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JP7776302B2 - Magnetic particle liquid for magnetic particle testing and magnetic particle testing method - Google Patents
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JP7776302B2 - Magnetic particle liquid for magnetic particle testing and magnetic particle testing method - Google Patents

Magnetic particle liquid for magnetic particle testing and magnetic particle testing method

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JP7776302B2
JP7776302B2 JP2021165543A JP2021165543A JP7776302B2 JP 7776302 B2 JP7776302 B2 JP 7776302B2 JP 2021165543 A JP2021165543 A JP 2021165543A JP 2021165543 A JP2021165543 A JP 2021165543A JP 7776302 B2 JP7776302 B2 JP 7776302B2
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直樹 斎藤
哲男 一本
卓也 大柴
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Marktec Corp
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Description

本発明は、磁粉探傷試験用の磁粉液及び磁粉探傷試験方法に関する。詳しくは、該磁粉液は、磁粉の色と磁粉を分散させる分散液の色とが異なる色の組み合わせである磁粉液であり、欠陥部と液だまりとを判別し易い磁粉液及び磁粉探傷試験方法に関する。 The present invention relates to a magnetic particle liquid for magnetic particle testing and a magnetic particle testing method. Specifically, the magnetic particle liquid is a magnetic particle liquid in which the magnetic particles and the dispersion liquid in which the magnetic particles are dispersed have different colors, and the magnetic particle liquid and magnetic particle testing method make it easy to distinguish between defects and liquid pools.

磁粉探傷試験とは、検査対象に対して磁場をかけることで、割れなどの欠陥部に磁極を発生させ、磁極に着色した鉄粉(以下「磁粉」という)を付着させ、欠陥部に付着した磁粉を観察することで欠陥を検出する探傷試験方法である。 Magnetic particle testing is a flaw detection testing method that applies a magnetic field to the object being inspected, generating magnetic poles in areas with cracks or other defects, causing colored iron powder (hereafter referred to as "magnetic powder") to adhere to the magnetic poles, and then detecting defects by observing the magnetic powder that has adhered to the defective areas.

しかし、実際の磁粉探傷試験においては磁極発生部以外にも磁粉が残る場合がある。 However, in actual magnetic particle testing, magnetic particles may remain in areas other than the magnetic pole generating area.

このような磁粉の残る部分を「液だまり」という。「液だまり」があると欠陥指示部とそれ以外の部分のコントラストが下がるため、水に浸漬させる等でバッククリーニングする方法が取られる。 These remaining magnetic particles are called "liquid pools." Because the presence of "liquid pools" reduces the contrast between the defect indication area and other areas, back-cleaning methods such as immersion in water are used.

しかしながらこの方法は設備コストの増加や検出力が低下するという問題がある。 However, this method has the drawback of increasing equipment costs and reducing detection power.

「液だまり」が残ったままで画像処理によって欠陥の検出を行う場合には、背景の明るさが上昇するため、欠陥か否かの閾値の設定が難しくなるという問題がある。 If defect detection is performed using image processing while the "puddle" remains, the background brightness increases, making it difficult to set a threshold for determining whether or not a defect exists.

また、液だまりは検査体全体に亘って均一ではないので、画像にぼかしフィルタなどを適用して検査画像全体に明るさ変化を求めた上で、場所によって明るさの補正を行なったり、場所によって閾値を変化させたりする必要があるため作業効率が悪いという問題がある。 Furthermore, because the liquid pools are not uniform across the entire test object, it is necessary to apply a blur filter or the like to the image to determine the brightness change across the entire test image, and then correct the brightness depending on the location or change the threshold depending on the location, which results in poor work efficiency.

また局所的に付着した液は、前述のような補正で消すことが難しく、欠陥でない部分まで欠陥として検出する虞があり欠陥検出精度が低下するという問題がある。 In addition, it is difficult to remove locally adhered liquid using the correction methods described above, and there is a risk that areas that are not defective may be detected as defective, resulting in reduced defect detection accuracy.

さらに液だまりに気泡が含まれていると、気泡部分を欠陥と誤検知してしまい、欠陥検出精度がさらに低下するという問題がある。 Furthermore, if the liquid pool contains air bubbles, the air bubbles may be mistakenly detected as defects, further reducing defect detection accuracy.

そこで、欠陥部か液だまりかを簡便な方法で判定できる磁粉液の開発が望まれている。 Therefore, there is a need to develop a magnetic particle liquid that can easily determine whether it is a defect or a liquid pool.

特開2000-11528JP 2000-11528

特許文献1には、磁化された鋼片の表面に蛍光磁粉を付着させ、該鋼片に付着した蛍光磁粉が発する蛍光を撮像し、得られた撮像画像の微分画像を生成し、前記微分画像から欠陥候補領域を抽出すると共に、前記撮像画像を2値化した画像に現れた領域の大きさ及び形状に基づいて前記欠陥候補領域から欠陥を特定することでノイズ成分から欠陥を分離する方法が記載されている。 Patent Document 1 describes a method for separating defects from noise components by attaching fluorescent magnetic particles to the surface of a magnetized piece of steel, capturing an image of the fluorescence emitted by the fluorescent magnetic particles attached to the piece of steel, generating a differential image of the captured image, extracting defect candidate areas from the differential image, and identifying defects from the defect candidate areas based on the size and shape of the areas that appear in a binarized image of the captured image.

しかし、特許文献1記載の方法は、欠陥部と、液だまりによるノイズとを分離できるが工程が多く手間がかかるという問題がある。 However, while the method described in Patent Document 1 can separate defects from noise caused by liquid pools, it has the problem of requiring many steps and being time-consuming.

本発明者らは、前記諸問題点を解決することを技術的課題とし、試行錯誤的な数多くの試作・実験を重ねた結果、磁粉の色と、磁粉を分散させる分散液の色とが異なる色の組み合わせである磁粉液であれば、画像処理によって、指示模様の色相に含まれる磁粉の色の成分と分散液の色の成分の比率を算出して、磁粉液の各色の成分の比率と比べて、磁粉の色の成分の比率が増えている指示模様を欠陥指示模様として判別することにより、液だまりによるノイズを除去して、欠陥を検出できるという刮目すべき知見を得て、前記技術的課題を達成したものである。 The inventors set out to solve the above-mentioned problems as their technical challenge, and after much trial and error and extensive trial and error, they discovered that if the magnetic powder liquid has a different color combination between the magnetic powder and the dispersion liquid in which the magnetic powder is dispersed, then image processing can be used to calculate the ratio of the magnetic powder color components to the dispersion liquid color components contained in the hue of the indication pattern, and indication patterns in which the ratio of the magnetic powder color component is increased compared to the ratio of each color component of the magnetic powder liquid can be identified as defect indication patterns. This makes it possible to remove noise caused by liquid pools and detect defects, thereby achieving the above-mentioned technical challenge.

本発明は、磁粉の色と、磁粉を分散させる分散液の色(但し、着色していない水の色を除く)とが異なる色の組み合わせである磁粉探傷試験用磁粉液である。 This invention is a magnetic particle liquid for magnetic particle testing in which the color of the magnetic particles and the color of the dispersion liquid in which the magnetic particles are dispersed (excluding the color of uncolored water) are different colors.

また本発明は、前記色の組み合わせが、一方の色と、該一方の色と色相環において45°以上、315°以下の範囲にあるもう一方の色との2色の色の組み合わせである前記の磁粉探傷試験用磁粉液である。 The present invention also relates to the magnetic particle liquid for magnetic particle testing, wherein the color combination is a two-color combination of one color and another color that is at an angle of 45° or more and 315° or less from the first color on the color wheel.

また本発明は、前記色の組み合わせが赤、緑、青の中から選択される2色の色の組み合わせである前記の磁粉探傷試験用磁粉液である。 The present invention also relates to the magnetic particle liquid for magnetic particle testing, wherein the color combination is a combination of two colors selected from red, green, and blue.

また本発明は、前記の磁粉探傷試験用磁粉液を使用する磁粉探傷試験方法である。 The present invention also relates to a magnetic particle testing method that uses the above-mentioned magnetic particle liquid for magnetic particle testing.

また本発明は、指示模様の色相に含まれる磁粉の色の成分と分散液の色の成分の各比率を算出して欠陥を検出する磁粉探傷試験方法である。 The present invention also provides a magnetic particle testing method that detects defects by calculating the ratios of the color components of the magnetic particles and the dispersion liquid contained in the hue of the indication pattern.

本明細書において「指示模様」とは、発色して模様を呈している部分を言い、欠陥指示模様のみではなく、液だまりやその他の原因によって発色して模様を呈している部分も含む語として使用する。 In this specification, the term "indication pattern" refers to an area that has developed a colored pattern, and is used to include not only defect indication patterns, but also areas that have developed a colored pattern due to liquid pooling or other causes.

本発明は、磁粉の色と、磁粉を分散させる分散液の色とが異なる色の組み合わせである磁粉液だから、画像処理によって指示模様の色相に含まれる磁粉の色の成分の比率と分散液の色の成分の比率とを算出し、磁粉液の色相に含まれる各色の成分に比べて磁粉の色の成分の比率が増えている指示模様を欠陥指示模様と判別するという簡便な方法で、液だまりによるノイズを除去して欠陥を検出することができる検出精度の高い磁粉液である。 The present invention uses a magnetic powder liquid in which the magnetic powder and the dispersion liquid in which the magnetic powder is dispersed have different color combinations. Image processing is used to calculate the ratio of the magnetic powder color components contained in the hue of the indication pattern to the ratio of the dispersion liquid color components, and indication patterns in which the ratio of the magnetic powder color components is higher than the color components of the magnetic powder liquid hue are identified as defect indication patterns. This simple method allows for the removal of noise caused by liquid pools and the detection of defects with high detection accuracy.

また、磁粉の色と分散液の色の2色の組み合わせが、一方の色と、該一方の色と色相環において、45°以上、315°以下の範囲にあるもう一方の色との2色の組み合わせや、赤、緑、青の中から選択される2色の色の組み合わせにすることで、画像処理によって色が分離し易くなるので、さらに高精度に欠陥指示模様か液だまりによるノイズかどうかを判別することができる。 Furthermore, by combining the two colors of the magnetic powder and the dispersion liquid, such as a combination of one color and another color that is at an angle of 45° or more and 315° or less on the color wheel to the first color, or a combination of two colors selected from red, green, and blue, the colors can be easily separated using image processing, making it possible to more accurately distinguish between a defect indication pattern and noise caused by a liquid puddle.

実施例と比較例のグレースケールの画像である。1 is a grayscale image of an example and a comparative example. 実施例の赤色成分と緑色成分をそれぞれ抽出した画像である。10 shows images in which red and green components are extracted in the embodiment. 比較例の赤色成分と緑色成分をそれぞれ抽出した画像である。10 is an image in which the red component and the green component are extracted, respectively, in a comparative example. 欠陥部、液だまり部、泡部を示す画像である。10 is an image showing defects, liquid pools, and bubbles.

本発明は、磁粉の色と磁粉を分散させる分散液の色とが異なる色の組み合わせである磁粉液である。 The present invention is a magnetic powder liquid in which the color of the magnetic powder and the color of the dispersion liquid in which the magnetic powder is dispersed are different colors.

本発明における「異なる色」とは、少なくとも磁粉探傷試験における欠陥検出時の観察条件下で異なる色を呈すればよい。 In this invention, "different colors" refers to colors that are different at least under the observation conditions used for defect detection in magnetic particle testing.

また、本発明における色及び色相は、可視光下の色及び色相であってもよいし、紫外線のような不可視光によって誘起される蛍光による色及び色相であってもよい。 Furthermore, the colors and hues referred to in this invention may be colors and hues under visible light, or may be colors and hues due to fluorescence induced by invisible light such as ultraviolet light.

また、本発明における色相環は特に限定されず、どのような色相環であってもよい。 Furthermore, the color wheel used in the present invention is not particularly limited and may be any color wheel.

なお、本発明における「異なる色の組み合わせ」は、着色していない水の色との組み合わせは除くものである。 Note that "combinations of different colors" in this invention exclude combinations with the color of uncolored water.

磁粉液は、通常、磁粉が分散液に均一に分散するように管理するので、磁粉の色と分散液の色とが均一に分布した色相を呈する。 Magnetic particle liquid is usually managed so that the magnetic particles are uniformly dispersed in the dispersion liquid, resulting in a hue where the colors of the magnetic particles and the dispersion liquid are evenly distributed.

磁極発生部では磁粉が磁極に引き寄せられるのに対して、分散液は磁極の影響を直接受けないから、欠陥に起因する磁極発生部では、通常の磁粉液と比べて磁粉が集中しているので、磁粉液の色相よりも磁粉の色が濃い状態になる。 In the magnetic pole generating area, the magnetic particles are attracted to the magnetic pole, whereas the dispersion liquid is not directly affected by the magnetic pole. Therefore, in the magnetic pole generating area caused by the defect, the magnetic particles are more concentrated than in normal magnetic particle liquid, and the color of the magnetic particles becomes darker than the hue of the magnetic particle liquid.

したがって、欠陥部では通常の磁粉液に比べて磁粉の色の成分の比率が増える。 Therefore, the proportion of magnetic powder color components increases in the defective area compared to normal magnetic powder liquid.

磁粉の色と分散液の色とが画像処理によって分離できる色の組み合わせであれば、磁粉探傷試験によって得られた指示模様の色相に含まれる磁粉の色の成分と分散液の色の成分の各比率によって、欠陥部にできた欠陥指示模様か液だまりによるノイズかの判定を行うことができ、従来よりも適切な閾値を設定することができる。 If the color of the magnetic powder and the color of the dispersion liquid are a color combination that can be separated using image processing, it is possible to determine whether the indication pattern obtained by magnetic particle testing is a defect indication pattern formed in a defective area or noise caused by a liquid pool based on the respective ratios of the color components of the magnetic powder and the color components of the dispersion liquid contained in the hue of the indication pattern, making it possible to set a more appropriate threshold than before.

磁粉の色と分散液の色は使用する色空間において互いに分離しやすい色であることが好ましい。 It is preferable that the colors of the magnetic powder and the dispersion liquid are easily separable from each other in the color space used.

分離し易い色とは、例えば、色相環において、類似色相配色ではない色の組み合わせである。 Easy-to-separate colors are, for example, color combinations that are not analogous hues on the color wheel.

類似色相配色ではない色の組み合わせは、一方の色ともう一方の色とが色素環において、45°以上、かつ、315°以下離れている色の組み合わせであることが好ましい。 Color combinations that are not analogous hue combinations are preferably those in which one color is more than 45° and less than 315° apart on the pigment wheel.

RGB画像を使用する場合は、磁粉の色と分散液の色を赤、緑、青から2色を選択すればよい。 When using an RGB image, simply select two colors from red, green, and blue for the magnetic powder and dispersion liquid.

カラー画像から画像処理によって分離し易いからである。 This is because it is easy to separate from color images using image processing.

例えば、紫外線照射時に緑色の蛍光を発する磁粉であれば、紫外線照射時に赤色又は青色を発光する分散液に分散するとよい。 For example, magnetic particles that emit green fluorescence when irradiated with ultraviolet light can be dispersed in a dispersion liquid that emits red or blue light when irradiated with ultraviolet light.

本発明における磁粉液の磁粉と分散液との割合は分散液が磁粉と同程度の蛍光を発する濃度が好ましい。 The ratio of magnetic particles to dispersion in the magnetic particle liquid of the present invention is preferably a concentration at which the dispersion emits fluorescence at the same level as the magnetic particles.

例えば、分散液1Lに対して磁粉0.3g~1.5g/Lと赤色蛍光体0.28g/L~1.0g/Lを分散させて作製することができる。 For example, it can be produced by dispersing 0.3g to 1.5g/L of magnetic powder and 0.28g/L to 1.0g/L of red phosphor in 1L of dispersion liquid.

本発明に係る磁粉液は分散剤を含有してもよい。 The magnetic powder liquid of the present invention may contain a dispersant.

本発明で使用する画像編集ソフトは公知の画像編集ソフトを使用すればよく、GIMPやフォトショップ(登録商標)を例示する。 The image editing software used in this invention may be any known image editing software, such as GIMP or Photoshop (registered trademark).

本発明を実施例及び比較例を挙げてより詳しく説明するが、本発明はこれに限られるものではない。 The present invention will be explained in more detail using examples and comparative examples, but the present invention is not limited to these.

紫外線照射下で赤く発光する蛍光顔料(SINLOIHI COLOR FZ-6037 Pink/シンロイヒ株式会社製)を水500mLに対して0.5gの比率で混ぜたものを、1g/Lの濃度で作製したものを分散液とした。 A fluorescent pigment that emits red light under ultraviolet light (SINLOIHI COLOR FZ-6037 Pink, manufactured by SINLOIHI Co., Ltd.) was mixed with 500 mL of water at a ratio of 0.5 g to prepare a dispersion at a concentration of 1 g/L.

蛍光磁粉LY-30(マークテック株式会社製)液と作製した分散液を1:1の比率で混ぜた磁粉液を実施例とした。 The magnetic powder liquid used in this example was a 1:1 mixture of fluorescent magnetic powder LY-30 (manufactured by Marktec Co., Ltd.) and the dispersion liquid prepared.

蛍光磁粉LY-30(マークテック株式会社製)液と着色しない水で1g/Lの濃度とした磁粉液を比較例とした。 The comparative examples were a fluorescent magnetic powder LY-30 (manufactured by Marktec Co., Ltd.) solution and a magnetic powder solution with a concentration of 1 g/L in uncolored water.

蛍光磁粉LY-30は紫外線照射下で緑に発光する。 Fluorescent magnetic powder LY-30 emits green light under ultraviolet light.

検査体には、スリットを加工したギアを模した模擬欠陥部を有する試験片を使用した。 The specimen used for testing was a test piece with a simulated defect that resembled a gear with a slit cut into it.

検査体を軸通電法にて磁化し、連続法で検査液を適用して磁粉探傷試験を行なった。 The specimen was magnetized using the axial current method, and magnetic particle testing was performed by applying the test liquid using the continuous method.

探傷試験後の検査体は、RGBに感度をもつカラーCMOS(Complementary Metal Oxide Semiconductor)カメラにて画像を撮影した。 After the flaw detection test, the specimen was photographed using a color CMOS (Complementary Metal Oxide Semiconductor) camera sensitive to RGB.

(画像処理)
画像編集ソフトを使用して次の(1)~(4)の手順で画像処理を行った。
(1)得られた画像を開く
(2)選択ツールを使って対象領域を選択
(3)ヒストグラムダイアログを使って(2)で選択した領域から赤色成分の平均輝度(8bit画素値)を取得
(4)ヒストグラムダイアログを使って(2)で選択した領域から緑色成分の平均輝度(8bit画素値)を取得
(Image Processing)
Image processing was carried out using image editing software according to the following steps (1) to (4).
(1) Open the resulting image. (2) Use the selection tool to select the target area. (3) Use the histogram dialog to obtain the average luminance (8-bit pixel value) of the red component from the area selected in (2). (4) Use the histogram dialog to obtain the average luminance (8-bit pixel value) of the green component from the area selected in (2).

探傷試験後の検査体をカラー画像で撮影し、グレースケールとしたものを図1に示す。 Figure 1 shows a color image of the test piece taken after the flaw detection test, which was then converted to grayscale.

実施例の探傷試験後の検査体をカラー画像で撮影し、緑色成分と赤色成分を抽出したものを図2に示す。 Figure 2 shows a color image of the test object after the flaw detection test in this example, with the green and red components extracted.

比較例の探傷試験後の検査体をカラー画像で撮影し、緑色成分と赤色成分を抽出したものを図3に示す。 Figure 3 shows a color image of the specimen after the comparative example flaw detection test, with the green and red components extracted.

実施例及び比較例の各模擬欠陥部、液だまり部、及び、泡部(図4)の赤色成分、緑色成分の8bit画素値を表1及び表2に示す。 Tables 1 and 2 show the 8-bit pixel values of the red and green components of each simulated defect, puddle, and bubble (Figure 4) in the example and comparative example.

実施例の磁粉液であれば、磁極が発生する欠陥部は赤色成分と比べて緑色成分が高い値となり、磁極の発生していない液だまり部や泡部は赤色成分と緑色成分がほぼ同じ値となるので、欠陥指示模様と液だまりによるノイズと判別し、ノイズを除去できることが証明された。 With the magnetic powder liquid of the example, defective areas where magnetic poles occur have higher values for the green component than for the red component, while puddles and bubble areas where no magnetic poles occur have roughly the same values for the red and green components. This proves that it is possible to distinguish between defect indication patterns and noise caused by puddles, and to remove the noise.

本発明は、磁粉の色と磁粉を分散させる分散液の色とが異なる色の組み合わせである磁粉液だから、磁極の発生しない液だまりと比べて、磁極の発生する欠陥部は磁粉液の色相と比べて磁粉の色が濃くなるため、画像処理によって、指示模様の色相に含まれる磁粉の色の成分と分散液の色の成分の比率を算出して、磁粉液の各色の成分の比率と比べて、磁粉の色の成分の比率が増えている指示模様を欠陥指示模様として判別することにより、液だまりによるノイズを分離して、欠陥部を検出できるので、簡便な方法で、精度の高い磁粉探傷試験を行うことができる磁粉液及び磁粉探傷方法である。
よって、本発明の産業上の利用可能性は高い。
Since the present invention uses a magnetic particle liquid in which the color of the magnetic powder and the color of the dispersion liquid in which the magnetic powder is dispersed are different colors, the color of the magnetic powder in defective areas where magnetic poles are generated is darker than the hue of the magnetic particle liquid, compared to puddles where no magnetic poles are generated.Therefore, by using image processing to calculate the ratio of the color components of the magnetic powder and the color components of the dispersion liquid contained in the hue of the indication pattern, and by distinguishing indication patterns in which the ratio of the color component of the magnetic powder is increased compared to the ratio of each color component of the magnetic particle liquid, as defect indication patterns, it is possible to separate out the noise caused by puddles and detect defective areas, resulting in a magnetic particle liquid and magnetic particle inspection method that allows for highly accurate magnetic particle inspection testing in a simple manner.
Therefore, the present invention has high industrial applicability.

Claims (4)

磁粉の色と、磁粉を分散させる分散液の色(但し、着色していない水の色を除く)とが異なる色の組み合わせであり、前記色の組み合わせが、一方の色と、該一方の色と色相環において45°以上、315°以下の範囲にあるもう一方の色との2色の色の組み合わせである磁粉探傷試験用磁粉液 A magnetic particle liquid for magnetic particle inspection testing, in which the color of the magnetic particle and the color of the dispersion liquid in which the magnetic particle is dispersed (excluding the color of uncolored water) are different colors, and the color combination is a combination of two colors, one color and another color that is at an angle of 45° or more and 315° or less from the first color on the color wheel . 前記色の組み合わせが、赤、緑、青の中から選択される2色の色の組み合わせである請求項記載の磁粉探傷試験用磁粉液。 2. The magnetic particle liquid for magnetic particle testing according to claim 1 , wherein the color combination is a combination of two colors selected from the group consisting of red, green, and blue. 請求項1又は2記載の磁粉探傷試験用磁粉液を使用する磁粉探傷試験方法。 A magnetic particle testing method using the magnetic particle liquid for magnetic particle testing according to claim 1 or 2 . 指示模様の色相に含まれる磁粉の色の成分と分散液の色の成分の各比率を算出して欠陥を検出する請求項3記載の磁粉探傷試験方法。 4. A magnetic particle testing method according to claim 3 , wherein defects are detected by calculating the ratio of the color components of the magnetic particles contained in the hue of the indication pattern to the color components of the dispersion liquid.
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JP2003279545A (en) 2002-03-26 2003-10-02 Osaka Gas Co Ltd Magnetic flaw detection method
JP2006046937A (en) 2004-07-30 2006-02-16 Marktec Corp Liquid dispersant for preparing magnetic powder liquid
JP2009109423A (en) 2007-10-31 2009-05-21 Marktec Corp Concentrated magnetic powder dispersion for wet magnetic particle testing
JP2018100917A (en) 2016-12-21 2018-06-28 マークテック株式会社 Magnetic particle flaw detection device, magnetic particle flaw detection method, and suspension for magnetic particle flaw detection

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