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JP7819626B2 - Single-sided polishing method for SOI wafer - Google Patents
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JP7819626B2 - Single-sided polishing method for SOI wafer - Google Patents

Single-sided polishing method for SOI wafer

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JP7819626B2
JP7819626B2 JP2022203775A JP2022203775A JP7819626B2 JP 7819626 B2 JP7819626 B2 JP 7819626B2 JP 2022203775 A JP2022203775 A JP 2022203775A JP 2022203775 A JP2022203775 A JP 2022203775A JP 7819626 B2 JP7819626 B2 JP 7819626B2
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昭太 大槻
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Sumco Corp
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Description

本発明は、SOIウェーハの片面研磨方法に関する。 The present invention relates to a method for single-sided polishing of SOI wafers.

近年、高集積CMOS素子、高耐圧素子、イメージセンサ等の種々の半導体デバイス用途において、SOI(Silicon on Insulator)構造を有するSOIウェーハが注目されている。 In recent years, SOI wafers with an SOI (Silicon on Insulator) structure have been attracting attention for various semiconductor device applications, such as highly integrated CMOS elements, high-voltage elements, and image sensors.

SOIウェーハは一般的に、単結晶シリコンウェーハからなる支持基板ウェーハ上に、酸化シリコン(SiO)等の絶縁層及びデバイス活性層として使用される単結晶シリコン層などの半導体層が順次形成された構造を有する。なお、この半導体層は活性層又はSOI層とも呼ばれ、以下、本明細書では「活性層」と称する。バルクの単結晶シリコンウェーハでは素子と基板部分との間に発生し得る寄生容量が比較的大きいものの、活性層は絶縁層上に設けられるために寄生容量を大幅に低減できる。そのため、SOIウェーハはデバイスの高速化、高耐圧化、低消費電力化等の点で有利である。 An SOI wafer generally has a structure in which an insulating layer such as silicon oxide (SiO 2 ) and a semiconductor layer such as a single-crystal silicon layer used as a device active layer are sequentially formed on a support substrate wafer made of a single-crystal silicon wafer. This semiconductor layer is also called an active layer or SOI layer, and will be referred to as the "active layer" hereinafter in this specification. While bulk single-crystal silicon wafers have a relatively large parasitic capacitance that can occur between the device and the substrate, the active layer is provided on an insulating layer, which significantly reduces the parasitic capacitance. Therefore, SOI wafers are advantageous in terms of increasing device speed, increasing breakdown voltage, and reducing power consumption.

半導体デバイスの高集積化はますます加速しており、半導体ウェーハの平坦度などの表面品質の改善が求められている。この要望に応えるため、半導体ウェーハの研磨装置及び研磨方法の改良が幅広く行われている。 As semiconductor devices become increasingly highly integrated, there is a demand for improvements in the surface quality of semiconductor wafers, such as flatness. To meet this demand, improvements are being made to semiconductor wafer polishing equipment and methods.

例えば特許文献1に記載の半導体ウェーハの研磨装置では、研磨圧力に伴う半導体ウェーハの変形を防止するため、複数の圧力室をえる研磨ヘッドが用いられている。 For example, in the semiconductor wafer polishing apparatus described in Patent Document 1, a polishing head having a plurality of pressure chambers is used to prevent deformation of the semiconductor wafer due to the polishing pressure.

また、特許文献2では、活性層の膜厚分布を均一にするために、SOIウェーハ全体の厚み分布ではなく活性層の径方向膜厚分布に着目し、研磨に先立ち活性層の径方向膜厚分布を測定している。そして、特許文献2ではこの測定結果に基づいて研磨ヘッドにおける加圧制御室の加圧分布を適正制御する。 Furthermore, in Patent Document 2, in order to achieve a uniform film thickness distribution in the active layer, the radial film thickness distribution of the active layer is measured prior to polishing, focusing on the radial film thickness distribution of the active layer rather than the thickness distribution of the entire SOI wafer. Patent Document 2 then appropriately controls the pressure distribution in the pressure control chamber in the polishing head based on the measurement results.

また特許文献2では、光学式膜厚測定部を有する研磨装置を用いて、研磨中の膜厚を評価している。この光学式膜厚測定部は、測定光を入射可能な光源及びこの測定光の反射光を受光可能な受光センサを有する。そして、光源からの測定光の入射光を、光ファイバを経由してレンズにより集光し、定盤の窓部を介して測定光をSOIウェーハのSOI層(活性層)の露出面に入射させ、絶縁層によって反射された測定光を、レンズ及び光ファイバを経由して、受光センサが当該測定光の反射光を受光する。こうすることで、特許文献2の片面研磨装置は研磨中にSOI層(活性層)の膜厚を測定している。 Patent Document 2 also describes a polishing apparatus with an optical film thickness measurement unit that evaluates film thickness during polishing. This optical film thickness measurement unit has a light source that can emit measurement light and a light-receiving sensor that can receive the reflected light of this measurement light. The incident measurement light from the light source is then collected by a lens via an optical fiber, and the measurement light is then incident on the exposed surface of the SOI layer (active layer) of the SOI wafer through a window in the surface plate. The measurement light is reflected by the insulating layer and transmitted via the lens and optical fiber to the light-receiving sensor, where it is received. In this way, the single-sided polishing apparatus of Patent Document 2 measures the film thickness of the SOI layer (active layer) during polishing.

特開2009-131920号公報JP 2009-131920 A 特開2021-106193号公報Japanese Patent Application Laid-Open No. 2021-106193

近年、SOIウェーハの活性層の平坦性の改善がますます求められている。活性層に求められる仕様の一つに「膜厚レンジ」がある。研磨仕上げ後の活性層の目標厚みを表記する場合、活性層の膜厚分布のうち、最も厚い側と最も薄い側に許容されるそれぞれの厚み誤差をaと表記すれば、活性層の膜厚分布を[目標厚み]±aの範囲内に収める必要がある。すなわち、膜厚最大値と膜厚最小値との差を2aに収める必要がある。膜厚レンジはこの膜厚最大値と膜厚最小値との差を意味する。膜厚レンジを従来技術よりもさらに小さくすることのできるSOIウェーハの片面研磨方法が求められる。 In recent years, there has been an increasing demand for improved flatness in the active layer of SOI wafers. One of the specifications required for the active layer is the "film thickness range." When expressing the target thickness of the active layer after polishing, if the allowable thickness error on the thickest and thinnest sides of the active layer's film thickness distribution is denoted as a, then the film thickness distribution of the active layer must fall within the range of [target thickness] ± a. In other words, the difference between the maximum and minimum film thickness values must fall within 2a. The film thickness range refers to the difference between this maximum and minimum film thickness values. There is a need for a single-sided polishing method for SOI wafers that can further narrow the film thickness range compared to conventional techniques.

そこで本発明は、活性層の膜厚分布をより均一化できるSOIウェーハの片面研磨方法を提供することを目的とする。 SUMMARY OF THE INVENTION It is therefore an object of the present invention to provide a method for polishing one side of an SOI wafer, which can make the film thickness distribution of the active layer more uniform.

上記課題を解決すべく本発明者らは鋭意検討した。そして、SOIウェーハの活性層の中央部及び外周部のそれぞれの厚み平均の差である凹凸指数なる指標を用いることを本発明者らは着想した。そして、この凹凸指数を用いて研磨中にまず凹凸指数の値を絶対値として小さくなるよう研磨を行い、研磨中の凹凸指数が所定条件を満足した後、活性層全面の厚みを全体的に減少させることにより、活性層の膜厚分布を均一化できることを本発明者らは知見した。上記知見に基づき完成した本発明の要旨構成は以下のとおりである。 The inventors conducted extensive research to solve the above problem. They came up with the idea of using an index known as the roughness index, which is the difference between the average thicknesses of the central and peripheral portions of the active layer of an SOI wafer. They then discovered that by using this roughness index during polishing to first reduce the absolute value of the roughness index, and then reducing the overall thickness of the entire active layer after the roughness index during polishing satisfies certain conditions, they can achieve a uniform film thickness distribution in the active layer. The gist of the present invention, which was completed based on the above findings, is as follows:

(1)SOIウェーハの活性層の膜厚分布を測定しながら前記活性層を研磨するSOIウェーハの片面研磨方法であって、
研磨開始前の前記活性層の膜厚分布を測定して、前記研磨開始前における前記活性層の前記膜厚分布に基づく凹凸指数を計算する第1工程と、
前記研磨開始前の前記凹凸指数に基づき初期研磨条件を決定する第2工程と、
前記初期研磨条件に基づき前記活性層を研磨しつつ、前記活性層における中央部及び外周部の膜厚を研磨中に複数回測定して、研磨中での前記凹凸指数を計算する第3工程と、
前記研磨中の前記凹凸指数の絶対値が目標値以下となったときに前記初期研磨条件での研磨を終了する第4工程と、
前記活性層の中央部と外周部の膜厚平均値が目標厚みに到達するまで、仕上げ研磨条件に基づき前記活性層を研磨する第5工程と、を含み、
前記凹凸指数は、前記活性層の中央部及び外周部のそれぞれの厚み平均の差である、SOIウェーハの片面研磨方法。
(1) A method for polishing a single side of an SOI wafer, in which an active layer of the SOI wafer is polished while measuring a film thickness distribution of the active layer, comprising the steps of:
a first step of measuring a film thickness distribution of the active layer before the start of polishing and calculating a roughness index based on the film thickness distribution of the active layer before the start of polishing;
a second step of determining initial polishing conditions based on the unevenness index before the start of polishing;
a third step of measuring the film thicknesses of the central and peripheral portions of the active layer multiple times during polishing while polishing the active layer based on the initial polishing conditions, and calculating the unevenness index during polishing;
a fourth step of terminating polishing under the initial polishing conditions when the absolute value of the unevenness index during polishing becomes equal to or less than a target value;
a fifth step of polishing the active layer under finish polishing conditions until an average film thickness of the central portion and the outer periphery of the active layer reaches a target thickness;
The method for polishing a single side of an SOI wafer, wherein the unevenness index is a difference between the average thicknesses of the central portion and the outer periphery of the active layer.

(2) 前記第3工程において、前記中央部及び外周部での膜厚の測定回数は研磨ヘッドが一周期の揺動を完了するまでに測定される回数である、(1)に記載のSOIウェーハの片面研磨方法。 (2) A method for polishing a single side of an SOI wafer according to (1), wherein in the third step, the number of times the film thickness is measured at the central and peripheral portions is the number of times the film thickness is measured until the polishing head completes one oscillation cycle.

(3) 研磨時に前記活性層が受ける径方向加圧分布と、前記凹凸指数の矯正力との指数矯正関係をあらかじめ求めておき、前記第2工程では、前記指数矯正関係に基づき前記研磨開始前の前記凹凸指数に対応する前記初期研磨条件を決定する、(1)又は(2)に記載のSOIウェーハの片面研磨方法。 (3) A single-sided polishing method for an SOI wafer according to (1) or (2), in which an exponential correction relationship between the radial pressure distribution received by the active layer during polishing and the correction force for the unevenness index is determined in advance, and in the second step, the initial polishing conditions corresponding to the unevenness index before the start of polishing are determined based on the exponential correction relationship.

本発明によれば、活性層の膜厚分布をより均一化できるSOIウェーハの片面研磨方法を提供することができる。 The present invention provides a method for polishing one side of an SOI wafer that can achieve a more uniform film thickness distribution in the active layer.

点平均凹凸指数の計算方法の一例を説明する模式図である。FIG. 10 is a schematic diagram illustrating an example of a method for calculating a point-average unevenness index. 領域凹凸指数の計算方法の一例を説明する模式図である。FIG. 10 is a schematic diagram illustrating an example of a method for calculating a region unevenness index. 凹凸指数と膜厚レンジとの関係の一例を示す図である。FIG. 10 is a diagram showing an example of the relationship between the unevenness index and the film thickness range. 膜厚凹形状ウェーハにおける指数矯正関係の一例を示した図である。FIG. 10 is a diagram showing an example of an index correction relationship in a wafer with a concave film thickness. 膜厚凸形状ウェーハにおける指数矯正関係の一例を示した図である。FIG. 10 is a diagram showing an example of an index correction relationship in a wafer with a convex film thickness. 本発明の一実施形態に従うSOIウェーハの片面研磨装置の一部を示した図である。1 is a diagram showing a portion of a single-sided polishing apparatus for an SOI wafer according to an embodiment of the present invention. 実施例1において測定した研磨前後における径方向膜厚分布である。1 shows the radial film thickness distribution measured before and after polishing in Example 1. 比較例1において測定した研磨前後における径方向膜厚分布である。1 shows the radial film thickness distribution measured before and after polishing in Comparative Example 1. 実施例1及び比較例1において、研磨前のウェーハに対して測定した活性層の膜厚の変動幅を示すグラフである。1 is a graph showing the range of variation in film thickness of an active layer measured on a wafer before polishing in Example 1 and Comparative Example 1. 実施例1及び比較例1において、研磨後のウェーハに対して測定した活性層の膜厚の変動幅を示すグラフである。1 is a graph showing the range of variation in film thickness of an active layer measured on a wafer after polishing in Example 1 and Comparative Example 1.

実施形態の説明に先立ち、研磨時の膜厚分布の評価方法と実際に測定される膜厚分布との関係について確認すべく、以下の予備実験を実施した。 Prior to explaining the embodiments, the following preliminary experiment was conducted to confirm the relationship between the evaluation method for film thickness distribution during polishing and the film thickness distribution actually measured.

(予備実験)
前述した膜厚レンジは活性層の膜厚の誤差を正確に説明できるものの、研磨中の膜厚測定によってウェーハ全面の膜厚分布を評価することは測定点数の観点で時間的に困難である。さらに、研磨中の測定であれば必然的に膜厚測定中にも研磨が進行するため、正確な膜厚分布を評価することはできない。一般的に、SOIウェーハの活性層の厚みは、中央部から外周部に向かうほど線形減少(中央部が凸型)または線形増加(中央部が凹型)していく。そこで研磨加工中でも膜厚レンジの状態を簡易的に把握するために、以下に詳述する活性層の中央部及び外周部のそれぞれの厚み平均の差を用いた「凹凸指数」なる指標の導入を検討し、その実効性を本発明者らは検証した。
(Preliminary experiment)
Although the aforementioned film thickness range can accurately account for errors in the active layer film thickness, evaluating the film thickness distribution across the entire wafer by measuring the film thickness during polishing is time-consuming due to the number of measurement points. Furthermore, if measurements are performed during polishing, polishing inevitably progresses even during film thickness measurement, making it impossible to accurately evaluate the film thickness distribution. Generally, the thickness of the active layer of an SOI wafer linearly decreases (the center is convex) or linearly increases (the center is concave) from the center to the periphery. Therefore, to easily grasp the state of the film thickness range during polishing, the inventors considered introducing an index called a "roughness index," which uses the difference in the average thickness between the center and periphery of the active layer, as described in detail below, and verified its effectiveness.

<凹凸指数>
本明細書において、SOIウェーハの活性層の中央部及び外周部のそれぞれの厚み平均の差を「凹凸指数」と称する。まず、図1Aを参照して、本予備実験で用いた具体的な凹凸指数(便宜上、「点平均凹凸指数」と称する)を説明する。点平均凹凸指数においては、中央部の代表値としてSOIウェーハ100の中心点101の活性層の膜厚と、SOIウェーハ100の中心からウェーハ半径の10%の円周111上の活性層の膜厚との平均値(算術平均値を指し、以下、単に「平均値」という。)を用いた。そして同様に外周部の代表値としてSOIウェーハ100の中心からウェーハ半径の90%の円周191上の活性層の膜厚の平均値を用い、このときの中央部の膜厚平均値から外周部の膜厚平均値を差し引いた値([中央部膜厚平均値]-[外周部膜厚平均値])を特に点平均凹凸指数と称し、図1Bを参照して後述する領域平均凹凸指数と区別する。
<Roughness index>
In this specification, the difference in the average thickness between the central and peripheral portions of the active layer of an SOI wafer is referred to as the "roughness index." First, with reference to FIG. 1A , the specific roughness index (for convenience, referred to as the "point-average roughness index") used in this preliminary experiment will be described. In the point-average roughness index, the average value (referring to the arithmetic average value, hereinafter simply referred to as the "average") of the active layer film thickness at the center point 101 of the SOI wafer 100 and the active layer film thickness on a circumference 111 that is 10% of the wafer radius from the center of the SOI wafer 100 is used as a representative value of the central portion. Similarly, the average value of the active layer film thickness on a circumference 191 that is 90% of the wafer radius from the center of the SOI wafer 100 is used as a representative value of the peripheral portion. The value obtained by subtracting the average film thickness of the peripheral portion from the average film thickness of the central portion ([average central film thickness] - [average peripheral film thickness]) is specifically referred to as the point-average roughness index, and is distinguished from the area-average roughness index described later with reference to FIG. 1B.

上記点平均凹凸指数と、実際に直径200mmのSOIウェーハ全面について膜厚測定して求めた膜厚レンジとを比較したグラフを図2に示す。この結果から、凹凸指数と膜厚レンジには良好な相関が見られることが分かった。すなわち、SOIウェーハの活性層の膜厚の凹凸指数を把握することで、膜厚レンジを精度よく予測できることが分かった。例えば凹凸指数が正の値(この場合、中央部が凸型である)であれば、一段階目の研磨では外周部の研磨取り代が比較的小さく、中央部の研磨取り代が比較的大きい研磨条件を採用する。そうして一段目の研磨で凹凸指数を絶対値でできるだけ小さくしてから一段階目の研磨を終え、二段階目の研磨では単に活性層の厚みを目標厚みにまで減じるだけの研磨をすれば、実質的に目標とする膜厚レンジのSOIウェーハを得ることができる。反対に、例えば凹凸指数が負の値(この場合、中央部が凹型である)であれば、一段階目の研磨では外周部の研磨取り代が比較的大きく、中央部の研磨取り代が比較的小さい研磨条件を採用する。そうして一段目の研磨で、凹凸指数を絶対値でできるだけ小さくしてから同様に二段階目の研磨を行えば、実質的に目標とする膜厚レンジのSOIウェーハを得ることができる。 Figure 2 shows a graph comparing the point-average irregularity index with the film thickness range determined by actual film thickness measurements across the entire surface of a 200 mm diameter SOI wafer. These results demonstrate a good correlation between the irregularity index and the film thickness range. In other words, by determining the irregularity index of the active layer film thickness of an SOI wafer, the film thickness range can be accurately predicted. For example, if the irregularity index is a positive value (in this case, the central portion is convex), polishing conditions are adopted in the first stage of polishing in which the polishing allowance at the periphery is relatively small and the polishing allowance at the central portion is relatively large. By completing the first stage of polishing after minimizing the absolute value of the irregularity index in the first stage of polishing, and then simply polishing the active layer to the target thickness in the second stage of polishing, an SOI wafer with a substantially targeted film thickness range can be obtained. Conversely, if the irregularity index is a negative value (in this case, the central portion is concave), polishing conditions are adopted in the first stage of polishing in which the polishing allowance at the periphery is relatively large and the polishing allowance at the central portion is relatively small. Then, by making the absolute value of the unevenness index as small as possible in the first stage of polishing and then similarly performing the second stage of polishing, an SOI wafer having a film thickness substantially within the target range can be obtained.

(SOIウェーハの片面研磨方法)
すなわち、本発明に従うSOIウェーハの片面研磨方法は、SOIウェーハの活性層の膜厚分布を測定しながら活性層を研磨するSOIウェーハの片面研磨方法であって、研磨開始前の活性層の膜厚分布を測定して、研磨開始前における活性層の膜厚分布に基づく凹凸指数を計算する第1工程と、研磨開始前の凹凸指数に基づき初期研磨条件を決定する第2工程と、初期研磨条件に基づき活性層を研磨しつつ、活性層における中央部及び外周部の膜厚を研磨中に複数回測定して、研磨中での凹凸指数を計算する第3工程と、研磨中の凹凸指数の絶対値が目標値以下となったときに初期研磨条件での研磨を終了する第4工程と、活性層の中央部と外周部の膜厚平均値が目標厚みに到達するまで、仕上げ研磨条件に基づき活性層を研磨する第5工程と、を含む。また、ここで凹凸指数は、活性層の中央部及び外周部のそれぞれの厚み平均の差である。以下、各工程の詳細を順次説明する。
(Method for polishing one side of SOI wafer)
That is, the single-sided polishing method for SOI wafers according to the present invention is a method for polishing an active layer of an SOI wafer while measuring the film thickness distribution of the active layer of the SOI wafer. It includes the following steps: a first step of measuring the film thickness distribution of the active layer before the start of polishing and calculating a roughness index based on the film thickness distribution of the active layer before the start of polishing; a second step of determining initial polishing conditions based on the roughness index before the start of polishing; a third step of measuring the film thickness of the central and peripheral portions of the active layer multiple times during polishing while polishing the active layer under the initial polishing conditions and calculating the roughness index during polishing; a fourth step of terminating polishing under the initial polishing conditions when the absolute value of the roughness index during polishing falls below a target value; and a fifth step of polishing the active layer under the finish polishing conditions until the average film thickness of the central and peripheral portions of the active layer reaches the target thickness. Here, the roughness index is the difference between the average thicknesses of the central and peripheral portions of the active layer. Details of each step are explained below.

<第1工程>
第1工程では、研磨開始前の活性層の膜厚分布を測定して、研磨開始前における活性層の膜厚分布に基づく凹凸指数を計算する。研磨開始前の膜厚分布の測定方法は特に限定されず、研磨装置とは別のフーリエ変換赤外分光法などを用いた任意の装置を用いてもよいし、例えば特許文献2で前述したような、研磨装置に組み込まれた光学式の膜厚測定機構を用いてもよい。
<First step>
In the first step, the thickness distribution of the active layer before the start of polishing is measured, and a roughness index is calculated based on the thickness distribution of the active layer before the start of polishing. The method for measuring the thickness distribution before the start of polishing is not particularly limited, and any device using Fourier transform infrared spectroscopy or the like separate from the polishing device may be used, or an optical film thickness measurement mechanism incorporated in the polishing device, such as that described in Patent Document 2, may be used.

<<凹凸指数>>
凹凸指数は、上述のとおり、活性層の膜厚分布の指標として導入する指数であり、活性層の中央部及び外周部のそれぞれの厚み平均の差によって定義される。活性層の膜厚分布の全面を評価して膜厚レンジを求める際の測定点数よりも、凹凸指数を算出するための測定点数は少なくてよい。そのため、活性層の凹凸形状を簡易的に評価することが可能である。凹凸指数を計算する際に中央部及び外周部の具体的な範囲は限定されないが、中央部とはウェーハ中心から概ねウェーハ半径の30%以下までの範囲を指し、外周部とは概ねウェーハ半径の70%以上100%以下の範囲を指す。図2で示したとおり、膜厚レンジと凹凸指数との間には良い一次相関が見られるため、任意の計算方法で得られた凹凸数から膜厚レンジを容易に予想することができる。図1Aを参照して説明した点平均凹凸指数を凹凸指数として採用してもよい。なお図1AではSOIウェーハの中心膜厚及び中心からウェーハ半径の10%の円周上の膜厚値と、中心からウェーハ半径の90%の円周上の膜厚値を利用しているが、これは例示に過ぎない。
<<Irregularity index>>
As described above, the roughness index is an index introduced as an indicator of the film thickness distribution of the active layer and is defined as the difference in the average thickness between the central and peripheral portions of the active layer. The number of measurement points required to calculate the roughness index is fewer than the number of measurement points required to evaluate the entire surface of the active layer's film thickness distribution and determine the film thickness range. This allows for a simple evaluation of the active layer's roughness shape. While the specific ranges of the central and peripheral portions are not limited when calculating the roughness index, the central portion refers to the range from the wafer center to approximately 30% of the wafer radius, and the peripheral portion refers to the range from approximately 70% to 100% of the wafer radius. As shown in Figure 2, a good linear correlation is observed between the film thickness range and the roughness index, so the film thickness range can be easily predicted from the roughness index obtained by any calculation method. The point-average roughness index described with reference to Figure 1A may also be used as the roughness index. Note that Figure 1A uses the central film thickness of the SOI wafer, the film thickness value on a circle 10% of the wafer radius from the center, and the film thickness value on a circle 90% of the wafer radius from the center, but this is merely an example.

-領域平均凹凸指数-
また、図1Bを参照して説明するとおり、領域平均での凹凸指数(以下、「領域平均凹凸指数」と称する)を凹凸指数として採用しても構わない。例えば、SOIウェーハ100の中心からウェーハ半径の10%以下の円状領域112上の活性層の膜厚の平均値から、SOIウェーハ100の中心からウェーハ半径の90%以上100%以下の環状領域192の活性層の膜厚の平均値を差し引いた値を領域平均凹凸指数とすることができる。
-Area average unevenness index-
1B, the area-averaged unevenness index (hereinafter referred to as the "area-averaged unevenness index") may be used as the unevenness index. For example, the area-averaged unevenness index may be calculated by subtracting the average thickness of the active layer in an annular region 192 extending from the center of the SOI wafer 100 to 90% to 100% of the wafer radius from the average thickness of the active layer in a circular region 112 extending from the center of the SOI wafer 100 to 10% of the wafer radius.

なお、本工程では膜厚分布を研磨中に測定するわけではないので、第3工程において後述する測定点数の制限はなく、ウェーハ全面の測定結果を用いて凹凸指数を計算してもよいし、数点~数十点程度の測定点数から凹凸指数を計算してもよい。 In this process, the film thickness distribution is not measured during polishing, so there is no limit to the number of measurement points in the third process, as described below. The unevenness index can be calculated using the measurement results for the entire wafer, or it can be calculated from several to several tens of measurement points.

<第2工程>
第2工程では、第1工程により求めた研磨開始前の凹凸指数に基づき初期研磨条件を決定する。研磨後のSOIウェーハの凹凸指数の絶対値が小さくなるよう、適宜に初期研磨条件を採用すればよい。具体的には、活性層の研磨前の凹凸を緩和するようなウェーハ径方向加圧分布を設定すればよく、例えば凹凸指数が正の値である(活性層の膜厚の中央部が外周部よりも大きく、凸形状である)場合にはウェーハを保持する部材のウェーハ中央部の加圧を比較的大きくすればよい。反対に、凹凸指数が負の値である(活性層の膜厚の外周部が中央部よりも大きく、凹形状である)場合にはウェーハを保持する部材のウェーハ中央部の加圧を比較的小さくすればよい。
<Second process>
In the second step, initial polishing conditions are determined based on the roughness index before polishing determined in the first step. The initial polishing conditions can be appropriately selected so that the absolute value of the roughness index of the polished SOI wafer is small. Specifically, a radial pressure distribution of the wafer can be set to reduce the roughness of the active layer before polishing. For example, if the roughness index is a positive value (the active layer has a larger thickness at the center than at the periphery, resulting in a convex shape), the pressure applied to the center of the wafer by the member holding the wafer can be relatively large. Conversely, if the roughness index is a negative value (the active layer has a larger thickness at the periphery than at the center, resulting in a concave shape), the pressure applied to the center of the wafer by the member holding the wafer can be relatively small.

<第3工程>
第3工程では、上記第2工程で決定した初期研磨条件に基づき活性層を研磨しつつ、活性層における中央部及び外周部の膜厚を研磨中に複数回測定して、研磨中での凹凸指数を計算する。例えば特許文献2に例示される測定機構を用いれば、このような研磨中の測定を行うことができる。
<3rd process>
In the third step, the active layer is polished based on the initial polishing conditions determined in the second step, and the thicknesses of the central and peripheral portions of the active layer are measured multiple times during the polishing process to calculate the roughness index during the polishing process. For example, the measurement mechanism illustrated in Patent Document 2 can be used to perform such measurements during the polishing process.

膜厚測定精度の観点からは、より正確な平均値を得るために、中央部及び外周部でそれぞれ2回以上測定することが好ましい。一方で、膜厚測定の際には研磨も同時進行してしまうこともあり、正確性、迅速性の観点から、凹凸指数を計算するための中央部及び外周部の各部の膜厚の測定回数は少ない方がよく、後述するとおり研磨ヘッドがSOIウェーハの直径分の距離を行き来する一周期の揺動を完了するまでに測定される回数とすることができる。一周期の揺動で中央部と外周部は各2度通過するため、それぞれで複数回の測定が行われる。 From the perspective of film thickness measurement accuracy, it is preferable to measure the center and outer periphery at least twice each to obtain a more accurate average value. However, since polishing may also be carried out simultaneously when film thickness is measured, from the perspective of accuracy and speed, it is better to measure the film thickness at each of the center and outer periphery the fewer times to calculate the unevenness index. As described below, this can be the number of measurements taken until the polishing head completes one oscillation cycle, traveling a distance equal to the diameter of the SOI wafer. Since the center and outer periphery are each passed over twice during one oscillation cycle, multiple measurements are taken at each.

<第4工程>
第4工程では、研磨中の凹凸指数の絶対値が目標値以下となったときに、第2工程で決定した初期研磨条件での研磨を終了する。なお、特定条件を満足した場合に加工を終えることは終点検知とも呼ばれる。終点検知の判定条件となる本工程での目標値は適宜定めればよい。研磨装置の加工精度によっても異なるものの、絶対値で0μmに近い値を目標値に設定した場合、研磨中に目標値を検知できず過剰に研磨するおそれがあり、過剰な研磨の進行に伴い膜厚の形状は悪化し凹凸指数が目標値に収束しないため、目標値は100分の数μm程度とすることが好ましい。前述の予備実験を用いて説明したとおり、研磨中の凹凸指数の絶対値が目標値以下となっていれば、活性層の凹凸を十分に解消して膜厚レンジを小さくできたと判断できる。
<4th step>
In the fourth step, when the absolute value of the roughness index during polishing falls below the target value, polishing is terminated under the initial polishing conditions determined in the second step. The completion of processing when specific conditions are satisfied is also referred to as end-point detection. The target value in this step, which serves as the determination condition for end-point detection, can be appropriately determined. Although this will vary depending on the processing accuracy of the polishing machine, if the target value is set to an absolute value close to 0 μm, there is a risk that the target value cannot be detected during polishing and excessive polishing will occur. As excessive polishing progresses, the film thickness shape will deteriorate and the roughness index will not converge to the target value. Therefore, it is preferable to set the target value to approximately a few hundredths of μm. As explained using the preliminary experiment above, if the absolute value of the roughness index during polishing falls below the target value, it can be determined that the roughness of the active layer has been sufficiently eliminated and the film thickness range has been narrowed.

<第5工程>
そこで、続く第5工程では活性層の中央部と外周部の膜厚平均値が目標厚みに到達するまで、仕上げ研磨条件に基づき活性層を研磨する。第5工程では凹凸指数を計算する必要はないが、引き続き研磨を続けながら活性層の膜厚を測定しながら研磨を進める。
<5th step>
Therefore, in the subsequent fifth step, the active layer is polished under the finish polishing conditions until the average film thickness of the central and peripheral parts of the active layer reaches the target thickness. Although it is not necessary to calculate the roughness index in the fifth step, polishing is continued while measuring the film thickness of the active layer.

ここで、仕上げ研磨条件は通常、初期研磨条件とは異なる。仕上げ研磨条件は、初期研磨条件を用いた研磨により活性層の凹凸が除去、あるいは少なくとも緩和された状態のSOIウェーハの活性層に対し、膜厚の凹凸傾向を概ね維持したまま活性層の中央部と外周部の膜厚平均値が目標厚みに到達するまで研磨する条件である。研磨装置の特性に応じて加圧分布を設定すればよく、ウェーハ中央部及び外周部の加圧分布を均等にしてもよいし、装置傾向に応じて調整を加えるなどすることも好ましい。一般的には、研磨開始前の凹凸指数が正の値(中央部凸型)であれば初期研磨条件ではウェーハ中央部の加圧を比較的大きくし、仕上げ研磨条件ではウェーハ中央部の加圧を初期研磨条件よりも小さくすればよい。反対に、研磨開始前の凹凸指数が負の値(中央部凹型)であれば、初期研磨条件ではウェーハ外周部の加圧を比較的大きくし、仕上げ研磨条件ではウェーハ外周部の加圧を初期研磨条件よりも小さくすればよい。第5工程による活性層の研磨取り代は、所望の仕上げ研磨後の活性層の膜厚と、研磨開始前の膜厚と、第3工程から第4工程までの研磨取り代に応じて定まる。 The finish polishing conditions are typically different from the initial polishing conditions. The finish polishing conditions are used to polish the active layer of an SOI wafer, after the initial polishing conditions have removed or at least reduced the active layer irregularities, until the average film thickness of the active layer at the center and periphery reaches the target thickness while roughly maintaining the film thickness irregularity trend. The pressure distribution can be set according to the characteristics of the polishing equipment. The pressure distribution at the center and periphery of the wafer can be uniform, or it is preferable to make adjustments based on the equipment characteristics. Generally, if the irregularity index before polishing is positive (convex center), the initial polishing conditions should apply a relatively high pressure at the wafer center, while the finish polishing conditions should apply a lower pressure at the wafer center than the initial polishing conditions. Conversely, if the irregularity index before polishing is negative (concave center), the initial polishing conditions should apply a relatively high pressure at the wafer periphery, while the finish polishing conditions should apply a lower pressure at the wafer periphery than the initial polishing conditions. The polishing amount of the active layer in the fifth step is determined based on the desired film thickness of the active layer after finish polishing, the film thickness before polishing begins, and the polishing amount from the third step to the fourth step.

以上のとおり、本発明に従う片面研磨方法では研磨中に凹凸指数を計算して、目標とする凹凸指数を初期段階での終点検知に用い、続く仕上げ研磨条件での研磨を行うため、活性層の膜厚レンジを従来技術で達成できる水準よりも小さくすることができる。 As described above, the single-sided polishing method according to the present invention calculates the roughness index during polishing, uses the target roughness index to detect the endpoint at an early stage, and then performs polishing under finish polishing conditions, thereby making it possible to narrow the film thickness range of the active layer compared to the level achievable with conventional technology.

<指数矯正関係>
また、本発明に係るSOIウェーハの片面研磨方法において、活性層の膜厚分布をさらに均一化するために、活性層が受ける径方向加圧分布と、凹凸指数の矯正力との関係を予め求めておくことが好ましい。この関係を「指数矯正関係」と以下では称し、図3にその一例を示す。図3Aでは、外周部の膜厚の方が大きいSOIウェーハ(膜厚凹形状ウェーハ)に対して研磨装置の外周部の圧力を変えていった場合の凹凸指数の矯正力を示し、図3Bでは中央部の膜厚の方が大きいSOIウェーハ(膜厚凸形状ウェーハ)に対して研磨装置の中央部の圧力を変更した場合の凹凸指数の矯正力を示す。ここで図3において示される「ゾーン1」及び「ゾーン3」は、図4を参照して後述する片面研磨装置の加圧制御室の一部領域を示す名称であり、それぞれ加圧制御室45A、45Cに対応する。矯正力は圧力に対して線形の関係である。そこで、第2工程において、指数矯正関係に基づき研磨開始前の凹凸指数に対応する初期研磨条件を決定すれば、終点検知を行うための精度の良い初期研磨条件を設定することができる。
<Index correction>
In addition, in the single-sided polishing method for SOI wafers according to the present invention, it is preferable to determine in advance the relationship between the radial pressure distribution applied to the active layer and the correction force of the unevenness index in order to further uniformize the film thickness distribution of the active layer. This relationship will be referred to as the "exponential correction relationship" below, and an example is shown in FIG. 3. FIG. 3A shows the correction force of the unevenness index when the pressure at the outer periphery of the polishing apparatus is changed for an SOI wafer with a larger film thickness at the periphery (a wafer with a concave film thickness), while FIG. 3B shows the correction force of the unevenness index when the pressure at the center of the polishing apparatus is changed for an SOI wafer with a larger film thickness at the center (a wafer with a convex film thickness). Here, "Zone 1" and "Zone 3" shown in FIG. 3 are names indicating partial regions of the pressure control chamber of the single-sided polishing apparatus, which will be described later with reference to FIG. 4, and correspond to pressure control chambers 45A and 45C, respectively. The correction force has a linear relationship with the pressure. Therefore, in the second step, by determining initial polishing conditions corresponding to the unevenness index before the start of polishing based on the exponential correction relationship, accurate initial polishing conditions for endpoint detection can be set.

また、研磨装置はその使用部材の交換直後(部材使用開始時)や交換直前(部材使用末期)かで、同じ加圧条件を用いても得られる研磨取り代は大きく異なりうる。そのため、予め使用部材の使用時期に応じた指数矯正関係を求めておくことで、研磨前のSOIウェーハの活性層の膜厚の凹凸指数に基づいてより正確な初期研磨条件を決定することができ、好ましい。 Furthermore, even if the same pressure conditions are used, the polishing removal amount obtained can vary greatly depending on whether the polishing equipment is used immediately after replacing the components (at the beginning of use) or immediately before replacement (at the end of use). Therefore, it is preferable to determine the index correction relationship in advance according to the time of use of the components, as this allows more accurate initial polishing conditions to be determined based on the unevenness index of the film thickness of the active layer of the SOI wafer before polishing.

なお、上述した実施形態では初期研磨と仕上げ研磨の段階での研磨条件の変更による膜厚レンジの改善を説明したが、段階以上の多段階で研磨条件を変更しても構わない。その際に、最終段階以外は凹凸指数を用いて終点検知することが好ましい。仕上げ状態のみ、ウェーハ全体の厚みを減ずるような片面研磨を行うことが好ましい。 In the above-described embodiment, the film thickness range is improved by changing the polishing conditions in two stages, the initial polishing and the finish polishing. However, the polishing conditions may be changed in multiple stages, such as three or more stages. In this case, it is preferable to detect the end point using the unevenness index except for the final stage. It is preferable to perform single-sided polishing only in the finish state so as to reduce the thickness of the entire wafer.

以下では、本発明に適用可能な具体的態様についてより詳細に説明する。ただし、本発明が以下の具体例に限定されないことは当然に理解される。 Specific embodiments applicable to the present invention are described in more detail below. However, it should be understood that the present invention is not limited to the following specific examples.

<SOIウェーハ>
研磨対象であるSOIウェーハをあらためて説明すると、SOIウェーハは支持基板ウェーハと、支持基板ウェーハの一方の表面に設けられた絶縁層と、絶縁層の表面に設けられた活性層とを有する。ここで、研磨前のSOIウェーハの活性層の膜厚分布は特に限定されないが、一般的にSOIウェーハは、周方向ばらつきよりも径方向ばらつきの方が大きく、径方向に対して一様に増大又は減少していく特徴がある。なお、研磨前のSOIウェーハの全体の厚みは概ね400~1200μm程度である。
<SOI wafer>
To explain the SOI wafer to be polished again, the SOI wafer has a support substrate wafer, an insulating layer provided on one surface of the support substrate wafer, and an active layer provided on the surface of the insulating layer. Here, the film thickness distribution of the active layer of the SOI wafer before polishing is not particularly limited, but generally, SOI wafers have a feature that the radial variation is larger than the circumferential variation, and the thickness increases or decreases uniformly in the radial direction. The total thickness of the SOI wafer before polishing is approximately 400 to 1200 μm.

<<支持基板ウェーハ>>
シリコン単結晶からなる単結晶シリコンウェーハを支持基板ウェーハに用いることができる。単結晶シリコンウェーハは、チョクラルスキー法(CZ法)や浮遊帯域溶融法(FZ法)等により育成された単結晶シリコンインゴットをワイヤーソー等でスライスしたものを使用することができる。また、単結晶シリコンウェーハには炭素および/または窒素が添加されていてもよい。さらに、任意の不純物を添加して、n型またはp型としてもよい。
<<Support substrate wafer>>
A single crystal silicon wafer made of a silicon single crystal can be used as the support substrate wafer. The single crystal silicon wafer can be obtained by slicing a single crystal silicon ingot grown by the Czochralski method (CZ method) or the floating zone melting method (FZ method) using a wire saw or the like. Carbon and/or nitrogen may be added to the single crystal silicon wafer. Furthermore, any impurity may be added to make the wafer n-type or p-type.

<<絶縁層>>
絶縁層は通常、酸化シリコン膜が用いられる。もっとも、絶縁性のある材料であれば他の材料からなる膜を用いても構わない。
<<Insulating layer>>
The insulating layer is usually a silicon oxide film, although films made of other materials may also be used as long as they have insulating properties.

<<活性層>>
活性層は、シリコン単結晶からなる単結晶シリコンウェーハを、絶縁層を介して支持基板ウェーハと貼合せた後、研削するなどして薄膜化したものである。支持基板ウェーハと導電型(p型およびn型)を揃えてもよいし、異ならせても構わない。
<<Active layer>>
The active layer is formed by bonding a single crystal silicon wafer made of single crystal silicon to a support substrate wafer via an insulating layer, and then thinning the wafer by grinding, etc. The conductivity type (p-type or n-type) of the active layer may be the same as or different from that of the support substrate wafer.

(片面研磨装置)
ここで、上述した本発明に係るSOIウェーハの研磨方法に適用可能な片面研磨装置の一例について、図4を参照してその要部を例示説明する。図4におけるSOIウェーハの片面研磨装置の研磨対象は、支持基板ウェーハ11と、支持基板ウェーハ11の一方の表面に設けられた絶縁層12と、絶縁層12の表面に設けられた活性層13とを有するSOIウェーハ10の、活性層13の表面である。そして、このSOIウェーハの片面研磨装置(以下、「片面研磨装置」)は、定盤20と、窓部21と、研磨パッド30と、研磨ヘッド40と、光学式膜厚測定部60と、を備える。そして、光学式膜厚測定部60はさらに光源61とセンサ62を備え、活性層13の少なくとも径方向の膜厚分布を測定し、これに基づき研磨ヘッド40によるSOIウェーハ10への加圧分布を制御して活性層13の表面を研磨する。膜厚分布の測定は、光源61からの測定光60Lの入射光を、光ファイバ63を経由してレンズ65により集光し、定盤20の窓部21を介して測定光60LをSOIウェーハ10の活性層13の露出面に入射することにより行うことができる。
(Single-sided polishing device)
An example of a single-sided polishing apparatus applicable to the above-described SOI wafer polishing method according to the present invention will now be described with reference to Fig. 4 . The object to be polished by the single-sided polishing apparatus for SOI wafers shown in Fig. 4 is the surface of an active layer 13 of an SOI wafer 10, which includes a support substrate wafer 11, an insulating layer 12 provided on one surface of the support substrate wafer 11, and an active layer 13 provided on the surface of the insulating layer 12. This single-sided polishing apparatus for SOI wafers (hereinafter referred to as the "single-sided polishing apparatus") includes a surface plate 20, a window 21, a polishing pad 30, a polishing head 40, and an optical film thickness measurement unit 60. The optical film thickness measurement unit 60 further includes a light source 61 and a sensor 62, and measures the film thickness distribution of the active layer 13 at least in the radial direction. Based on this measurement, the surface of the active layer 13 is polished by controlling the pressure distribution applied to the SOI wafer 10 by the polishing head 40. The film thickness distribution can be measured by collecting the incident light of the measurement light 60L from the light source 61 by a lens 65 via an optical fiber 63, and irradiating the measurement light 60L onto the exposed surface of the active layer 13 of the SOI wafer 10 through the window portion 21 of the surface plate 20.

ここで、定盤20は回転軸25の回転による回転機構を備え、一方研磨ヘッド40は回転機構及び揺動機構を備えることもできる。また、このような装置においては、定盤が回転して光源61の位置と窓部21の位置が重なるタイミングで膜厚が測定されることとなるため、定盤の1回転につき一度、膜厚が測定されることとなる。研磨ヘッド40は光学式膜厚測定部60の測定範囲内で揺動しており、その一周期の揺動でSOIウェーハの測定位置は中心部を通りその直径の長さだけ行き来する。光学式膜厚測定部60により測定された活性層の厚みは研磨ヘッド内蔵の位置センサや図4に図示する外部カメラ70などで得られる測定位置情報と共に記録され、紐づけられる。 Here, the surface plate 20 is equipped with a rotation mechanism that rotates the rotary shaft 25, while the polishing head 40 can also be equipped with a rotation mechanism and an oscillation mechanism. In such an apparatus, the film thickness is measured when the surface plate rotates and the position of the light source 61 overlaps with the position of the window 21, so the film thickness is measured once per rotation of the surface plate. The polishing head 40 oscillates within the measurement range of the optical film thickness measurement unit 60, and with one oscillation cycle, the measurement position of the SOI wafer passes through the center and moves back and forth by the length of its diameter. The thickness of the active layer measured by the optical film thickness measurement unit 60 is recorded and linked to measurement position information obtained by a position sensor built into the polishing head or an external camera 70 shown in Figure 4.

また、片面研磨装置は研磨ヘッド40を備え、研磨ヘッド40によってSOIウェーハ10を保持することができる。この研磨ヘッド40は、ヘッド本体部41と、ヘッド本体部41の下面中央部に設けられ、支持基板ウェーハ11の他方の面(すなわち、絶縁層12とは反対側の面)を吸着可能なバッキングプレート43を有する。また、研磨ヘッド40には、研磨中のSOIウェーハ10の飛び出しを防止するためのリテーナリング47を設けてもよい。そして、ヘッド本体部41はこのバッキングプレート43を介して径方向に加圧分布を設定可能な加圧制御室45(45A、45B、45C)え、45A~Cに対応する領域を、それぞれゾーン1~3などと呼ぶことがある。なお、図4では、径方向に対称に配置された圧力制御室45A、45B、45Cが加圧制御室45を構成する場合を図示するものであるが、これは例示に過ぎない。2以上の圧力制御室があれば加圧分布を設定することは可能である。圧力制御室45A、45B、45Cを隔壁膜などにより区分することができ、加圧空気などの流体によって各圧力制御室の加圧力を制御することで、活性層の膜厚分布を均一化することができる。 The single-sided polishing apparatus also includes a polishing head 40, which can hold the SOI wafer 10. The polishing head 40 includes a head main body 41 and a backing plate 43, which is provided in the center of the underside of the head main body 41 and can adsorb the other side of the support substrate wafer 11 (i.e., the side opposite the insulating layer 12). The polishing head 40 may also be provided with a retainer ring 47 to prevent the SOI wafer 10 from popping out during polishing. The head main body 41 includes pressure control chambers 45 (45A, 45B, 45C ) that can set a pressure distribution in the radial direction via the backing plate 43. The regions corresponding to 45A to 45C are sometimes referred to as zones 1 to 3, respectively. Note that FIG. 4 illustrates a case in which the pressure control chamber 45 is made up of pressure control chambers 45A, 45B, and 45C arranged symmetrically in the radial direction, but this is merely an example. It is possible to set a pressure distribution if there are two or more pressure control chambers. The pressure control chambers 45A, 45B, and 45C can be separated by partition membranes or the like, and the film thickness distribution of the active layer can be made uniform by controlling the pressure in each pressure control chamber with a fluid such as pressurized air.

以下、実施例を用いて本発明をさらに詳細に説明するが、本発明は以下の実施例に何ら限定されるものではない。なお、下記の実施例1及び比較例1における凹凸指数の計算は上述した点平均凹凸指数の計算方法を用いた。 The present invention will be explained in more detail below using examples, but the present invention is not limited to the following examples. Note that the calculation of the unevenness index in Example 1 and Comparative Example 1 below was performed using the method for calculating the point-average unevenness index described above.

(実施例1)
図4を参照して説明した片面研磨装置を用いて、直径200mmの1枚のSOIウェーハの片面研磨を行った。まず、径方向膜厚分布として活性層の全面の膜厚分布を測定し、測定結果に基づき凹凸指数を計算したところ、0.4μmであった。得られた膜厚分布を図5Aに示す。凹凸指数が正の値であったので、段階目の研磨では外周部よりも中央部の取り代が大きくなるよう初期研磨条件を設定する必要がある。初期研磨条件及び仕上げ研磨条件の径方向加圧分布を表1のとおりとし、特に初期研磨条件におけるゾーン3の圧力を5.3psiとした。なお、この加圧分布は図4に示した3つの加圧制御室の径方向の
圧力分布であり、ゾーン3は中心位置含む中央部の加圧制御室に対応する。
Example 1
Using the single-sided polishing apparatus described with reference to FIG. 4, a single-sided polishing of a 200 mm diameter SOI wafer was performed. First, the film thickness distribution across the entire active layer was measured as the radial film thickness distribution. The unevenness index was calculated based on the measurement results and was found to be 0.4 μm. The resulting film thickness distribution is shown in FIG. 5A. Because the unevenness index was a positive value, the initial polishing conditions must be set so that the removal rate in the central portion is greater than that in the peripheral portion in the first stage of polishing. The radial pressure distribution for the initial polishing conditions and the finish polishing conditions was as shown in Table 1. In particular, the pressure in Zone 3 under the initial polishing conditions was set to 5.3 psi. Note that this pressure distribution is the radial pressure distribution of the three pressure control chambers shown in FIG. 4, and Zone 3 corresponds to the central pressure control chamber including the center position.

次に、凹凸指数の目標値を0.04μmとして、凹凸指数を測定しつつ、目標値に到達するまで、決定した初期研磨条件としての径方向の加圧分布で活性層を研磨した。このとき一回の凹凸指数を計算するにあたり、中央部の膜厚及び外周部の膜厚をそれぞれ2回ずつ測定した。そして、凹凸指数が目標値の0.04μm以下となった時点で、初期研磨条件での研磨を終了した。初期研磨条件での研磨における研磨取り代は1.0μmであった。 Next, the target value for the unevenness index was set to 0.04 μm, and the active layer was polished using the radial pressure distribution determined as the initial polishing conditions while measuring the unevenness index until the target value was reached. To calculate one unevenness index, the film thickness at the center and the film thickness at the outer periphery were each measured twice. When the unevenness index reached the target value of 0.04 μm or less, polishing under the initial polishing conditions was terminated. The polishing stock removal under the initial polishing conditions was 1.0 μm.

さらに、凹凸を除去した初期研磨に引き続き、仕上げ研磨条件で、この膜厚形状を維持したまま活性層の中央部と外周部の膜厚平均値が目標厚みに到達するまで研磨した。このとき、終点検知としては、仕上げ研磨中常時膜厚を測定し、研磨ヘッドが一周期の揺動を完了するまでに測定された中央部と外周部の膜厚値で算出した平均値を用いた。仕上げ研磨条件としての径方向の加圧分布を表1に示す。仕上げ研磨条件での研磨における研磨取り代は1.0μmであった。仕上げ研磨後の膜厚分布を図5Aに示す。 Following the initial polishing to remove any irregularities, polishing was continued under finish polishing conditions while maintaining this film thickness profile until the average film thickness at the center and periphery of the active layer reached the target thickness. The endpoint was determined by constantly measuring the film thickness during finish polishing, and using the average film thickness measured at the center and periphery until the polishing head completed one oscillation cycle. The radial pressure distribution under the finish polishing conditions is shown in Table 1. The polishing stock removal during polishing under the finish polishing conditions was 1.0 μm. The film thickness distribution after finish polishing is shown in Figure 5A.

(比較例1)
次に、直径が200mmのSOIウェーハであって、活性層の膜厚分布を測定した際の凹凸指数が実施例1と同じであるウェーハに対し、初期研磨条件として実施例1と同じ径方向の加圧分布を採用し、研磨途中において凹凸指数を測定することなく、目標厚みになるまでで研磨を完了した。なお、比較例1の研磨開始前の凹凸指数は実施例1と同
じであるが、膜厚分布は図5Bのとおり、図5Aで示す実施例1の膜厚分布とは異なる。このときの、初期研磨条件での研磨における研磨取り代は2.5μmであった。研磨完了
後の膜厚分布を図5Bに示す。
(Comparative Example 1)
Next, for an SOI wafer having a diameter of 200 mm and having the same roughness index as in Example 1 when measuring the film thickness distribution of the active layer, the same radial pressure distribution as in Example 1 was adopted as the initial polishing conditions, and polishing was completed in one step until the target thickness was reached without measuring the roughness index during polishing. Note that the roughness index before polishing in Comparative Example 1 was the same as in Example 1, but the film thickness distribution, as shown in Figure 5B, differs from the film thickness distribution in Example 1 shown in Figure 5A. In this case, the polishing stock removal during polishing under the initial polishing conditions was 2.5 μm. The film thickness distribution after polishing was completed is shown in Figure 5B.

実施例1及び比較例1による片面研磨を行う前後での径方向膜厚分布を図5A、図5Bのそれぞれに示し、各凹凸指数及び膜厚レンジを表2に示す。比較例1の研磨後の凹凸指数が-0.1μmであるのに対して、実施例1の凹凸指数は0.04μmであり、実施例1において研磨後の活性層の膜厚分布を均一化できていることが確認できた。 Figures 5A and 5B show the radial film thickness distribution before and after single-sided polishing in Example 1 and Comparative Example 1, respectively, and Table 2 shows the respective unevenness indices and film thickness ranges. While the unevenness indices after polishing in Comparative Example 1 were -0.1 μm, the unevenness indices in Example 1 were 0.04 μm, confirming that Example 1 achieved a uniform film thickness distribution for the active layer after polishing.

実施例1及び比較例1において測定した、研磨前及び研磨後の活性層の膜厚の変動幅を図6A、図6Bのそれぞれに示す。膜厚の変動幅とは、目標厚みと膜厚測定値の厚み誤差([膜厚測定値-目標厚み])を表す。なお、これらグラフは、実施例1及び比較例1のそれぞれのSOIウェーハの全面における膜厚の測定値を各点毎にプロットしたものであり、それぞれ1枚のSOIウェーハから得た測定値である。図6Aは研磨前の膜厚分布の変動幅を示し、図6Bは研磨後の膜厚の変動幅を示す。研磨前の膜厚分布の変動幅には有意差といえるほどの差はなかったものの、研磨後の活性層の膜厚分布の変動幅を実施例1と比較例1とで比較すると、実施例1の方が膜厚の変動幅の方が小さく、大幅な膜厚精度の向上を確認することができた。なお、活性層の膜厚の変動幅における標準偏差は、実施例1では0.04μmであり、比較例1では0.08μmであった。 The fluctuation range of the active layer film thickness measured in Example 1 and Comparative Example 1 before and after polishing is shown in Figures 6A and 6B, respectively. The fluctuation range of the film thickness represents the thickness error between the target thickness and the measured film thickness ([measured film thickness - target thickness]). These graphs plot the measured film thickness values over the entire surface of each SOI wafer in Example 1 and Comparative Example 1 at each point, and each represents a measurement value obtained from a single SOI wafer. Figure 6A shows the fluctuation range of the film thickness distribution before polishing, and Figure 6B shows the fluctuation range of the film thickness after polishing. Although there was no significant difference in the fluctuation range of the film thickness distribution before polishing, when the fluctuation range of the active layer film thickness distribution after polishing was compared between Example 1 and Comparative Example 1, the film thickness fluctuation range was smaller in Example 1, confirming a significant improvement in film thickness accuracy. The standard deviation of the fluctuation range of the active layer film thickness was 0.04 μm in Example 1 and 0.08 μm in Comparative Example 1.

本発明によれば、活性層の膜厚分布をより均一化できるSOIウェーハの片面研磨方法を提供することができる。 The present invention provides a method for polishing one side of an SOI wafer that can achieve a more uniform film thickness distribution in the active layer.

10 SOIウェーハ
20 定盤
21 窓部
25 回転軸
30 研磨パッド
40 研磨ヘッド
41 ヘッド本体部
43 バッキングプレート
45 加圧制御室
60 光学式膜厚測定部
65 レンズ
70 外部カメラ
REFERENCE SIGNS LIST 10 SOI wafer 20 surface plate 21 window portion 25 rotation shaft 30 polishing pad 40 polishing head 41 head main body portion 43 backing plate 45 pressure control chamber 60 optical film thickness measurement portion 65 lens 70 external camera

Claims (3)

SOIウェーハの活性層の膜厚分布を測定しながら前記活性層を研磨するSOIウェーハの片面研磨方法であって、
研磨開始前の前記活性層の膜厚分布を測定して、前記研磨開始前における前記活性層の前記膜厚分布に基づき、前記活性層の中央部及び外周部のそれぞれの厚み平均の差である凹凸指数を計算する第1工程と、
前記研磨開始前の前記凹凸指数に基づき初期研磨条件の径方向加圧分布を決定する第2工程と、
前記初期研磨条件に基づき前記活性層を研磨しつつ、前記活性層における中央部及び外周部の膜厚を研磨中に複数回測定して、研磨中での前記凹凸指数を計算する第3工程と、
前記研磨中の前記凹凸指数の絶対値が目標値以下となったときに前記初期研磨条件での研磨を終了する第4工程と、
前記活性層の中央部と外周部の膜厚平均値が目標厚みに到達するまで、仕上げ研磨条件に基づき前記活性層を研磨する第5工程と、を含み、
前記第5工程では、前記第4工程における前記活性層の膜厚形状を維持するよう、前記仕上げ研磨条件の径方向加圧分布を設定する、SOIウェーハの片面研磨方法。
1. A method for polishing a single side of an SOI wafer, comprising: polishing an active layer of the SOI wafer while measuring a film thickness distribution of the active layer;
a first step of measuring a film thickness distribution of the active layer before the start of polishing, and calculating an unevenness index , which is a difference between the average thicknesses of a central portion and an average thickness of an outer periphery of the active layer, based on the film thickness distribution of the active layer before the start of polishing;
a second step of determining a radial pressure distribution of an initial polishing condition based on the unevenness index before the start of polishing;
a third step of measuring the film thicknesses of the central and peripheral portions of the active layer multiple times during polishing while polishing the active layer based on the initial polishing conditions, and calculating the unevenness index during polishing;
a fourth step of terminating polishing under the initial polishing conditions when the absolute value of the unevenness index during polishing becomes equal to or less than a target value;
a fifth step of polishing the active layer under finish polishing conditions until an average film thickness of the central portion and the outer periphery of the active layer reaches a target thickness;
In the fifth step, a radial pressure distribution of the finish polishing conditions is set so as to maintain the film thickness profile of the active layer in the fourth step .
前記第3工程において、前記中央部及び外周部での膜厚の測定回数は研磨ヘッドが一周期の揺動を完了するまでに測定される回数である、請求項1に記載のSOIウェーハの片面研磨方法。 The method for single-sided polishing of an SOI wafer according to claim 1, wherein in the third step, the film thickness at the central and peripheral portions is measured the number of times until the polishing head completes one oscillation cycle. 研磨時に前記活性層が受ける径方向加圧分布と、前記凹凸指数の矯正力との指数矯正関係をあらかじめ求めておき、前記第2工程では、前記指数矯正関係に基づき前記研磨開始前の前記凹凸指数に対応する前記初期研磨条件の径方向加圧分布を決定する、請求項1又は2に記載のSOIウェーハの片面研磨方法。 3. The method for single-sided polishing of an SOI wafer according to claim 1, wherein an exponential correction relationship between a radial pressure distribution received by the active layer during polishing and a correction force for the unevenness index is determined in advance, and in the second step, the radial pressure distribution of the initial polishing conditions corresponding to the unevenness index before the start of polishing is determined based on the exponential correction relationship.
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JP2004022839A (en) 2002-06-17 2004-01-22 Sumitomo Mitsubishi Silicon Corp SOI substrate polishing method and apparatus
US20130288571A1 (en) 2012-04-25 2013-10-31 Jeffrey Drue David Feed forward and feed-back techniques for in-situ process control
JP2015070013A (en) 2013-09-27 2015-04-13 株式会社Sumco Manufacturing method of SOI wafer
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