. Each of the through holes 26b, 26c, 26e, and 26f shown in FIG. 10 also communicates the opening provided on the side surface of the substantially conical end with the opening provided on the other end. Further, the through hole 25 shown in FIG. 9 communicates the opening 223 provided at the apex of the substantially conical end and the opening 224 at the other end.

開口223以外の複数の開口は、略円錐状の端部の側面に設けられているため、流路管10内のガスの進行方向に対して斜めになる。したがって、流路管10内部を上流側から流れてきたガスの一部が、複数の開口の少なくとも一部に入り、導入部材220の内壁に衝突して進行方向を変えられ、当該貫通孔を通してチャンバ5に導入され、他の貫通孔を通って開口223及び開口221d等から流路管10の内部に還流する。   Since the plurality of openings other than the opening 223 are provided on the side surfaces of the substantially conical end portions, they are inclined with respect to the gas traveling direction in the flow channel tube 10. Accordingly, a part of the gas flowing from the upstream side in the flow channel pipe 10 enters at least a part of the plurality of openings, collides with the inner wall of the introduction member 220, and changes its traveling direction, and passes through the through-hole to the chamber. 5, and returns to the inside of the flow pipe 10 through the other through-holes from the opening 223 and the opening 221 d.

また、図1に示すように導入部材20の開口21が1個しかない場合、図1に示すようなねじによる接続部を用いると、ねじ込み具合によって開口21が上流側に対向しているか否か、外部から目視確認が困難である場合が生じうる。これに対し、図9及び図10に示す導入部材220は、略円錐状の端部の側面に円周上に等間隔に設けられた少なくとも3つ以上の複数の開口を有する。そのため、流路管10内に導入部材220をいずれの向きに挿入しても、複数の開口のいずれかを、流路管10の上流向かせることが可能となる。ここで「開口のいずれかを、流路管10の上流に向かせる」とは、開口全体が完全に上流を向いていることを必ずしも意味しない。流路管10の上流側から導入部材220を見たときに、少なくともいずれかの開口の一部が見える状態であれば良い。なお、図9においては、導入部材220が雄ねじ13内の貫通孔14に挿入されている例を示しているが、導入部材220と雄ねじ13を一体的に成形してもよい。   In addition, when there is only one opening 21 of the introduction member 20 as shown in FIG. 1, whether or not the opening 21 faces the upstream side due to the screwing condition when using a screw connection as shown in FIG. 1. In some cases, visual confirmation from the outside is difficult. On the other hand, the introduction member 220 shown in FIGS. 9 and 10 has a plurality of openings of at least three or more provided on the side surface of the substantially conical end portion at equal intervals on the circumference. Therefore, even if the introduction member 220 is inserted into the flow channel pipe 10 in any direction, any of the plurality of openings can be directed upstream of the flow channel pipe 10. Here, “directing any of the openings toward the upstream of the flow pipe 10” does not necessarily mean that the entire opening is completely directed upstream. It suffices if at least a part of the opening is visible when the introduction member 220 is viewed from the upstream side of the flow channel tube 10. Although FIG. 9 shows an example in which the introduction member 220 is inserted into the through hole 14 in the male screw 13, the introduction member 220 and the male screw 13 may be integrally formed.

(第3の実施の形態)
図11及びXII−XII方向から見た断面図である図12に示すように、第3の実施の形態に係る測定装置1の雄ねじ13の貫通孔14に挿入された導入部材320は、断面において放射状に配置された複数の仕切り板32A,32B,32C,32Dを備える。複数の仕切り板32A,32B,32C,32Dは、雄ねじ13の貫通孔14を4つの空間に仕切る。また、導入部材320の複数の仕切り板32A,32B,32C,32Dは、流路管10内に突出する。
(Third embodiment)
As shown in FIG. 11 and FIG. 12, which is a cross-sectional view seen from the XII-XII direction, the introduction member 320 inserted into the through hole 14 of the male screw 13 of the measuring apparatus 1 according to the third embodiment is A plurality of partition plates 32A, 32B, 32C, and 32D that are arranged radially are provided. The plurality of partition plates 32A, 32B, 32C, and 32D partition the through hole 14 of the male screw 13 into four spaces. Further, the plurality of partition plates 32 </ b> A, 32 </ b> B, 32 </ b> C, 32 </ b> D of the introduction member 320 protrude into the flow channel tube 10.

流路管10内部を上流側から流れてきたガスの一部は、複数の仕切り板32A,32B,32C,32Dの少なくとも一部に衝突して進行方向を変えられ、4つに仕切られた雄ねじ13の貫通孔14の一部を通って、チャンバ5に導入される。なお、少なくとも3つ以上の仕切り板を設けることにより、流路管10内に導入部材320をいずれの向きに挿入しても、仕切り板のいずれかを流路管10の上流側に対向させることが可能となる。なお、図11においては、導入部材320が雄ねじ13内の貫通孔14に挿入されている例を示しているが、導入部材320と雄ねじ13を一体的に成形してもよい。   A part of the gas flowing from the upstream side in the flow channel pipe 10 collides with at least a part of the plurality of partition plates 32A, 32B, 32C, 32D, the direction of travel is changed, and the male screw partitioned into four 13 is introduced into the chamber 5 through a part of the through holes 14. In addition, by providing at least three or more partition plates, even if the introduction member 320 is inserted into the flow channel pipe 10 in any direction, any one of the partition plates faces the upstream side of the flow channel tube 10. Is possible. 11 shows an example in which the introduction member 320 is inserted into the through hole 14 in the male screw 13, the introduction member 320 and the male screw 13 may be integrally formed.

(実施例)
図1、図8、及び図11に示す測定装置1のチャンバ5に充填された濃度100%の窒素(N2)ガスを、濃度100%の二酸化炭素(CO2)ガスに置換するために要する時間を計測した結果を、図13に示す。図13において、横軸は流路管10内のガスの流速を示し、縦軸はチャンバ5内に充填されたガスの置換に要した時間を示す。導入部材を有さない図8に示す測定装置1の場合、流路管10内のガスの流速が2m/s以下ではチャンバ5内のガスの置換は長い時間を要した。また、流路管10内のガスの流速が2m/sより早くなっても、チャンバ5内のガスを置換するために数分を要した。これに対し、図1及び図11に示す測定装置1の場合、流路管10内のガスの流速が2m/s以下となっても、チャンバ5内のガスを20秒以内に置換することが可能であった。よって、本発明の実施の形態に係る導入部材により、チャンバ5内のガスの置換を効率的に行えることが示された。
(Example)
It is necessary to replace the 100% concentration nitrogen (N 2 ) gas filled in the chamber 5 of the measuring apparatus 1 shown in FIGS. 1, 8, and 11 with a 100% concentration carbon dioxide (CO 2 ) gas. The result of measuring time is shown in FIG. In FIG. 13, the horizontal axis indicates the flow rate of the gas in the flow path pipe 10, and the vertical axis indicates the time required for replacing the gas filled in the chamber 5. In the case of the measuring apparatus 1 shown in FIG. 8 that does not have an introduction member, the replacement of the gas in the chamber 5 took a long time when the flow rate of the gas in the flow path pipe 10 was 2 m / s or less. Further, even if the flow velocity of the gas in the channel tube 10 is faster than 2 m / s, it took several minutes to replace the gas in the chamber 5. On the other hand, in the case of the measuring apparatus 1 shown in FIGS. 1 and 11, the gas in the chamber 5 can be replaced within 20 seconds even if the flow velocity of the gas in the flow channel pipe 10 is 2 m / s or less. It was possible. Therefore, it has been shown that the gas in the chamber 5 can be efficiently replaced by the introduction member according to the embodiment of the present invention.

(その他の実施の形態)
上記のように本発明を実施の形態によって記載したが、この開示の一部をなす記述及び図面はこの発明を限定するものであると理解するべきではない。この開示から当業者には様々な代替実施の形態、実施例及び運用技術が明らかになるはずである。
(Other embodiments)
Although the present invention has been described by the embodiments as described above, it should not be understood that the description and drawings constituting a part of this disclosure limit the present invention. From this disclosure, various alternative embodiments, examples and operational techniques should be apparent to those skilled in the art.

例えば、図1において、雄ねじ13と雌ねじ12を用いてチャンバ5と流路管10を接続する例を説明したが、フランジ(図示せず)を用いてチャンバ5と流路管10を接続してもよい。雄ねじ13と導入部材20を一体化すると、雄ねじ13をどの程度まで回転させて雌ねじ12にねじ込むか(回転角)によって、導入部材20の開口21の向きが異なってしまい、開口21を上流に向かせて配置することが困難な場合が生じうる。これに対し、フランジを用いることにより、例えばチャンバ5に固定された導入部材20の開口21を上流に向けたまま、チャンバ5と流路管10を接続することが可能となる。すなわち、測定装置1において貫通孔14を有する筒状部分の開口端に一方のフランジが設けられ、流路管10において開口11の周囲に立ち上げた筒状部分の開口端に他方のフランジが設けられている。これらのフランジにはそれぞれ締結用の複数のボルト孔が予め設けられており、それぞれのボルト孔の位置が合うように両フランジを突き合わせてボルト・ナットにより締結する。両フランジの各ボルト孔の位置がそれぞれ適切に配置されていれば、開口21を正確に上流に向けて固定することができる。   For example, in FIG. 1, although the example which connected the chamber 5 and the flow path pipe 10 using the external thread 13 and the internal thread 12 was demonstrated, the chamber 5 and the flow path pipe 10 were connected using the flange (not shown). Also good. When the male screw 13 and the introduction member 20 are integrated, the direction of the opening 21 of the introduction member 20 differs depending on how much the male screw 13 is rotated and screwed into the female screw 12 (rotation angle), and the opening 21 is directed upstream. There are cases where it is difficult to arrange them in a sparse manner. On the other hand, by using the flange, for example, the chamber 5 and the flow path pipe 10 can be connected with the opening 21 of the introduction member 20 fixed to the chamber 5 facing upstream. That is, one flange is provided at the opening end of the cylindrical portion having the through hole 14 in the measuring apparatus 1, and the other flange is provided at the opening end of the cylindrical portion raised around the opening 11 in the flow channel tube 10. It has been. Each of these flanges is provided with a plurality of bolt holes for fastening in advance. Both flanges are brought into contact with each other so that the positions of the respective bolt holes are matched, and are fastened by bolts and nuts. If the positions of the bolt holes of both flanges are appropriately arranged, the opening 21 can be accurately fixed upstream.

あるいは、図1において、チャンバ5の周囲に回転自在かつ脱落不能に設けられた図示しない袋ナット(中央に貫通孔を有し、この貫通孔にチャンバ5が挿入されているもの)を用いて、測定装置1と流路管10とを結合する構造を採ることもできる。この場合、測定装置1の円筒部の外周面と、流路管10の開口11の周囲に立ち上げた円筒部の内周面とには、それぞれ雄ねじ13および雌ねじ12は形成せずに、単なる嵌め合い状態とする。そして、流路管10の開口11の周囲に立ち上げた円筒部の外周面に雄ネジを形成し、これに対応する雌ねじを上記袋ナットの内周面に形成し、両者を締結することで測定装置1を流路管10に固定する。この構成によれば、測定装置1と流路管10との位置関係を固定したまま袋ナットを回転させて両者の締結を行えるので、開口21を正確に上流に向けた状態で固定することができる。上記以外にも、測定装置1と流路管10との位置関係に回転を生じさせない締結構造は種々のものが公知であるので、用途に応じて適宜採用することができる。   Alternatively, in FIG. 1, by using a cap nut (not shown) provided around the chamber 5 so as to be rotatable and non-detachable (having a through hole in the center, and the chamber 5 is inserted into the through hole), It is also possible to adopt a structure in which the measuring device 1 and the flow channel tube 10 are coupled. In this case, the male screw 13 and the female screw 12 are not formed on the outer peripheral surface of the cylindrical portion of the measuring apparatus 1 and the inner peripheral surface of the cylindrical portion raised around the opening 11 of the flow channel tube 10, respectively. It is in a fitted state. Then, a male screw is formed on the outer peripheral surface of the cylindrical portion raised around the opening 11 of the flow channel tube 10, a corresponding female screw is formed on the inner peripheral surface of the cap nut, and both are fastened. The measuring device 1 is fixed to the flow channel tube 10. According to this configuration, since the cap nut can be rotated and the both can be fastened while the positional relationship between the measuring device 1 and the flow channel tube 10 is fixed, it is possible to fix the opening 21 in a state where the opening 21 is directed accurately upstream. it can. In addition to the above, various fastening structures that do not cause rotation in the positional relationship between the measuring device 1 and the flow channel tube 10 are known, and can be appropriately employed depending on the application.

また、図14に示すように、管状の導入部材420の側壁を周回するように少なくとも3つ以上の複数の開口42a,42b,42cを設けてもよい。図8に示す流路管10内に、図14に示す導入部材420をいずれの向きに挿入しても、複数の開口42a,42b,42cのいずれかが、流路管10の上流側に対向する。また、複数の開口42a,42b,42cは管状の導入部材420の側壁に設けられているため、流路管10内のガスの進行方向に対して垂直になる。そのため、ガスを効率的に導入部材420の内部に取り込むことも可能となる。また、ねじ締結を用いる部分以外については、管・筒・孔の断面形状が円形に限定されるものではない。角管・角筒・角孔であっても良い。この様に、本発明はここでは記載していない様々な実施の形態等を包含するということを理解すべきである。   Moreover, as shown in FIG. 14, you may provide the some opening 42a, 42b, 42c of at least 3 or more so that the side wall of the tubular introduction member 420 may go around. Even if the introduction member 420 shown in FIG. 14 is inserted in any direction into the flow channel pipe 10 shown in FIG. 8, any one of the plurality of openings 42 a, 42 b, 42 c faces the upstream side of the flow path pipe 10. To do. Further, since the plurality of openings 42 a, 42 b, 42 c are provided on the side wall of the tubular introduction member 420, the openings 42 a, 42 b, 42 c are perpendicular to the gas traveling direction in the flow channel tube 10. Therefore, the gas can be efficiently taken into the introduction member 420. In addition to the portions that use screw fastening, the cross-sectional shape of the tube, tube, and hole is not limited to a circle. It may be a square tube, a square tube, or a square hole. Thus, it should be understood that the present invention includes various embodiments and the like not described herein.

1 測定装置
5 チャンバ
8 マイクロチップ
10 流路管
11 開口
14 貫通孔
18 断熱部材
20,220,320 導入部材
21,221a,221d,223 開口
22,222a,222d,224 開口
25,26a,26b,26c,26d,26e,26f 貫通孔
30 計測ユニット
32A,32B,32C,32D 仕切り板
60 基板
61 発熱抵抗体
62 測温抵抗素子
63 測温抵抗素子
64 ガス温度センサ
65 絶縁膜
66 キャビティ
100 回路基板
171 オペアンプ
181,182,183 抵抗素子
301 放熱係数算出部
302 熱伝導率算出部
303 濃度算出部
352 熱伝導率記憶装置
353 濃度記憶装置
DESCRIPTION OF SYMBOLS 1 Measuring apparatus 5 Chamber 8 Microchip 10 Channel pipe 11 Opening 14 Through-hole 18 Thermal insulation member 20,220,320 Introduction member 21,221a, 221d, 223 Opening 22,222a, 222d, 224 Opening 25,26a, 26b, 26c , 26d, 26e, 26f Through-hole 30 Measuring unit 32A, 32B, 32C, 32D Partition plate 60 Substrate 61 Heating resistor 62 Temperature measuring element 63 Temperature measuring element 64 Gas temperature sensor 65 Insulating film 66 Cavity 100 Circuit board 171 Operational amplifier 181, 182, 183 Resistance element 301 Heat radiation coefficient calculation unit 302 Thermal conductivity calculation unit 303 Concentration calculation unit 352 Thermal conductivity storage device 353 Concentration storage device

Claims (8)

流体を流す流路管に配置される測定装置であって、
前記流路管の外部に配置されるチャンバと、
前記流路管内部に突出するよう配置される、前記流路管内部から前記チャンバに前記流体を導入する筒状の導入部材であって、前記流路管内に位置する略円錐状の端部を有する導入部材と、
前記チャンバに配置され、前記流体の物性を測定するセンサと、
を備え
前記チャンバには、前記流路管に設けられた雌ねじ開口部にねじ込められる雄ねじ部が設けられており、
前記雄ねじ部には、前記流路管内部と前記チャンバ内部とを連通させる雄ねじ貫通孔が設けられており、
前記導入部材は、前記雄ねじ貫通孔内から前記流路管内部に突出し、
前記導入部材内部には、前記チャンバ内部と前記流路管内部とを連通させる複数の貫通孔が設けられており、
前記導入部材の略円錐状の端部の頂点及び側面に、前記複数の貫通孔の開口が設けられており、
前記略円錐状の端部の側面において、3つ以上の前記複数の開口が円周上に一定の間隔をおいて設けられており、
前記流路管から前記複数の開口の少なくとも一つに入った前記流体が当該導入部材の貫通孔の内壁に衝突して進行方向を変えられ、前記チャンバ内に導入される、
測定装置。
A measuring device arranged in a flow channel pipe for flowing a fluid,
A chamber disposed outside the channel tube;
Is arranged to protrude into the flow pipe section, said a tubular introduction member for introducing said fluid into the chamber from the flow pipe section, substantially conical end portion located on the flow pipe An introduction member having
Disposed in said chamber, a sensor for measuring the physical properties of the fluid,
Equipped with a,
The chamber is provided with a male screw portion that can be screwed into a female screw opening provided in the flow channel pipe,
The male screw part is provided with a male screw through-hole that allows the inside of the flow channel tube and the inside of the chamber to communicate with each other.
The introduction member protrudes from the inside of the male screw through hole into the flow channel pipe,
In the introduction member, a plurality of through-holes are provided for communicating the inside of the chamber and the inside of the flow channel pipe,
Openings of the plurality of through holes are provided at the apex and side surfaces of the substantially conical end of the introduction member,
On the side surface of the substantially conical end, three or more of the plurality of openings are provided on the circumference at regular intervals,
The fluid that has entered at least one of the plurality of openings from the flow channel tube collides with the inner wall of the through hole of the introduction member to change the traveling direction, and is introduced into the chamber.
measuring device.
流体を流す流路管に配置される測定装置であって、  A measuring device arranged in a flow channel pipe for flowing a fluid,
前記流路管の外部に配置されるチャンバと、  A chamber disposed outside the channel tube;
前記チャンバ内に配置され、前記流路管から前記チャンバ内に導入された前記流体の物性を測定するセンサと、  A sensor that is disposed in the chamber and that measures physical properties of the fluid introduced into the chamber from the flow path pipe;
を備え、  With
前記チャンバには、前記流路管に設けられた雌ねじ開口部にねじ込められる雄ねじ部が設けられており、  The chamber is provided with a male screw portion that can be screwed into a female screw opening provided in the flow channel pipe,
前記雄ねじ部には、前記チャンバ内部と前記流路管内部とを連通させる雄ねじ貫通孔が設けられており、  The male screw portion is provided with a male screw through hole for communicating the inside of the chamber and the inside of the flow channel tube,
前記雄ねじ貫通孔には、断面において放射状に配置された少なくとも3つ以上の複数の仕切り板が配置されており、  In the male screw through hole, a plurality of partition plates of at least three or more arranged radially in cross section are arranged,
前記複数の仕切り板が、前記貫通孔内から前記流路管内部に突出するよう配置され、  The plurality of partition plates are arranged so as to protrude from the through hole into the flow channel pipe,
前記流路管内部において前記複数の仕切り板に衝突した前記流体が進行方向を変えられ、前記チャンバ内に導入される、  The fluid that has collided with the plurality of partition plates inside the channel pipe is changed in the traveling direction, and is introduced into the chamber.
測定装置。  measuring device.
前記導入部材の略円錐状の端部の側面に設けられた前記開口が、前記流路管内の流体の進行方向に対して斜めになる、請求項1に記載の測定装置。 The measuring apparatus according to claim 1, wherein the opening provided on a side surface of the substantially conical end portion of the introduction member is inclined with respect to a traveling direction of the fluid in the flow channel pipe. 前記導入部材の略円錐状の端部の側面に設けられた前記開口の少なくとも一部が、前記流路管の上流を向く、請求項1又は3に記載の測定装置。 At least a portion of said opening substantially provided on the side surface of the conical end portion of the introducing member, faces the upstream of the flow pipe, measuring device according to claim 1 or 3. 前記流体が、ガスである、請求項1乃至のいずれか1項に記載の測定装置。 Wherein the fluid is a gas, the measurement apparatus according to any one of claims 1 to 4. 前記流体の物性が、前記ガスの放熱係数である、請求項に記載の測定装置。 The measuring apparatus according to claim 5 , wherein the physical property of the fluid is a heat dissipation coefficient of the gas. 前記流体の物性が、前記ガスの熱伝導率である、請求項に記載の測定装置。 The measuring apparatus according to claim 5 , wherein the physical property of the fluid is a thermal conductivity of the gas. 前記放熱係数に基づいて、前記ガスの濃度を算出する濃度算出部を更に備える、請求項に記載の測定装置。 The measurement apparatus according to claim 6 , further comprising a concentration calculation unit that calculates the concentration of the gas based on the heat dissipation coefficient.
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