Deprecated: The each() function is deprecated. This message will be suppressed on further calls in /home/zhenxiangba/zhenxiangba.com/public_html/phproxy-improved-master/index.php on line 456
JP6885257B2 - Surface treatment method for metal materials and manufacturing method for metal materials - Google Patents
[go: Go Back, main page]

JP6885257B2 - Surface treatment method for metal materials and manufacturing method for metal materials - Google Patents

Surface treatment method for metal materials and manufacturing method for metal materials Download PDF

Info

Publication number
JP6885257B2
JP6885257B2 JP2017152961A JP2017152961A JP6885257B2 JP 6885257 B2 JP6885257 B2 JP 6885257B2 JP 2017152961 A JP2017152961 A JP 2017152961A JP 2017152961 A JP2017152961 A JP 2017152961A JP 6885257 B2 JP6885257 B2 JP 6885257B2
Authority
JP
Japan
Prior art keywords
metal material
rotary tool
defect
metal
exposed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2017152961A
Other languages
Japanese (ja)
Other versions
JP2019030887A (en
Inventor
承一郎 廣池
承一郎 廣池
山下 浩二
浩二 山下
卓也 須賀
卓也 須賀
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JFE Steel Corp
Original Assignee
JFE Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JFE Steel Corp filed Critical JFE Steel Corp
Priority to JP2017152961A priority Critical patent/JP6885257B2/en
Publication of JP2019030887A publication Critical patent/JP2019030887A/en
Application granted granted Critical
Publication of JP6885257B2 publication Critical patent/JP6885257B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Forging (AREA)
  • Pressure Welding/Diffusion-Bonding (AREA)
  • Metal Rolling (AREA)

Description

本発明は、金属材の表面に露出している欠陥を消失させる金属材の表面処理方法および金属材の製造方法に関する。 The present invention relates to a method for surface treatment of a metal material and a method for producing the metal material, which eliminates defects exposed on the surface of the metal material.

一般的に、鋼板(厚板、薄板)は連続鋳造や分解圧延、鍛造などのプロセスを経た鋼片を素材とし、熱間圧延や冷間圧延を行って製造されるが、この際、鋼片表面に空隙や割れといった欠陥が露出した状態で加熱および圧延を行うと、製品の表面性状の悪化や割れが生じる原因となる。 Generally, steel sheets (thick plates, thin plates) are manufactured by hot rolling or cold rolling using steel pieces that have undergone processes such as continuous casting, disassembly rolling, and forging. If heating and rolling are performed with defects such as voids and cracks exposed on the surface, the surface properties of the product may deteriorate or cracks may occur.

そこで、従来は、グラインダーを用いて鋼片(スラブ)表面を砥石で研削して、スラブ表面の欠陥を除去する鋼片表面手入れが行われている(例えば特許文献1)。また、プラノミラ等の工作機械を用いて鋼片(スラブ)表面をフライス工具で切削する鋼片表面手入れ方法も存在する(例えば特許文献2)。 Therefore, conventionally, the surface of a steel piece (slab) is ground with a grindstone using a grinder to remove defects on the surface of the slab (for example, Patent Document 1). There is also a method for caring for the surface of a steel piece (slab) by cutting the surface of the steel piece (slab) with a milling tool using a machine tool such as Planomira (for example, Patent Document 2).

特開昭51−18937号公報Japanese Unexamined Patent Publication No. 51-18937 特開平9−108725号公報Japanese Unexamined Patent Publication No. 9-108725

特許文献1のようなグラインダーによる研削加工で鋼片表面の手入れを行う方法は、一般的で広く使用されている手法であるものの、以下のような問題がある。すなわち、欠陥の除去に際して、ピンポイントで欠陥を除去しようとすると、欠陥除去部分が凹形状となり圧延品質にも悪影響を与えるため、通常は欠陥周辺の表層も除去し、急激な傾斜を作らないようにする。しかしながら、欠陥は鋼材内部に多数存在しているため、欠陥周辺の表層を除去した際に、もともと鋼材内部に存在していた別の欠陥が手入れにより表面に露出してしまう。特許文献2に示す技術についても、研削と切削の違いはあるものの、内部に隠れていた欠陥を露出してしまう問題は同様に存在する。このような問題は、鋼片に限らず、他の金属材においても同様に生じる。 The method of polishing the surface of a steel piece by grinding with a grinding machine as in Patent Document 1 is a general and widely used method, but has the following problems. That is, when removing defects, if a pinpoint attempt is made to remove the defects, the defect removing portion becomes concave and adversely affects the rolling quality. Therefore, normally, the surface layer around the defects should also be removed so as not to make a steep slope. To. However, since many defects are present inside the steel material, when the surface layer around the defects is removed, another defect originally existing inside the steel material is exposed to the surface by maintenance. Regarding the technique shown in Patent Document 2, although there is a difference between grinding and cutting, there is also a problem of exposing defects hidden inside. Such a problem occurs not only in steel pieces but also in other metal materials.

したがって、本発明は、金属材表面に新たな欠陥を露出させることなく表面に露出した欠陥を消失させることができる金属材の表面処理方法および金属材の製造方法を提供することを課題とする。 Therefore, it is an object of the present invention to provide a surface treatment method for a metal material and a method for producing a metal material, which can eliminate the defects exposed on the surface without exposing new defects on the surface of the metal material.

上記課題を解決するため、本発明は以下の(1)〜(12)を提供する。 In order to solve the above problems, the present invention provides the following (1) to (12).

(1)表面に欠陥の露出部を有する金属材に対し、前記金属材表面の欠陥の露出部に、前記金属材よりも硬い材質の回転工具を、回転させながら接触させて、その際に発生する摩擦熱と圧力により前記金属材の前記回転工具との接触部分を塑性流動させ、かつ塑性流動部分に加熱された金属粉が供給された状態とし、前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させて、前記金属粉を巻き込みながら、前記金属材における前記回転工具の移動部分を順次塑性流動させ、前記金属材の欠陥の露出部を塞ぐことを特徴とする金属材の表面処理方法。 (1) A rotating tool made of a material harder than the metal material is brought into contact with the exposed portion of the defect on the surface of the metal material while rotating with respect to the metal material having the exposed portion of the defect on the surface. The contact portion of the metal material with the rotary tool is plastically flowed by the frictional heat and pressure, and the heated metal powder is supplied to the plastic flow portion, and the rotary tool is rotated while being defective. The metal powder is moved along the distribution of the exposed portion of the metal material, and the moving portion of the rotary tool in the metal material is sequentially plastically flowed while entraining the metal powder to close the exposed portion of the defect of the metal material. Surface treatment method for metal materials.

(2)前記金属粉を、予め前記金属材表面の欠陥の露出部が存在する部分に供給しておくことを特徴とする(1)に記載の金属材の表面処理方法。 (2) The method for surface treating a metal material according to (1), wherein the metal powder is supplied in advance to a portion of the surface of the metal material where an exposed portion of a defect exists.

(3)前記金属粉を、前記金属材の前記回転工具により塑性流動された部分に供給しながら、前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させることを特徴とする(1)に記載の金属材の表面処理方法。 (3) The metal powder is supplied to a portion of the metal material that has been plastically flowed by the rotary tool, and the rotary tool is moved along the distribution of exposed portions of defects while being rotated. The surface treatment method for a metal material according to (1).

(4)前記回転工具は、その直径が欠陥の露出部の短尺側寸法以上であることを特徴とする(1)から(3)のいずれかに記載の金属材の表面処理方法。 (4) The method for surface treating a metal material according to any one of (1) to (3), wherein the rotary tool has a diameter equal to or larger than the short side dimension of the exposed portion of the defect.

(5)前記回転工具による金属材を塑性流動させる表面処理に先立って、処理前の金属材表面の欠陥の露出部をマーキングし、金属材のマーキングした部分を前記回転工具により塑性流動させることを特徴とする(1)から(4)のいずれかに記載の金属材の表面処理方法。 (5) Prior to the surface treatment of plastically flowing the metal material by the rotary tool, the exposed portion of the defect on the surface of the metal material before the treatment is marked, and the marked portion of the metal material is plastically flowed by the rotary tool. The method for surface-treating a metal material according to any one of (1) to (4).

(6)前記金属材は、連続鋳造または分塊圧延、鍛造プロセスを経た鋼片であることを特徴とする(1)から(5)のいずれかに記載の金属材の表面処理方法。 (6) The method for surface treating a metal material according to any one of (1) to (5), wherein the metal material is a steel piece that has undergone continuous casting, slabbing rolling, or a forging process.

(7)表面に欠陥の露出部を有する素材金属材を準備する工程と、
前記素材金属材表面の欠陥の露出部に、前記素材金属材よりも硬い材質の回転工具を、回転させながら接触させて、その際に発生する摩擦熱と圧力により前記素材金属材の前記回転工具との接触部分を塑性流動させる工程と、
塑性流動部分に加熱された金属が供給された状態とする工程と、
前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させて、前記金属粉を巻き込みながら、前記金属材における前記回転工具の移動部分を順次塑性流動させる工程と
を有し、
素材金属材の塑性流動により、欠陥の露出部を塞ぐことを特徴とする金属材の製造方法。
(7) A process of preparing a material metal material having an exposed portion of a defect on the surface, and
A rotating tool made of a material harder than the material metal material is brought into contact with the exposed portion of the defect on the surface of the material metal material while rotating, and the rotating tool of the material metal material is subjected to frictional heat and pressure generated at that time. The process of plastically flowing the contact part with
The process of supplying heated metal to the plastic flow part, and
The rotary tool is moved along the distribution of the exposed portion of the defect while being rotated, and the moving portion of the rotary tool in the metal material is sequentially plastically flowed while entraining the metal powder. ,
Material A method for manufacturing a metal material, which comprises closing an exposed part of a defect by plastic flow of the metal material.

(8)前記塑性流動部分に加熱された金属が供給された状態とする工程は、前記金属粉を、予め前記金属材表面の欠陥の露出部が存在する部分に供給しておくことにより行われることを特徴とする(7)に記載の金属材の製造方法。 (8) The step of supplying the heated metal to the plastic flow portion is performed by supplying the metal powder to the portion of the surface of the metal material where the exposed portion of the defect exists in advance. The method for producing a metal material according to (7).

(9)前記塑性流動部分に加熱された金属が供給された状態とする工程は、前記金属粉を、前記金属材の前記回転工具により塑性流動された部分に供給しながら、前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させることにより行われることを特徴とする(7)に記載の金属材の製造方法。 (9) In the step of supplying the heated metal to the plastic flow portion, the rotary tool is rotated while supplying the metal powder to the portion of the metal material that has been plastically flowed by the rotary tool. The method for producing a metal material according to (7), wherein the metal material is moved along the distribution of exposed portions of defects in the state of being kept.

(10)前記回転工具は、その直径が欠陥の露出部の短尺側寸法以上であることを特徴とする(7)から(9)のいずれかに記載の金属材の製造方法。 (10) The method for producing a metal material according to any one of (7) to (9), wherein the rotary tool has a diameter equal to or larger than the short side dimension of the exposed portion of the defect.

(11)前記回転工具による素材金属材を塑性流動させる表面処理に先立って、素材金属材表面の欠陥の露出部をマーキングし、素材金属材のマーキングした部分を前記回転工具により塑性流動させることを特徴とする(7)から(10)のいずれかに記載の金属材の製造方法。 (11) Prior to the surface treatment of plastically flowing the material metal material by the rotary tool, the exposed portion of the defect on the surface of the material metal material is marked, and the marked portion of the material metal material is plastically flowed by the rotary tool. The method for producing a metal material according to any one of (7) to (10).

(12)前記素材金属材は、連続鋳造または分塊圧延、鍛造プロセスを経た素材鋼片であることを特徴とする(7)から(11)のいずれかに記載の金属材の製造方法。 (12) The method for producing a metal material according to any one of (7) to (11), wherein the material metal material is a material steel piece that has undergone continuous casting, slabbing rolling, or a forging process.

本発明によれば、処理前の金属材の表面に存在する欠陥の露出部に、金属材よりも硬い材質の回転工具を、回転させながら接触させて、その際に発生す摩擦熱と圧力により金属材の接触部分を塑性流動させ、かつ塑性流動部分に加熱された金属粉が供給された状態とし、回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させて、金属粉を巻き込みながら、金属材における回転工具の移動部分を順次塑性流動させ、欠陥の露出部を塞ぐので、金属材表面に新たな欠陥を露出させることなく、表面に露出する欠陥を消失させることができる。 According to the present invention, a rotating tool made of a material harder than the metal material is brought into contact with the exposed portion of the defect existing on the surface of the metal material before the treatment while rotating, and the frictional heat and pressure generated at that time are used. The contact part of the metal material is plastically flowed, and the heated metal powder is supplied to the plastic flow part, and the rotating tool is moved along the distribution of the exposed part of the defect while being rotated to obtain the metal. While entraining the powder, the moving parts of the rotating tool in the metal material are sequentially plastically flowed to close the exposed parts of the defects, so that the defects exposed on the surface can be eliminated without exposing new defects on the surface of the metal material. it can.

連続鋳造や分解圧延、鍛造などのプロセスを経た鋼片を模式的に示す断面図である。It is sectional drawing which shows typically the steel piece which went through the process such as continuous casting, disassembly rolling, and forging. 図1の状態から酸化スケールを除去して、実施形態の表面処理方法に供される素材鋼片とした状態を模式的に示す断面図である。It is sectional drawing which shows typically the state which removed the oxide scale from the state of FIG. 1 and made into the material steel piece to be used for the surface treatment method of embodiment. 本発明の第1の実施形態に係る表面処理方法の手順を示す図である。It is a figure which shows the procedure of the surface treatment method which concerns on 1st Embodiment of this invention. 本発明の第2の実施形態に係る表面処理方法の手順を示す図である。It is a figure which shows the procedure of the surface treatment method which concerns on 2nd Embodiment of this invention. 回転工具を示す正面図および底面図である。It is a front view and a bottom view which shows a rotary tool.

以下、添付図面を参照して本発明の実施の形態について説明する。
図1は連続鋳造や分解圧延、鍛造などのプロセスを経た鋼片を模式的に示す断面図、図2は図1の状態から酸化スケールを除去して、本実施形態の表面処理方法に供される素材鋼片とした状態を模式的に示す断面図、図3は第1の実施形態の表面処理方法の手順を示す図、図4は第2の実施形態の表面処理方法の手順を示す図である。
Hereinafter, embodiments of the present invention will be described with reference to the accompanying drawings.
FIG. 1 is a cross-sectional view schematically showing a steel piece that has undergone processes such as continuous casting, disassembly rolling, and forging, and FIG. 2 is a surface treatment method of the present embodiment in which the oxide scale is removed from the state of FIG. FIG. 3 is a cross-sectional view schematically showing a state in which the material is a steel piece, FIG. 3 is a diagram showing a procedure of the surface treatment method of the first embodiment, and FIG. Is.

鋼片の鋼種は特に限定されないが、図1では一般的な高炭素鋼を用いた場合を示しており、連続鋳造や分解圧延、鍛造などのプロセスを経た状態では表面に黒皮と呼ばれる酸化スケール2を有した黒皮付き鋼片となっている。鋼片の内部には欠陥3が存在する。 The steel type of the steel piece is not particularly limited, but FIG. 1 shows the case where general high carbon steel is used, and the surface of the steel piece is an oxidation scale called black skin after undergoing processes such as continuous casting, disassembly rolling, and forging. It is a steel piece with black skin having 2. Defect 3 exists inside the steel piece.

図1の状態から事前に、ショット、研削、切削等の機械加工手段で、酸化スケール2を除去し、図2に示すような素材鋼片1とする。この素材鋼片1は、表面に空隙や割れといった欠陥3の露出部3aを有している。 From the state of FIG. 1, the oxide scale 2 is removed in advance by machining means such as shot, grinding, and cutting to obtain the material steel piece 1 as shown in FIG. The material steel piece 1 has an exposed portion 3a of defects 3 such as voids and cracks on the surface.

本発明においては、この素材鋼片1に対して塑性流動加工を利用した表面処理を行う。 In the present invention, the material steel piece 1 is subjected to surface treatment using plastic flow processing.

最初に、表面処理方法の第1の実施形態について説明する。
表面処理方法の第1の実施形態は、図3の(a)〜(d)の手順で行う。
表面処理を行う前の事前準備として、最初に、素材鋼片1に存在する欠陥3の表面に露出している露出部3aの箇所を確認し、マーキングする。欠陥3の露出部3aの箇所の確認は目視で行うことができる。また、一般的に使用されている浸透探傷試験を行って欠陥3を浮かび上がらせてもよい。
First, a first embodiment of the surface treatment method will be described.
The first embodiment of the surface treatment method is carried out according to the procedures (a) to (d) of FIG.
As a preliminary preparation before performing the surface treatment, first, the portion of the exposed portion 3a exposed on the surface of the defect 3 existing in the material steel piece 1 is confirmed and marked. The portion of the exposed portion 3a of the defect 3 can be visually confirmed. In addition, a commonly used penetrant inspection may be performed to bring out the defect 3.

次に、素材鋼片1を工作機械にセットする。工作機械には、工具として図5に示す回転工具10を装着する。図5に示すように、回転工具10は全体が円柱状をなし、先端のフランジ部分が円錐台状となっている。回転工具10は、その回転軸を素材鋼片に対して傾けることが可能であり、傾き角は0.3〜3.0度程度が好ましい。傾く方向は、工具の進行方向に対して前方側が浮くような方向が好ましい。回転工具10は、素材鋼片1よりも硬い材質のものを用いる。回転工具10の材質としては、例えば、超硬(WCを主体とするもの)、Co合金、セラミックス、サーメット等を用いることができる。回転工具10の直径は、欠陥3の露出部3aの短尺側の寸法以上とすることが好ましい。なお、図5において、(a)は正面図、(b)は底面図である。 Next, the material steel piece 1 is set in the machine tool. The rotary tool 10 shown in FIG. 5 is attached to the machine tool as a tool. As shown in FIG. 5, the rotary tool 10 has a columnar shape as a whole, and the flange portion at the tip has a truncated cone shape. The rotary tool 10 can tilt its rotating shaft with respect to the material steel piece, and the tilt angle is preferably about 0.3 to 3.0 degrees. The tilting direction is preferably a direction in which the front side floats with respect to the traveling direction of the tool. As the rotary tool 10, a material harder than the material steel piece 1 is used. As the material of the rotary tool 10, for example, cemented carbide (mainly WC), Co alloy, ceramics, cermet and the like can be used. The diameter of the rotary tool 10 is preferably equal to or larger than the dimension on the short side of the exposed portion 3a of the defect 3. In FIG. 5, (a) is a front view and (b) is a bottom view.

また、工作機械には、金属粉を加熱し、加熱された金属粉を供給する装置が設置されており、この装置により予め金属粉を加熱しておく。 Further, the machine tool is equipped with a device for heating the metal powder and supplying the heated metal powder, and the metal powder is heated in advance by this device.

このように事前準備した後、最初に、マーキング部分4の上に予め加熱していた金属粉5を供給する(図3(a))。これにより、その部分の素材鋼片1の表面温度が上昇する。金属粉5は、素材鋼片1と同じ材料であることが好ましいが、後の工程で加熱およびスケール除去を行う場合は、異なる材料であってもかまわない。金属粉5は素材鋼片1の表面を適切に加熱できる温度であればよいが、供給する金属粉5の変態点以下が好ましい。金属粉5が鉄粉の場合は、700℃以下が好ましい。 After preparing in this way, first, the preheated metal powder 5 is supplied onto the marking portion 4 (FIG. 3 (a)). As a result, the surface temperature of the material steel piece 1 in that portion rises. The metal powder 5 is preferably made of the same material as the material steel piece 1, but may be made of a different material when heating and scale removal are performed in a later step. The metal powder 5 may have a temperature at which the surface of the material steel piece 1 can be appropriately heated, but is preferably equal to or lower than the transformation point of the supplied metal powder 5. When the metal powder 5 is iron powder, the temperature is preferably 700 ° C. or lower.

そして、回転工具10を回転させながら下降させ、素材鋼片1の欠陥3の露出部3aが存在するマーキング部4の端部に対応する位置に回転工具10を接触させ、その後、所定の深さ分、回転工具を素材鋼片1へ埋没させる(図3(b))。回転工具10の埋没させる深さは、回転工具10のフランジ高さ未満であり、底面の進行方向側が素材鋼片1から浮いていることが好ましい。このように回転工具10を回転させながら埋没させることで、回転工具10の摩擦と圧力により、素材鋼片1の回転工具10との接触部分が金属粉5を巻き込みながら塑性流動する。鋼片において塑性流動が開始する温度は、800〜1000℃程度であるので、そのような温度になるように、回転工具10の周速が設定される。回転工具10の周速は、50〜150mpm程度が好ましい。 Then, the rotary tool 10 is lowered while rotating, and the rotary tool 10 is brought into contact with the end portion of the marking portion 4 where the exposed portion 3a of the defect 3 of the material steel piece 1 exists, and then the rotary tool 10 is brought into contact with the predetermined depth. The rotary tool is buried in the material steel piece 1 for a minute (FIG. 3 (b)). It is preferable that the depth of the rotary tool 10 to be buried is less than the height of the flange of the rotary tool 10, and the bottom surface in the traveling direction is floated from the material steel piece 1. By burying the rotary tool 10 while rotating it in this way, the contact portion of the material steel piece 1 with the rotary tool 10 plastically flows while entraining the metal powder 5 due to the friction and pressure of the rotary tool 10. Since the temperature at which the plastic flow starts in the steel piece is about 800 to 1000 ° C., the peripheral speed of the rotary tool 10 is set so as to reach such a temperature. The peripheral speed of the rotary tool 10 is preferably about 50 to 150 mpm.

回転工具10の摩擦と圧力により、素材鋼片1の回転工具10との接触部分が塑性流動を開始したことを確認した後、欠陥3の露出部3aの分布に沿って回転している回転工具10を、金属粉5を巻き込んだ状態で移動させる(図3(c))。なお、塑性流動が開始されたことは、例えば、回転工具10のトルクの変化により確認することができる。 After confirming that the contact portion of the material steel piece 1 with the rotary tool 10 has started plastic flow due to the friction and pressure of the rotary tool 10, the rotary tool is rotating along the distribution of the exposed portion 3a of the defect 3. 10 is moved with the metal powder 5 involved (FIG. 3 (c)). The start of plastic flow can be confirmed, for example, by changing the torque of the rotary tool 10.

このように素材鋼片1の欠陥3の露出部3aを含む部分が回転工具10により塑性流動され、回転工具10が通過した後の素材鋼片1の表面部には塑性流動部分6が形成され、その部分に存在していた欠陥3の露出部3aが塞がる。 In this way, the portion of the material steel piece 1 including the exposed portion 3a of the defect 3 is plastically flowed by the rotary tool 10, and the plastic flow portion 6 is formed on the surface portion of the material steel piece 1 after the rotary tool 10 has passed. , The exposed portion 3a of the defect 3 existing in that portion is closed.

そして、図3(d)のように、回転工具10がマーキング部4の終端まで達した後、回転工具10を上昇させ、残留している金属粉を除去する。このような操作を、全ての欠陥3の露出部3aに対して行うことにより、露出部3aが消失した鋼片11が得られる。 Then, as shown in FIG. 3D, after the rotary tool 10 reaches the end of the marking portion 4, the rotary tool 10 is raised to remove the remaining metal powder. By performing such an operation on the exposed portions 3a of all the defects 3, the steel piece 11 in which the exposed portions 3a have disappeared can be obtained.

以上のように、回転工具10を回転させながら素材鋼片1に接触させることによる摩擦熱と圧力により、欠陥3の露出部3aが存在する鋼片部分を塑性流動させて露出部3aを塞ぐので、研削や切削による手入れのように新たな欠陥を露出させることなく、表面に露出する欠陥を消失させることができる。 As described above, the frictional heat and pressure generated by bringing the rotary tool 10 into contact with the material steel piece 1 while rotating the rotating tool 10 causes the steel piece portion in which the exposed portion 3a of the defect 3 exists to be plastically flowed to close the exposed portion 3a. It is possible to eliminate the defects exposed on the surface without exposing new defects as in the case of maintenance by grinding or cutting.

また、常温で摩擦攪拌する場合には、回転工具10の必要な圧力と摩擦負荷が過大となる場合があるが、欠陥3の露出部3aが存在するマーキング部4の上に加熱された金属粉5を供給することにより、その部分の素材鋼片1の表面温度を高くすることができるので、塑性流動しやすくなって回転工具10の圧力と摩擦負荷を軽減することができる。また、回転工具10による摩擦攪拌の際に形成される素材鋼片1の凹部を小さくすることもできる。 Further, in the case of friction stir welding at room temperature, the required pressure and friction load of the rotary tool 10 may become excessive, but the metal powder heated on the marking portion 4 in which the exposed portion 3a of the defect 3 exists. By supplying 5, the surface temperature of the material steel piece 1 at that portion can be raised, so that plastic flow can be easily performed and the pressure and friction load of the rotary tool 10 can be reduced. Further, the recess of the material steel piece 1 formed during friction stir welding by the rotary tool 10 can be reduced.

なお、特開2012−40584号公報には、摩擦攪拌を行う際に、素材を高周波加熱により加熱することが記載されているが、それを適用した場合には、加熱時間が処理時間に加算され、処理時間が長くなってしまう。また、エネルギーロスも大きくなる。これに対し、本実施形態では、金属粉5を供給することにより加熱したい部分のみを迅速に加熱するので、これらの問題は生じない。 Japanese Patent Application Laid-Open No. 2012-40584 describes that the material is heated by high-frequency heating when friction stir welding is performed, but when this is applied, the heating time is added to the processing time. , The processing time becomes long. In addition, energy loss also increases. On the other hand, in the present embodiment, since only the portion to be heated is rapidly heated by supplying the metal powder 5, these problems do not occur.

次に、表面処理方法の第2の実施形態について説明する。
表面処理方法の第2の実施形態は、図4の(a)〜(d)の手順で行う。
表面処理を行う前の事前準備として、最初に、第1の実施形態と同様、素材鋼片1に存在する欠陥3の表面に露出している露出部3aの箇所を確認し、マーキングする。
Next, a second embodiment of the surface treatment method will be described.
The second embodiment of the surface treatment method is carried out according to the procedures (a) to (d) of FIG.
As a preliminary preparation before performing the surface treatment, first, as in the first embodiment, the portion of the exposed portion 3a exposed on the surface of the defect 3 existing in the material steel piece 1 is confirmed and marked.

次に、素材鋼片1を工作機械にセットし、第1の実施形態と同様、工作機械に工具として回転工具10を装着する。また、工作機械には、金属粉を加熱し、加熱された金属粉を供給する装置が設置されており、この装置により予め金属粉を加熱しておく。そしてこの装置からノズルを介して金属粉を摩擦攪拌部分に直接供給できるようにしておく。 Next, the material steel piece 1 is set in the machine tool, and the rotary tool 10 is attached to the machine tool as a tool as in the first embodiment. Further, the machine tool is equipped with a device for heating the metal powder and supplying the heated metal powder, and the metal powder is heated in advance by this device. Then, the metal powder can be directly supplied from this device to the friction stir portion via the nozzle.

このように事前準備した後、最初に、回転工具10を回転させながら下降させ、素材鋼片1の欠陥3の露出部3aが存在するマーキング部4の端部に対応する位置に回転工具10を接触させ、その後、所定の深さ分、回転工具を素材鋼片1へ埋没させる(図4(a))。第1の実施形態と同様、回転工具10の埋没させる深さは、回転工具10のフランジ高さ未満であり、底面の進行方向側が素材鋼片1から浮いていることが好ましい。このように回転工具10を回転させながら埋没させることで、回転工具10の摩擦と圧力により、素材鋼片1の回転工具10との接触部分が塑性流動する。回転工具10の周速は第1の実施形態と同様、50〜150mpm程度が好ましい。 After preparing in advance in this way, first, the rotary tool 10 is lowered while rotating, and the rotary tool 10 is placed at a position corresponding to the end of the marking portion 4 where the exposed portion 3a of the defect 3 of the material steel piece 1 exists. After contacting, the rotary tool is embedded in the material steel piece 1 by a predetermined depth (FIG. 4 (a)). Similar to the first embodiment, it is preferable that the depth of the rotary tool 10 to be buried is less than the flange height of the rotary tool 10, and the traveling direction side of the bottom surface is floating from the material steel piece 1. By burying the rotary tool 10 while rotating it in this way, the contact portion of the material steel piece 1 with the rotary tool 10 plastically flows due to the friction and pressure of the rotary tool 10. The peripheral speed of the rotary tool 10 is preferably about 50 to 150 mpm, as in the first embodiment.

次に、ノズル7から塑性流動部分への金属粉5の供給を開始する(図4(b))。これにより、塑性流動部分に金属粉5が巻き込まれる。このとき、回転工具10の底面の進行方向側が浮いていることにより、金属粉5を供給しやすくなる。 Next, the supply of the metal powder 5 from the nozzle 7 to the plastic flow portion is started (FIG. 4 (b)). As a result, the metal powder 5 is involved in the plastic flow portion. At this time, since the bottom surface of the rotary tool 10 is floating on the traveling direction side, the metal powder 5 can be easily supplied.

回転工具10の摩擦と圧力により、素材鋼片1の回転工具10との接触部分が塑性流動を開始したことを確認した後、欠陥3の露出部3aの分布に沿って回転している回転工具10を、ノズル7から供給される金属粉5を巻き込んだ状態で移動させる(図4(c))。このとき、ノズル7も回転工具10とともに移動し、常に塑性流動が生じている部分に金属粉5が供給することができるようにする。 After confirming that the contact portion of the material steel piece 1 with the rotary tool 10 has started plastic flow due to the friction and pressure of the rotary tool 10, the rotary tool rotating along the distribution of the exposed portion 3a of the defect 3. 10 is moved in a state where the metal powder 5 supplied from the nozzle 7 is involved (FIG. 4 (c)). At this time, the nozzle 7 also moves together with the rotary tool 10 so that the metal powder 5 can be supplied to the portion where the plastic flow is always generated.

これにより、第1の実施形態と同様、素材鋼片1の欠陥3の露出部3aを含む部分が回転工具10により塑性流動され、回転工具10が通過した後の素材鋼片1の表面部には塑性流動部分6が形成され、その部分に存在していた欠陥3の露出部3aが塞がる。 As a result, as in the first embodiment, the portion of the material steel piece 1 including the exposed portion 3a of the defect 3 is plastically flowed by the rotary tool 10 and becomes the surface portion of the material steel piece 1 after the rotary tool 10 has passed. A plastic flow portion 6 is formed, and the exposed portion 3a of the defect 3 existing in the portion is closed.

そして、図4(d)のように、回転工具10がマーキング部4の終端まで達した後、回転工具10を上昇させ、残留している金属粉を除去する。このような操作を、全ての欠陥3の露出部3aに対して行うことにより、露出部3aが消失した鋼片11が得られる。 Then, as shown in FIG. 4D, after the rotary tool 10 reaches the end of the marking portion 4, the rotary tool 10 is raised to remove the remaining metal powder. By performing such an operation on the exposed portions 3a of all the defects 3, the steel piece 11 in which the exposed portions 3a have disappeared can be obtained.

第1の実施形態では、欠陥3の露出部3aが存在する部分に予め金属粉5を付着する作業が必要であり、作業者の労力が大きくなるとともに、金属粉を比較的多量に付着する必要があるのに対し、第2の実施形態では、素材鋼片1の露出部3aが存在する部分を塑性流動させながら、ノズル7から直接その部分に金属粉5を供給するので、事前の作業が不要であり、また、金属粉5は必要量であればよく、金属粉5の量を少なくすることができる。 In the first embodiment, it is necessary to attach the metal powder 5 to the portion of the defect 3 where the exposed portion 3a exists in advance, which increases the labor of the operator and requires that a relatively large amount of the metal powder is attached. On the other hand, in the second embodiment, the metal powder 5 is directly supplied from the nozzle 7 to the exposed portion 3a of the material steel piece 1 while being plastically flowed. It is unnecessary, and the amount of the metal powder 5 may be as long as it is necessary, and the amount of the metal powder 5 can be reduced.

なお、本発明は、上記実施の形態に限定されることなく、本発明の思想の範囲内で種々変形することが可能である。例えば、上記実施の形態では金属材として連続鋳造または分塊圧延、鍛造のプロセスを経た鋼片を用いた例を示したが、鋼片に限らず他の金属材でもよく、アルミニウム片等を用いることができる。 The present invention is not limited to the above-described embodiment, and can be variously modified within the scope of the idea of the present invention. For example, in the above embodiment, an example in which a steel piece that has undergone a continuous casting, ingot rolling, or forging process is used as the metal material is shown, but the steel piece is not limited to other metal materials, and an aluminum piece or the like is used. be able to.

次に、本発明の実施例について説明する。
ここでは、金属材として、高炭素鋼を連続鋳造して製造した鋼片を用いた。鋼片の寸法は、長さ500mm×幅500mm×厚さ250mmとした。この鋼片の表面に形成されている酸化スケール層を事前に機械加工により除去して、素材鋼片とし、素材鋼片に存在する欠陥の表面に露出している露出部の箇所を目視で確認しマーキングした。
Next, examples of the present invention will be described.
Here, as the metal material, a steel piece produced by continuously casting high carbon steel was used. The dimensions of the steel piece were 500 mm in length × 500 mm in width × 250 mm in thickness. The oxide scale layer formed on the surface of this steel piece is removed by machining in advance to obtain a material steel piece, and the exposed portion exposed on the surface of the defect existing in the material steel piece is visually confirmed. Marked.

次に、素材鋼片を工作機械にセットし、回転工具として、超硬(90WC−9Co)からなり、寸法が25mmφ×70mmのものを回転軸が斜めになるように装着した。金属粉の供給装置から500℃まで予熱した金属粉(成分規格が高炭素材相当の鉄粉)を、欠陥の露出部が存在するマーキング部に供給した。次いで、回転工具を900rpmで回転させながら下降させ、素材鋼片の欠陥の露出部が存在するマーキング部の端部に対応する位置に回転工具を接触させ、その後、回転工具の後方部分を1mm素材鋼片へ埋没させた。この状態で、回転工具のトルクの変化から素材鋼片の塑性流動が開始されたことを確認した後、回転工具を60mm/minの速度で欠陥の露出部の分布に沿って移動させた。そして、回転工具を欠陥の露出部の終端まで移動させた後、上昇させた。 Next, the material steel piece was set in the machine tool, and as a rotary tool, a cemented carbide (90WC-9Co) having a size of 25 mmφ × 70 mm was attached so that the rotation axis was slanted. Metal powder preheated to 500 ° C. (iron powder whose component standard is equivalent to a high carbon material) was supplied from the metal powder supply device to the marking portion where the exposed portion of the defect exists. Next, the rotary tool is lowered while rotating at 900 rpm, and the rotary tool is brought into contact with the position corresponding to the end of the marking portion where the exposed portion of the defect of the material steel piece is present. It was buried in a piece of steel. In this state, after confirming that the plastic flow of the material steel piece was started from the change in the torque of the rotary tool, the rotary tool was moved at a speed of 60 mm / min along the distribution of the exposed portion of the defect. Then, the rotary tool was moved to the end of the exposed portion of the defect and then raised.

その後、鋼片を取り外して、表面処理した部分を観察した結果、欠陥の露出部は塞がれており、新たな欠陥が露出していないことが確認された。 After that, as a result of removing the steel piece and observing the surface-treated part, it was confirmed that the exposed part of the defect was closed and no new defect was exposed.

1 素材鋼片(素材金属材)
2 酸化スケール
3 欠陥
3a 露出部
4 マーキング部
5 金属粉
6 塑性流動部分
7 ノズル
10 回転工具
11 表面処理後の鋼片
1 Material steel piece (material metal material)
2 Oxidation scale 3 Defects 3a Exposed part 4 Marking part 5 Metal powder 6 Plastic flow part 7 Nozzle 10 Rotating tool 11 Steel piece after surface treatment

Claims (12)

表面に欠陥の露出部を有する金属材に対し、前記金属材表面の欠陥の露出部に、前記金属材よりも硬い材質の回転工具を、回転させながら接触させて、その際に発生する摩擦熱と圧力により前記金属材の前記回転工具との接触部分を塑性流動させ、かつ塑性流動部分に変態点以下の温度に加熱された金属粉が供給された状態とし、前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させて、前記金属粉を巻き込みながら、前記金属材における前記回転工具の移動部分を順次塑性流動させ、前記金属材の欠陥の露出部を塞ぐことを特徴とする金属材の表面処理方法。 A rotating tool made of a material harder than the metal material is brought into contact with the exposed portion of the defect on the surface of the metal material while rotating the metal material having the exposed portion of the defect on the surface, and the frictional heat generated at that time. A state in which the contact portion of the metal material with the rotary tool is plastically flowed by the pressure and pressure, and the metal powder heated to a temperature below the transformation point is supplied to the plastic flow portion, and the rotary tool is rotated. While moving along the distribution of the exposed portion of the defect as it is, while entraining the metal powder, the moving portion of the rotating tool in the metal material is sequentially plastically flowed to close the exposed portion of the defect of the metal material. A characteristic surface treatment method for metal materials. 前記金属粉を、予め前記金属材表面の欠陥の露出部が存在する部分に供給しておくことを特徴とする請求項1に記載の金属材の表面処理方法。 The method for surface treating a metal material according to claim 1, wherein the metal powder is supplied in advance to a portion of the surface of the metal material where an exposed portion of a defect exists. 前記金属粉を、前記金属材の前記回転工具により塑性流動された部分に供給しながら、前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させることを特徴とする請求項1に記載の金属材の表面処理方法。 A claim characterized in that the metal powder is supplied to a portion of the metal material that has been plastically flowed by the rotary tool, and the rotary tool is moved along the distribution of exposed portions of defects while being rotated. Item 2. The method for surface treating a metal material according to Item 1. 前記回転工具は、その直径が欠陥の露出部の短尺側寸法以上であることを特徴とする請求項1から請求項3のいずれか1項に記載の金属材の表面処理方法。 The method for surface-treating a metal material according to any one of claims 1 to 3, wherein the rotary tool has a diameter equal to or larger than the short side dimension of the exposed portion of the defect. 前記回転工具による金属材を塑性流動させる表面処理に先立って、処理前の金属材表面の欠陥の露出部をマーキングし、金属材のマーキングした部分を前記回転工具により塑性流動させることを特徴とする請求項1から請求項4のいずれか1項に記載の金属材の表面処理方法。 Prior to the surface treatment of plastically flowing the metal material by the rotary tool, the exposed portion of the defect on the surface of the metal material before the treatment is marked, and the marked portion of the metal material is plastically flowed by the rotary tool. The method for surface treating a metal material according to any one of claims 1 to 4. 前記金属材は、連続鋳造または分塊圧延、鍛造プロセスを経た、表面に酸化スケールを有する鋼片であり、前記塑性流動させる処理に先立って、前記鋼片の表面の酸化スケールを除去して欠陥を露出させることを特徴とする請求項1から請求項5のいずれか1項に記載の金属材の表面処理方法。 The metal material, continuous casting or blooming, through the forging process, the steel strip der having an oxide scale on the surface is, prior to the process of the plastic flow, to remove the oxide scale on the surface of the steel strip The method for surface-treating a metal material according to any one of claims 1 to 5, wherein defects are exposed. 表面に欠陥の露出部を有する素材金属材を準備する工程と、
前記素材金属材表面の欠陥の露出部に、前記素材金属材よりも硬い材質の回転工具を、回転させながら接触させて、その際に発生する摩擦熱と圧力により前記素材金属材の前記回転工具との接触部分を塑性流動させる工程と、
塑性流動部分に変態点以下の温度に加熱された金属が供給された状態とする工程と、
前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させて、前記金属粉を巻き込みながら、前記素材金属材における前記回転工具の移動部分を順次塑性流動させる工程と
を有し、
素材金属材の塑性流動により、欠陥の露出部を塞ぐことを特徴とする金属材の製造方法。
The process of preparing a metal material with exposed parts on the surface and
A rotating tool made of a material harder than the material metal material is brought into contact with the exposed portion of the defect on the surface of the material metal material while rotating, and the rotating tool of the material metal material is subjected to frictional heat and pressure generated at that time. The process of plastically flowing the contact part with
The process of supplying metal powder heated to a temperature below the transformation point to the plastic flow part, and
The rotary tool is moved along the distribution of the exposed portion of the defect while being rotated, and the moving portion of the rotary tool in the material metal material is sequentially plastically flowed while entraining the metal powder. And
Material A method for manufacturing a metal material, which comprises closing an exposed part of a defect by plastic flow of the metal material.
前記塑性流動部分に変態点以下の温度に加熱された金属が供給された状態とする工程は、前記金属粉を、予め前記金属材表面の欠陥の露出部が存在する部分に供給しておくことにより行われることを特徴とする請求項7に記載の金属材の製造方法。 In the step of supplying the metal powder heated to a temperature below the transformation point to the plastic flow portion, the metal powder is supplied in advance to the portion where the defect exposed portion on the surface of the metal material exists. The method for producing a metal material according to claim 7, wherein the method is performed by the above. 前記塑性流動部分に変態点以下の温度に加熱された金属が供給された状態とする工程は、前記金属粉を、前記素材金属材の前記回転工具により塑性流動された部分に供給しながら、前記回転工具を回転させた状態のまま欠陥の露出部の分布に沿って移動させることにより行われることを特徴とする請求項7に記載の金属材の製造方法。 In the step of supplying the metal powder heated to a temperature below the transformation point to the plastic flow portion, the metal powder is supplied to the portion of the material metal material that has been plastically flowed by the rotary tool. The method for producing a metal material according to claim 7, wherein the rotary tool is moved along the distribution of exposed portions of defects while being rotated. 前記回転工具は、その直径が欠陥の露出部の短尺側寸法以上であることを特徴とする請求項7から請求項9のいずれか1項に記載の金属材の製造方法。 The method for manufacturing a metal material according to any one of claims 7 to 9, wherein the rotary tool has a diameter equal to or larger than the short side dimension of the exposed portion of the defect. 前記回転工具による素材金属材を塑性流動させる表面処理に先立って、素材金属材表面の欠陥の露出部をマーキングし、素材金属材のマーキングした部分を前記回転工具により塑性流動させることを特徴とする請求項7から請求項10のいずれか1項に記載の金属材の製造方法。 Prior to the surface treatment of plastically flowing the material metal material by the rotary tool, the exposed portion of the defect on the surface of the material metal material is marked, and the marked portion of the material metal material is plastically flowed by the rotary tool. The method for producing a metal material according to any one of claims 7 to 10. 前記素材金属材は、連続鋳造または分塊圧延、鍛造プロセスを経た、表面に酸化スケールを有する素材鋼片であり、前記塑性流動させる工程に先立って行われる、前記素材鋼片の表面の酸化スケールを除去して欠陥を露出させる工程をさらに有することを特徴とする請求項7から請求項11のいずれか1項に記載の金属材の製造方法。 The material metal material, continuous casting or blooming, through the forging process, material steel strip der having an oxide scale on the surface is, the performed prior to the step of plastically flow, oxidation of the surface of the material steel strip The method for producing a metal material according to any one of claims 7 to 11, further comprising a step of removing scale to expose defects.
JP2017152961A 2017-08-08 2017-08-08 Surface treatment method for metal materials and manufacturing method for metal materials Active JP6885257B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2017152961A JP6885257B2 (en) 2017-08-08 2017-08-08 Surface treatment method for metal materials and manufacturing method for metal materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2017152961A JP6885257B2 (en) 2017-08-08 2017-08-08 Surface treatment method for metal materials and manufacturing method for metal materials

Publications (2)

Publication Number Publication Date
JP2019030887A JP2019030887A (en) 2019-02-28
JP6885257B2 true JP6885257B2 (en) 2021-06-09

Family

ID=65523939

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2017152961A Active JP6885257B2 (en) 2017-08-08 2017-08-08 Surface treatment method for metal materials and manufacturing method for metal materials

Country Status (1)

Country Link
JP (1) JP6885257B2 (en)

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3753641B2 (en) * 2001-09-25 2006-03-08 株式会社日立製作所 Nondestructive inspection method
JP2003126971A (en) * 2001-10-16 2003-05-08 Ishikawajima Harima Heavy Ind Co Ltd Repair method of friction stir
JP4358807B2 (en) * 2005-09-21 2009-11-04 株式会社神戸製鋼所 Method for preventing cracks in continuous cast pieces of high-strength steel
US8875976B2 (en) * 2005-09-26 2014-11-04 Aeroprobe Corporation System for continuous feeding of filler material for friction stir welding, processing and fabrication
JP2007100129A (en) * 2005-09-30 2007-04-19 Mitsui Eng & Shipbuild Co Ltd Surface coating method and surface coating film
JP2007185683A (en) * 2006-01-12 2007-07-26 Mitsubishi Heavy Ind Ltd Crack repairing method

Also Published As

Publication number Publication date
JP2019030887A (en) 2019-02-28

Similar Documents

Publication Publication Date Title
CN102848150B (en) The processing method of water-cooled continuous casting machine bearing block
Dubey et al. Wear behaviour of friction stir weld joint of cast Al (4–10%) Cu alloy welded at different operating parameters
JP3951889B2 (en) Manufacturing method and equipment for hot-rolled steel
Zhang et al. Investigations of the hybrid laser polishing and high-temperature tribological properties of the 316L stainless steel formed by selective laser melting
CN116021091A (en) Machining method of hard alloy tooth circular saw blade
CN116275379B (en) Bimetal wear-resistant MPS intermediate-speed mill roller sleeve and composite build-up welding manufacturing method thereof
JP6885257B2 (en) Surface treatment method for metal materials and manufacturing method for metal materials
JP5601055B2 (en) Surface care method and apparatus for continuous cast slab
CN118237843A (en) A defect repair process for nickel-based high-temperature alloy castings
Bańkowski et al. The use of abrasive waterjet cutting to remove flash from castings
JP6373303B2 (en) Repair method for continuous casting mold
JP2018171651A (en) Method for treating the surface of metallic material, and method for producing metallic material
CN105349992B (en) It is a kind of to be directed to aircraft vertical pin, the laser melting coating restorative procedure of bolt piece surface
JP2018024087A (en) Tooth type roll manufacturing method, and steel plate processing method
KR20010024988A (en) Cooking vessel and method for producing same
JP2010149201A (en) Method of conditioning surface of hot slab
KR100777673B1 (en) Work roll chocks with improved wear resistance, manufacturing method and rolling apparatus
KR20200064474A (en) Apparatus and method for automatic grinding of billet
Carlone et al. The influence of pre-heating on the weldability of pure copper by FSW
CN102852983B (en) Continuous caster bearing pedestal and processing method thereof
JP2000153435A (en) Maintenance method and equipment for round steel bars
KR100799508B1 (en) Roll chalk with high corrosion resistance and abrasion resistance, manufacturing method and rolling apparatus
JP2005305480A (en) Method and apparatus for repairing casting defects in aluminum alloy castings
de Oliveira et al. Evaluation of Ground Surface Quality of 316L Stainless Steel Produced by Additive Manufacturing
CN102852981A (en) Bearing pedestal

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20190322

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20200219

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200303

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200416

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200908

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20210413

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20210426

R150 Certificate of patent or registration of utility model

Ref document number: 6885257

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250