JP7315985B2 - Soap composition using mountain ginseng and soap containing the same - Google Patents
Soap composition using mountain ginseng and soap containing the same Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
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- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
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- C12N1/20—Bacteria; Culture media therefor
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Description
本発明は、山養参を用いた石鹸組成物、及びそれを含む石鹸に係り、さらに詳しくは、敏感な肌にも安全であり、肌、髪の毛等の人体部位の汚染、体臭等に対する洗浄力に優れ、皮膚角質の除去及び保湿効果に優れた山養参を用いた石鹸組成物、及びそれを含む石鹸に関する。 The present invention relates to a soap composition using mountain ginseng and a soap containing the same, more particularly, it is safe for sensitive skin, and has detergency against contamination of human body parts such as skin and hair, body odor, etc. The present invention relates to a soap composition using mountain ginseng, which is excellent in skin keratin removal and moisturizing effects, and a soap containing the same.
石鹸(soap)は、日常生活において洗面及び洗顔の際に広く使われる生活必需品の一つである。特に、最近は、皮膚の清潔に役立つとともに、保湿やその他の様々な効果が期待できるように、様々な有効成分を含む化粧石鹸が競って開発され、また発売されている。 Soap is one of the daily necessities that are widely used for washing face and face in daily life. In particular, in recent years, cosmetic soaps containing various active ingredients have been actively developed and put on the market to help keep the skin clean, moisturizing and various other effects.
また、油脂特有の匂いをなくし、商品価値を高めるために、様々な色素及び香料が添加されることもある。広義では、飽和及び不飽和高級脂肪酸、トール油脂肪酸・樹脂酸、ナフテン酸等の金属塩の総称であり、狭義では、主に洗浄に使われる高級脂肪酸の水溶性アルカリ金属塩である。 In addition, various dyes and fragrances are sometimes added to remove the peculiar smell of oils and fats and to increase the commercial value. In a broad sense, it is a general term for metal salts of saturated and unsaturated higher fatty acids, tall oil fatty acids/resin acids, naphthenic acids, etc. In a narrow sense, it is a water-soluble alkali metal salt of higher fatty acids that is mainly used for washing.
脂肪酸としては、カプロン酸からベヘン酸までを使用し、アルカリは、一般にナトリウムとカリウムであるが、アンモニア・エタノールアミンやグアニジンのような有機塩基もあり、アルカリ金属塩及びこれらの有機塩基のみが任意の割合で水に溶けるので、洗浄用として用いられる。上記以外の金属塩は、殆ど水中でも溶けにくく、金属石鹸として区別される。 As fatty acids, caproic acid to behenic acid are used, and alkalis are generally sodium and potassium, but there are also organic bases such as ammonia, ethanolamine and guanidine, and only alkali metal salts and these organic bases are optional. It is used for washing because it dissolves in water at a ratio of Metal salts other than the above are hardly soluble in water and are classified as metal soaps.
多く用いられる香は、組み合わせ香であり、天然植物系香を添加した製品も好まれている。特に、ずいぶん前から民間療法として皮膚美容に用いられている自然植物(例えば、人参、キュウリ、杏、アロエ、レモン、ゆず、及びヨモギ等)の抽出物を添加するか、またはこれらの植物の特異臭を組み合わせて表現している製品が開発されている。 The incense that is often used is a combination incense, and products with natural plant-based incense are also popular. In particular, extracts of natural plants (e.g., ginseng, cucumber, apricot, aloe, lemon, yuzu, mugwort, etc.), which have long been used as folk remedies for skin care, are added, or the special properties of these plants are added. A product that expresses a combination of offensive odors has been developed.
一方、高麗人参(Panax ginseng)は、ウコギ科(Araliaceae)に属する植物であって、生育環境により、自然状態で自生した人参である山参と、人工的に育てた人参である栽培人参に大別され、山参は、さらに、その種まきの起源により、天然山参と山養参に分けられるが、山養参は、天然山参の種子を山中に種まきして作るもの、天然山参の幼根を山奥で採取して適当な位置の山林中に再移植して作るもの、栽培人参の種子を山林中に種まきして作るもの等に分類することができ、長脳参とも呼ばれる。 On the other hand, Korean ginseng (Panax ginseng) is a plant belonging to the Araliaceae family. Wild ginseng is further divided into natural wild ginseng and mountain ginseng according to the origin of seed sowing. Ginseng can be classified into those made by collecting radicles deep in the mountains and replanting them in forests at suitable locations, and those made by sowing seeds of cultivated ginseng in forests.
このような山養参は、人参よりも10倍、紅参よりも4~5倍多いサポニンが入っており、免疫力を高めるのに大きな効能があり、これとともに、血液循環、糖尿病の予防、消化力の増進、ストレス緩和、元気増進等の効能がある。 This mountain ginseng contains 10 times more saponin than ginseng and 4-5 times more saponin than red ginseng. It has effects such as improving digestion, relieving stress, and improving energy.
よって、本発明者は、多くの活性化サポニン成分を含む山養参を用いて石鹸を製造することにより、品質及び消費者の嗜好性が向上した石鹸を製造することができることを見出し、本発明を完成した。 Therefore, the present inventor found that soap with improved quality and consumer preference can be produced by producing soap using mountain ginseng containing many activated saponin components. completed.
本発明は、敏感な肌にも安全であり、肌、髪の毛等の人体部位の汚染、体臭等に対する洗浄力に優れ、皮膚角質の除去及び保湿効果に優れた山養参を用いた石鹸組成物、及びそれを含む石鹸を提供することを目的とする。 The present invention is a soap composition using mountain ginseng that is safe for sensitive skin, has excellent detergency against contamination of human body parts such as skin and hair, body odor, etc., and has excellent exfoliation and moisturizing effects. , and a soap containing the same.
本発明が解決しようとする様々な課題は、上述した課題に制限されず、言及されていないまた他の課題は、下記の記載から当業者にとって明確に理解されるであろう。 The various problems to be solved by the present invention are not limited to the above problems, and other problems not mentioned will be clearly understood by those skilled in the art from the following description.
本発明による山養参を用いた石鹸組成物は、山養参発酵抽出液を主要成分として含む。 The soap composition using wild ginseng according to the present invention contains a fermented extract of wild ginseng as a main component.
前記山養参発酵抽出液、シアバター、トコフェロール(ビタミンE)、アカマツ葉油、ホホバ種子油、ソープヌードルパーム油、ヒアルロン酸、グルコン酸亜鉛(Zinc Gluconate)、グルコン酸マグネシウム(Magnesium Gluconate)、及び玉粉を含んでもよい。 The wild ginseng fermented extract, shea butter, tocopherol (vitamin E), red pine leaf oil, jojoba seed oil, soap noodle palm oil, hyaluronic acid, zinc gluconate, magnesium gluconate, and It may contain egg powder.
前記山養参発酵抽出液にドクダミ抽出液またはプーアル茶抽出液がさらに含まれてもよい。 The fermented extract of mountain yang ginseng may further include houttuynia cordata extract or pu-erh tea extract.
前記山養参発酵抽出液20乃至40重量部、シアバター5乃至10重量部、トコフェロール(ビタミンE)3乃至7重量部、アカマツ葉油40乃至80重量部、ホホバ種子油30乃至70重量部、ソープヌードルパーム油500乃至1000重量部、ヒアルロン酸1乃至3重量部、グルコン酸亜鉛2乃至4重量部、グルコン酸マグネシウム1乃至3重量部、及び玉粉5乃至10重量部の重量割合で含まれてもよい。 20 to 40 parts by weight of the wild ginseng fermented extract, 5 to 10 parts by weight of shea butter, 3 to 7 parts by weight of tocopherol (vitamin E), 40 to 80 parts by weight of red pine leaf oil, 30 to 70 parts by weight of jojoba seed oil, Contains 500 to 1000 parts by weight of soap noodle palm oil, 1 to 3 parts by weight of hyaluronic acid, 2 to 4 parts by weight of zinc gluconate, 1 to 3 parts by weight of magnesium gluconate, and 5 to 10 parts by weight of egg powder may
前記山養参発酵抽出液100重量部に対して、ドクダミ抽出液は20乃至30重量部の重量割合で含まれ、前記プーアル茶抽出液は10乃至20重量部の重量割合で含まれてもよい。 The Houttuynia cordata extract may be included in a weight ratio of 20 to 30 parts by weight, and the pu-erh tea extract may be included in a weight ratio of 10 to 20 parts by weight based on 100 parts by weight of the fermented extract of mountain ginseng. .
前記山養参発酵抽出液は、山養参の根及び山養参の葉を分離して準備した後、洗浄し、前記山養参の根を水蒸気で加熱して蒸してから、硫黄で薫蒸するが、前記山養参の根を、130乃至140℃の温度及び1乃至3kgf/cm2の圧力で、30乃至100分間水蒸気で加熱した後、前記水蒸気で加熱された山養参の根を1乃至3分間硫黄で薫蒸し、前記硫黄で薫蒸された山養参の根を乾燥するが、前記乾燥は、硫黄で薫蒸された山養参の根を、25乃至30℃の温度で1乃至3日間行われ、前記乾燥した山養参の根を0.1乃至1.0cmの長さ単位で切断し、前記切断した山養参の根に乳酸菌を混合した後、熟成させるが、前記熟成は、前記乳酸菌と混合した山養参の根を、20乃至25℃の温度で10乃至30時間の間維持して熟成させ、前記乳酸菌としては、乳酸菌(Lactobacillales)、ストレプトコッカスサーモフィルス(Streptococcus thermophiles)、及びビフィドバクテリウムロングム(Bifidobacterium longum)からなる群より選ばれたいずれか一つの乳酸菌が用いられ、前記洗浄された山養参の生葉を水蒸気で加熱するが、前記加熱は、前記山養参の生葉を、110乃至120℃の温度及び1乃至3kgf/cm2の圧力で10乃至30分間水蒸気で加熱することにより行われ、前記水蒸気で加熱された山養参の生葉を乾燥するが、前記山養参の生葉の乾燥は、温度25乃至30℃で5乃至10時間の間行われ、前記乾燥した山養参の生葉を加熱して煎炒するが、前記煎炒は、乾燥した山養参の生葉を加熱容器に投入した後、90乃至95℃の温度で3乃至5分間1次煎炒を行い、前記1次煎炒を経た山養参の生葉を、130乃至140℃の温度で30乃至60秒間2次煎炒を行うステップにより行われ、前記洗浄された山養参の生葉に枯草菌浸出水を噴霧し、前記山養参の生葉を発酵させ、前記熟成された山養参の根と前記発酵された山養参の生葉を混合した後、発酵させて発酵山養参混合物を製造するが、前記熟成された山養参の根100重量部に対して、前記発酵された山養参の生葉を200乃至400重量部の重量割合で混合した後、60乃至65℃の温度及び55乃至60%の湿度で3乃至5日間発酵させて、発酵山養参混合物を製造し、前記発酵山養参混合物に溶媒を混合し、超音波を加えることにより、山養参発酵液を製造するが、前記溶媒は、前記山養参混合液100重量部に対して300乃至500重量部の重量割合で含まれ、前記溶媒としては、水が用いられ、前記混合液に加えられる超音波は、60乃至80KHzの振動周波数で50乃至100分間100乃至200ワット(watt)の出力を用い、前記山養参発酵液から固形分を除去し、前記固形分が除去された山養参発酵液を遠心分離して、山養参の根と生葉の微細粒子が位置する下層液と、前記下層液の上部に位置する重層液及び上層液に、位置的に分けて分離し、前記重層液及び上層液に位置する山養参発酵液を抽出して山養参発酵抽出液を製造するが、前記山養参発酵抽出液は、山養参発酵液2000乃至3000gを、70%(v/v)エタノール水溶液10~15lにより、85乃至90℃で3~4時間の間1次抽出した後、70%(v/v)エタノール水溶液4~6lにより、85乃至90℃で2~3時間の間2次抽出を完了し、真空回転蒸発器で1000乃至1500mlとなるまで抽出液を製造するステップと、前記抽出液にエタノールを加えて2乃至3倍の重量に希釈し、18,000~20,000rpmで30乃至40分間遠心分離して、前記山養参発酵液に含まれる高分子繊維素及び固形分を除去した後、集められた上澄液を15~20倍重量の酢酸で2回抽出するステップと、により製造されてもよい。 The wild ginseng fermented extract is prepared by separating the wild ginseng roots and the wild ginseng leaves, washing them, heating and steaming the wild ginseng roots with steam, and then fumigating them with sulfur. Steaming is performed by heating the mountain yam roots with steam for 30 to 100 minutes at a temperature of 130 to 140° C. and a pressure of 1 to 3 kgf/cm 2 , and then heating the roots of the mountain yam roots heated by the steam. is fumigated with sulfur for 1 to 3 minutes, and the sulfur-fumigated roots of mountain yam are dried. The dried mountain ginseng root is cut in units of 0.1 to 1.0 cm in length, and the cut roots of mountain ginseng are mixed with lactic acid bacteria and aged. The aging is carried out by maintaining the mountain ginseng root mixed with the lactic acid bacteria at a temperature of 20 to 25° C. for 10 to 30 hours, and the lactic acid bacteria include lactic acid bacteria (Lactobacillales), Streptococcus thermophilus ( Streptococcus thermophiles) and Bifidobacterium longum are used, and the washed fresh leaves of mountain ginseng are heated with steam. The fresh leaves of the wild ginseng are heated with steam for 10 to 30 minutes at a temperature of 110 to 120° C. and a pressure of 1 to 3 kgf/cm 2 , and the fresh leaves of the wild ginseng heated by the steam are dried. However, the drying of the fresh mountain ginseng leaves is carried out at a temperature of 25 to 30° C. for 5 to 10 hours, and the dried fresh mountain ginseng leaves are heated and fried. After the dried raw mountain ginseng leaves are put into a heating container, they are first roasted at a temperature of 90 to 95° C. for 3 to 5 minutes. ℃ for 30 to 60 seconds, spraying the washed fresh leaves of wild ginseng with Bacillus subtilis-infused water, fermenting the fresh leaves of wild ginseng, and fermenting the fresh leaves of wild ginseng. The fermented wild ginseng root and the fermented fresh leaves of wild ginseng are mixed and fermented to produce a fermented wild ginseng mixture. The fermented fresh leaves of mountain ginseng are mixed at a weight ratio of 200 to 400 parts by weight, and fermented at a temperature of 60 to 65° C. and a humidity of 55 to 60% for 3 to 5 days to obtain a fermented mountain ginseng mixture. A solvent is mixed with the fermented mountain ginseng mixture and ultrasonic waves are applied to produce a mountain ginseng fermented liquid. Water is used as the solvent, and ultrasonic waves applied to the mixed solution have a vibration frequency of 60 to 80 kHz and a power of 100 to 200 watts for 50 to 100 minutes. Using the output to remove solids from the fermented liquid of mountain ginseng, centrifuging the fermented liquid of mountain ginseng from which the solids have been removed, and obtaining a lower layer liquid in which fine particles of roots and fresh leaves of mountain ginseng are located Then, the fermented mountain ginseng liquid located in the upper layer liquid and the upper layer liquid is separated into an upper layer liquid and an upper layer liquid, and the fermented mountain ginseng extract is extracted from the upper layer liquid and the upper layer liquid. The fermented extract of mountain ginseng is prepared by first heating 2000 to 3000 g of mountain ginseng fermented liquid with 10 to 15 l of 70% (v/v) ethanol aqueous solution at 85 to 90° C. for 3 to 4 hours. After extraction, secondary extraction is completed with 4-6 liters of 70% (v/v) ethanol aqueous solution at 85-90° C. for 2-3 hours, and the extract is evaporated to 1000-1500 ml with a vacuum rotary evaporator. adding ethanol to the extract to dilute it to 2 to 3 times its weight, and centrifuging at 18,000 to 20,000 rpm for 30 to 40 minutes to remove the high and extracting the collected supernatant twice with 15-20 times its weight of acetic acid after removing molecular cellulose and solids.
その他、実施例の具体的な事項は、詳細な説明に含まれている。 Other specific matters of the embodiment are included in the detailed description.
本発明による石鹸は、敏感な肌にも安全であり、肌、髪の毛等の人体部位の汚染、体臭等に対する洗浄力に優れ、皮膚角質の除去及び保湿効果に優れる。 The soap according to the present invention is safe for sensitive skin, has excellent detergency against contamination of human body parts such as skin and hair, body odor, etc., and has excellent exfoliating and moisturizing effects.
本発明の技術的思想の実施例は、具体的に言及されていない様々な効果を提供することができることが十分に理解されるであろう。 It will be appreciated that embodiments of the technical idea of the present invention can provide various effects not specifically mentioned.
本発明の利点及び特徴、またそれらを達成する方法は、詳細に後述される実施例を参照すれば、明らかになるであろう。しかしながら、本発明は、ここで説明される実施例に限定されず、他の形態で具体化され得る。かえって、ここに紹介される実施例は、開示された内容が徹底かつ完全になるように、また当業者に本発明の思想が十分に伝達されるようにするために提供されるものである。 Advantages and features of the present invention, as well as the manner in which they are achieved, will become apparent with reference to the examples detailed below. This invention may, however, be embodied in other forms and is not limited to the embodiments set forth herein. Rather, the embodiments presented are provided so that this disclosure will be thorough and complete, and will fully convey the concepts of the invention to those skilled in the art.
この出願において用いられる用語は、単に特定の実施例を説明するために用いられたものであって、本発明を限定しようとする意図ではない。単数の表現は、文脈上明らかに異なる意味を有する場合を除き、複数の表現を含む。 The terminology used in this application is merely used to describe particular embodiments and is not intended to be limiting of the invention. Singular terms include plural terms unless the context clearly dictates otherwise.
異なる定義が無い限り、技術用語及び科学用語を含めて、ここに用いられる全ての用語は、本発明が属する技術分野における通常の知識を有する者によって一般に理解されるものと同じ意味を有する。一般に用いられる辞典に正義されている用語は、関連技術の文脈上有する意味と一致する意味を有するものと解釈されなければならず、本出願で明らかに定義しない限り、理想的または過度に形式的な意味と解釈されてはならない。 Unless defined otherwise, all terms, including technical and scientific terms, used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. Terms defined in commonly used dictionaries should be construed to have a meaning consistent with the meaning they have in the context of the relevant art, and unless expressly defined in this application, are ideal or overly formal terms. should not be construed as meaning
以下、本発明による山養参を用いた石鹸組成物について好適な実施例を挙げて詳しく説明する。 Hereinafter, the soap composition using wild ginseng according to the present invention will be described in detail with preferred examples.
本発明による山養参を用いた石鹸組成物は、山養参発酵抽出液、シアバター、トコフェロール(ビタミンE)、アカマツ葉油、ホホバ種子油、ソープヌードルパーム油、ヒアルロン酸、グルコン酸亜鉛、グルコン酸マグネシウム、及び玉粉を含む。 The soap composition using wild ginseng according to the present invention comprises a fermented extract of wild ginseng, shea butter, tocopherol (vitamin E), red pine leaf oil, jojoba seed oil, soap noodle palm oil, hyaluronic acid, zinc gluconate, Contains magnesium gluconate and egg flour.
また、本発明による山養参を用いた石鹸組成物は、山養参発酵抽出液20乃至40重量部、シアバター5乃至10重量部、トコフェロール(ビタミンE)3乃至7重量部、アカマツ葉油40乃至80重量部、ホホバ種子油30乃至70重量部、ソープヌードルパーム油500乃至1000重量部、ヒアルロン酸1乃至3重量部、グルコン酸亜鉛2乃至4重量部、グルコン酸マグネシウム1乃至3重量部、及び玉粉5乃至10重量部の重量割合で含まれてもよい。 The soap composition using mountain ginseng according to the present invention comprises 20 to 40 parts by weight of fermented extract of mountain ginseng, 5 to 10 parts by weight of shea butter, 3 to 7 parts by weight of tocopherol (vitamin E), and red pine leaf oil. 40 to 80 parts by weight, 30 to 70 parts by weight of jojoba seed oil, 500 to 1000 parts by weight of soap noodle palm oil, 1 to 3 parts by weight of hyaluronic acid, 2 to 4 parts by weight of zinc gluconate, 1 to 3 parts by weight of magnesium gluconate , and 5 to 10 parts by weight of egg flour.
また、本発明による山養参を用いた石鹸組成物は、ドクダミ抽出液またはプーアル茶抽出液をさらに含んでもよいが、前記ドクダミ抽出液は、前記山養参発酵抽出液100重量部に対して、20乃至30重量部の重量割合で含まれ、前記プーアル茶抽出液は、前記山養参発酵抽出液100重量部に対して、10乃至20重量部の重量割合で含まれてもよい。 In addition, the soap composition using mountain ginseng according to the present invention may further include houttuynia cordata extract or pu-erh tea extract. , 20 to 30 parts by weight, and the pu-erh tea extract may be included in a weight ratio of 10 to 20 parts by weight based on 100 parts by weight of the fermented ginseng extract.
前記山養参発酵抽出物は、山養参の根及び山養参の葉を用いて製造されてもよいが、前記山養参には、人参よりも10倍、紅参よりも4~5倍多いサポニンが入っており、免疫力を高めるのに大きな効能があり、これとともに、血液循環、糖尿病の予防、消化力の増進、ストレス緩和、元気増進等の効能がある。 The fermented extract of mountain ginseng may be prepared by using roots and leaves of mountain ginseng, and mountain ginseng contains 10 times more than ginseng and 4-5 times more than red ginseng. It contains twice as much saponin and is highly effective in enhancing immunity, along with blood circulation, diabetes prevention, digestion enhancement, stress relief, and vitality enhancement.
前記山養参発酵抽出液は、下記の製造方法で製造された山養参発酵抽出液が用いられてもよい。 As the fermented extract of mountain ginseng, a fermented extract of mountain ginseng manufactured by the following method may be used.
まず、山養参の根及び山養参の葉を分離して準備した後、洗浄してもよい。 First, the roots and leaves of the mountain yam may be separated and prepared, and then washed.
次に、前記山養参の根を水蒸気で加熱して蒸した後、硫黄で薫蒸してもよい。 Next, the root of the mountain yam may be steamed by heating with steam, and then fumigated with sulfur.
前記ステップでは、前記山養参の根を、130乃至140℃の温度及び1乃至3kgf/cm2の圧力で、30乃至100分間水蒸気で加熱した後、前記水蒸気で加熱された山養参の根を1乃至3分間硫黄で薫蒸してもよい。 In the step, the mountain yam root is heated with steam for 30 to 100 minutes at a temperature of 130 to 140° C. and a pressure of 1 to 3 kgf/cm 2 , and then the steam-heated mountain ginseng root may be fumigated with sulfur for 1-3 minutes.
前記ステップにおいて、前記硫黄を使用すれば、前記山養参に含まれたタンニン物質等のポリフェノールが乾燥中に酸化して黒変することを防止し、追って工程において微生物が繁殖することを防止することができる。 In the above step, if the sulfur is used, the polyphenols such as tannins contained in the mountain ginseng can be prevented from being oxidized and turned black during drying, and later, the propagation of microorganisms in the process can be prevented. be able to.
次に、前記硫黄で薫蒸された山養参の根を乾燥してもよい。 Then, the sulfur-fumigated mountain yang root may be dried.
前記ステップでは、硫黄で薫蒸された山養参の根を25乃至30℃の温度で1乃至3日間乾燥してもよい。 In the above step, the sulfur-fumigated mountain ginseng roots may be dried at a temperature of 25-30° C. for 1-3 days.
続いて、前記乾燥した山養参の根を一定の長さ単位で切断するが、例えば、前記乾燥した山養参の根を0.1乃至1.0cmの長さ単位で切断してもよい。 Subsequently, the dried roots of the wild ginseng are cut into a certain length unit. .
次に、前記切断した山養参の根に乳酸菌を混合した後、熟成させてもよい。 Next, the cut roots of wild ginseng may be mixed with lactic acid bacteria and then aged.
前記ステップにおいて、前記熟成は、前記乳酸菌と混合された山養参の根を、20乃至25℃の温度で10乃至30時間の間維持して熟成させてもよい。 In the step, the aging may be carried out by maintaining the mountain ginseng root mixed with the lactic acid bacteria at a temperature of 20 to 25° C. for 10 to 30 hours.
例えば、前記乳酸菌としては、乳酸菌(Lactobacillales)、ストレプトコッカスサーモフィルス(Streptococcus thermophiles)、及びビフィドバクテリウムロングム(Bifidobacterium longum)からなる群より選ばれたいずれか一つの公知された乳酸菌が用いられてもよい。 For example, as the lactic acid bacterium, any one known lactic acid bacterium selected from the group consisting of Lactobacillus, Streptococcus thermophiles, and Bifidobacterium longum may be used. good.
次に、前記洗浄された山養参の生葉を水蒸気で加熱してもよい。 Next, the washed fresh leaves of wild ginseng may be heated with steam.
前記ステップでは、前記山養参の生葉を110乃至120℃の温度及び1乃至3kgf/cm2の圧力で、10乃至30分間水蒸気で加熱することにより行われてもよい。 The step may be carried out by heating the fresh leaves of the wild ginseng with steam at a temperature of 110 to 120° C. and a pressure of 1 to 3 kgf/cm 2 for 10 to 30 minutes.
続いて、前記水蒸気で加熱された山養参の生葉を乾燥してもよい。 Subsequently, the steam-heated fresh leaves of wild ginseng may be dried.
前記ステップでは、日光乾燥時、前記山養参の生葉の葉緑素が破壊され、有用成分が揮発されることを防止するために、前記山養参の生葉を温度25乃至30℃で5乃至10時間の間乾燥してもよい。 In the above step, in order to prevent chlorophyll from being destroyed and useful components from being volatilized during sun-drying, the fresh leaves of the wild ginseng are dried at a temperature of 25 to 30° C. for 5 to 10 hours. Allow to dry for a while.
次に、前記乾燥した山養参の生葉を加熱して煎炒してもよい。 Next, the dried fresh leaves of wild ginseng may be heated and roasted.
前記ステップは、前記乾燥した山養参の生葉を加熱容器(例えば、釜)に投入した後、90乃至95℃の温度で3乃至5分間1次煎炒を行い、前記1次煎炒された山養参の生葉を、130乃至140℃の温度で30乃至60秒間2次煎炒を行うステップにより行われてもよい。 In the above step, after the dried fresh leaves of mountain ginseng are put into a heating container (eg, a pot), they are first roasted at a temperature of 90 to 95° C. for 3 to 5 minutes, and the first roasted leaves are dried. It may be performed by secondarily roasting the fresh leaves of mountain yang ginseng at a temperature of 130-140° C. for 30-60 seconds.
次に、前記洗浄された山養参の生葉に枯草菌浸出水を噴霧して、前記山養参の生葉を発酵させてもよい。 Next, the washed fresh leaves of wild ginseng may be sprayed with Bacillus subtilis-infused water to ferment the fresh leaves of wild ginseng.
前記枯草菌浸出水は、前記乾燥した山養参の生葉の発酵を促進させるものであって、前記乾燥した山養参の生葉100重量部に対して枯草菌培養液を30乃至50重量部の重量割合で噴霧し、55乃至60℃の温度及び60乃至65%の湿度が維持されるようにした後、2乃至4日間発酵させてもよい。 The Bacillus subtilis leaching water promotes the fermentation of the dried fresh leaves of the wild ginseng. After spraying at a weight rate and maintaining a temperature of 55-60° C. and a humidity of 60-65%, it may be fermented for 2-4 days.
前記枯草菌培養液は、枯草菌と水を混合して生成されるものであって、前記枯草菌は、声飯に黒糖を10乃至12重量%混合し、用意された培地上にエコ栽培籾殻を置き、布切れを覆った後、25℃の温度で1日2回の生育に水分を噴霧しながら、1週間培養させて枯草菌を生成させ、これを、米ぬかと黒糖が50:50の重量比で混合された培地にさらに接種し、25℃で1週間培養して、本発明に用いられる枯草菌浸出水として用いてもよい。 The Bacillus subtilis culture solution is produced by mixing Bacillus subtilis and water. After covering the piece of cloth, it is cultured for a week at a temperature of 25°C while spraying water twice a day to grow Bacillus subtilis. The medium mixed at a weight ratio may be further inoculated, cultured at 25° C. for one week, and used as the Bacillus subtilis leaching solution used in the present invention.
本発明において、前記枯草菌は、バチルスサブチルス(Bacillus subtilis)、バチルスサブチルススピジゼピアイ(Bacillus subtilis)、バチルスメガテリウム(Bacillusmegaterium)、バチルスリケニフォルミス(Bacillus licheniformis)、及びバチルスプミルス(Bacillus pumilus)からなる群より選ばれたいずれか一つ以上が用いられてもよい。 In the present invention, the Bacillus subtilis includes Bacillus subtilis, Bacillus subtilis, Bacillus megaterium, Bacillus licheniformis, and Bacillus spmilus ( Bacillus pumilus) may be used.
次に、前記熟成された山養参の根と、前記発酵された山養参の生葉を混合した後、発酵させて、発酵山養参混合物を製造してもよい。 Next, the aged mountain ginseng root and the fermented mountain ginseng fresh leaves may be mixed and fermented to prepare a fermented mountain ginseng mixture.
前記ステップでは、前記熟成された山養参の根100重量部に対して前記発酵された山養参の生葉を200乃至400重量部の重量割合で混合した後、60乃至65℃の温度及び55乃至60%の湿度で3乃至5日間発酵させて、発酵山養参混合物を製造してもよい。 In the step, 200 to 400 parts by weight of the fermented fresh leaves of the ginseng were mixed with 100 parts by weight of the matured root of the mountain ginseng, and then the mixture was heated to 60 to 65° C. and 55% by weight. A fermented mountain ginseng mixture may be produced by fermenting at a humidity of ∼60% for 3 to 5 days.
次に、前記発酵山養参混合物に溶媒を混合し、超音波を加えることにより、山養参発酵液を製造してもよい。 Next, the fermented mountain ginseng mixture may be mixed with a solvent and subjected to ultrasonic waves to produce a fermented liquid of mountain ginseng.
前記山養参発酵液を製造するために、前記発酵山養参混合物を溶媒と混合して混合液を製造した後、超音波抽出器に投入し、前記混合液に超音波を加えることにより、山養参発酵液を製造するが、前記溶媒は、前記山養参混合液100重量部に対して300乃至500重量部の重量割合で含まれ、前記溶媒としては水が用いられてもよい。 In order to prepare the fermented liquid of wild ginseng, the fermented wild ginseng mixture is mixed with a solvent to prepare a liquid mixture, which is then put into an ultrasonic extractor to apply ultrasonic waves to the liquid mixture. The fermented liquid of wild ginseng is prepared, and the solvent is included in a weight ratio of 300 to 500 parts by weight with respect to 100 parts by weight of the mixed liquid of wild ginseng, and water may be used as the solvent.
また、前記山養参発酵液を製造するために、前記混合液に加えられる超音波は、60乃至80KHzの振動周波数で、50乃至100分間、100乃至200ワットの出力を用いて抽出してもよい。 In addition, in order to produce the fermented liquid of mountain ginseng, the ultrasonic waves applied to the mixed liquid may be extracted with a vibration frequency of 60 to 80 KHz and an output of 100 to 200 watts for 50 to 100 minutes. good.
続いて、前記山養参発酵液から、山養参の根、山養参の生葉のような固形分を除去してもよい。 Subsequently, solids such as roots of wild ginseng and fresh leaves of wild ginseng may be removed from the fermented liquid of wild ginseng.
前記ステップにおいて、山養参の根、山養参の生葉のような固形分の分離は、篩(sieve)等のような公知のフィルタネットを用いてもよい。 In the above step, the separation of solids such as roots of wild ginseng and fresh leaves of wild ginseng may be performed using a known filter net such as a sieve.
次に、前記固形分が除去された山養参発酵液を遠心分離してもよい。 Next, the mountain ginseng fermented liquid from which the solid content has been removed may be centrifuged.
前記ステップでは、固形分が除去された山養参発酵液を遠心分離することにより、山養参の根と生葉の微細粒子が位置する下層液、前記下層液の上部に位置する重層液及び上層液に、位置的に区分して分離してもよい。 In the above step, by centrifuging the fermented liquid of mountain ginseng from which the solid content has been removed, a lower layer liquid in which fine particles of roots and fresh leaves of mountain ginseng are located, a layer liquid located above the lower layer liquid, and an upper layer The liquid may be separated by positional division.
次に、前記重層液及び上層液に位置する山養参発酵液を抽出して、山養参の有用性分で、山養参発酵抽出液を製造してもよい。 Next, the mountain ginseng fermented liquid located in the overlying liquid and the upper layer liquid may be extracted to produce a mountain ginseng fermented extract based on the usefulness of the mountain ginseng.
前記ステップにおいて、前記山養参発酵抽出液は、山養参発酵液2000乃至3000gを、70%(v/v)エタノール水溶液10~15lにより、85乃至90℃で3~4時間の間1次抽出した後、70%(v/v)エタノール水溶液4~6lにより、85乃至90℃で2~3時間の間2次抽出を完了し、真空回転蒸発器により、1000乃至1500mlとなるまで抽出液を製造するステップと、前記抽出液にエタノールを加えて2乃至3倍の重量に希釈し、18,000~20,000rpmで30乃至40分間遠心分離して、前記山養参発酵液に含まれる高分子繊維素及び固形分を完全に除去した後、集められた上澄液を15~20倍重量の酢酸で2回抽出するステップと、により製造されてもよい。 In the above step, the fermented extract of mountain ginseng is prepared by first heating 2000 to 3000 g of fermented mountain ginseng with 10 to 15 liters of 70% (v/v) ethanol aqueous solution at 85 to 90° C. for 3 to 4 hours. After extraction, secondary extraction is completed with 4-6 liters of 70% (v/v) ethanol aqueous solution at 85-90° C. for 2-3 hours, and the extract liquid is reduced to 1000-1500 ml with a vacuum rotary evaporator. adding ethanol to the extract to dilute it to 2 to 3 times its weight, and centrifuge it at 18,000 to 20,000 rpm for 30 to 40 minutes to obtain the extract contained in the mountain ginseng fermented liquid and extracting the collected supernatant twice with 15 to 20 times the weight of acetic acid after completely removing the macromolecular fibrin and solids.
前記シアバター(Siea butter)は、アフリカの民間治療剤として長期間使われてきたシアーバターノキ(shea tree)の種子の胚から得られる植物性油脂であって、ザラザラして乾燥した肌に水分を供給して、しっとりする肌を作り、傷を再生する効能が極めて高いと知られ、化粧品の保湿制や軟化制として広く用いられている。フランス語でカリテ(karite)と呼ばれるシアーバターノキは、アフリカのマリ、カメルーン、コンゴ、ガーナ、ギニア、セネガル、スーダン、ナイジェリア、ブルキナファソ、ウガンダ、コートジボワール等の地で育つが、最近は、ウィテラリアパラドクサ(Vitellaria paradoxa)とも言われる。特に、シアーバターノキの種子の実は、その外観がバターに似ており、シアバターと呼ばれている。シアバターは、黄緑色の油脂であり、香りと味が良く、西アフリカでは、食用でも用いられるが、ココアと混ぜて使うか、チョコレートを作るとき、ココアバターの代用として使う。シアバターは、肌の保湿及び再生効果以外も、抗酸化及び抗炎症効果もあると知られている。また、シアバターには、紫外線遮断効果もあるが、紫外線遮断効果は、約SPF(sun protection factor)6である。また、毛細血管を刺激して、髪と頭皮を潤沢にし、栄養供給と再生力を増加させるので、ヘアコンディショナーとしても用いられる。 The Siea butter is a vegetable oil obtained from the seeds of the shea tree, which has been used as a folk remedy in Africa for a long time. It is known to be extremely effective in making moist skin and regenerating wounds by supplying it, and is widely used as a moisturizing agent and a softening agent in cosmetics. Shea butternut tree, called karite in French, grows in Africa such as Mali, Cameroon, Congo, Ghana, Guinea, Senegal, Sudan, Nigeria, Burkina Faso, Uganda, Ivory Coast. (Vitellaria paradoxa). In particular, the seeds of the shea butternut tree resemble butter in appearance and are called shea butter. Shea butter is a yellow-green oil with a good aroma and taste. In West Africa, it is also used as food. It is mixed with cocoa or used as a substitute for cocoa butter when making chocolate. Besides moisturizing and regenerating skin, shea butter is also known to have antioxidant and anti-inflammatory effects. In addition, shea butter also has an ultraviolet shielding effect, but the ultraviolet shielding effect is about SPF (sun protection factor) 6. It is also used as a hair conditioner as it stimulates capillaries to lubricate the hair and scalp, increasing nourishment and regeneration.
前記トコフェロール(ビタミンE)は、自然保湿機能を有するので、乾燥肌をしっとりかつつやつや肌にし、皮膚の細胞膜を外部の侵入から保護する。すなわち、肌が紫外線、汚染物質、老化により損傷することを防ぎ、肌の奥まで保湿を行うので、肌の呼吸と新陳代謝に役立ち、しわ予防効果が良い。また、強力な抗酸化作用により、天然石鹸や化粧品に使えば、酸敗を防止し、保存期間を増やし、細胞と細胞膜を酸化要因から保護する。 The tocopherol (vitamin E) has a natural moisturizing function, so it makes dry skin moist and glossy and protects the skin cell membrane from external invasion. In other words, it prevents the skin from being damaged by ultraviolet rays, pollutants, and aging, and moisturizes the skin deep inside, which helps the skin breathe and regenerate, and has a good anti-wrinkle effect. Due to its powerful antioxidant properties, it also prevents rancidity, increases shelf life, and protects cells and cell membranes from oxidative agents when used in natural soaps and cosmetics.
前記アカマツ葉油は、松葉蒸溜濃縮液であって、ベータカロチン、ルチン、必須アミノ酸等を多量含んでいる。前記アカマツ葉油は、抗糖尿病、血液循環促進、血清コレステロール低下、血圧降下作用、抗酸化作用、抗炎症作用、免疫機能等の作用を示す。 The red pine leaf oil is a concentrate distilled from pine needles and contains large amounts of beta-carotene, rutin, essential amino acids, and the like. The red pine leaf oil exhibits antidiabetic, blood circulation promoting, serum cholesterol lowering, blood pressure lowering, antioxidant, anti-inflammatory, and immune functions.
前記ホホバ種子油は、砂漠地帯で育つホホバという植物の種子を圧搾して抽出したオイルであって、液体のワックス状で抽出されるオイルである。前記ホホバ種子油は、肌に吸収されやすく、毛穴に詰まらず、肌の奥まで水分を伝達して、肌バランスを取るのに効果的である。前記ホホバ種子油は、乾燥肌や老化肌によく、肌に水分膜を形成して水分が奪われないようにする優れた保湿効果を示す。 The jojoba seed oil is extracted by squeezing the seeds of the jojoba plant, which grows in desert areas, and is extracted in the form of a liquid wax. The jojoba seed oil is easily absorbed into the skin, does not clog pores, and is effective in delivering moisture deep into the skin to maintain skin balance. The jojoba seed oil is good for dry skin and aged skin, and exhibits excellent moisturizing effect by forming a moisture film on the skin to prevent dehydration.
前記ソープヌードルパーム油(parm oil)は、脂肪酸油脂であって、石鹸が固まるようにし、稠密な泡を生成させ、オレイン酸が含まれており、保湿にも役立つ。すなわち、前記ソープヌードルパーム油は、石鹸の硬度を上昇させ、稠密かつ安定的に泡を生じる。 The soap noodle palm oil is a fatty acid oil that makes the soap harden, produces a dense foam, contains oleic acid, and is also useful for moisturizing. That is, the soap noodle palm oil increases the hardness of soap and produces dense and stable lather.
前記ヒアルロン酸は、主に、動物の関節液や眼球の硝子体ゲル、臍帯、真皮表層等の結合組織、ラウス肉腫等のある種の腫瘍から見い出されるもの以外に、A型、C型の溶血性連鎖球菌(Streptococcus)を始めとして、いくつかの細菌では、莢膜の成分となっている。動物組織、例えば、牛の鼻軟骨では、大型コンドロイチン硫酸プロテオグリカン(aggrecan)や結合タンパク質と合わせられて、巨大な分子集合体を形成する。糖鎖の長さは、分子量が105~106として極めて長いものが多いが、材料に応じて異なり、また同一の材料であっても決して均一でない。多量の水と結合してゲルを作る性質があり、これが、関節の潤滑作用、肌の柔軟性等、生体内での機能と結び付いている。 The hyaluronic acid is mainly found in synovial fluid of animals, vitreous gel of the eyeball, umbilical cord, connective tissue such as dermis surface layer, and certain tumors such as Rous sarcoma. In some bacteria, including Streptococcus, it is a component of the capsule. In animal tissue, eg bovine nasal cartilage, it is combined with large chondroitin sulfate proteoglycans (aggrecans) and binding proteins to form large molecular assemblies. The length of the sugar chain is very long with a molecular weight of 10 5 to 10 6 in many cases, but it varies depending on the material, and even if the material is the same, it is never uniform. It has the property of forming a gel by combining with a large amount of water, and this is associated with in vivo functions such as joint lubricating action and skin flexibility.
また、結合組織に損傷が生じると、急速な回復のために、ヒアルロン酸の合成が一時的に活発になることがあり、組織の再構築において細胞活動の一環を形成していると思われる。細胞表面のヒアルロン酸結合タンパク質として、CD44が見い出された。精巣、皮膚、肝等の動物組織や、毒ヘビ、蛭、細菌、放線菌から、それぞれヒアルロン酸のグルコサミニドまたはグルクロニド結合を加水分解または脱離切断する酵素が見い出されている。また、結合組織に損傷が生じると、急速な回復のために、ヒアルロン酸の合成が一時的に活発になることがあり、組織の再構築において細胞活動の一環を形成していると思われる。 In addition, when connective tissue is damaged, hyaluronan synthesis may be temporarily activated for rapid recovery, and it is thought to form a part of cellular activities in tissue remodeling. CD44 was found as a cell surface hyaluronic acid binding protein. Enzymes that hydrolyze or cleave glucosaminide or glucuronide bonds of hyaluronic acid have been found in animal tissues such as testis, skin and liver, as well as poisonous snakes, leeches, bacteria and actinomycetes, respectively. In addition, when connective tissue is damaged, hyaluronan synthesis may be temporarily activated for rapid recovery, and it is thought to form a part of cellular activities in tissue remodeling.
前記グルコン酸亜鉛は、皮膚コンディショニング剤として用いられ、抗ウイルス性により、炎症性ニキビ等に効果的である。また、前記グルコン酸亜鉛は、刺激された頭皮を鎮静させ、肌の痒み等を解消するのに効果的である。 The zinc gluconate is used as a skin conditioning agent and is effective for inflammatory acne and the like due to its antiviral properties. In addition, the zinc gluconate is effective in soothing the irritated scalp and relieving itching of the skin.
前記グルコン酸マグネシウムは、グルコン酸(luconic Acid)のマグネシウム塩成分であって、化学式はC12H22MgO14またはC12H22MgO14・2H2Oであり、分子量は414.61であり、健康かつ良好な肌を作るのに役立つ。 The magnesium gluconate is a magnesium salt component of luconic acid, has a chemical formula of C12H22MgO14 or C12H22MgO14.2H2O , and has a molecular weight of 414.61; Helps create healthy and good looking skin.
前記玉粉は、肌のキメを柔らかくきれいに仕上げ、肌に栄養成分を効果的で伝達して、保湿効果を向上させる機能をする。玉は、硬玉と軟玉に大別され、硬玉は、輝石族に属する鉛輝石鉱物であり、ケイ酸、酸化アルミニウム、ソーダからなる単斜晶系物質である。硬度は、水晶のように緻密な塊であり、色は、黒色、青緑、緑色、透明または半透明であるものであり、普通、玉と言えば、この硬玉を称する。軟玉は、イノけい酸塩(Inosilicate)の単斜晶系パイリボール鉱物体であり、ドロマイト質大理石のうち、軟玉と蛇紋岩化超塩基性軟玉に分けられ、これらの品質は、その微細な構造、すなわち透角閃石-陽起石晶子が束組と繊維からなる粗細の程度で決まり、繊維が極めて細いほど品質が優れていることで知られている。 The egg powder makes the skin texture soft and clean, effectively delivers nutrients to the skin, and improves the moisturizing effect. Jade is roughly classified into jadeite and nephrite. Jadeite is a lead pyroxene mineral belonging to the pyroxene group, and is a monoclinic substance composed of silicic acid, aluminum oxide, and soda. The hardness is a dense mass like crystal, and the color is black, bluish green, green, transparent or translucent. Nephrite is a monoclinic pyribor mineral body of Inosilicate, and among dolomitic marbles, it is divided into nephrite and serpentinized ultrabasic nephrite, these qualities are determined by its fine structure, That is, it is known that the degree of coarseness and fineness of the tremophyllite-hyokiseki crystallite consisting of bundles and fibers determines the quality, and the finer the fibers, the better the quality.
前記ドクダミ抽出液は、ドクダミを抽出して製造されたものであって、ドクダミ(Houttuynia cordata thunb)は、ドクダミ科(Saururaceae)の植物であるギョセイソウの全草であって、東南アジアと、特に、日本、韓国等の地に棲息する。前記ドクダミは、十の薬効があるとのことから十薬とも呼ばれ、幹は、サツマイモの葉と同じであり、生葉に触れると、生臭い匂いがすることから由来して、魚腥草とも呼ばれている。ドクダミは、薬用及び食用が可能であり、大韓民国食品公典における食品原材料分類には、副原料として最小量のみを使用可能な動植物に分類されており、薬理的には、強心、利尿、抗菌、解毒、抗癌の効能があると広く知られており、民間では、解毒と美容を助ける化粧品及び健康機能食品として用いられている。 The Houttuynia cordata extract is produced by extracting Houttuynia cordata thunb. , South Korea, etc. Said dokudami is also called ten medicines because it has ten medicinal effects, and the stem is the same as the leaves of sweet potato, and when the fresh leaves are touched, it smells fishy, so it is also called fish. is Houttuynia cordata can be used for medicinal and edible purposes. According to the classification of food raw materials in the Korean Food Codex, Houttuynia cordata is classified as an animal and plant that can be used in the minimum amount as an auxiliary ingredient. It is widely known to have anti-cancer effects, and is used in the private sector as a cosmetic and health functional food that aids detoxification and beauty.
前記ドクダミ抽出液は、下記の製造方法で製造されたドクダミ抽出液が用いられてもよい。 As the Houttuynia cordata extract, the Houttuynia cordata extract manufactured by the following manufacturing method may be used.
まず、ドクダミ抽出液を製造するために、ドクダミを準備した後、洗浄してもよい。 First, in order to prepare Houttuynia cordata extract, Houttuynia cordata may be prepared and then washed.
次に、前記洗浄されたドクダミを一定の粒度で粉砕してもよい。 Next, the washed Houttuynia cordata may be pulverized to a certain particle size.
前記ステップでは、前記ドクダミを一定の粒度で粉砕することにより、前記ドクダミの有効性分が十分に抽出されるが、前記ステップにおいて、ドクダミの粉砕は、粒径が500乃至2500μmの範囲となるように粉砕してもよい。前記ステップにおいて、前記ドクダミの粒径が500μm未満で粉砕される場合は、粉砕時間が長くかかり、また粒子が小さすぎ、後工程において粒子間の凝集現象が生じることがあり、2500μmを超えて粉砕される場合は、前記ドクダミから有用成分を効果的に抽出し難いという問題が発生する。 In the step, the Houttuynia cordata is pulverized to a certain particle size so that the effective components of the Houttuynia cordata are sufficiently extracted. It can be ground to In the above step, when the Houttuynia cordata is pulverized with a particle size of less than 500 μm, the pulverization time is long, and the particles are too small. In this case, there is a problem that it is difficult to effectively extract useful ingredients from the Houttuynia cordata.
次に、前記粉砕されたドクダミを低温減圧の雰囲気で、超音波を加えて抽出することにより、ドクダミ抽出混合液を製造してもよい。 Next, the pulverized Houttuynia cordata may be extracted in a low-temperature, reduced-pressure atmosphere by applying ultrasonic waves to prepare a Houttuynia cordata extract mixture.
前記ステップでは、前記粉砕されたドクダミを溶媒と混合して混合液を製造した後、超音波抽出器に投入し、前記混合液に超音波を加えることにより、ドクダミ抽出混合液を製造することができるが、前記溶媒は、前記粉砕されたドクダミ100重量部に対して1000乃至2000重量部の重量割合で混合され、前記溶媒としては、水または炭素数1乃至4(C1乃至C4)のアルコールのうちから選ばれたいずれか一つ以上の溶媒が用いられてもよい。 In the step, the pulverized Houttuynia cordata may be mixed with a solvent to prepare a mixed solution, and then the mixed solution may be introduced into an ultrasonic extractor and ultrasonic waves may be applied to the mixed solution to prepare a Houttuynia cordata extract mixed solution. However, the solvent is mixed in a weight ratio of 1000 to 2000 parts by weight with respect to 100 parts by weight of the pulverized Houttuynia cordata, and the solvent is water or an alcohol having 1 to 4 carbon atoms (C1 to C4). Any one or more solvents selected from them may be used.
また、前記ステップは、20乃至25℃の温度及び0.1乃至0.5kgf/cm2の圧力下で、前記混合液に加えられる超音波は、30乃至50KHzの振動周波数で、30乃至60分間100乃至200ワットの出力を用いて抽出してもよい。 Further, the step includes applying ultrasonic waves to the mixed solution at a temperature of 20 to 25° C. and a pressure of 0.1 to 0.5 kgf/cm 2 for 30 to 60 minutes at a vibration frequency of 30 to 50 KHz. It may be extracted using a power of 100-200 Watts.
続いて、前記ドクダミ抽出混合液から、粉砕されたドクダミのような固形物を除去した後、10乃至20℃の温度で1乃至3時間の間熟成させることにより、ドクダミ抽出液を製造してもよい。 Subsequently, solids such as pulverized Houttuynia cordata are removed from the Houttuynia cordata extract mixture, and the mixture is aged at a temperature of 10 to 20° C. for 1 to 3 hours to prepare a Houttuynia cordata extract. good.
前記ステップにおいて、前記ドクダミ抽出混合液から、粉砕されたドクダミのような固形物の除去は、篩のような公知のフィルタネットを用いて、固形物を分離して除去することにより行われてもよい。 In the above step, the removal of solids such as pulverized Houttuynia cordata from the Houttuynia cordata extract mixture may be performed by separating and removing the solids using a known filter net such as a sieve. good.
前記プーアル茶抽出液は、プーアル茶を用いて製造されるが、前記プーアル茶は、中国雲南省の大葉種茶ノ木(Camellia sinensis LINNE)で加工した晒青毛茶を緊圧または散茶の状態で自然発酵する黒茶系の後発酵茶である。 The pu-erh tea extract is produced using pu-erh tea, and the pu-erh tea is naturally extracted from bleached green tea processed by Camellia sinensis LINNE in Yunnan Province, China, under pressure or in a loose state. It is a post-fermented black tea that is fermented.
中国文献である本草綱目拾遺では、プーアル茶は、香が独特であり、二日酔い解消と消化を助け、痰を切り、胃をきれいにし、喉の渇きの解消、人体に有害な脂身を除去する作用があると記録されている。また、プーアル茶は、長期服用しても副作用がないので、日本、フランス、ドイツ、イタリア、マカオ等では、美容茶、ダイエット茶、長寿茶等と呼ばれられている(Son et al,Food & Nutr 18:219-224、2005)。 According to the Chinese literature, Bencao Gangmoku, pu-erh tea has a unique aroma, relieves hangovers, aids digestion, clears phlegm, clears the stomach, quenches thirst, and removes fat that is harmful to the human body. It is recorded that there is In Japan, France, Germany, Italy, Macau, etc., pu-erh tea is called beauty tea, diet tea, longevity tea, etc., because it has no side effects even when taken for a long period of time (Son et al., Food & Nutr 18:219-224, 2005).
一方、プーアル茶を用いた研究により、ICR系マウスに対して、アルコールを亜急性状態に誘導したとき、プーアル茶抽出物摂取群の血中アルコール濃度は、正常対照群と有意な差がなく(Park et al、J East Asian Soc dietary Life、14:634-639,2004)、プーアル茶とプーアル茶の抗酸化効果について調べた結果、水で抽出したプーアル茶とプーアル茶の場合、総ポリフェノールの含量と電子供与性が類似するという事実が立証されたことがある(Son et al,Korea JFood & Nutr,18:219-224,2005)。 On the other hand, in a study using pu-erh tea, when alcohol was induced in a subacute state in ICR mice, the blood alcohol concentration of the pu-erh tea extract intake group did not differ significantly from that of the normal control group ( Park et al, J East Asian Soc dietary Life, 14:634-639, 2004), pu-erh tea and pu-erh tea antioxidant effects were investigated. It has been established that the electron-donating properties are similar to those of J. (Son et al, Korea J Food & Nutr, 18:219-224, 2005).
前記プーアル茶抽出液を製造するために、まず、プーアル茶の生葉を準備した後、洗浄して、前記プーアル茶の生葉に付着している異物を除去した後、前記洗浄されたプーアル茶の生葉を乾燥してもよい。 In order to prepare the pu-erh tea extract, first, fresh pu-erh tea leaves are prepared, washed to remove foreign matter adhering to the fresh pu-erh tea leaves, and then washed fresh pu-erh tea leaves. may be dried.
本発明において、前記プーアル茶の生葉の乾燥は、日光乾燥時、前記プーアル茶の生葉の葉緑素が破壊され、有用成分が揮発することを防止するために、前記プーアル茶の生葉を、温度25乃至30℃で5乃至10時間の間乾燥してもよい。 In the present invention, the drying of the fresh pu-erh tea leaves is carried out at a temperature of 25 to 25 degrees Celsius in order to prevent the chlorophyll of the fresh pu-erh tea leaves from being destroyed and the useful ingredients from volatilizing during drying in the sun. It may be dried at 30°C for 5-10 hours.
次に、前記乾燥したプーアル茶の生葉を加熱し、煎炒してもよい。 Next, the dried fresh pu-erh tea leaves may be heated and roasted.
前記ステップは、前記乾燥したプーアル茶の生葉を加熱容器(例えば、釜)に投入した後、90乃至100℃の温度で3乃至5分間1次煎炒を行い、前記1次煎炒が行われたプーアル茶の生葉を、130乃至140℃の温度で30乃至60秒間2次煎炒を行うステップにより行われてもよい。 In the step, after the dried fresh pu-erh tea leaves are put into a heating container (eg, a kettle), the primary roasting is performed at a temperature of 90 to 100° C. for 3 to 5 minutes, and the primary roasting is performed. It may be carried out by secondarily roasting fresh pu-erh tea leaves at a temperature of 130-140° C. for 30-60 seconds.
次に、前記煎炒されたプーアル茶の生葉に溶媒を混合し、超音波を加えることにより、プーアル茶混合液を製造してもよい。 Next, a pu-erh tea mixed solution may be produced by mixing a solvent with the roasted fresh leaves of pu-erh tea and applying ultrasonic waves.
前記ステップでは、前記煎炒されたプーアル茶の生葉と溶媒を混合した後、超音波抽出器に投入し、前記煎炒されたプーアル茶の生葉及び溶媒からなる混合物に超音波を加えることにより、プーアル茶液を製造してもよいが、前記溶媒は、前記プーアル茶の生葉100重量部に対して300乃至600重量部の重量割合で混合され、前記溶媒としては、水が用いられてもよい。 In the step, the roasted raw pu-erh tea leaves and the solvent are mixed, and then put into an ultrasonic extractor to apply ultrasonic waves to the mixture of the roasted fresh pu-erh tea leaves and the solvent. Pu-erh tea liquid may be prepared, and the solvent may be mixed at a weight ratio of 300 to 600 parts by weight with respect to 100 parts by weight of fresh pu-erh tea leaves, and water may be used as the solvent. .
また、前記煎炒されたプーアル茶の生葉及び溶媒からなる混合物に加えられる超音波は、60乃至80KHzの振動周波数で、30乃至60分間300乃至400ワットの出力を用いて抽出してもよい。 Alternatively, the ultrasonic waves applied to the mixture of fresh roasted pu-erh tea leaves and solvent may be extracted using a power output of 300-400 Watts for 30-60 minutes at a vibration frequency of 60-80 KHz.
続いて、前記プーアル茶混合液からプーアル茶の生葉のような固形分を分離して除去した後、熟成してプーアル茶抽出液を製造してもよい。 Subsequently, solids such as fresh pu-erh tea leaves may be separated from the pu-erh tea mixture and then aged to prepare a pu-erh tea extract.
前記ステップにおいて、前記プーアル茶の生葉のような固形分の分離は、篩等のような公知のフィルタネットが用いられてもよく、前記熟成は、前記固形分が除去されたプーアル茶抽出液を、10乃至15℃の温度で3乃至7時間の間保管することにより行われてもよい。 In the step, a known filter net such as a sieve may be used to separate solids such as fresh leaves of the pu-erh tea, and the aging is performed by removing the solids from the pu-erh tea extract. , at a temperature of 10-15° C. for 3-7 hours.
以下、本発明による山養参を用いた石鹸組成物についての好適な実施例及び比較例を挙げ、さらに詳細に説明する。 Preferred examples and comparative examples of the soap composition using wild ginseng according to the present invention will be described below in more detail.
山養参発酵抽出液30重量部、シアバター70重量部、トコフェロール(ビタミンE)5重量部、アカマツ葉油60重量部、ホホバ種子油50重量部、ソープヌードルパーム油800重量部、ヒアルロン酸2重量部、グルコン酸亜鉛3重量部、グルコン酸マグネシウム2重量部、及び玉粉7重量部の重量割合で含まれた石鹸組成物を用いて石鹸を製造した。 Mountain ginseng fermented extract 30 parts by weight, shea butter 70 parts by weight, tocopherol (vitamin E) 5 parts by weight, red pine leaf oil 60 parts by weight, jojoba seed oil 50 parts by weight, soap noodle palm oil 800 parts by weight, hyaluronic acid 2 parts by weight, 3 parts by weight of zinc gluconate, 2 parts by weight of magnesium gluconate, and 7 parts by weight of egg powder were used to produce soap.
前記実施例1と同じ組成物を用いて石鹸を製造したが、実施例2では、前記山養参発酵抽出液100重量部に対してドクダミ抽出液を25重量部の重量割合でさらに含ませて石鹸を製造した。 A soap was produced using the same composition as in Example 1, but in Example 2, 25 parts by weight of Houttuynia cordata extract was added to 100 parts by weight of the fermented extract of mountain ginseng. made soap.
前記実施例1と同じ組成物を用いて石鹸を製造したが、実施例3では、前記山養参発酵抽出液100重量部に対してプーアル茶抽出液を15重量部の重量割合でさらに含ませて石鹸を製造した。 A soap was produced using the same composition as in Example 1, but in Example 3, 15 parts by weight of pu-erh tea extract was added to 100 parts by weight of the fermented mountain ginseng extract. made soap.
<比較例1>
実施例1と同じ方法で石鹸を製造したが、比較例1では、石鹸組成物に山養参発酵抽出液を使用しなかった。
<Comparative Example 1>
A soap was produced in the same manner as in Example 1, but in Comparative Example 1, the fermented extract of wild ginseng was not used in the soap composition.
<比較例2>
市販されている石鹸(L社製造)を準備し、これを比較例2による石鹸として用いた。
<Comparative Example 2>
A commercially available soap (manufactured by Company L) was prepared and used as the soap according to Comparative Example 2.
1.石鹸の刺激実験
上記のように製造された石鹸に対する刺激実験を次の通り行った。
1. Soap Irritation Experiment Irritation experiment for the soap produced as described above was conducted as follows.
まず、臨床実験は、10歳~50歳の健常者20名(男性7名、女性13名)を対象としたが、前記石鹸で洗顔後、化粧品や保湿制等を塗らず、3時間後、肌状態(紅斑、浮腫、丘疹等)を観察し、下記の表1のような評価表による定性評価を行った。 First, the clinical experiment was conducted on 20 healthy subjects aged 10 to 50 (7 males and 13 females). The skin conditions (erythema, edema, papules, etc.) were observed and qualitatively evaluated according to the evaluation table shown in Table 1 below.
前記表1の刺激程度に対する実験対象者の評価結果は、下記の表2の通りである。 Table 2 below shows the evaluation results of the test subjects with respect to the degree of stimulation in Table 1 above.
前記表2から分かるように、実施例による石鹸は、刺激や肌状態の変化が殆どないものであり、紅斑、浮腫等の刺激が殆どない安全な物質であることが確認された。 As can be seen from Table 2 above, the soaps of the examples cause little irritation or changes in skin conditions, and are confirmed to be safe substances that cause little irritation such as erythema and edema.
2.石鹸の肌刺激性実験
20歳~50歳の女性10名に対して、実施例及び比較例による人体洗浄用ハブ石鹸で洗顔後、化粧品や保湿制等を塗らず、3時間後、顔の皮膚刺激性を評価し、その結果を下記の表3に示した。
2. Soap Skin Irritation Test Ten women aged 20 to 50 were asked to wash their face with the human cleansing hub soap according to the Examples and Comparative Examples. Irritation was evaluated and the results are shown in Table 3 below.
下記評価は、5点評価法を用いて実施したが、0点-全くない、1点-極めて軽い症状、2点-明らかな症状、3点-少し酷い症状、4点-酷い症状に分けて評価した。 The following evaluations were performed using a 5-point scale, divided into 0 points - no symptoms, 1 point - very mild symptoms, 2 points - obvious symptoms, 3 points - slightly severe symptoms, 4 points - severe symptoms. evaluated.
前記表3を参照すれば、実施例及び比較例による石鹸で洗顔した後、紅斑、痒み、浮腫等の症状が示さなかったと報告された。 Referring to Table 3, it was reported that symptoms such as erythema, itching, and edema were not observed after washing the face with the soaps of Examples and Comparative Examples.
3.皮膚弾力及び保湿改善実験
20歳~50歳の女性10名に対して、実施例により製造された石鹸で1日3回ずつ2週間洗顔した後に行ったアンケート調査において、皮膚弾力及び保湿改善について評価し、その結果を下記の表4に示した。
3. Skin Elasticity and Moisturizing Improvement Experiment A questionnaire survey was conducted on 10 females aged 20 to 50 after washing their faces with the soap produced according to the example three times a day for 2 weeks. The results are shown in Table 4 below.
前記評価は、1点から5点のスケールの5点評価法で評価し、点数が高いほどよいことを意味する。 The evaluation is based on a 5-point evaluation method on a scale of 1 to 5, and the higher the score, the better.
前記表4を参照すれば、実施例1により製造された石鹸を1日3回ずつ2週間洗顔した後に行ったアンケート調査において、実験者のうち7名が皮膚弾力及び保湿性が向上したと答え、そのうち3名は、遥かに向上したと答えた。 Referring to Table 4, in a questionnaire survey conducted after washing the face with the soap prepared in Example 1 three times a day for two weeks, seven of the experimenters answered that skin elasticity and moisturizing properties were improved. , 3 of them said they were much better.
4.剤形安定性実験
前記実施例1, 2, 3により製造された石鹸の剤形安定化程度を評価した。
4. Formulation Stability Test Formulation stability of the soaps prepared in Examples 1, 2 and 3 was evaluated.
前記剤形安定化程度の評価は、実施例1,2,3により製造された石鹸試料を、それぞれ40℃、室温、―20℃の温度で30日間保管し、相安定性を確認することにより行い、その結果を下記の表5に示した。 The degree of stabilization of the dosage form was evaluated by storing the soap samples produced in Examples 1, 2, and 3 at temperatures of 40°C, room temperature, and -20°C for 30 days, respectively, and confirming the phase stability. The results are shown in Table 5 below.
前記表5を参照すれば、実施例1,2,3により製造された石鹸は、剤形安定性が良好であることが確認された。 Referring to Table 5, it was confirmed that the soaps prepared according to Examples 1, 2 and 3 had good formulation stability.
5.抗菌力評価実験
実施例1及び比較例2により製造された石鹸の抗菌力を評価するために、下記のような実験を行った。抗菌力評価実験では、供試菌としてニキビ菌であるプロピオニバクテリウム・アクネス(Propionibacterium acnes ATCC 6919)を使用した。
5. Antibacterial Activity Evaluation Experiment In order to evaluate the antibacterial activity of the soaps prepared according to Example 1 and Comparative Example 2, the following experiments were conducted. In the antibacterial activity evaluation experiment, Propionibacterium acnes (Propionibacterium acnes ATCC 6919), which is acne bacterium, was used as a test bacterium.
ニキビ菌をそれぞれBHIブロス(broth)に接種し、前培養してから、それぞれの組成物が5%含有された滅菌した新たなBHIブロス100mlに1%の濃度で接種した後、嫌気性培養器内で2日間培養した後、菌数を測定した。 Acne bacteria were each inoculated into BHI broth, pre-incubated, and then inoculated into 100 ml of sterilized fresh BHI broth containing 5% of each composition at a concentration of 1%, followed by anaerobic incubator. After culturing for 2 days, the number of bacteria was measured.
前記表6を参照すれば、実施例1により製造された人体洗浄用ハブ石鹸は、ニキビ菌に対する抗菌力が大いに向上したことが分かる。 Referring to Table 6, it can be seen that the hub soap for washing the human body prepared according to Example 1 has significantly improved antibacterial activity against acne bacteria.
6.毛髪コンディショニング効果試験(官能評価)
前記実施例1,2,3及び比較例1,2により製造した石鹸を用いて、20~40歳の20名で構成される評価パネルに1週間使用させた後、アンケート項目に5点(大変悪い、悪い、普通、良い、大変良い)アンケートにより品質を評価し、その結果を表3に示した。
6. Hair conditioning effect test (sensory evaluation)
Using the soaps produced in Examples 1, 2, 3 and Comparative Examples 1, 2, an evaluation panel consisting of 20 people aged 20 to 40 used the soaps for 1 week. Bad, bad, normal, good, very good) was used to evaluate the quality, and Table 3 shows the results.
以上、本発明の好適な一実施例を説明したが、本発明が属する技術分野における通常の知識を有する者であれば、本発明が、その技術的思想や必須的な特徴を変更することなく、他の具体的な形態で実施され得ることが理解されるであろう。そのため、上述した一実施例は、全ての面において例示的なものであり、限定的ではないものと理解されなければならない。 Although one preferred embodiment of the present invention has been described above, a person having ordinary knowledge in the technical field to which the present invention pertains will be able to realize the present invention without changing its technical idea or essential features. , may be embodied in other specific forms. As such, the described embodiment is to be considered in all respects as illustrative and not restrictive.
Claims (3)
前記山養参発酵抽出液、シアバター、トコフェロール(ビタミンE)、アカマツ葉油、ホホバ種子油、ソープヌードルパーム油、ヒアルロン酸、グルコン酸亜鉛(Zinc Gluconate)、グルコン酸マグネシウム(Magnesium Gluconate)、及び、玉粉を含む山養参を用いた石鹸組成物であって、
前記山養参発酵抽出液20乃至40重量部、シアバター5乃至10重量部、トコフェロール(ビタミンE)3乃至7重量部、アカマツ葉油40乃至80重量部、ホホバ種子油30乃至70重量部、ソープヌードルパーム油500乃至1000重量部、ヒアルロン酸1乃至3重量部、グルコン酸亜鉛2乃至4重量部、グルコン酸マグネシウム1乃至3重量部、及び玉粉5乃至10重量部の重量割合で含まれることを特徴とする山養参を用いた石鹸組成物。 A soap composition using mountain ginseng containing a fermented extract of mountain ginseng as a main component,
The wild ginseng fermented extract, shea butter, tocopherol (vitamin E), red pine leaf oil, jojoba seed oil, soap noodle palm oil, hyaluronic acid, zinc gluconate, magnesium gluconate, and , A soap composition using wild ginseng containing ball powder,
20 to 40 parts by weight of the wild ginseng fermented extract, 5 to 10 parts by weight of shea butter, 3 to 7 parts by weight of tocopherol (vitamin E), 40 to 80 parts by weight of red pine leaf oil, 30 to 70 parts by weight of jojoba seed oil, Contains 500 to 1000 parts by weight of soap noodle palm oil, 1 to 3 parts by weight of hyaluronic acid, 2 to 4 parts by weight of zinc gluconate, 1 to 3 parts by weight of magnesium gluconate, and 5 to 10 parts by weight of egg powder A soap composition using wild ginseng characterized by:
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| PCT/KR2020/006050 WO2020226442A1 (en) | 2019-05-07 | 2020-05-07 | Soap composition using mountain-cultivated ginseng, and soap comprising same |
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| KR102052086B1 (en) * | 2019-07-25 | 2019-12-04 | 복세원 | Protective agent for teat of dairy cattles and manufacturing method thereof |
| KR102279117B1 (en) * | 2019-11-29 | 2021-07-19 | 농업회사법인 마동이주식회사 | Soap for improving natural atopy using fermented loofah cucumber powder and manufacturing method thereof |
| KR102174199B1 (en) * | 2020-01-29 | 2020-11-04 | 양숙현 | Manufacturing method for fermented oil of houttuynia cordata comprising wood-cultivated ginseng ingredient and fermented oil of houttuynia cordata manufactured by the same |
| KR102342896B1 (en) | 2021-08-08 | 2021-12-24 | 김수현 | Soap composition having main ingredient of natural material and the manufacturing method of eco-friendly soap |
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