JP5283016B2 - Diamond sintered body for cutting tools containing coarse diamond particles - Google Patents
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Description
本発明は、ダイヤモンドを主成分として刃先に有する切削工具を製造するためのダイヤモンド焼結体に関する。 The present invention relates to a diamond sintered body for manufacturing a cutting tool having diamond as a main component at a cutting edge.
従来、アルミ合金等、軟質金属の超精密加工に単結晶ダイヤモンド工具が用いられている。しかし、大きなサイズの単結晶ダイヤモンドが高価であることから、単結晶ダイヤモンド工具は製造コストが高いという問題点がある。また、ダイヤモンド粉末をCo等の結合材により焼結した多結晶ダイヤモンド焼結体は、単結晶ダイヤモンド工具よりも安価であるが、多結晶体であるがゆえに超精密加工で要求されるRzで0.5μm以下の面粗度は得られず、被削材の表面にも筋が発生するという問題もある。 Conventionally, single crystal diamond tools have been used for ultra-precision machining of soft metals such as aluminum alloys. However, since a large size single crystal diamond is expensive, the single crystal diamond tool has a problem of high manufacturing cost. In addition, a polycrystalline diamond sintered body obtained by sintering diamond powder with a binding material such as Co is less expensive than a single crystal diamond tool, but because it is a polycrystalline body, Rz required for ultraprecision machining is 0. There is also a problem that a surface roughness of 0.5 μm or less cannot be obtained, and streaks are generated on the surface of the work material.
そこで、本発明は、上記問題点に鑑みて、耐摩耗性に優れ、被削材の面粗度の改善が可能な切削工具を安価に製造することを可能とする切削工具用ダイヤモンド焼結体を提供することを課題とする。 Therefore, in view of the above problems, the present invention provides a diamond sintered body for a cutting tool that can be manufactured at low cost with a cutting tool that has excellent wear resistance and can improve the surface roughness of the work material. It is an issue to provide.
被削材を切削加工する場合、図3に示すように、横切れ刃境界部で被削材が大きく切り取られ、前切れ刃境界部により仕上げ面の形成が行われる。このため、被削材表面には前切れ刃境界部の形状が転写されることとなる。したがって、前切れ刃境界部の摩耗が進行して前切れ刃の表面粗さが悪くなると、被削材表面も粗くなり仕上がり状態が悪くなる。また、被削材表面に筋が発生し始めると境界摩耗が更に発達して前切れ刃境界部に溝が形成され、上記問題が一層顕著となり、短時間で加工表面粗さが悪化してしまう。(図4参照) When cutting a work material, as shown in FIG. 3, the work material is largely cut off at the lateral cutting edge boundary portion, and a finished surface is formed by the front cutting edge boundary portion. For this reason, the shape of the front cutting edge boundary portion is transferred to the surface of the work material. Therefore, if the wear of the front cutting edge boundary progresses and the surface roughness of the front cutting edge deteriorates, the surface of the work material also becomes rough and the finished state deteriorates. In addition, when the streak begins to occur on the surface of the work material, boundary wear further develops and grooves are formed at the front cutting edge boundary, and the above problem becomes more prominent, and the machining surface roughness deteriorates in a short time. . (See Figure 4)
本発明者等は、工具刃先の前切れ刃境界部の摩耗が、なるべく平滑に進行するようにすることができれば、被削材の面粗さが悪化しにくく、長寿命で高精度加工が行えることを見出した。すなわち、少なくとも、切れ刃の切削時における前境界部分を、ダイヤモンド単結晶体にすることが有効であることを見出し、本発明を完成させた。なお、「平滑に摩耗する」とは、前切れ刃境界部の摩耗が抑制され、段差や溝(筋)の形成が押さえられて滑らかになる状態のことをいう。
以上のように、本発明者等は、ダイヤモンド切削工具による切削加工において被削材の面粗度を改善させるべく鋭意研究を重ねた結果、切削では切れ刃の各部位で異なった特性が要求されることを見出した。
If the wear of the front cutting edge boundary part of the tool edge can proceed as smoothly as possible, the present inventors can prevent the surface roughness of the work material from being deteriorated, and can perform high-precision machining with a long life. I found out. That is, it has been found that it is effective to make at least the front boundary portion at the time of cutting of the cutting edge a diamond single crystal, and the present invention has been completed. “Smoothly wear” refers to a state in which wear at the front cutting edge boundary portion is suppressed and formation of a step or a groove (streak) is suppressed to make it smooth.
As described above, the present inventors have intensively studied to improve the surface roughness of the work material in cutting with a diamond cutting tool, and as a result, different characteristics are required for each part of the cutting edge in cutting. I found out.
しかしながら、従来のダイヤモンド焼結体は様々なダイヤモンド粒径の焼結体が用いられているが、これら従来の焼結体ではダイヤモンド粒子の粒径が連続的に分布しており、かつ、焼結体中でダイヤモンド粒子の粒度分布が焼結体全体のダイヤモンド粒度分布に近い状態となっているため、切れ刃を作製した場合に該切れ刃の任意の部分の機能は等しいものとなっている。このため、従来のダイヤモンド焼結体中の任意の部分の機能が等しい焼結体では、上述したような切れ刃の部位によって異なる要求特性に対して、共に機能が発揮されるように材料設計がなされるが、各部位の要求特性に対する最適な材料設計とはならず、性能に限度がある。 However, the conventional diamond sintered bodies use sintered bodies having various diamond particle diameters. In these conventional sintered bodies, the diameters of the diamond particles are continuously distributed, and the sintered bodies are sintered. Since the particle size distribution of the diamond particles in the body is close to the diamond particle size distribution of the entire sintered body, the function of an arbitrary part of the cutting edge is equal when the cutting edge is manufactured. For this reason, in a sintered body having an equal function in any part of a conventional diamond sintered body, the material design is such that both functions can be exhibited with respect to the required characteristics that differ depending on the portion of the cutting edge as described above. However, it is not an optimum material design for the required characteristics of each part, and there is a limit in performance.
本発明者等は以上の点に着目し、粗粒のダイヤモンド粒子と微粒のダイヤモンド粒子とが適切に混合されたダイヤモンド焼結体により、各部位の要求特性が最適なものとなる切れ刃を提供できることを見出し、本発明を完成させた。すなわち、本発明は以下の特徴を有する。 The present inventors pay attention to the above points, and provide a cutting edge in which the required characteristics of each part are optimized by a diamond sintered body in which coarse diamond particles and fine diamond particles are appropriately mixed. The present invention has been completed by finding out what can be done. That is, the present invention has the following features.
(1)本発明に係る切削工具用ダイヤモンド焼結体は、
ダイヤモンド含有率が70−98体積%であり、
第1ダイヤモンド粒子群と第2ダイヤモンド粒子群とを有し、
該第1ダイヤモンド粒子群の平均粒径が50μm以上であり、かつ、第2ダイヤモンド粒子群の平均粒径の5倍以上であり、
第2ダイヤモンド粒子群の平均粒径が20μm以下であり、かつ、第2ダイヤモンド粒子群の含有率が50体積%以上であり、
結合相が少なくとも鉄族金属を有することを特徴とする。
(2)上記(1)に記載のダイヤモンド焼結体であって、前記鉄族金属として、Fe、Co、Niのいずれかを有することを特徴とする。
(3)上記(1)又は(2)に記載のダイヤモンド焼結体であって、前期第1ダイヤモンド粒子群の平均粒径(粒子直径)が100μm以上であり、前記第2ダイヤモンド粒子群の平均粒径が8μm以下であることを特徴とする。
(1) A diamond sintered body for a cutting tool according to the present invention comprises:
The diamond content is 70-98% by volume;
A first diamond particle group and a second diamond particle group;
The average particle size of the first diamond particle group is 50 μm or more, and is 5 times or more the average particle size of the second diamond particle group,
The average particle size of the second diamond particle group is 20 μm or less, and the content of the second diamond particle group is 50% by volume or more,
The binder phase has at least an iron group metal.
(2) The diamond sintered body according to (1), wherein the iron group metal includes any one of Fe, Co, and Ni.
(3) The diamond sintered body according to (1) or (2) above, wherein an average particle diameter (particle diameter) of the first diamond particle group is 100 μm or more, and an average of the second diamond particle group The particle size is 8 μm or less.
本発明に係るダイヤモンド焼結体中には、所定以上の粒子直径を有するダイヤモンド粒子が配置されているため、大粒径のダイヤモンド単結晶体を切れ刃、もしくは切れ刃の一部とする、ダイヤモンド焼結体工具の生産が可能となる。これら大粒径のダイヤモンド単結晶体を、切れ刃の前境界部に用いることにより軟質金属の超精密加工でRz(十点平均粗さ)が0.5μm以下の優れた面粗度が得られる。また、単結晶ダイヤモンドからなる従来の切削工具よりも安価な工具の生産を可能とするダイヤモンド焼結体を提供することができる。 In the diamond sintered body according to the present invention, diamond particles having a particle diameter of a predetermined size or more are arranged, so that a diamond single crystal having a large particle diameter is used as a cutting edge or a part of a cutting edge. Sintered body tools can be produced. By using these large-diameter diamond single crystals at the front boundary of the cutting edge, an excellent surface roughness with an Rz (ten-point average roughness) of 0.5 μm or less can be obtained by ultra-precision machining of a soft metal. . Further, it is possible to provide a diamond sintered body that enables production of a tool that is cheaper than a conventional cutting tool made of single crystal diamond.
本発明に係るダイヤモンド焼結体は、第1ダイヤモンド粒子群と第2ダイヤモンド粒子群とを有し、該第1ダイヤモンド粒子群の平均粒径(粒子直径)が50μm以上であり、かつ、第1ダイヤモンド粒子群の平均粒径が第2ダイヤモンド粒子群の平均粒径の5倍以上であることを特徴とする。平均粒径が50μm以上の粗粒ダイヤモンド粒子(単結晶体)と、平均粒径が該粗粒ダイヤモンド粒子の1/5以下である微粒のダイヤモンド粒子とを有することにより、切削工具の切れ刃の任意の部分に所期の機能を持たせることが可能となる。 The diamond sintered body according to the present invention has a first diamond particle group and a second diamond particle group, the average particle diameter (particle diameter) of the first diamond particle group is 50 μm or more, and the first The average particle size of the diamond particle group is at least five times the average particle size of the second diamond particle group. By having coarse diamond particles (single crystal) having an average particle size of 50 μm or more and fine diamond particles having an average particle size of 1/5 or less of the coarse diamond particles, It is possible to give the desired function to an arbitrary part.
例えば、前切れ刃境界部を含む前切れ刃部分に粗粒のダイヤモンド単結晶体を配置することにより、前切れ刃の摩耗を平滑に進行させて、被削材の面粗度を良好にすることができる。この観点から、前記第1ダイヤモンド粒子群の、より好ましい平均粒径は100μm以上である。 For example, by arranging a coarse-grained diamond single crystal on the front cutting edge portion including the front cutting edge boundary portion, the wear of the front cutting edge is smoothly advanced, and the surface roughness of the work material is improved. be able to. From this viewpoint, the more preferable average particle diameter of the first diamond particle group is 100 μm or more.
一方、ダイヤモンド単結晶体の劈開性によるチッピング等が問題となる場合には、その切れ刃部分を微粒のダイヤモンド粒子群によるダイヤモンド多結晶体により構成すれば良い。また、前切れ刃部分以外の切れ刃部分をダイヤモンド多結晶体により形成すれば、ダイヤモンド単結晶体のみから工具を作製する場合に比べて低コストで提供することが可能となるメリットもある。これらの観点から、前記第2ダイヤモンド粒子群のより好ましい平均粒径は8μm以下である。 On the other hand, when chipping due to the cleavage property of the diamond single crystal is a problem, the cutting edge portion may be formed of a diamond polycrystal formed by a group of fine diamond particles. In addition, if the cutting edge portion other than the front cutting edge portion is formed of a polycrystalline diamond, there is an advantage that it can be provided at a lower cost compared to the case where a tool is produced from only a diamond single crystal. From these viewpoints, a more preferable average particle diameter of the second diamond particle group is 8 μm or less.
上記ダイヤモンド焼結体は、ダイヤモンド含有率が70−98体積%であることを特徴とする。ダイヤモンドの含有率がこれらの範囲にあることにより、焼結体の強度と耐摩耗性を両立させることが可能となる。より好ましいダイヤモンド含有率の範囲は、80〜95体積%である。 The diamond sintered body has a diamond content of 70 to 98% by volume. When the content of diamond is within these ranges, it is possible to achieve both the strength and wear resistance of the sintered body. A more preferable range of the diamond content is 80 to 95% by volume.
更に、焼結体の結合相が、少なくとも鉄族金属を有することを特徴とする。該鉄族金属としては、Fe、Co、Niから選ばれるいずれか1種以上を有することが好ましい。これらの結合材成分により、ダイヤモンド焼結体の耐摩耗性及び強度を向上させることができる。当然、これらの成分以外にも不可避的に不純物が含まれていても構わない。 Furthermore, the binder phase of the sintered body has at least an iron group metal. The iron group metal preferably has at least one selected from Fe, Co, and Ni. With these binder components, the wear resistance and strength of the diamond sintered body can be improved. Of course, impurities other than these components may inevitably be contained.
本発明に係るダイヤモンド焼結体により、例えば、以下のような切削工具の製造が可能となる。
<前切れ刃境界部が単結晶体である切削工具の作製>
前述のように、被削材表面を平滑に仕上るには、前切れ刃境界部付近の刃先摩耗は凹凸無く平滑に進行することが好ましい。図3に示すように、前切れ刃境界部により仕上り面の形成が行われるため、被削材表面には前切れ刃境界部の形状が転写されるからである。なお、「平滑に摩耗する」とは、前切れ刃境界部の摩耗が抑制され、段差や溝(筋)の形成が押さえられて滑らかになる状態のことをいう。
With the diamond sintered body according to the present invention, for example, the following cutting tool can be manufactured.
<Preparation of a cutting tool whose front edge boundary is a single crystal>
As described above, in order to finish the surface of the work material smoothly, it is preferable that the edge wear near the front cutting edge boundary portion proceeds smoothly without unevenness. As shown in FIG. 3, since the finished surface is formed by the front cutting edge boundary portion, the shape of the front cutting edge boundary portion is transferred to the surface of the work material. “Smoothly wear” refers to a state in which wear at the front cutting edge boundary portion is suppressed and formation of a step or a groove (streak) is suppressed to make it smooth.
したがって、被削材の面粗度を良好にするためには、図1に示すように、被削材と接触する切れ刃部分において、切り込み量が最大となる点から、送り方向の切れ刃は切り込み量のx%(x≧10)が、送りと反対方向の切れ刃は切り込み量のy%(y≧10)がダイヤモンド単結晶体で形成されていることが好ましい。これにより、前切れ刃境界部分もダイヤモンド単結晶体により形成されるため、耐摩耗性に優れた前切れ刃となる。このため、ダイヤモンド多結晶体で切削した場合のような被削材表面の面粗度の悪化、筋の発生を抑制すると同時に、前切れ刃境界部分が平滑に摩耗するようになり、長寿命の切削工具となる。 Therefore, in order to improve the surface roughness of the work material, as shown in FIG. 1, the cutting edge in the feed direction is selected from the point where the cutting amount becomes maximum at the cutting edge portion in contact with the work material. It is preferable that the cutting edge in the direction opposite to the feed with x% (x ≧ 10) of the cutting amount is y% (y ≧ 10) of the cutting amount is formed of a diamond single crystal. Thereby, since the front cutting edge boundary part is also formed of the diamond single crystal, the front cutting edge is excellent in wear resistance. For this reason, the surface roughness of the work material surface, such as when cutting with a polycrystalline diamond, is suppressed, and at the same time, the front edge of the cutting edge wears smoothly and has a long service life. It becomes a cutting tool.
一方、横切れ刃境界部分は、被削材を大きく切り取る部分であり、特に仕上げ面の面粗さに影響を与えることは無い。このため、前記切り込み量が最大となる点から、送り方向の切れ刃は切り込み量のx%(x≧10)を、送りと反対方向の切れ刃は切り込み量のy%(y≧10)を越える部分をダイヤモンド多結晶体で形成すれば、ダイヤモンド単結晶体のみから工具を作製する場合に比べて低コストで提供することが可能となる。また、xとyは各々80を超えると刃先の研磨コストが高くなるため、80以下であることが好ましい。 On the other hand, the horizontal cutting edge boundary portion is a portion where the work material is largely cut, and does not particularly affect the surface roughness of the finished surface. For this reason, the cutting edge in the feed direction has x% (x ≧ 10) of the cutting amount and the cutting edge in the direction opposite to the feeding has y% (y ≧ 10) of the cutting amount from the point where the cutting amount becomes maximum. If the exceeding portion is formed of a diamond polycrystal, it can be provided at a lower cost than when a tool is produced only from a diamond single crystal. Moreover, since x and y each exceed 80 and the grinding | polishing cost of a blade edge will become high, it is preferable that it is 80 or less.
このような切削工具を作製するためには、本発明に係るダイヤモンド焼結体から、前切れ刃部分がダイヤモンド単結晶体により、横切れ刃部分がダイヤモンド多結晶体により構成されるように切り出せば良い(図2参照)。このとき、切削時に被削材に接触する切れ刃のうち、切り込み量が最大となる点から、送り方向の切れ刃は切り込み量のx%(x≧10)まで、送りと反対方向の切れ刃は切り込み量のy%(y≧10)までが、粒子直径が50μm以上のダイヤモンド粒子により構成されることが好ましい。該ダイヤモンド単結晶体の粒子直径は100μm以上であることがより好ましい。 In order to produce such a cutting tool, it suffices to cut from the diamond sintered body according to the present invention so that the front cutting edge portion is constituted by a diamond single crystal and the side cutting edge portion is constituted by a diamond polycrystal. (See FIG. 2). At this time, among cutting edges that come into contact with the work material at the time of cutting, the cutting edge in the feed direction is up to x% (x ≧ 10) of the cutting amount from the point where the cutting amount is maximum, and the cutting edge in the direction opposite to the feeding direction Is preferably constituted by diamond particles having a particle diameter of 50 μm or more, up to y% (y ≧ 10) of the cutting depth. More preferably, the diamond single crystal has a particle diameter of 100 μm or more.
被削材がアルミ合金や無酸素銅等である場合に、超精密切削加工を行うには、一般的に、切り込み量は0.01〜0.15mm、送り量は0.001〜0.2mm/revの条件で行われる。このような場合、摩耗の進展により刃先が後退するため、前記ダイヤモンド焼結体工具のノーズ先端部分から送り方向の切れ刃は切り込み量のx%が、送りと反対方向の切れ刃は切り込み量のy%がダイヤモンド単結晶体で形成され、x、yが10以上であることが望ましい。これにより、前切れ刃境界部分が、ダイヤモンド単結晶体で構成され、横切れ刃境界部分はダイヤモンド多結晶体で構成されることとなる。 When the work material is an aluminum alloy, oxygen-free copper or the like, in order to perform ultra-precise cutting, in general, the cut amount is 0.01 to 0.15 mm, and the feed amount is 0.001 to 0.2 mm. This is performed under the condition of / rev. In such a case, since the cutting edge moves backward due to the progress of wear, the cutting edge in the feed direction from the nose tip of the diamond sintered body tool has x% of the cutting amount, and the cutting edge in the direction opposite to the feeding has the cutting amount. It is desirable that y% is formed of a diamond single crystal, and x and y are 10 or more. As a result, the front cutting edge boundary portion is composed of a diamond single crystal, and the lateral cutting edge boundary portion is composed of a diamond polycrystal.
超硬合金製のポット及びボールを用いて、ダイヤモンド粒子とCo、WC等の結合材材料を混合してから熱処理を施し、この粉末をCo板と共にMo製容器に充填し、圧力5.5GPa、温度1,410℃で22分焼結し、表1に記載のダイヤモンド焼結体を得た。この焼結体を切断し、基材として超硬合金製の台金にロー材を用いて接合した後、研磨加工を実施し、切削工具(TPGN110308)を作製した。このとき、工具の前切れ刃境界部に粗粒のダイヤモンド単結晶体が配置され、被削材と接触する切れ刃部分において、切込みが最大となる点から、送り方向の切れ刃は切り込み量の30%が、送りと反対方向の切れ刃は切り込み量の40%がダイヤモンド単結晶体で形成され、被削材と接触する他の切れ刃部分がダイヤモンド多結晶体で形成されるように焼結体中の粗粒ダイヤモンド単結晶粒子の位置を確認した後、切断、接合、研磨を実施した。 Using cemented carbide pots and balls, diamond particles and binder materials such as Co and WC are mixed and then heat-treated, and this powder is filled into a Mo container together with a Co plate, with a pressure of 5.5 GPa, Sintering was performed at a temperature of 1,410 ° C. for 22 minutes, and diamond sintered bodies shown in Table 1 were obtained. This sintered body was cut and joined to a base metal made of cemented carbide using a brazing material as a base material, and then subjected to polishing to produce a cutting tool (TPGN110308). At this time, a coarse diamond single crystal body is arranged at the front cutting edge boundary portion of the tool, and the cutting edge in the feed direction has a cutting amount from the point where the cutting becomes the maximum at the cutting edge portion in contact with the work material. 30% of the cutting edge in the direction opposite to the feed is sintered so that 40% of the cutting depth is formed of a diamond single crystal, and the other cutting edge portion in contact with the work material is formed of a polycrystalline diamond. After confirming the position of the coarse diamond single crystal particles in the body, cutting, joining and polishing were performed.
この切削工具を用いて、被削材として無酸素銅を用い、表2に記載の条件で切削試験を実施した。その結果、寿命判定基準をRzで0.4μmとして、表2に記載の工具寿命が得られた。 Using this cutting tool, oxygen-free copper was used as a work material, and a cutting test was performed under the conditions shown in Table 2. As a result, the tool life shown in Table 2 was obtained by setting the life criterion as 0.4 μm in Rz.
Claims (3)
第1ダイヤモンド粒子群と第2ダイヤモンド粒子群とを有し、
第1ダイヤモンド粒子群の平均粒径が50μm以上であり、かつ、第2ダイヤモンド粒子群の平均粒径の5倍以上であり、
第2ダイヤモンド粒子群の平均粒径が20μm以下であり、かつ、第2ダイヤモンド粒子群の含有率が50体積%以上であり、
結合相が少なくとも鉄族金属を有することを特徴とする切削工具用ダイヤモンド焼結体。 The diamond content is 70-98% by volume;
A first diamond particle group and a second diamond particle group;
The average particle size of the first diamond particle group is 50 μm or more, and is 5 times or more the average particle size of the second diamond particle group,
The average particle size of the second diamond particle group is 20 μm or less, and the content of the second diamond particle group is 50% by volume or more,
A diamond sintered body for a cutting tool, wherein the binder phase has at least an iron group metal.
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