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JP6420201B2 - Air separation device - Google Patents
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JP6420201B2 - Air separation device - Google Patents

Air separation device Download PDF

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JP6420201B2
JP6420201B2 JP2015095114A JP2015095114A JP6420201B2 JP 6420201 B2 JP6420201 B2 JP 6420201B2 JP 2015095114 A JP2015095114 A JP 2015095114A JP 2015095114 A JP2015095114 A JP 2015095114A JP 6420201 B2 JP6420201 B2 JP 6420201B2
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nitrogen
flow path
unit
temperature
liquid
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JP2016211777A (en
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啓 岸本
啓 岸本
井上 憲一
憲一 井上
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Kobe Steel Ltd
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Kobe Steel Ltd
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/044Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a single pressure main column system only
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04048Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams
    • F25J3/0406Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams of nitrogen
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    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
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    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04109Arrangements of compressors and /or their drivers
    • F25J3/04115Arrangements of compressors and /or their drivers characterised by the type of prime driver, e.g. hot gas expander
    • F25J3/04133Electrical motor as the prime mechanical driver
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    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
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    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04333Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using quasi-closed loop internal vapor compression refrigeration cycles, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04351Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using quasi-closed loop internal vapor compression refrigeration cycles, e.g. of intermediate or oxygen enriched (waste-)streams of nitrogen
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    • F25J3/04521Coupling of the air fractionation unit to an air gas-consuming unit, so-called integrated processes
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    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04521Coupling of the air fractionation unit to an air gas-consuming unit, so-called integrated processes
    • F25J3/04612Heat exchange integration with process streams, e.g. from the air gas consuming unit
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04781Pressure changing devices, e.g. for compression, expansion, liquid pumping
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    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
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    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04866Construction and layout of air fractionation equipments, e.g. valves, machines
    • HELECTRICITY
    • H02GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
    • H02KDYNAMO-ELECTRIC MACHINES
    • H02K55/00Dynamo-electric machines having windings operating at cryogenic temperatures
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10NELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N60/00Superconducting devices
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    • F25J2200/00Processes or apparatus using separation by rectification
    • F25J2200/40Features relating to the provision of boil-up in the bottom of a column
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    • F25J2230/00Processes or apparatus involving steps for increasing the pressure of gaseous process streams
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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Description

本発明は、深冷分離法によって原料空気を分離する空気分離装置に関する。   The present invention relates to an air separation device for separating raw material air by a cryogenic separation method.

空気を分離して酸素と窒素とを大規模に製造する場合、現在、深冷分離法が広く用いられている。深冷分離法では、空気を液化し、酸素と窒素との沸点差を利用して蒸留(精留)することにより、空気を酸素と窒素とに分離する。深冷分離と言われるのは、空気の液化温度が−170〜−190℃付近であり、深冷分離法が断熱された極低温の系で実施されるからである。   In the case of producing oxygen and nitrogen on a large scale by separating air, a cryogenic separation method is currently widely used. In the cryogenic separation method, air is liquefied and distilled (rectification) using a difference in boiling points between oxygen and nitrogen to separate air into oxygen and nitrogen. The reason for the cryogenic separation is that the liquefaction temperature of air is around -170 to -190 ° C., and the cryogenic separation method is carried out in an insulated cryogenic system.

深冷分離法を用いる空気分離装置は、精留塔を備えており、精留塔は、原料空気の組成である窒素、酸素の液化温度まで原料空気を冷却することで、気液分離によって純度の高い窒素および酸素を生成する。   The air separation apparatus using the cryogenic separation method includes a rectifying column, and the rectifying column is purified by gas-liquid separation by cooling the raw air to the liquefaction temperature of nitrogen and oxygen which are the composition of the raw air. Produces high nitrogen and oxygen.

深冷分離法を用いる空気分離装置として、窒素を還流する凝縮回路を備える空気分離装置がある(例えば、特許文献1,2参照)。凝縮回路は、精留塔から取り出された気体状態の窒素(製品窒素)のうち、一部の窒素を液化して精留塔に戻す。この空気分離装置よれば、窒素の凝縮回路を備え、これにより、窒素の凝縮熱を酸素の蒸発熱として与えることで、熱循環量が増えるので、凝縮回路を備えない空気分離装置と比べて、空気分離装置のエネルギー消費を20〜30%削減できることが知られている。   As an air separation device using a cryogenic separation method, there is an air separation device provided with a condensing circuit for refluxing nitrogen (see, for example, Patent Documents 1 and 2). The condensing circuit liquefies part of the nitrogen (product nitrogen) extracted from the rectification column and returns it to the rectification column. According to this air separation device, it is provided with a nitrogen condensing circuit, thereby giving the heat of nitrogen condensation as the heat of evaporation of oxygen, so that the amount of heat circulation increases, so compared to an air separation device without a condensing circuit, It is known that the energy consumption of air separation devices can be reduced by 20-30%.

特許第5415192号明細書Japanese Patent No. 5415192 特許第5684058号明細書Japanese Patent No. 5684058

近年、地球温暖化の抑制、及び、エネルギー価格の高騰により、省エネルギーが強く要請されており、空気分離装置も例外ではない。   In recent years, there has been a strong demand for energy saving due to suppression of global warming and rising energy prices, and air separation devices are no exception.

本発明の目的は、精留塔から取り出された気体状態の窒素のうち、一部の窒素を液化して精留塔に戻す凝縮回路を備える空気分離装置に関して、省エネルギー化を図ることである。   An object of the present invention is to save energy with respect to an air separation apparatus including a condensing circuit that liquefies a part of nitrogen in a gaseous state taken out from a rectification column and returns it to the rectification column.

本発明に係る空気分離装置は、液体状態の原料空気を深冷分離して気体状態の窒素を生成する精留塔と、前記精留塔から取り出された気体状態の窒素のうち、一部の窒素が供給され、供給された窒素を気体状態から液体状態に変化させて前記精留塔に戻す凝縮回路と、冷却回路と、を備え、前記凝縮回路は、液体窒素の沸点より高い臨界温度を有する超電導材料で構成された超電導磁石を含む超電導モータと、前記超電導モータによって駆動され、前記凝縮回路を流れる気体状態の窒素を圧縮する圧縮部と、を備え、前記冷却回路は、前記凝縮回路を流れる液体状態の窒素、又は、前記凝縮回路を流れ、前記圧縮部に導かれる前の気体状態の窒素を用いて、前記超電導磁石を前記臨界温度以下に冷却する。   An air separation apparatus according to the present invention includes a rectifying column that cryogenically separates raw material air in a liquid state to generate gaseous nitrogen, and a part of the gaseous nitrogen extracted from the rectifying column. A condensing circuit for supplying nitrogen, changing the supplied nitrogen from a gaseous state to a liquid state and returning the nitrogen to the rectification column, and a cooling circuit, the condensing circuit having a critical temperature higher than the boiling point of liquid nitrogen. A superconducting motor including a superconducting magnet composed of a superconducting material, and a compression unit that is driven by the superconducting motor and compresses nitrogen in a gas state flowing through the condensing circuit, and the cooling circuit includes the condensing circuit. The superconducting magnet is cooled to the critical temperature or lower using flowing nitrogen in the liquid state or nitrogen in the gas state before flowing through the condensation circuit and being led to the compression unit.

超電導モータは、超電導磁石を構成する超電導材料の臨界温度以下に、超電導磁石が冷却された状態で使用される。超電導磁石の冷却には、臨界温度以下の温度を有する冷媒が用いられる。冷媒の温度を臨界温度以下にするには、冷凍機が必要となるが、これより、空気分離装置のエネルギー消費が増加する。   The superconducting motor is used in a state where the superconducting magnet is cooled below the critical temperature of the superconducting material constituting the superconducting magnet. For cooling the superconducting magnet, a refrigerant having a temperature lower than the critical temperature is used. In order to make the temperature of the refrigerant below the critical temperature, a refrigerator is required, but this increases the energy consumption of the air separation device.

本発明に係る空気分離装置では、超電導磁石を臨界温度以下に冷却する冷媒として、窒素を還流する凝縮回路を流れる液体状態又は気体状態の窒素を用いる。従って、本発明に係る空気分離装置によれば、冷凍機が不要なので、空気分離装置の省エネルギー化を図ることができる。   In the air separation device according to the present invention, liquid or gaseous nitrogen flowing in a condensing circuit for refluxing nitrogen is used as a refrigerant for cooling the superconducting magnet to a critical temperature or lower. Therefore, according to the air separation device of the present invention, since a refrigerator is not required, energy saving of the air separation device can be achieved.

気体状態の窒素を冷媒に用いる場合、圧縮部に導かれる前の気体状態の窒素としたのは、この窒素は、ボイルオフガスであり、温度が77K(液化窒素の沸点)だからである。   When nitrogen in the gaseous state is used as the refrigerant, the nitrogen in the gaseous state before being introduced to the compression unit is because this nitrogen is a boil-off gas and has a temperature of 77 K (the boiling point of liquefied nitrogen).

上記構成において、前記凝縮回路は、前記精留塔と前記圧縮部とを接続し、前記精留塔から供給された気体状態の窒素を前記圧縮部に導く第1の流路をさらに備え、前記冷却回路は、前記第1の流路と接続され、前記第1の流路を流れる気体状態の窒素の一部を前記超電導磁石に供給する第2の流路と、前記第1の流路と接続され、前記第2の流路によって前記超電導磁石に供給された気体状態の窒素を前記第1の流路に戻す第3の流路と、を備える。   In the above-described configuration, the condensing circuit further includes a first flow path that connects the rectification column and the compression unit and guides nitrogen in a gaseous state supplied from the rectification column to the compression unit, The cooling circuit is connected to the first flow path, and a second flow path for supplying a part of the gaseous nitrogen flowing through the first flow path to the superconducting magnet; the first flow path; A third flow path that is connected and returns the nitrogen in the gaseous state supplied to the superconducting magnet by the second flow path to the first flow path.

この構成は、凝縮回路を流れ、圧縮部に導かれる前の気体状態の窒素を用いて、超電導磁石を臨界温度以下に冷却する。   In this configuration, the superconducting magnet is cooled to a critical temperature or lower using nitrogen in a gas state before flowing into the condensing circuit and being led to the compression unit.

上記構成において、前記凝縮回路は、前記圧縮部によって圧縮された気体状態の窒素を膨張させることにより、窒素を気体状態から液体状態に変化させる膨張部と、前記膨張部と前記精留塔とを接続し、液体状態の窒素を前記精留塔に導く第4の流路と、をさらに備え、前記冷却回路は、前記第4の流路に接続され、前記第4の流路を流れる液体状態の窒素の一部を前記超電導磁石に供給する第5の流路と、前記第4の流路に接続され、前記第5の流路によって前記超電導磁石に供給された液体状態の窒素を前記第4の流路に戻す第6の流路と、を備える。   In the above configuration, the condensing circuit expands the nitrogen in a gas state compressed by the compression unit, thereby expanding an expansion unit that changes nitrogen from a gas state to a liquid state, the expansion unit, and the rectification tower. And a fourth flow path for guiding nitrogen in a liquid state to the rectification tower, wherein the cooling circuit is connected to the fourth flow path and flows in the fourth flow path A fifth flow path for supplying a part of the nitrogen to the superconducting magnet and the fourth flow path, and the liquid nitrogen supplied to the superconducting magnet by the fifth flow path is supplied to the superconducting magnet. A sixth flow path returning to the fourth flow path.

超電導モータの運転中に、急激な負荷変動等が発生したとき、超電導モータには渦電流による発熱が生じる。この発熱で超電導磁石の微小部分で超電導状態が破れると、そこから局所的に発熱し、これが原因で超電導モータが破損することがある。   When a sudden load change or the like occurs during operation of the superconducting motor, the superconducting motor generates heat due to eddy current. If the superconducting state is broken at a minute portion of the superconducting magnet due to this heat generation, heat is locally generated from the superconducting magnet, which may cause damage to the superconducting motor.

従って、上記渦電流による発熱が生じたとき、この発熱を速やかに冷却する必要がある。液体は気体に比べて熱伝達係数が大きい。この構成によれば、液体状態の窒素(すなわち、液化窒素)を用いて、超電導磁石を冷却するので、上記渦電流による発熱が生じても、その発熱を速やかに冷却することができる。   Therefore, when heat generation due to the eddy current occurs, it is necessary to quickly cool the heat generation. Liquid has a larger heat transfer coefficient than gas. According to this configuration, since the superconducting magnet is cooled using liquid nitrogen (that is, liquefied nitrogen), even if heat is generated by the eddy current, the heat can be quickly cooled.

上記構成において、前記冷却回路は、前記第6の流路の替わりに、前記精留塔に接続され、前記第5の流路によって前記超電導磁石に供給された液体状態の窒素を前記精留塔に導く第7の流路を備える。   In the above configuration, the cooling circuit is connected to the rectifying column instead of the sixth flow channel, and the nitrogen in the liquid state supplied to the superconducting magnet by the fifth flow channel is used as the rectifying column. A seventh flow path leading to

精留塔内は、第4の流路内より圧力が低いので、第5の流路によって超電導コイルに供給された液体状態の窒素を、第4の流路に戻すよりも、精留塔に戻す方が、液体状態の窒素を速やかに精留塔に戻すことができる。従って、この構成によれば、超電導磁石の冷却効率を高めることができる。   Since the pressure in the rectifying column is lower than that in the fourth channel, the liquid nitrogen supplied to the superconducting coil by the fifth channel is returned to the rectifying column rather than returning to the fourth channel. Returning can return nitrogen in a liquid state to the rectification column more quickly. Therefore, according to this configuration, the cooling efficiency of the superconducting magnet can be increased.

上記構成において、前記冷却回路は、前記第5の流路又は前記第7の流路を流れる液体状態の窒素の流量を調節する第1の弁部と、前記超電導磁石の温度を測定する第1の測定部と、前記第1の測定部で測定された温度が、前記臨界温度以下の予め定められた値より小さいとき、前記超電導磁石に供給する液体状態の窒素の流量が少なくなり、前記第1の測定部で測定された温度が前記予め定められた値より大きいとき、前記超電導磁石に供給する液体状態の窒素の流量が多くなり、前記第1の測定部で測定された温度が前記予め定められた値のとき、前記超電導磁石に供給する液体状態の窒素の流量が変わらないように、前記第1の弁部の開閉量を制御する第1の制御部と、をさらに備える。   In the above configuration, the cooling circuit includes a first valve unit that adjusts a flow rate of nitrogen in a liquid state flowing through the fifth channel or the seventh channel, and a first temperature that measures the temperature of the superconducting magnet. When the temperature measured by the first measurement unit and the temperature measured by the first measurement unit is smaller than a predetermined value equal to or lower than the critical temperature, the flow rate of liquid nitrogen supplied to the superconducting magnet decreases, and the first When the temperature measured by one measuring unit is larger than the predetermined value, the flow rate of liquid nitrogen supplied to the superconducting magnet increases, and the temperature measured by the first measuring unit is And a first control unit that controls an opening / closing amount of the first valve unit so that a flow rate of liquid nitrogen supplied to the superconducting magnet does not change at a predetermined value.

この構成によれば、超電導磁石に供給する液体状態の窒素の量を必要最小限度にしつつ、超電導コイルの温度を予め定められた値に自動的に制御することができる。   According to this configuration, it is possible to automatically control the temperature of the superconducting coil to a predetermined value while minimizing the amount of nitrogen in the liquid state supplied to the superconducting magnet.

また、この構成によれば、超電導磁石の温度を直接測定するので、超電導磁石の温度を正確に制御できる。   Further, according to this configuration, since the temperature of the superconducting magnet is directly measured, the temperature of the superconducting magnet can be accurately controlled.

上記構成において、前記冷却回路は、前記第5の流路を流れる液体状態の窒素の流量を調節する第2の弁部と、前記第7の流路を流れる液体状態の窒素の温度を測定する第2の測定部と、前記第2の測定部で測定された温度が、前記臨界温度以下の予め定められた値より小さいとき、前記超電導磁石に供給する液体状態の窒素の流量が少なくなり、前記第2の測定部で測定された温度が前記予め定められた値より大きいとき、前記超電導磁石に供給する液体状態の窒素の流量が多くなり、前記第2の測定部で測定された温度が前記予め定められた値のとき、前記超電導磁石に供給する液体状態の窒素の流量が変わらないように、前記第2の弁部の開閉量を制御する第2の制御部と、をさらに備える。   In the above-described configuration, the cooling circuit measures the temperature of the liquid nitrogen flowing through the seventh flow path, and the second valve unit that adjusts the flow rate of liquid nitrogen flowing through the fifth flow path. When the temperature measured by the second measuring unit and the second measuring unit is smaller than a predetermined value below the critical temperature, the flow rate of liquid nitrogen supplied to the superconducting magnet is reduced, When the temperature measured by the second measuring unit is larger than the predetermined value, the flow rate of liquid nitrogen supplied to the superconducting magnet increases, and the temperature measured by the second measuring unit is A second control unit that controls an opening / closing amount of the second valve unit so that a flow rate of liquid nitrogen supplied to the superconducting magnet does not change at the predetermined value.

この構成によれば、超電導磁石に供給する液体状態の窒素の量を必要最小限度にしつつ、超電導磁石の温度を予め定められた値に自動的に制御することができる。   According to this configuration, it is possible to automatically control the temperature of the superconducting magnet to a predetermined value while minimizing the amount of liquid nitrogen supplied to the superconducting magnet.

また、この構成によれば、何らかの理由で超電導磁石の温度を直接測定できないとき、第7の流路を流れる液体状態の窒素の温度から間接的に超電導磁石の温度を推定して超電導磁石の温度を制御する。   Further, according to this configuration, when the temperature of the superconducting magnet cannot be directly measured for some reason, the temperature of the superconducting magnet is estimated by indirectly estimating the temperature of the superconducting magnet from the temperature of nitrogen in the liquid state flowing through the seventh flow path. To control.

上記構成において、前記冷却回路は、前記第4の流路と前記第5の流路との接続部より下流に設けられ、前記第4の流路を流れる液体状態の窒素の流量を調節する第3の弁部をさらに備え、前記第1の制御部は、前記第3の弁部を開けた状態で、前記第1の弁部の前記開閉量を制御しており、前記第1の弁部が全開の状態で、前記第1の測定部で測定された温度が前記予め定められた値より大きいとき、前記第3の弁部を所定量閉じる制御をする。   In the above configuration, the cooling circuit is provided downstream of a connection portion between the fourth flow path and the fifth flow path, and adjusts a flow rate of nitrogen in a liquid state flowing through the fourth flow path. 3, and the first control unit controls the opening / closing amount of the first valve unit in a state where the third valve unit is opened, and the first valve unit When the temperature measured by the first measuring unit is larger than the predetermined value in a fully open state, the third valve unit is controlled to close by a predetermined amount.

この構成によれば、第1の制御部は、第1の弁部が全開の状態で、第1の測定部で測定された温度が予め定められた値より大きいとき、第3の弁部を所定量閉じる制御をする。これにより、第4の流路を流れる液体状態の窒素の量が減り、第5の流路を流れる液体状態の窒素の量を増やすことができるので、超電導磁石をより冷却することができる。   According to this configuration, when the first valve unit is fully open and the temperature measured by the first measurement unit is greater than a predetermined value, the first control unit turns the third valve unit on. Control to close a predetermined amount. As a result, the amount of nitrogen in the liquid state flowing through the fourth flow path can be reduced and the amount of nitrogen in the liquid state flowing through the fifth flow path can be increased, so that the superconducting magnet can be further cooled.

上記構成において、前記冷却回路は、前記第4の流路と前記第5の流路との接続部より下流に設けられ、前記第4の流路を流れる液体状態の窒素の流量を調節する第3の弁部をさらに備え、前記第2の制御部は、前記第3の弁部を開けた状態で、前記第2の弁部の前記開閉量を制御しており、前記第2の弁部が全開の状態で、前記第2の測定部で測定された温度が前記予め定められた値より大きいとき、前記第3の弁部を所定量閉じる制御をする。   In the above configuration, the cooling circuit is provided downstream of a connection portion between the fourth flow path and the fifth flow path, and adjusts a flow rate of nitrogen in a liquid state flowing through the fourth flow path. 3, and the second control unit controls the opening / closing amount of the second valve unit with the third valve unit opened. The second valve unit When the temperature measured by the second measuring unit is larger than the predetermined value in a fully open state, the third valve unit is controlled to be closed by a predetermined amount.

この構成によれば、第2の制御部は、第2の弁部が全開の状態で、第2の測定部で測定された温度が予め定められた値より大きいとき、第3の弁部を所定量閉じる制御をする。これにより、第4の流路を流れる液体状態の窒素の量が減り、第5の流路を流れる液体状態の窒素の量を増やすことができるので、超電導磁石をより冷却することができる。   According to this configuration, the second control unit moves the third valve unit when the second valve unit is fully opened and the temperature measured by the second measurement unit is greater than a predetermined value. Control to close a predetermined amount. As a result, the amount of nitrogen in the liquid state flowing through the fourth flow path can be reduced and the amount of nitrogen in the liquid state flowing through the fifth flow path can be increased, so that the superconducting magnet can be further cooled.

上記構成において、前記精留塔は、液体状態の原料空気を深冷分離して液体状態の酸素を生成し、前記凝縮回路は、前記精留塔から取り出された液体状態の酸素と、前記圧縮部によって圧縮された気体状態の窒素とで熱交換させることによって、気体状態の窒素を冷却し、かつ、液体状態の酸素を気体状態にする熱交換部をさらに備える。   In the above configuration, the rectification column cryogenicly separates the raw material air in a liquid state to generate liquid oxygen, and the condensing circuit includes the liquid oxygen extracted from the rectification column and the compression It further includes a heat exchanging unit that cools the gaseous nitrogen and changes the liquid oxygen to the gaseous state by exchanging heat with the gaseous nitrogen compressed by the unit.

この構成によれば、精留塔に貯留されている液体状態の酸素を利用して、圧縮された気体状態の窒素を冷却するので、圧縮された気体状態の窒素を冷却する冷媒を新たに用意する必要がない。   According to this configuration, since the compressed gaseous nitrogen is cooled using the liquid oxygen stored in the rectification column, a new refrigerant for cooling the compressed gaseous nitrogen is prepared. There is no need to do.

上記構成において、前記超電導モータ及び前記圧縮部を収容する断熱密閉容器をさらに備える。   The said structure WHEREIN: The heat insulation airtight container which accommodates the said superconducting motor and the said compression part is further provided.

この構成によれば、超電導モータ及び圧縮部を断熱密閉容器に収容することにより、これらをユニット化している。従って、凝縮回路の組み立て作業を容易にすることができる。   According to this configuration, the superconducting motor and the compression unit are accommodated in the heat-insulated sealed container, thereby unitizing them. Therefore, the assembly work of the condensation circuit can be facilitated.

本発明によれば、精留塔から取り出された気体状態の窒素のうち、一部の窒素を液化して精留塔に戻す凝縮回路を備える空気分離装置に関して、省エネルギー化を図ることができる。   ADVANTAGE OF THE INVENTION According to this invention, energy saving can be achieved regarding an air separation apparatus provided with the condensation circuit which liquefies some nitrogen among the gaseous nitrogen taken out from the rectification tower, and returns it to a rectification tower.

第1実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 1st Embodiment. 第2実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 2nd Embodiment. 第3実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 3rd Embodiment. 第4実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 4th Embodiment. 第4実施形態において、第1の弁部、第1の測定部及び第1の制御部の関係を示すブロック図である。In 4th Embodiment, it is a block diagram which shows the relationship between a 1st valve part, a 1st measurement part, and a 1st control part. 第4実施形態において、第1の弁部の制御を説明するフローチャートである。In 4th Embodiment, it is a flowchart explaining control of the 1st valve part. 第5実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 5th Embodiment. 第5実施形態において、第2の弁部、第2の測定部及び第2の制御部の関係を示すブロック図である。In 5th Embodiment, it is a block diagram which shows the relationship between a 2nd valve part, a 2nd measurement part, and a 2nd control part. 第6実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 6th Embodiment. 第6実施形態において、第1の弁部、第3の弁部、第1の測定部及び第1の制御部の関係を示すブロック図である。In 6th Embodiment, it is a block diagram which shows the relationship between a 1st valve part, a 3rd valve part, a 1st measurement part, and a 1st control part. 第6実施形態において、第1の弁部及び第3の弁部の制御を説明するフローチャートである。In 6th Embodiment, it is a flowchart explaining control of the 1st valve part and the 3rd valve part. 第7実施形態に係る空気分離装置の構成を示す構成図である。It is a block diagram which shows the structure of the air separation apparatus which concerns on 7th Embodiment. 第7実施形態において、第2の弁部、第3の弁部、第2の測定部及び第2の制御部の関係を示すブロック図である。In 7th Embodiment, it is a block diagram which shows the relationship between a 2nd valve part, a 3rd valve part, a 2nd measurement part, and a 2nd control part. 超電導モータ及び圧縮部を収容している断熱密閉容器の模式図である。It is a schematic diagram of the heat insulation airtight container which accommodates the superconducting motor and the compression part. 超電導モータの構成を示す断面図である。It is sectional drawing which shows the structure of a superconducting motor.

以下、図面に基づいて本発明の実施形態を詳細に説明する。各図において、同一符号を付した構成は、同一の構成であることを示し、その構成について、既に説明している内容については、その説明を省略する。   Hereinafter, embodiments of the present invention will be described in detail with reference to the drawings. In each figure, the structure which attached | subjected the same code | symbol shows that it is the same structure, The description is abbreviate | omitted about the content which has already demonstrated the structure.

図1は、第1実施形態に係る空気分離装置1aの構成を示す構成図である。空気分離装置1aは、圧縮部2、熱交換部3、膨張部4、精留塔5、凝縮回路6及び冷却回路7を備える。第1実施形態及び後で説明する第2〜7実施形態は、冷却回路7の構成が異なる。第1実施形態の冷却回路7は、例えば、温度が77Kの気体状態の窒素を用いて、超電導モータ60に備えられる超電導コイル601を冷却する。   FIG. 1 is a configuration diagram showing a configuration of an air separation device 1a according to the first embodiment. The air separation device 1 a includes a compression unit 2, a heat exchange unit 3, an expansion unit 4, a rectification tower 5, a condensation circuit 6, and a cooling circuit 7. The first embodiment and the second to seventh embodiments described later are different in the configuration of the cooling circuit 7. The cooling circuit 7 of the first embodiment cools the superconducting coil 601 provided in the superconducting motor 60 using, for example, nitrogen in a gaseous state having a temperature of 77K.

圧縮部2は、室温の原料空気を断熱圧縮する圧縮機である。これにより、原料空気の温度は、室温より高くなる。圧縮部2で断熱圧縮された原料空気は、流路8aを流れて、熱交換部3に送られる。流路8a、及び、後で説明する流路8b〜流路8o、流路70a〜流路70eは、配管やラインとも称される。   The compression unit 2 is a compressor that adiabatically compresses raw material air at room temperature. Thereby, the temperature of raw material air becomes higher than room temperature. The raw material air adiabatically compressed by the compression unit 2 flows through the flow path 8 a and is sent to the heat exchange unit 3. The flow path 8a, and the flow paths 8b to 8o and the flow paths 70a to 70e, which will be described later, are also referred to as pipes or lines.

熱交換部3には、流路8a、流路8b、流路8c、流路8d、流路8e及び流路8fが接続されている。上述したように、圧縮部2で断熱圧縮された原料空気は、流路8aを流れて、熱交換部3に送られる。精留塔5から取り出された製品窒素は、流路8bを流れて、熱交換部3に送られる。精留塔5から取り出された製品酸素は、流路8cを流れて、熱交換部3に送られる。   The heat exchange unit 3 is connected to a flow path 8a, a flow path 8b, a flow path 8c, a flow path 8d, a flow path 8e, and a flow path 8f. As described above, the raw material air adiabatically compressed by the compression unit 2 flows through the flow path 8 a and is sent to the heat exchange unit 3. The product nitrogen taken out from the rectification column 5 flows through the flow path 8b and is sent to the heat exchange unit 3. The product oxygen taken out from the rectification column 5 flows through the flow path 8 c and is sent to the heat exchange unit 3.

熱交換部3は、次の二つの熱交換をする熱交換器である。熱交換部3は、圧縮部2で断熱圧縮された、温度が例えば室温程度の原料空気と、精留塔5から送られてきた、温度が77Kの気体状態の製品窒素とで熱交換をさせ、製品窒素の温度を上昇させる。また、熱交換部3は、圧縮部2で断熱圧縮された、温度が例えば室温程度の原料空気と、精留塔5から送られてきた、温度が90Kの液体状態の製品酸素とで熱交換をさせ、製品酸素の温度を上昇させる。   The heat exchange unit 3 is a heat exchanger that performs the following two heat exchanges. The heat exchanging unit 3 performs heat exchange between the raw material air that has been adiabatically compressed in the compressing unit 2 and the raw material air having a temperature of, for example, about room temperature, and the product nitrogen in a gaseous state having a temperature of 77 K sent from the rectifying tower 5. Increase the temperature of the product nitrogen. The heat exchanging unit 3 exchanges heat between the raw material air that is adiabatically compressed by the compressing unit 2 and the raw material air having a temperature of, for example, about room temperature, and the product oxygen in a liquid state having a temperature of 90 K sent from the rectifying column 5. To increase the product oxygen temperature.

熱交換部3で熱交換された製品窒素及び製品酸素は、それぞれ、流路8d、流路8eを流れて、次の工程に送られる。圧縮部2で断熱膨張された原料空気は、熱交換部3で製品窒素及び製品酸素に熱を供給することにより温度が下げられ、流路8fを流れて膨張部4に送られる。   The product nitrogen and product oxygen exchanged by the heat exchange unit 3 flow through the flow path 8d and the flow path 8e, respectively, and are sent to the next step. The raw material air adiabatically expanded in the compression unit 2 is cooled by supplying heat to the product nitrogen and product oxygen in the heat exchange unit 3, flows through the flow path 8 f, and is sent to the expansion unit 4.

膨張部4は、送られてきた原料空気を断熱膨張する膨張タービンである。膨張部4として、膨張タービンの替わりに膨張弁を用いることもできる。   The expansion part 4 is an expansion turbine that adiabatically expands the supplied raw material air. An expansion valve can be used as the expansion unit 4 instead of the expansion turbine.

膨張部4で断熱膨張されて、液体状態にされた原料空気は、流路8gを流れて、精留塔5に送られる。   The raw material air that has been adiabatically expanded in the expansion section 4 to be in a liquid state flows through the flow path 8 g and is sent to the rectification tower 5.

精留塔5は、単式(1塔式)であり、液体状態の原料空気を深冷分離して、気体状態の窒素と液体状態の酸素とを生成する。窒素は、精留塔5の上部に溜められ、酸素は、精留塔5の下部に溜められる。精留塔5として、単式の替わりに、複式(2塔式)を用いることもできる。   The rectifying column 5 is a single type (one-column type), and cryogenic-separates liquid source air to generate gaseous nitrogen and liquid oxygen. Nitrogen is stored in the upper part of the rectifying column 5, and oxygen is stored in the lower part of the rectifying column 5. As the rectification column 5, a double system (two-column system) can be used instead of a single system.

精留塔5の塔頂部には、流路8hが接続されている。精留塔5から取り出された、温度が77Kの気体状態の窒素(ボイルオフガス)は、流路8hを流れる。流路8hは、流路8bと流路8iとに分岐している。流路8hを流れる気体状態の窒素は、流路8bを流れて、熱交換部3に送られるか、流路8iを流れて、後で説明する凝縮回路6に送られる。   A flow path 8 h is connected to the top of the rectifying column 5. Nitrogen (boil-off gas) in a gaseous state having a temperature of 77 K taken out from the rectification column 5 flows through the flow path 8h. The flow path 8h is branched into a flow path 8b and a flow path 8i. The nitrogen in the gaseous state flowing through the flow path 8h flows through the flow path 8b and is sent to the heat exchange unit 3, or flows through the flow path 8i and is sent to the condensation circuit 6 described later.

精留塔5の塔底部には、流路8jが接続されている。流路8jは、流路8cと流路8kとに分岐している。流路8jを流れる液体状態の酸素は、流路8cを流れて、熱交換部3に送られるか、流路8kを流れて、熱交換部62に送られる。   A flow path 8j is connected to the bottom of the rectifying column 5. The flow path 8j is branched into a flow path 8c and a flow path 8k. The liquid oxygen flowing through the flow path 8j flows through the flow path 8c and is sent to the heat exchange unit 3 or flows through the flow path 8k and is sent to the heat exchange unit 62.

凝縮回路6は、精留塔5から取り出された気体状態の窒素のうち、一部の窒素が供給され、供給された窒素を気体状態から液体状態に変化させて精留塔5に戻すモジュールである。凝縮回路6は、精留塔5で液体状態から気体状態にされた窒素について、その一部を、再び、液体状態にするので、凝縮回路6を再凝縮回路と称することもできる。   The condensing circuit 6 is a module to which a part of the nitrogen in the gaseous state taken out from the rectifying column 5 is supplied, and the supplied nitrogen is changed from the gaseous state to the liquid state and returned to the rectifying column 5. is there. Since the condensing circuit 6 makes a part of the nitrogen that has been changed from a liquid state to a gas state in the rectification column 5 again into a liquid state, the condensing circuit 6 can also be referred to as a recondensing circuit.

凝縮回路6は、超電導モータ60、圧縮部61、熱交換部62、膨張部63及び流路(流路8i、流路8l、流路8m、流路8o)を備える。   The condensing circuit 6 includes a superconducting motor 60, a compression unit 61, a heat exchange unit 62, an expansion unit 63, and a flow path (flow path 8i, flow path 81, flow path 8m, flow path 8o).

超電導モータ60は、超電導磁石を利用して回転子を回転させるモータである。超電導磁石とは、例えば、超電導コイル601と、これが巻かれた磁性体芯とで構成される磁石や、超電導バルク磁石である。本実施形態では、前者の磁石を例にして説明する。   Superconducting motor 60 is a motor that rotates a rotor using a superconducting magnet. The superconducting magnet is, for example, a magnet composed of a superconducting coil 601 and a magnetic core around which it is wound, or a superconducting bulk magnet. In the present embodiment, the former magnet will be described as an example.

超電導コイル601は、後で説明する冷却回路7によって、そのコイルを構成する超電導材料の臨界温度以下に冷却される。超電導コイル601を冷却する冷媒は、温度が77Kの窒素である。よって、超電導コイル601を構成する超電導材料は、臨界温度が77Kより高くなければならない。このような超電導材料として、例えば、Bi系(BiSrCaCu)又はY系(YBaCu)がある。77Kは、液体状態の窒素(すなわち、液化窒素)の沸点である。 Superconducting coil 601 is cooled below the critical temperature of the superconducting material constituting the coil by cooling circuit 7 described later. The refrigerant for cooling the superconducting coil 601 is nitrogen having a temperature of 77K. Therefore, the superconducting material constituting the superconducting coil 601 must have a critical temperature higher than 77K. As such a superconducting material, for example, there are Bi-based (Bi 2 Sr 2 Ca 2 Cu 3 O y ) and Y-based (YBa 2 Cu 3 O 7 ). 77K is the boiling point of liquid nitrogen (ie, liquefied nitrogen).

流路8iは、圧縮部61に接続されている。流路8iを流れる気体状態の窒素は、圧縮部61に送られる。流路8h及び流路8iにより、第1の流路が構成される。第1の流路は、精留塔5と圧縮部61とを接続し、精留塔5から供給された気体状態の窒素を圧縮部61に導く。   The flow path 8 i is connected to the compression unit 61. The nitrogen in the gas state flowing through the flow path 8 i is sent to the compression unit 61. The first flow path is configured by the flow path 8h and the flow path 8i. The first flow path connects the rectification column 5 and the compression unit 61, and guides nitrogen in the gaseous state supplied from the rectification column 5 to the compression unit 61.

圧縮部61は、超電導モータ60によって駆動され、流路8iを流れる(すなわち、凝縮回路6を流れる)気体状態の窒素を断熱圧縮する。圧縮部61は、例えば、スクリュー型の圧縮機である。超電導モータ60の回転軸603は、圧縮部61のスクリュー(不図示)と直接又は間接に連結されている。超電導モータ60の駆動力は、回転軸603を介して、スクリューに伝達されて、スクリューが回転する。   The compression unit 61 is driven by the superconducting motor 60 and adiabatically compresses gaseous nitrogen flowing in the flow path 8i (that is, flowing in the condensation circuit 6). The compression unit 61 is, for example, a screw type compressor. The rotation shaft 603 of the superconducting motor 60 is directly or indirectly connected to a screw (not shown) of the compression unit 61. The driving force of the superconducting motor 60 is transmitted to the screw via the rotating shaft 603, and the screw rotates.

熱交換部62には、流路8k、流路8l、流路8m及び流路8nが接続されている。圧縮部61で断熱圧縮された気体状態の窒素は、流路8lを流れて、熱交換部62に送られる。精留塔5に貯留されている液体状態の酸素は、流路8j及び流路8kを流れて、熱交換部62に送られる。   The heat exchange unit 62 is connected to a flow path 8k, a flow path 81, a flow path 8m, and a flow path 8n. The gaseous nitrogen adiabatically compressed by the compression unit 61 flows through the flow path 8 l and is sent to the heat exchange unit 62. The liquid oxygen stored in the rectification column 5 flows through the flow path 8j and the flow path 8k and is sent to the heat exchange unit 62.

熱交換部62は、圧縮部61で断熱圧縮された気体状態の窒素と、精留塔5から送られてきた、温度が90Kの液体状態の酸素とで熱交換をさせ、酸素を液体状態から気体状態に変える。断熱圧縮された気体状態の窒素は、温度が90Kの液体状態の酸素と熱交換するので、窒素の温度を、断熱圧縮により90Kより高くする必要がある。   The heat exchanging unit 62 exchanges heat between nitrogen in the gas state adiabatically compressed by the compressing unit 61 and oxygen in a liquid state having a temperature of 90 K sent from the rectifying tower 5, so that the oxygen is converted from the liquid state. Change to gaseous state. Since adiabatic-compressed gaseous nitrogen exchanges heat with liquid oxygen having a temperature of 90K, the temperature of nitrogen needs to be higher than 90K by adiabatic compression.

断熱圧縮により温度が上昇した窒素を用いて、酸素を液体状態から気体状態にする。このため、流路8lを流れる気体状態の窒素の温度と流路8kを流れる液体状態の酸素の温度との差が大きいとき、気体状態の窒素の温度の上昇量が大きくなければならないので、気体状態の窒素を圧縮する動力が大きくなる。逆に、それらの温度差が小さいとき、気体状態の窒素の温度の上昇量は小さくてよいので、気体状態の窒素を圧縮する動力を小さくできる。   Oxygen is changed from a liquid state to a gaseous state using nitrogen whose temperature has been increased by adiabatic compression. For this reason, when the difference between the temperature of the gaseous nitrogen flowing through the flow path 8l and the temperature of the liquid oxygen flowing through the flow path 8k is large, the amount of increase in the temperature of the gaseous nitrogen must be large. The power to compress the nitrogen in the state increases. Conversely, when the temperature difference between them is small, the amount of increase in the temperature of the gaseous nitrogen may be small, so that the power for compressing the gaseous nitrogen can be reduced.

精留塔5に貯留されている液体状態の酸素を利用して、圧縮された気体状態の窒素を冷却するので、圧縮された気体状態の窒素を冷却する冷媒を新たに用意する必要がない。   Since the compressed gaseous nitrogen is cooled using the liquid oxygen stored in the rectifying column 5, it is not necessary to prepare a new refrigerant for cooling the compressed gaseous nitrogen.

圧縮部61で断熱圧縮された気体状態の窒素は、熱交換部62で酸素に熱を供給することにより温度が下げられ、流路8mを流れて膨張部63に送られる。   The nitrogen in the gas state adiabatically compressed by the compression unit 61 is lowered in temperature by supplying heat to oxygen by the heat exchange unit 62, flows through the flow path 8 m, and is sent to the expansion unit 63.

膨張部63は、送られてきた窒素を断熱膨張する膨張弁である。膨張部63として、膨張弁の替わりに膨張タービンを用いることもできる。   The expansion part 63 is an expansion valve that adiabatically expands the sent nitrogen. An expansion turbine can be used as the expansion unit 63 instead of the expansion valve.

熱交換部62で凝縮し液化された窒素は、流路8mを流れて膨張部63に送られ、膨張部63で断熱膨張されて温度が低下し、流路8oを流れて、精留塔5に戻される。   The nitrogen condensed and liquefied in the heat exchange section 62 flows through the flow path 8m and is sent to the expansion section 63. The nitrogen is adiabatically expanded in the expansion section 63, the temperature is lowered, and flows through the flow path 8o. Returned to

このように、圧縮部61で断熱圧縮された気体状態の窒素は、熱交換部62において、精留塔5から供給された液体状態の酸素により冷却されることにより、凝縮し液化され、その後、膨張部63で断熱膨張されて温度が低下する。従って、冷熱源を新たに設けることなく、窒素を液体状態にすることができる。   Thus, the nitrogen in the gas state adiabatically compressed by the compression unit 61 is condensed and liquefied by being cooled by the liquid state oxygen supplied from the rectification tower 5 in the heat exchange unit 62, and then The temperature is lowered by adiabatic expansion at the expansion portion 63. Therefore, nitrogen can be made into a liquid state without newly providing a cold heat source.

熱交換部62で気体状態にされた酸素は、流路8nを流れて、精留塔5に送られる。この気体状態の酸素は、精留塔5で再液化される。   Oxygen that has been changed to a gas state in the heat exchange section 62 flows through the flow path 8 n and is sent to the rectification column 5. This gaseous oxygen is reliquefied in the rectification column 5.

空気分離装置1aは、以上の処理を繰り返すことにより、原料空気から製品窒素及び製品酸素を製造する。   The air separation device 1a produces product nitrogen and product oxygen from the raw air by repeating the above processing.

冷却回路7は、超電導モータ60に含まれる超電導コイル601を、このコイルを構成する超電導材料の臨界温度以下に冷却する。冷却回路7は、流路70a(第2の流路)及び流路70b(第3の流路)を備える。   The cooling circuit 7 cools the superconducting coil 601 included in the superconducting motor 60 below the critical temperature of the superconducting material constituting the coil. The cooling circuit 7 includes a flow path 70a (second flow path) and a flow path 70b (third flow path).

流路70aは、流路8i(第1の流路)と接続され、流路8iを流れる、温度が77Kの気体状態の窒素の一部を、超電導モータ60の超電導コイル601に供給する。これにより、超電導コイル601を臨界温度以下に冷却する。気体状態の窒素を冷媒に用いる場合、圧縮部61に導かれる前の気体状態の窒素としたのは、この窒素は、ボイルオフガスであり、温度が77K(液化窒素の沸点)だからである。   The flow path 70 a is connected to the flow path 8 i (first flow path), and supplies a part of nitrogen in a gaseous state having a temperature of 77 K flowing through the flow path 8 i to the superconducting coil 601 of the superconducting motor 60. Thereby, the superconducting coil 601 is cooled below the critical temperature. When nitrogen in the gaseous state is used as the refrigerant, the nitrogen in the gaseous state before being introduced to the compressing unit 61 is because this nitrogen is a boil-off gas and has a temperature of 77 K (the boiling point of liquefied nitrogen).

流路70bは、流路70aより下流で流路8iと接続され、流路70aによって超電導コイル601に供給された気体状態の窒素を流路8iに戻す。この窒素は、流路8iを流れて、圧縮部61に送られる。   The flow path 70b is connected to the flow path 8i downstream from the flow path 70a, and returns nitrogen in the gaseous state supplied to the superconducting coil 601 by the flow path 70a to the flow path 8i. The nitrogen flows through the flow path 8 i and is sent to the compression unit 61.

第1実施形態の主な効果を説明する。第1実施形態に係る空気分離装置1aは、以下の観点から省エネルギー化を図ることができる。   The main effects of the first embodiment will be described. The air separation device 1a according to the first embodiment can save energy from the following viewpoints.

圧縮部61のスクリューを駆動するモータを常電導モータにした場合、常電導モータのコイルの銅損が原因となる熱負荷が発生する。例えば、常電導モータの回転軸を圧縮部61のスクリューに直接連結する場合、常電導モータを凝縮回路6と同じ環境(77Kの窒素が存在する環境)下に設置しなければならず、常電導モータが原因となる熱負荷がその環境の温度を上昇させる。常電導モータを室温環境下に設置し、常電導モータの回転軸と圧縮部61のスクリューとを断熱層を介して、軸で連結した場合、この軸からの熱進入が原因となる熱負荷が、上記環境の温度を上昇させる。   When the motor that drives the screw of the compression unit 61 is a normal conducting motor, a thermal load is generated due to copper loss in the coil of the normal conducting motor. For example, when the rotating shaft of the normal conducting motor is directly connected to the screw of the compression unit 61, the normal conducting motor must be installed in the same environment as the condensing circuit 6 (an environment where 77K of nitrogen exists). The heat load caused by the motor raises the temperature of the environment. When a normal conducting motor is installed in a room temperature environment and the rotating shaft of the normal conducting motor and the screw of the compression unit 61 are connected by a shaft through a heat insulating layer, the heat load caused by the heat entering from this shaft is reduced. Increase the temperature of the environment.

この入熱分は、原料空気の圧縮仕事で補う必要があるため、凝縮回路6を設けても、空気分離装置1aの消費エネルギーを少なくする効果が小さくなる。   Since this heat input needs to be supplemented by the compression work of the raw material air, even if the condensing circuit 6 is provided, the effect of reducing the energy consumption of the air separation device 1a is reduced.

第1実施形態では、圧縮部61のスクリューを駆動するモータを超電導モータ60にしている。超電導状態の超電導コイル601は、抵抗がゼロなので発熱しない。このため、凝縮回路6で発生する損失は、圧縮部61等で生じる機械損、並びに、凝縮回路6の流路(例えば、流路8i、流路8k)を流れる流体(窒素、酸素)とこれらの流路との摩擦による流体損のみとなる。このため、空気分離装置1aが凝縮回路6を備えることによる生じる熱負荷を大幅に低下させることができる。   In the first embodiment, the motor that drives the screw of the compression unit 61 is the superconducting motor 60. The superconducting coil 601 in the superconducting state does not generate heat because its resistance is zero. For this reason, the loss generated in the condensing circuit 6 includes the mechanical loss generated in the compression unit 61 and the like, the fluid (nitrogen, oxygen) flowing through the flow path (for example, the flow path 8i, the flow path 8k) of the condensing circuit 6 and these. Only the fluid loss due to the friction with the flow path. For this reason, the heat load which arises when the air separation apparatus 1a is provided with the condensation circuit 6 can be reduced significantly.

超電導モータ60は、超電導コイル601を構成する超電導材料の臨界温度以下に超電導コイル601が冷却された状態で使用される。超電導コイル601の冷却には、臨界温度以下の沸点をもつ冷媒が用いられる。   Superconducting motor 60 is used in a state where superconducting coil 601 is cooled below the critical temperature of the superconducting material constituting superconducting coil 601. For cooling the superconducting coil 601, a refrigerant having a boiling point below the critical temperature is used.

第1実施形態に係る空気分離装置1aでは、超電導コイル601を臨界温度以下に冷却する冷媒として、窒素を還流する凝縮回路6を流れる窒素を用いる。従って、第1実施形態に係る空気分離装置1aによれば、常電導モータを用いた場合に比べ入熱量が小さくなるため省エネルギー化を図ることができる。   In the air separation device 1a according to the first embodiment, nitrogen flowing through the condensing circuit 6 that circulates nitrogen is used as a refrigerant for cooling the superconducting coil 601 to a critical temperature or lower. Therefore, according to the air separation device 1a according to the first embodiment, the amount of heat input is reduced as compared with the case where the normal conducting motor is used, so that energy saving can be achieved.

第2実施形態について、図1に示す第1実施形態との相違点を中心に説明する。図2は、第2実施形態に係る空気分離装置1bの構成を示す構成図である。第2実施形態の冷却回路7は、温度が77Kの液体状態の窒素を用いて、超電導コイル601を冷却する。   The second embodiment will be described with a focus on differences from the first embodiment shown in FIG. FIG. 2 is a configuration diagram illustrating a configuration of an air separation device 1b according to the second embodiment. The cooling circuit 7 of the second embodiment cools the superconducting coil 601 by using liquid nitrogen having a temperature of 77K.

流路8oは、膨張部63と精留塔5とを接続し、液体状態の窒素を精留塔5に導く第4の流路である。   The flow path 8 o is a fourth flow path that connects the expansion unit 63 and the rectifying tower 5 and guides liquid nitrogen to the rectifying tower 5.

冷却回路7は、流路70c(第5の流路)及び流路70d(第6の流路)を備える。流路70cは、流路8oと接続され、流路8oを流れる、温度が77Kの液体状態の窒素の一部を超電導コイル601に供給する。これにより、超電導コイル601を臨界温度以下に冷却する。   The cooling circuit 7 includes a flow path 70c (fifth flow path) and a flow path 70d (sixth flow path). The flow path 70c is connected to the flow path 8o, and supplies a part of the liquid nitrogen having a temperature of 77K flowing through the flow path 8o to the superconducting coil 601. Thereby, the superconducting coil 601 is cooled below the critical temperature.

流路70dは、流路70cより下流で流路8oと接続され、流路70cによって超電導コイル601に供給された気体状態の窒素を流路8oに戻す。この窒素は、流路8oを流れて、精留塔5に送られる。   The flow path 70d is connected to the flow path 8o downstream from the flow path 70c, and returns nitrogen in the gaseous state supplied to the superconducting coil 601 by the flow path 70c to the flow path 8o. This nitrogen flows through the flow path 8 o and is sent to the rectification column 5.

第2実施形態の主な効果を説明する。精留塔5から取り出され、流路8iを流れる気体状態の窒素の温度と、流路8oを流れる液体状態の窒素の温度とは、同じ程度なので、いずれを冷媒にしても、超電導コイル601を臨界温度以下に冷却することができる。   The main effects of the second embodiment will be described. The temperature of the nitrogen in the gas state that is taken out from the rectification column 5 and flows through the flow path 8i is approximately the same as the temperature of the nitrogen in the liquid state that flows through the flow path 8o. It can be cooled below the critical temperature.

超電導モータ60の運転中に、急激な負荷変動等が発生したとき、超電導モータ60には渦電流による発熱を生じる。この発熱で超電導コイル601の微小部分で超電導状態が破れると、そこから局所的に発熱し、これが原因で超電導モータ60が破損することがある。   When a sudden load change or the like occurs during operation of the superconducting motor 60, the superconducting motor 60 generates heat due to eddy current. If the superconducting state is broken at a minute portion of the superconducting coil 601 due to this heat generation, heat is generated locally from this, and the superconducting motor 60 may be damaged due to this.

従って、上記渦電流による発熱が生じたとき、この発熱を速やかに冷却する必要がある。液体は、気体に比べて熱伝達係数が大きい。第2実施形態では、液体状態の窒素(すなわち、液化窒素)を用いて、超電導コイル601を冷却するので、上記渦電流による発熱が生じても、その発熱を速やかに冷却することができる。   Therefore, when heat generation due to the eddy current occurs, it is necessary to quickly cool the heat generation. Liquid has a larger heat transfer coefficient than gas. In the second embodiment, since the superconducting coil 601 is cooled using nitrogen in a liquid state (that is, liquefied nitrogen), even if heat generation due to the eddy current occurs, the heat generation can be quickly cooled.

第3実施形態について、図2に示す第2実施形態との相違点を中心に説明する。図3は、第3実施形態に係る空気分離装置1cの構成を示す構成図である。第3実施形態の冷却回路7は、図2に示す流路70d(第6の流路)の替わりに、流路70e(第7の流路)を備える。流路70eは、精留塔5に接続され、流路70c(第5の流路)によって超電導コイル601に供給された液体状態の窒素を精留塔5に導く。   The third embodiment will be described with a focus on differences from the second embodiment shown in FIG. FIG. 3 is a configuration diagram showing a configuration of an air separation device 1c according to the third embodiment. The cooling circuit 7 of the third embodiment includes a flow path 70e (seventh flow path) instead of the flow path 70d (sixth flow path) shown in FIG. The flow path 70 e is connected to the rectification column 5, and guides liquid nitrogen supplied to the superconducting coil 601 through the flow path 70 c (fifth flow path) to the rectification column 5.

第3実施形態の主な効果を説明する。精留塔5内は、流路8o内より圧力が低いので、途中の流路形状にもよるが、流路70cによって超電導コイル601に供給された液体状態の窒素を、流路8oに戻すよりも、精留塔5に戻す方が、液体状態の窒素を速やかに精留塔5に戻すことができる。   The main effects of the third embodiment will be described. Since the pressure in the rectifying column 5 is lower than that in the flow path 8o, the liquid state nitrogen supplied to the superconducting coil 601 by the flow path 70c is returned to the flow path 8o depending on the shape of the flow path in the middle. However, returning to the rectification column 5 can quickly return liquid nitrogen to the rectification column 5.

第4実施形態について、図3に示す第3実施形態との相違点を中心に説明する。図4は、第4実施形態に係る空気分離装置1dの構成を示す構成図である。図5は、第4実施形態において、第1の弁部71、第1の測定部72及び第1の制御部73の関係を示すブロック図である。第4実施形態の冷却回路7は、第1の弁部71、第1の測定部72及び第1の制御部73を備える。   The fourth embodiment will be described with a focus on differences from the third embodiment shown in FIG. FIG. 4 is a configuration diagram showing a configuration of an air separation device 1d according to the fourth embodiment. FIG. 5 is a block diagram illustrating a relationship among the first valve unit 71, the first measurement unit 72, and the first control unit 73 in the fourth embodiment. The cooling circuit 7 of the fourth embodiment includes a first valve unit 71, a first measurement unit 72, and a first control unit 73.

図4及び図5を参照して、第1の弁部71は、流路70e(第7の流路)を流れる液体状態の窒素の流量を調節する電磁弁である。なお、第1の弁部71を、流路70c(第5の流路)に設置し、流路70cを流れる液体状態の窒素の流量を調節してもよい。   Referring to FIGS. 4 and 5, the first valve portion 71 is an electromagnetic valve that adjusts the flow rate of nitrogen in a liquid state that flows through the flow path 70 e (seventh flow path). The first valve portion 71 may be installed in the flow path 70c (fifth flow path) to adjust the flow rate of liquid nitrogen flowing through the flow path 70c.

第1の測定部72は、超電導コイル601の温度を測定する温度センサである。第1の測定部72の測定子721は、超電導コイル601に接触してもよいし、接触していなくてもよい。   The first measurement unit 72 is a temperature sensor that measures the temperature of the superconducting coil 601. The measuring element 721 of the first measuring unit 72 may be in contact with the superconducting coil 601 or may not be in contact.

第1の制御部73は、CPU、RAM及びROMを備え、これらにより、以下の機能を実現する。超電導コイル601を構成する超電導材料の臨界温度以下の予め定められた値を基準値とする。第1の制御部73は、第1の測定部72で測定された温度が基準値(すなわち、予め定められた値)以下のとき、超電導コイル601に供給する液体状態の窒素の流量が少なくなり、第1の測定部72で測定された温度が基準値より大きいとき、超電導コイル601に供給する液体状態の窒素の流量が多くなり、第1の測定部72で測定された温度が基準値のとき、超電導コイル601に供給する液体状態の窒素の流量が変わらないように、第1の弁部71の開閉量を制御する。   The first control unit 73 includes a CPU, a RAM, and a ROM, and realizes the following functions. A predetermined value below the critical temperature of the superconducting material constituting the superconducting coil 601 is set as a reference value. When the temperature measured by the first measurement unit 72 is equal to or lower than a reference value (that is, a predetermined value), the first control unit 73 reduces the flow rate of liquid nitrogen supplied to the superconducting coil 601. When the temperature measured by the first measuring unit 72 is larger than the reference value, the flow rate of liquid nitrogen supplied to the superconducting coil 601 increases, and the temperature measured by the first measuring unit 72 is the reference value. At this time, the opening / closing amount of the first valve portion 71 is controlled so that the flow rate of liquid nitrogen supplied to the superconducting coil 601 does not change.

基準値は、ピンポイントの値(例えば、77K)でもよいし、範囲を有する値(例えば、70K〜77K)でもよい。   The reference value may be a pinpoint value (for example, 77K) or a value having a range (for example, 70K to 77K).

図6は、第4実施形態において、第1の弁部71の制御を説明するフローチャートである。第1の測定部72は、超電導コイル601の温度を測定し、その温度を示すデータを第1の制御部に送る(ステップS1)。第1の制御部73は、ステップS1で測定された超電導コイル601の温度が、基準値と同じか否かを判断する(ステップS2)。   FIG. 6 is a flowchart illustrating control of the first valve unit 71 in the fourth embodiment. The first measurement unit 72 measures the temperature of the superconducting coil 601 and sends data indicating the temperature to the first control unit (step S1). The first controller 73 determines whether or not the temperature of the superconducting coil 601 measured in step S1 is the same as the reference value (step S2).

第1の制御部73が、超電導コイル601の温度が基準値と同じと判断したとき(ステップS2でYes)、ステップS1に戻る。   When the first control unit 73 determines that the temperature of the superconducting coil 601 is the same as the reference value (Yes in step S2), the process returns to step S1.

第1の制御部73が、超電導コイル601の温度が基準値と同じでないと判断したとき(ステップS2でNo)、第1の制御部73は、ステップS1で測定された超電導コイル601の温度が、基準値より大きいか否かを判断する(ステップS3)。   When the first controller 73 determines that the temperature of the superconducting coil 601 is not the same as the reference value (No in step S2), the first controller 73 determines that the temperature of the superconducting coil 601 measured in step S1 is Then, it is determined whether or not it is larger than the reference value (step S3).

第1の制御部73が、超電導コイル601の温度が基準値より小さいと判断したとき(ステップS3でNo)、第1の制御部73は、第1の弁部71を制御して、第1の弁部71を所定量閉じて、流路70c及び流路70eを流れる液体状態の窒素の流量を少なくする(ステップS4)。そして、ステップS1に戻る。   When the first control unit 73 determines that the temperature of the superconducting coil 601 is lower than the reference value (No in step S3), the first control unit 73 controls the first valve unit 71 to perform the first operation. Is closed by a predetermined amount to reduce the flow rate of nitrogen in the liquid state flowing through the flow path 70c and the flow path 70e (step S4). Then, the process returns to step S1.

第1の制御部73が、超電導コイル601の温度が基準値より大きいと判断したとき(ステップS3でYes)、第1の制御部73は、第1の弁部71が全開か否かを判断する(ステップS5)。   When the first control unit 73 determines that the temperature of the superconducting coil 601 is higher than the reference value (Yes in step S3), the first control unit 73 determines whether or not the first valve unit 71 is fully opened. (Step S5).

第1の制御部73が、第1の弁部71が全開でないと判断したとき(ステップS5でNo)、第1の制御部73は、第1の弁部71を制御して、第1の弁部71を所定量開けて、流路70c及び流路70eを流れる液体状態の窒素の流量を多くする(ステップS6)。そして、ステップS1に戻る。   When the first control unit 73 determines that the first valve unit 71 is not fully open (No in step S5), the first control unit 73 controls the first valve unit 71 to perform the first operation. The valve portion 71 is opened by a predetermined amount, and the flow rate of liquid nitrogen flowing through the flow path 70c and the flow path 70e is increased (step S6). Then, the process returns to step S1.

第1の制御部73が、第1の弁部71が全開と判断したとき(ステップS5でYes)、第1の制御部73は、所定の報知部(例えば、ランプ、スピーカ)を作動させて、超電導コイル601の温度が基準値より大きいことを、空気分離装置1dの運転を管理する者に報知する(ステップS7)。   When the first control unit 73 determines that the first valve unit 71 is fully open (Yes in step S5), the first control unit 73 operates a predetermined notification unit (for example, a lamp or a speaker). The person who manages the operation of the air separation device 1d is notified that the temperature of the superconducting coil 601 is higher than the reference value (step S7).

第4実施形態によれば、超電導コイル601に供給する液体状態の窒素の量を必要最小限度にしつつ、超電導コイル601の温度を基準値(予め定められた値)に自動的に制御することができる。   According to the fourth embodiment, the temperature of the superconducting coil 601 is automatically controlled to the reference value (predetermined value) while the amount of liquid nitrogen supplied to the superconducting coil 601 is minimized. it can.

また、第4実施形態によれば、超電導コイル601の温度を直接測定するので、超電導コイル601の温度を正確に制御できる。   Further, according to the fourth embodiment, since the temperature of the superconducting coil 601 is directly measured, the temperature of the superconducting coil 601 can be accurately controlled.

第5実施形態について、図4及び図5に示す第4実施形態との相違点を中心に説明する。図7は、第5実施形態に係る空気分離装置1eの構成を示す構成図である。図8は、第5実施形態において、第2の弁部74、第2の測定部75及び第2の制御部76の関係を示すブロック図である。第5実施形態の冷却回路7は、第2の弁部74、第2の測定部75及び第2の制御部76を備える。   The fifth embodiment will be described with a focus on differences from the fourth embodiment shown in FIGS. 4 and 5. FIG. 7 is a configuration diagram showing a configuration of an air separation device 1e according to the fifth embodiment. FIG. 8 is a block diagram illustrating a relationship among the second valve unit 74, the second measurement unit 75, and the second control unit 76 in the fifth embodiment. The cooling circuit 7 of the fifth embodiment includes a second valve unit 74, a second measurement unit 75, and a second control unit 76.

図7及び図8を参照して、第2の弁部74は、流路70c(第5の流路)を流れる液体状態の窒素の流量を調節する電磁弁である。   Referring to FIGS. 7 and 8, the second valve unit 74 is an electromagnetic valve that adjusts the flow rate of nitrogen in a liquid state flowing through the flow path 70c (fifth flow path).

第2の測定部75は、流路70e(第7の流路)を流れる液体状態の窒素の温度を測定する温度センサである。第2の測定部75の測定子751が、流路70eを流れる液体状態の窒素に接触している。   The second measuring unit 75 is a temperature sensor that measures the temperature of nitrogen in a liquid state flowing through the flow path 70e (seventh flow path). A measuring element 751 of the second measuring unit 75 is in contact with liquid nitrogen flowing through the flow path 70e.

第2の制御部76は、CPU、RAM及びROMを備え、第1の制御部73と同様の機能を有する。すなわち、超電導コイル601を構成する超電導材料の臨界温度以下の予め定められた値を基準値とする。第2の制御部76は、第2の測定部75で測定された温度が基準値以下のとき、超電導コイル601に供給する液体状態の窒素の流量が少なくなり、第2の測定部75で測定された温度が基準値より大きいとき、超電導コイル601に供給する液体状態の窒素の流量が多くなり、第2の測定部75で測定された温度が基準値のとき、超電導コイル601に供給する液体状態の窒素の流量が変わらないように、第2の弁部74の開閉量を制御する。   The second control unit 76 includes a CPU, a RAM, and a ROM, and has the same function as the first control unit 73. That is, a predetermined value equal to or lower than the critical temperature of the superconducting material constituting the superconducting coil 601 is set as a reference value. When the temperature measured by the second measuring unit 75 is equal to or lower than the reference value, the second control unit 76 reduces the flow rate of nitrogen in the liquid state supplied to the superconducting coil 601 and measures the second measuring unit 75. When the measured temperature is higher than the reference value, the flow rate of nitrogen in the liquid state supplied to the superconducting coil 601 increases, and the liquid supplied to the superconducting coil 601 when the temperature measured by the second measuring unit 75 is the reference value. The opening / closing amount of the second valve portion 74 is controlled so that the flow rate of nitrogen in the state does not change.

基準値(予め定められた値)は、第4実施形態で説明した基準値と同様に、ピンポイントの値(例えば、77K)でもよいし、範囲を有する値(例えば、70K〜77K)でもよい。   The reference value (predetermined value) may be a pinpoint value (for example, 77K) or a value having a range (for example, 70K to 77K), similar to the reference value described in the fourth embodiment. .

第2の弁部74の制御は、図6を用いて既に説明した第4実施形態の第1の弁部71の制御と同じなので説明を省略する。   The control of the second valve unit 74 is the same as the control of the first valve unit 71 of the fourth embodiment already described with reference to FIG.

第5実施形態によれば、何らかの理由で超電導コイル601の温度を直接測定できないとき、流路70eを流れる液体状態の窒素の温度から間接的に超電導コイル601の温度を推定して超電導コイル601の温度を制御する。   According to the fifth embodiment, when the temperature of the superconducting coil 601 cannot be directly measured for some reason, the temperature of the superconducting coil 601 is estimated indirectly from the temperature of nitrogen in the liquid state flowing through the flow path 70e. Control the temperature.

第5実施形態によれば、第4の実施形態と同様に、超電導コイル601に供給する液体状態の窒素の量を必要最小限度にしつつ、超電導コイル601の温度を予め定められた値に自動的に制御することができる。   According to the fifth embodiment, as in the fourth embodiment, the temperature of the superconducting coil 601 is automatically set to a predetermined value while the amount of nitrogen in the liquid state supplied to the superconducting coil 601 is minimized. Can be controlled.

第6実施形態について、図4〜図6に示す第4実施形態との相違点を中心に説明する。図9は、第6実施形態に係る空気分離装置1fの構成を示す構成図である。図10は、第6実施形態において、第1の弁部71、第3の弁部77、第1の測定部72及び第1の制御部73の関係を示すブロック図である。第6実施形態の冷却回路7は、第1の弁部71、第1の測定部72及び第1の制御部73に加えて、さらに第3の弁部77を備える。第6実施形態は、第1の弁部71を全開にしても、超電導コイル601の温度が基準値より大きい場合に対処することができる。   The sixth embodiment will be described focusing on differences from the fourth embodiment shown in FIGS. FIG. 9 is a configuration diagram illustrating a configuration of an air separation device 1f according to the sixth embodiment. FIG. 10 is a block diagram illustrating a relationship among the first valve unit 71, the third valve unit 77, the first measurement unit 72, and the first control unit 73 in the sixth embodiment. The cooling circuit 7 according to the sixth embodiment further includes a third valve unit 77 in addition to the first valve unit 71, the first measurement unit 72, and the first control unit 73. The sixth embodiment can cope with the case where the temperature of the superconducting coil 601 is higher than the reference value even if the first valve portion 71 is fully opened.

図9及び図10を参照して、第3の弁部77は、流路8o(第4の流路)と流路70c(第5の流路)との接続部より下流に設けられ、流路8oを流れる液体状態の窒素の流量を調節する電磁弁である。   Referring to FIG. 9 and FIG. 10, the third valve portion 77 is provided downstream from the connection portion between the flow path 8o (fourth flow path) and the flow path 70c (fifth flow path). This is a solenoid valve that adjusts the flow rate of nitrogen in the liquid state flowing through the passage 8o.

第1の制御部73は、第3の弁部77を開けた状態で(すなわち、液体状態の窒素が流路8oを流れて、精留塔5に戻された状態で)、第4実施形態で説明した第1の弁部71の開閉量を制御している。第1の制御部73は、第1の弁部71が全開の状態で、第1の測定部73で測定された温度が基準値(予め定められた値)より大きいとき、第3の弁部77を所定量閉じる制御をする。これにより、流路8oを流れる液体状態の窒素の量が減り、流路70cを流れる液体状態の窒素の量を増やすことができるので、超電導コイル601をより冷却することができる。   The first control unit 73 is in a state where the third valve unit 77 is opened (that is, in a state where liquid nitrogen flows through the flow path 8o and is returned to the rectification column 5). The opening / closing amount of the first valve portion 71 described in the above is controlled. The first control unit 73 has a third valve unit when the first valve unit 71 is fully open and the temperature measured by the first measurement unit 73 is larger than a reference value (predetermined value). 77 is controlled to close a predetermined amount. Thereby, the amount of nitrogen in the liquid state flowing through the flow path 8o is reduced, and the amount of nitrogen in the liquid state flowing through the flow path 70c can be increased, so that the superconducting coil 601 can be further cooled.

図11は、第6実施形態において、第1の弁部71及び第3の弁部77の制御を説明するフローチャートである。図6のフローチャートと同じ処理については、同一符号を付すことにより説明を省略する。   FIG. 11 is a flowchart illustrating control of the first valve unit 71 and the third valve unit 77 in the sixth embodiment. About the same process as the flowchart of FIG. 6, description is abbreviate | omitted by attaching | subjecting the same code | symbol.

第1の制御部73が、第1の弁部71が全開と判断したとき(ステップS5でYes)、第1の制御部73は、第3の弁部77が全閉か否かを判断する(ステップS8)。   When the first control unit 73 determines that the first valve unit 71 is fully open (Yes in step S5), the first control unit 73 determines whether or not the third valve unit 77 is fully closed. (Step S8).

第1の制御部73が、第3の弁部77が全閉でないと判断したとき(ステップS8でNo)、第1の制御部73は、第3の弁部77を所定量閉じる制御をする(ステップS9)。そして、ステップS1に戻る。   When the first control unit 73 determines that the third valve unit 77 is not fully closed (No in step S8), the first control unit 73 performs control to close the third valve unit 77 by a predetermined amount. (Step S9). Then, the process returns to step S1.

第1の制御部73が、第3の弁部77が全閉と判断したとき(ステップS8でYes)、第1の制御部73は、所定の報知部(例えば、ランプ、スピーカ)を作動させて、超電導コイル601の温度が基準値より大きいことを、空気分離装置1fの運転を管理する者に報知する(ステップS7)。   When the first control unit 73 determines that the third valve unit 77 is fully closed (Yes in step S8), the first control unit 73 operates a predetermined notification unit (for example, a lamp or a speaker). Then, the person who manages the operation of the air separation device 1f is notified that the temperature of the superconducting coil 601 is higher than the reference value (step S7).

図12は、第7実施形態に係る空気分離装置1gの構成を示す構成図である。図13は、第7実施形態において、第2の弁部74、第3の弁部77、第2の測定部75及び第2の制御部76の関係を示すブロック図である。第7実施形態は、図7及び図8に示す第5実施形態に、図9及び図10に示す第6実施形態の第3の弁部77を設けたことを特徴とする。第7実施形態は、第2の弁部74を全開にしても、超電導コイル601の温度が基準値より大きい場合に対処することができる。   FIG. 12 is a configuration diagram showing a configuration of an air separation device 1g according to the seventh embodiment. FIG. 13 is a block diagram illustrating a relationship among the second valve unit 74, the third valve unit 77, the second measurement unit 75, and the second control unit 76 in the seventh embodiment. The seventh embodiment is characterized in that the third valve portion 77 of the sixth embodiment shown in FIGS. 9 and 10 is provided in the fifth embodiment shown in FIGS. 7 and 8. The seventh embodiment can cope with the case where the temperature of the superconducting coil 601 is higher than the reference value even when the second valve portion 74 is fully opened.

第2の制御部76は、第3の弁部77を開けた状態で(すなわち、液体状態の窒素が流路8oを流れて、精留塔5に戻された状態で)、第5実施形態で説明した第2の弁部74の開閉量を制御している。第2の制御部76は、第2の弁部74が全開の状態で、第2の測定部75で測定された温度が基準値より大きいとき、第3の弁部77を所定量閉じる制御をする。これにより、流路8oを流れる液体状態の窒素の量が減り、流路70cを流れる液体状態の窒素の量を増やすことができるので、超電導コイル601をより冷却することができる。   The second control unit 76 is in a state where the third valve unit 77 is opened (that is, in a state where liquid nitrogen flows through the flow path 8o and is returned to the rectification column 5). The opening / closing amount of the second valve portion 74 described in the above is controlled. The second control unit 76 performs control to close the third valve unit 77 by a predetermined amount when the second valve unit 74 is fully opened and the temperature measured by the second measurement unit 75 is higher than the reference value. To do. Thereby, the amount of nitrogen in the liquid state flowing through the flow path 8o is reduced, and the amount of nitrogen in the liquid state flowing through the flow path 70c can be increased, so that the superconducting coil 601 can be further cooled.

第1実施形態から第7実施形態について、共通に適用される技術について、図1に示す第1実施形態に係る空気分離装置1aを例にして説明する。   Regarding the first to seventh embodiments, a commonly applied technique will be described using the air separation device 1a according to the first embodiment shown in FIG. 1 as an example.

図14は、超電導モータ60及び圧縮部61を収容している断熱密閉容器9の模式図である。断熱密閉容器9内には、超電導モータ60と、回転軸603に連結された圧縮部61とが配置されている。断熱密閉容器9は、例えば、精留塔5の塔頂近傍において、精留塔5の壁面に取り付ける。   FIG. 14 is a schematic view of the heat-insulated sealed container 9 that houses the superconducting motor 60 and the compression unit 61. A superconducting motor 60 and a compressing unit 61 connected to a rotating shaft 603 are disposed in the heat insulating sealed container 9. The heat insulating sealed container 9 is attached to the wall surface of the rectifying column 5, for example, in the vicinity of the top of the rectifying column 5.

この構成によれば、超電導モータ60及び圧縮部61を断熱密閉容器9に収容することにより、これらをユニット化している。従って、凝縮回路6の組み立て作業を容易にすることができる。   According to this configuration, the superconducting motor 60 and the compressing unit 61 are accommodated in the heat-insulated airtight container 9 to unitize them. Therefore, the assembly operation of the condensation circuit 6 can be facilitated.

図15は、超電導モータ60の構成を示す断面図である。超電導モータ60は、回転軸603、第1の固定子33a、第2の固定子33b、第3の固定子33c、第1の回転子34a、第2の回転子34b、第3の回転子34c及び第4の回転子34dを備える。圧縮部61から回転軸603の延びる方向に沿って、間隔をあけて、第1の固定子33a、第2の固定子33b、第3の固定子33cが配置されている。   FIG. 15 is a cross-sectional view showing the configuration of the superconducting motor 60. The superconducting motor 60 includes a rotating shaft 603, a first stator 33a, a second stator 33b, a third stator 33c, a first rotor 34a, a second rotor 34b, and a third rotor 34c. And a fourth rotor 34d. A first stator 33a, a second stator 33b, and a third stator 33c are arranged at intervals along the direction in which the rotation shaft 603 extends from the compression unit 61.

第1の固定子33aは、W相を生成するための固定子である。第1の固定子33aは、断熱容器35、軸受36、超電導コイル601及び隔壁38を備える。   The first stator 33a is a stator for generating a W phase. The first stator 33 a includes a heat insulating container 35, a bearing 36, a superconducting coil 601, and a partition wall 38.

断熱容器35の材料は、非磁性金属材である。断熱容器35は、円盤形状を有する。断熱容器35の中央部に軸受36が配置されている。軸受36は、回転軸603を回転自在に保持する。   The material of the heat insulation container 35 is a nonmagnetic metal material. The heat insulation container 35 has a disk shape. A bearing 36 is disposed at the center of the heat insulating container 35. The bearing 36 holds the rotating shaft 603 rotatably.

断熱容器35は、中空の構造を有する。断熱容器35内には、超電導コイル601が、軸受36を囲んで配置されている。超電導コイル601は、断熱容器35内に固定されている磁性体芯(不図示)に巻かれている。この磁性体芯と超電導コイル601とにより超電導磁石が構成される。断熱容器35内は、精留塔5から供給された冷媒、すなわち、気体状態の窒素(ボイルオフガス)で満たされている。第2実施形態から第7実施形態では、断熱容器35内が、凝縮回路6で生成された液体状態の窒素で満たされている。   The heat insulating container 35 has a hollow structure. A superconducting coil 601 is disposed in the heat insulating container 35 so as to surround the bearing 36. The superconducting coil 601 is wound around a magnetic core (not shown) fixed in the heat insulating container 35. The magnetic core and the superconducting coil 601 constitute a superconducting magnet. The inside of the heat insulating container 35 is filled with the refrigerant supplied from the rectification tower 5, that is, nitrogen in a gaseous state (boil-off gas). In the second embodiment to the seventh embodiment, the inside of the heat insulating container 35 is filled with nitrogen in a liquid state generated in the condensation circuit 6.

断熱容器35は、超電導コイル601と対向する箇所に、環状の貫通穴を有する。隔壁38によって、貫通穴が塞がれている。隔壁38は、断熱性、非磁性及び絶縁性、又は、断熱性、非磁性及び高抵抗の性質を有する。隔壁38の材料は、例えば、硬質ガラス、セラミックス、硬質プラスチックである。   The heat insulating container 35 has an annular through hole at a location facing the superconducting coil 601. The through hole is closed by the partition wall 38. The partition 38 has a heat insulating property, a non-magnetic property and an insulating property, or a heat insulating property, a non-magnetic property and a high resistance property. The material of the partition wall 38 is, for example, hard glass, ceramics, or hard plastic.

隔壁38が断熱性を有するのは、冷媒で満たされた断熱容器35内と、低温大気又は真空である断熱容器35外とを断熱するためである。隔壁38が、非磁性を有するのは、超電導コイル601及びこれが巻かれている磁性体芯(不図示)と、永久磁石41,43とを磁気的に結合させるためである。隔壁38が、絶縁性又は高抵抗性を有するのは、隔壁38に渦電流が発生しないようにするためである。上記磁気的結合が原因で発生する変動磁場によって、隔壁38に渦電流が発生すれば、隔壁38が発熱するからである。   The reason why the partition wall 38 has a heat insulating property is to insulate the inside of the heat insulating container 35 filled with the refrigerant from the outside of the heat insulating container 35 which is a low-temperature atmosphere or a vacuum. The reason why the partition wall 38 is non-magnetic is to magnetically couple the superconducting coil 601 and a magnetic core (not shown) around which the superconducting coil 601 is wound to the permanent magnets 41 and 43. The reason why the partition 38 has an insulating property or a high resistance is to prevent an eddy current from being generated in the partition 38. This is because the partition wall 38 generates heat if an eddy current is generated in the partition wall 38 due to the fluctuating magnetic field generated due to the magnetic coupling.

第2の固定子33bは、V相を生成するための固定子であり、第3の固定子33cは、U相を生成するための固定子である。第2の固定子33b及び第3の固定子33cの構成は、第1の固定子33aの構成と同じなので、説明を省略する。   The second stator 33b is a stator for generating a V phase, and the third stator 33c is a stator for generating a U phase. The configurations of the second stator 33b and the third stator 33c are the same as the configuration of the first stator 33a, and thus the description thereof is omitted.

第1の固定子33a、第2の固定子33b及び第3の固定子33cがそれぞれ備える超電導コイル601の構成は、例えば、特開2014−54092号公報に開示された固定子に備えられるコイルと同じ構成を採用することができる。   The configuration of the superconducting coil 601 provided in each of the first stator 33a, the second stator 33b, and the third stator 33c is, for example, a coil provided in the stator disclosed in Japanese Patent Application Laid-Open No. 2014-54092. The same configuration can be adopted.

圧縮部61から回転軸603の延びる方向に沿って、間隔をあけて、第1の回転子34a、第2の回転子34b、第3の回転子34c、第4の回転子34dが配置されている。第1の固定子33aは、第1の回転子34aと第2の回転子34bとによって、所定の間隔をあけて挟まれている。第2の固定子33bは、第2の回転子34bと第3の回転子34cとによって、所定の間隔をあけて挟まれている。第3の固定子33cは、第3の回転子34cと第4の回転子34dとによって、所定の間隔をあけて挟まれている。   A first rotor 34a, a second rotor 34b, a third rotor 34c, and a fourth rotor 34d are arranged at intervals along the direction in which the rotation shaft 603 extends from the compression unit 61. Yes. The first stator 33a is sandwiched between the first rotor 34a and the second rotor 34b at a predetermined interval. The second stator 33b is sandwiched between the second rotor 34b and the third rotor 34c at a predetermined interval. The third stator 33c is sandwiched between the third rotor 34c and the fourth rotor 34d at a predetermined interval.

回転軸603は、第1の回転子34a、第2の回転子34b、第3の回転子34c、第4の回転子34dのそれぞれの中心部に固定されており、第1の回転子34a、第2の回転子34b、第3の回転子34c、第4の回転子34dが回転することにより、回転軸603が回転する。   The rotation shaft 603 is fixed to the center of each of the first rotor 34a, the second rotor 34b, the third rotor 34c, and the fourth rotor 34d, and the first rotor 34a, As the second rotor 34b, the third rotor 34c, and the fourth rotor 34d rotate, the rotation shaft 603 rotates.

第1の回転子34aは、磁性材ヨーク40及び永久磁石41を備える。磁性材ヨーク40は、円盤形状を有する。第1の固定子33aと対向する、磁性材ヨーク40の面には、永久磁石41が配置されている。永久磁石41は、回転軸603を囲み、かつ、第1の固定子33aに備えられる隔壁38及び超電導コイル601と対向して配置されている。   The first rotor 34 a includes a magnetic material yoke 40 and a permanent magnet 41. The magnetic material yoke 40 has a disk shape. A permanent magnet 41 is disposed on the surface of the magnetic material yoke 40 facing the first stator 33a. The permanent magnet 41 surrounds the rotating shaft 603 and is disposed to face the partition wall 38 and the superconducting coil 601 provided in the first stator 33a.

第2の回転子34bは、構造部材42及び永久磁石43を備える。構造部材42は、円盤形状を有する。構造部材42の周面に、永久磁石43が配置されている。永久磁石43は、回転軸603を囲み、かつ、第1の固定子33aに備えられる隔壁38及び超電導コイル601、並びに、第2の固定子33bに備えられる隔壁38及び超電導コイル601と対向して配置されている。   The second rotor 34 b includes a structural member 42 and a permanent magnet 43. The structural member 42 has a disk shape. A permanent magnet 43 is disposed on the peripheral surface of the structural member 42. The permanent magnet 43 surrounds the rotating shaft 603 and faces the partition wall 38 and the superconducting coil 601 provided in the first stator 33a and the partition wall 38 and the superconducting coil 601 provided in the second stator 33b. Has been placed.

第3の回転子34cは、第2の回転子34bと同じ構成を有する。第3の回転子34cの永久磁石43は、回転軸603を囲み、かつ、第2の固定子33bに備えられる隔壁38及び超電導コイル601、並びに、第3の固定子33cに備えられる隔壁38及び超電導コイル601と対向して配置されている。   The third rotor 34c has the same configuration as the second rotor 34b. The permanent magnet 43 of the third rotor 34c surrounds the rotating shaft 603, and includes the partition wall 38 and the superconducting coil 601 provided in the second stator 33b, and the partition wall 38 provided in the third stator 33c and It is arranged to face the superconducting coil 601.

第4の回転子34dは、第1の回転子34aと同じ構成を有する。第4の回転子34dの永久磁石41は、回転軸603を囲み、かつ、第3の固定子33cに備えられる隔壁38及び超電導コイル601と対向して配置されている。   The fourth rotor 34d has the same configuration as the first rotor 34a. The permanent magnet 41 of the fourth rotor 34d surrounds the rotating shaft 603 and is disposed to face the partition wall 38 and the superconducting coil 601 provided in the third stator 33c.

永久磁石41,43は、例えば、希土類系永久磁石である。希土類系永久磁石は、強力な保磁力を有するので、第1実施形態〜第7実施形態では、高トルク密度の超電導モータ60を実現できる。   The permanent magnets 41 and 43 are, for example, rare earth permanent magnets. Since the rare earth-based permanent magnet has a strong coercive force, the superconducting motor 60 having a high torque density can be realized in the first to seventh embodiments.

近年、バルク状の酸化物超電導体のピン止め効果を利用して、その内部に磁束を閉じ込めることにより強力な永久磁石を実現する研究が進められている。該永久磁石を、超電導バルク磁石としてもよい。超電導バルク磁石は、従来の永久磁石以上の高い保磁力を有するので、これを従来の永久磁石に替えることにより高効率な超電導モータ60を実現できる。   In recent years, research has been conducted to realize a strong permanent magnet by confining magnetic flux inside the bulk oxide superconductor by using the pinning effect of the bulk oxide superconductor. The permanent magnet may be a superconducting bulk magnet. Since the superconducting bulk magnet has a higher coercive force than the conventional permanent magnet, a highly efficient superconducting motor 60 can be realized by replacing this with a conventional permanent magnet.

回転軸603の方向に沿って、第1の管部44a、第2の管部44b、第3の管部44cが配置されている。第1の管部44aは、第1の固定子33aの断熱容器35と第2の固定子33bの断熱容器35とを接続する。第1の管部44aを介して、第1の固定子33aの断熱容器35の内部と第2の固定子33bの断熱容器35の内部とが連通している。第2の管部44bは、第2の固定子33bの断熱容器35と第3の固定子33cの断熱容器35とを接続する。第2の管部44bを介して、第2の固定子33bの断熱容器35の内部と第3の固定子33cの断熱容器35の内部とが連通している。   A first tube portion 44a, a second tube portion 44b, and a third tube portion 44c are arranged along the direction of the rotation shaft 603. The 1st pipe part 44a connects the heat insulation container 35 of the 1st stator 33a, and the heat insulation container 35 of the 2nd stator 33b. The inside of the heat insulation container 35 of the first stator 33a and the inside of the heat insulation container 35 of the second stator 33b communicate with each other through the first pipe portion 44a. The second pipe portion 44b connects the heat insulating container 35 of the second stator 33b and the heat insulating container 35 of the third stator 33c. The inside of the heat insulating container 35 of the second stator 33b and the inside of the heat insulating container 35 of the third stator 33c communicate with each other through the second pipe portion 44b.

第3の管部44cは、一端が第3の固定子33cと接続されている。流路70aは、第3の管部44cの他端から第3の管部44cに入り、第3の固定子33cの断熱容器35の内部、第2の管部44b、第2の固定子33bの断熱容器35の内部、第1の管部44a、第1の固定子33aの断熱容器35の内部に通されている。流路70bは、第3の管部44cの他端から第3の管部44cに通されている。精留塔5から供給された気体状態の窒素(冷媒)は、流路70aを通り、第1の固定子33a、第2の固定子33b及び第3の固定子33cのそれぞれの断熱容器35に送られる。これらの断熱容器35に送られた冷媒は、流路70bを通り、図1に示す流路8iに戻される。このように、冷媒は、凝縮回路6と、第1の固定子33a、第2の固定子33b及び第3の固定子33cのそれぞれの断熱容器35との間で循環している。   One end of the third tube portion 44c is connected to the third stator 33c. The flow path 70a enters the third tube portion 44c from the other end of the third tube portion 44c, and the inside of the heat insulating container 35 of the third stator 33c, the second tube portion 44b, and the second stator 33b. Are passed through the inside of the heat insulating container 35, the first pipe portion 44a, and the heat insulating container 35 of the first stator 33a. The flow path 70b is passed from the other end of the third tube portion 44c to the third tube portion 44c. Nitrogen (refrigerant) in a gaseous state supplied from the rectification tower 5 passes through the flow path 70a and enters the heat insulating containers 35 of the first stator 33a, the second stator 33b, and the third stator 33c. Sent. The refrigerant sent to these heat insulation containers 35 returns to the flow path 8i shown in FIG. 1 through the flow path 70b. Thus, the refrigerant circulates between the condensation circuit 6 and the heat insulating containers 35 of the first stator 33a, the second stator 33b, and the third stator 33c.

第1の管部44a、第2の管部44b及び第3の管部44cは、気密性が要求されるため、通常、金属で構成される。超電導モータ60は、常温環境で組み立てられ、臨界温度以下の環境で使用される。このため、第1の管部44a、第2の管部44b及び第3の管部44cの熱変形を吸収するために、これらの管部は、蛇腹構造を有する。   Since the first tube portion 44a, the second tube portion 44b, and the third tube portion 44c are required to be airtight, they are usually made of metal. The superconducting motor 60 is assembled in a normal temperature environment and used in an environment below a critical temperature. For this reason, in order to absorb the thermal deformation of the 1st pipe part 44a, the 2nd pipe part 44b, and the 3rd pipe part 44c, these pipe parts have a bellows structure.

1a,1b,1c,1d,1e,1f,1g 空気分離装置
5 精留塔
6 凝縮回路
7 冷却回路
8i 流路(第1の流路の具体例)
8o 流路(第4の流路の具体例)
60 超電導モータ
61 圧縮部
62 熱交換部
63 膨張部
70a 流路(第2の流路の具体例)
70b 流路(第3の流路の具体例)
70c 流路(第5の流路の具体例)
70d 流路(第6の流路の具体例)
70e 流路(第7の流路の具体例)
71 第1の弁部
72 第1の測定部
73 第1の制御部
74 第2の弁部
75 第2の測定部
76 第2の制御部
77 第3の弁部
601 超電導コイル(超電導磁石の具体例)
1a, 1b, 1c, 1d, 1e, 1f, 1g Air separation device 5 Rectifying tower 6 Condensing circuit 7 Cooling circuit 8i Flow path (specific example of the first flow path)
8o channel (specific example of the fourth channel)
60 Superconducting motor 61 Compression unit 62 Heat exchange unit 63 Expansion unit 70a Flow path (specific example of second flow path)
70b channel (specific example of the third channel)
70c channel (specific example of the fifth channel)
70d channel (specific example of sixth channel)
70e channel (specific example of seventh channel)
71 1st valve part 72 1st measurement part 73 1st control part 74 2nd valve part 75 2nd measurement part 76 2nd control part 77 3rd valve part 601 Superconducting coil (specific of superconducting magnet) Example)

Claims (7)

液体状態の原料空気を深冷分離して気体状態の窒素を生成する精留塔と、
前記精留塔から取り出された気体状態の窒素のうち、一部の窒素が供給され、供給された窒素を気体状態から液体状態に変化させて前記精留塔に戻す凝縮回路と、
冷却回路と、を備え、
前記凝縮回路は、
液体窒素の沸点より高い臨界温度を有する超電導材料で構成された超電導磁石を含む超電導モータと、
前記超電導モータによって駆動され、前記凝縮回路を流れる気体状態の窒素を圧縮する圧縮部と、を備え、
前記冷却回路は、前記凝縮回路を流れる液体状態の窒素を用いて、前記超電導磁石を前記臨界温度以下に冷却し
前記凝縮回路は、
前記圧縮部によって圧縮された気体状態の窒素を膨張させることにより、窒素を気体状態から液体状態に変化させる膨張部と、
前記膨張部と前記精留塔とを接続し、液体状態の窒素を前記精留塔に導く第4の流路と、をさらに備え、
前記冷却回路は、
前記第4の流路に接続され、前記第4の流路を流れる液体状態の窒素の一部を前記超電導磁石に供給する第5の流路と、
前記精留塔に接続され、前記第5の流路によって前記超電導磁石に供給された液体状態の窒素を前記精留塔に導く第7の流路と、を備える、空気分離装置。
A rectifying column that cryogenically separates the raw material air in the liquid state to generate nitrogen in the gaseous state;
Among the nitrogen in the gaseous state taken out from the rectification column, a part of the nitrogen is supplied, a condensation circuit for changing the supplied nitrogen from a gaseous state to a liquid state and returning the nitrogen to the rectification column,
A cooling circuit,
The condensing circuit is
A superconducting motor including a superconducting magnet composed of a superconducting material having a critical temperature higher than the boiling point of liquid nitrogen;
A compression unit that is driven by the superconducting motor and compresses nitrogen in a gas state flowing through the condensing circuit;
The cooling circuit uses the nitrogen in the liquid state through said condensing circuit, cooling the superconducting magnet below the critical temperature,
The condensing circuit is
An inflating part for changing nitrogen from a gaseous state to a liquid state by inflating nitrogen in a gaseous state compressed by the compressing part;
A fourth flow path for connecting the expansion section and the rectification column and guiding nitrogen in a liquid state to the rectification column,
The cooling circuit is
A fifth flow path connected to the fourth flow path and supplying a part of the liquid nitrogen flowing through the fourth flow path to the superconducting magnet;
An air separation device , comprising: a seventh channel connected to the rectification column and guiding nitrogen in a liquid state supplied to the superconducting magnet by the fifth channel to the rectification column .
前記冷却回路は、
前記第5の流路又は前記第7の流路を流れる液体状態の窒素の流量を調節する第1の弁部と、
前記超電導磁石の温度を測定する第1の測定部と、
前記第1の測定部で測定された温度が、前記臨界温度以下の予め定められた値より小さいとき、前記超電導磁石に供給する液体状態の窒素の流量が少なくなり、前記第1の測定部で測定された温度が前記予め定められた値より大きいとき、前記超電導磁石に供給する液体状態の窒素の流量が多くなり、前記第1の測定部で測定された温度が前記予め定められた値のとき、前記超電導磁石に供給する液体状態の窒素の流量が変わらないように、前記第1の弁部の開閉量を制御する第1の制御部と、をさらに備える請求項に記載の空気分離装置。
The cooling circuit is
A first valve section for adjusting a flow rate of nitrogen in a liquid state flowing through the fifth flow path or the seventh flow path;
A first measuring unit for measuring the temperature of the superconducting magnet;
When the temperature measured by the first measurement unit is smaller than a predetermined value equal to or lower than the critical temperature, the flow rate of nitrogen in a liquid state supplied to the superconducting magnet decreases, and the first measurement unit When the measured temperature is greater than the predetermined value, the flow rate of liquid nitrogen supplied to the superconducting magnet increases, and the temperature measured by the first measurement unit is the predetermined value. The air separation according to claim 1 , further comprising: a first control unit that controls an opening / closing amount of the first valve unit so that a flow rate of liquid nitrogen supplied to the superconducting magnet does not change. apparatus.
前記冷却回路は、
前記第5の流路を流れる液体状態の窒素の流量を調節する第2の弁部と、
前記第7の流路を流れる液体状態の窒素の温度を測定する第2の測定部と、
前記第2の測定部で測定された温度が、前記臨界温度以下の予め定められた値より小さいとき、前記超電導磁石に供給する液体状態の窒素の流量が少なくなり、前記第2の測定部で測定された温度が前記予め定められた値より大きいとき、前記超電導磁石に供給する液体状態の窒素の流量が多くなり、前記第2の測定部で測定された温度が前記予め定められた値のとき、前記超電導磁石に供給する液体状態の窒素の流量が変わらないように、前記第2の弁部の開閉量を制御する第2の制御部と、をさらに備える請求項に記載の空気分離装置。
The cooling circuit is
A second valve portion for adjusting a flow rate of nitrogen in a liquid state flowing through the fifth flow path;
A second measuring unit for measuring a temperature of nitrogen in a liquid state flowing through the seventh flow path;
When the temperature measured by the second measurement unit is smaller than a predetermined value not more than the critical temperature, the flow rate of liquid nitrogen supplied to the superconducting magnet decreases, and the second measurement unit When the measured temperature is greater than the predetermined value, the flow rate of liquid nitrogen supplied to the superconducting magnet is increased, and the temperature measured by the second measurement unit is equal to the predetermined value. The air separation according to claim 1 , further comprising: a second control unit that controls an opening / closing amount of the second valve unit so that a flow rate of liquid nitrogen supplied to the superconducting magnet does not change. apparatus.
前記冷却回路は、前記第4の流路と前記第5の流路との接続部より下流に設けられ、前記第4の流路を流れる液体状態の窒素の流量を調節する第3の弁部をさらに備え、
前記第1の制御部は、前記第3の弁部を開けた状態で、前記第1の弁部の前記開閉量を制御しており、前記第1の弁部が全開の状態で、前記第1の測定部で測定された温度が前記予め定められた値より大きいとき、前記第3の弁部を所定量閉じる制御をする請求項に記載の空気分離装置。
The cooling circuit is provided downstream of a connection portion between the fourth flow path and the fifth flow path, and a third valve portion that adjusts a flow rate of liquid nitrogen flowing through the fourth flow path. Further comprising
The first control unit controls the opening / closing amount of the first valve unit with the third valve unit opened, and the first valve unit is fully opened with the first valve unit opened. The air separation device according to claim 2 , wherein when the temperature measured by one measuring unit is larger than the predetermined value, the third valve unit is controlled to be closed by a predetermined amount.
前記冷却回路は、前記第4の流路と前記第5の流路との接続部より下流に設けられ、前記第4の流路を流れる液体状態の窒素の流量を調節する第3の弁部をさらに備え、
前記第2の制御部は、前記第3の弁部を開けた状態で、前記第2の弁部の前記開閉量を制御しており、前記第2の弁部が全開の状態で、前記第2の測定部で測定された温度が前記予め定められた値より大きいとき、前記第3の弁部を所定量閉じる制御をする請求項に記載の空気分離装置。
The cooling circuit is provided downstream of a connection portion between the fourth flow path and the fifth flow path, and a third valve portion that adjusts a flow rate of liquid nitrogen flowing through the fourth flow path. Further comprising
The second control unit controls the opening / closing amount of the second valve unit with the third valve unit opened, and the second valve unit is fully opened with the second valve unit opened fully. when the temperature measured by the second measurement section is greater than the predetermined value, the air separation unit according to claim 3, a predetermined amount close control the third valve portion.
前記精留塔は、液体状態の原料空気を深冷分離して液体状態の酸素を生成し、
前記凝縮回路は、前記精留塔から取り出された液体状態の酸素と、前記圧縮部によって圧縮された気体状態の窒素とで熱交換させることによって、気体状態の窒素を冷却し、かつ、液体状態の酸素を気体状態にする熱交換部をさらに備える請求項1〜のいずれか一項に記載の空気分離装置。
The rectification column is a cryogenic separation of liquid source air to produce liquid oxygen.
The condensing circuit cools the gaseous nitrogen by causing heat exchange between the liquid oxygen extracted from the rectification column and the gaseous nitrogen compressed by the compression unit, and the liquid state The air separation device according to any one of claims 1 to 5 , further comprising a heat exchanging unit that converts the oxygen of the gas into a gaseous state.
前記超電導モータ及び前記圧縮部を収容する断熱密閉容器をさらに備える請求項1〜のいずれか一項に記載の空気分離装置。 The superconducting motor and the air separation unit as claimed in any one of claims 1 to 6, further comprising a heat insulating hermetic container for accommodating the compressing unit.
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