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JPS5835674B2 - A method of brewing sake, etc., in which lipase is added during soaking of rice. - Google Patents
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JPS5835674B2 - A method of brewing sake, etc., in which lipase is added during soaking of rice. - Google Patents

A method of brewing sake, etc., in which lipase is added during soaking of rice.

Info

Publication number
JPS5835674B2
JPS5835674B2 JP51070429A JP7042976A JPS5835674B2 JP S5835674 B2 JPS5835674 B2 JP S5835674B2 JP 51070429 A JP51070429 A JP 51070429A JP 7042976 A JP7042976 A JP 7042976A JP S5835674 B2 JPS5835674 B2 JP S5835674B2
Authority
JP
Japan
Prior art keywords
rice
sake
lipase
brewing
fatty acids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP51070429A
Other languages
Japanese (ja)
Other versions
JPS52154597A (en
Inventor
淑 吉沢
雄章 石川
元宏 池見
喜久雄 野白
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KOKUZEICHO CHOKAN
Original Assignee
KOKUZEICHO CHOKAN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by KOKUZEICHO CHOKAN filed Critical KOKUZEICHO CHOKAN
Priority to JP51070429A priority Critical patent/JPS5835674B2/en
Publication of JPS52154597A publication Critical patent/JPS52154597A/en
Publication of JPS5835674B2 publication Critical patent/JPS5835674B2/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L7/00Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10Cereal-derived products
    • A23L7/104Fermentation of farinaceous cereal or cereal material; Addition of enzymes or microorganisms

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Cereal-Derived Products (AREA)
  • Alcoholic Beverages (AREA)

Description

【発明の詳細な説明】 本発明は、清酒等酒類の原料米の浸漬水にリパゼを添加
して米を浸漬し、その中に含1れる脂肪酸、%にもろみ
での香気成分である芳香性エステルの生成を妨げる不飽
和脂肪酸を減少せしめた蒸米を調製し、それを用いて香
味の良い清酒等の酒類を製造する方法lこ関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention involves adding lipase to the soaking water of rice as a raw material for alcoholic beverages such as sake, and soaking the rice. This invention relates to a method for preparing steamed rice with reduced unsaturated fatty acids that inhibit ester production and using it to produce alcoholic beverages such as sake with good flavor.

現在、米を原料とする酒類、例えば清酒や合成清酒の製
造には清米歩合70多程度の高精白米が用いられるが、
この理由は玄米の外層部に多く含1れ、酒造上有害とさ
れる脂質、灰分、たん白質を減少させ、良質の酒類を得
ること(こある。
Currently, highly polished rice with a refined rice ratio of about 70 is used to produce alcoholic beverages made from rice, such as sake and synthetic sake.
The reason for this is to reduce fat, ash, and protein, which are found in large amounts in the outer layer of brown rice and are considered harmful to sake brewing, and to obtain high-quality alcoholic beverages.

一般に、玄米には2係以上の脂質が含1れ、その大部分
は芽を含む外層に多く、内部は少ない。
In general, brown rice contains lipids of factor 2 or higher, most of which are present in the outer layer, including the sprouts, and less in the interior.

その構成脂肪酸はリノール酸、オレイン酸を主体とした
不飽和脂肪酸が多いが、内層程不飽和酸は減少し、パル
ミチン酸等飽和脂肪酸が多くなっている〔日本農芸化学
会誌、47巻、713(1973)〕。
Its constituent fatty acids are mainly unsaturated fatty acids such as linoleic acid and oleic acid, but as the inner layer approaches, unsaturated acids decrease and saturated fatty acids such as palmitic acid increase [Journal of the Japanese Society of Agricultural Chemistry, Vol. 47, 713 ( 1973)].

そして、清酒の重要な香気成分である酢酸イソアミル等
のエステルは酵母lこより生成されるが、飽和脂肪酸に
より生成は促進され、不飽和脂肪酸により強く抑えられ
る。
Ester such as isoamyl acetate, which is an important aroma component of sake, is produced by yeast, but its production is promoted by saturated fatty acids and strongly suppressed by unsaturated fatty acids.

従って、もろみ中の脂肪酸の大部分が原料米に由来する
清酒醸造では不飽和脂肪酸を多く除いた高精白米を用い
ることが香の良い清酒を醸造する要件となっている〔日
本農芸化学会誌、50巻、115(1976)、l。
Therefore, in sake brewing, where most of the fatty acids in mash are derived from raw rice, it is necessary to use highly polished rice with a large amount of unsaturated fatty acids removed in order to brew sake with a good aroma [Journal of the Japanese Society of Agricultural Chemistry, 50, 115 (1976), l.

しかしながら、香の良い清酒を醸造するためにすべての
醸造米を高度に精白すると、例えば5割搗で米は半分(
こなってし1うように、清酒の醸造(こ大量の米を必要
とするようになり、ひいては清酒の価格が著るしく高い
ものになってし1う。
However, in order to brew fragrant sake, if all the brewed rice is polished to a high degree, for example, if 50% of the rice is milled, the rice will be half (
As a result, the brewing of sake began to require a large amount of rice, which in turn caused the price of sake to become extremely high.

本発明者らは、一般の清酒醸造(こおいて香味の良い清
酒を醸造するために研究を進めたところ、原料米の浸漬
時にリパーゼを添加すること(こより解決することがで
きた。
The present inventors conducted research to brew sake with a good flavor using general sake brewing, and were able to solve the problem by adding lipase to the raw rice during soaking.

本発明においては、原料米の浸漬水中にリパーゼを添加
して原料米を浸漬すればよい。
In the present invention, the raw rice may be soaked by adding lipase to the water in which the raw rice is soaked.

リパーゼの量はごく微量から大量添加1で格別の差異は
ないが、白米1kq(tこ対し力価1〜5×103単位
が好ましい。
There is no particular difference in the amount of lipase added from a very small amount to a large amount of 1, but a titer of 1 to 5 x 103 units per 1 kq (t) of polished rice is preferred.

しかし、特に粗白米やもち米、ビール醸造等fこ用いら
れる砕米や米ぬか、米粉等の処理に当っては適宜使用量
を変更する必要があり、また、浸漬時間が極端(こ短か
い場合や浸漬温度が5℃以下と極度に低い場合などもリ
パーゼの量は適宜増加させなければならない。
However, especially when processing coarse white rice, glutinous rice, broken rice, rice bran, rice flour, etc. used in beer brewing, etc., it is necessary to change the amount used appropriately, and the soaking time is extremely short (sometimes too short). Even when the soaking temperature is extremely low, such as 5° C. or lower, the amount of lipase must be increased appropriately.

原料米の浸漬は3〜4時間から長い場合で10〜20時
間行なわれるが、3〜4時間でほとんど吸水が完了し、
その間(こりパーゼは米粒の表面から浸透し、脂質に作
用し、遊離の脂肪酸を生成せしめる。
The raw rice is soaked for 3 to 4 hours, sometimes for 10 to 20 hours, but most of the water absorption is completed within 3 to 4 hours.
During that time (kori pase penetrates through the surface of the rice grain, acts on the lipids, and generates free fatty acids.

米粒の表面に近いほど不飽和脂肪酸の脂質が多いため、
本発明では効率的に不飽和脂肪酸を遊離の状態とするこ
とができるのである。
Because the closer to the surface of the rice grain there are more unsaturated fatty acids,
In the present invention, unsaturated fatty acids can be efficiently liberated.

浸漬が終了し、リパーゼ処理された浸漬米は、蒸きより
処理されるが、この蒸きょうによって米粒で遊離となっ
た脂肪酸、特(こ不飽和脂肪酸は分解乃至は揮散させら
れ、米粒中の不飽和脂肪酸の量を著るしく低減せしめる
ことができる。
After soaking is completed, the soaked rice that has been treated with lipase is steamed, and the steaming process decomposes or volatilizes the fatty acids, especially unsaturated fatty acids, that are liberated in the rice grains. The amount of unsaturated fatty acids can be significantly reduced.

そして、この蒸きょうによって添加したリパーゼは完全
に失活させられ、もろみ中に移行することはない。
The added lipase is completely inactivated by this steaming and does not migrate into the mash.

本発明の方法は、浸漬水にリパーゼを添加して原料米を
リパーゼ処理し、原料米の不飽和脂肪酸含量を著るしく
低減させることに成功し、ひいては香味の良い清酒を醸
造することができたものである。
In the method of the present invention, lipase is added to the soaking water to treat the raw rice with lipase, and the unsaturated fatty acid content of the raw rice is successfully reduced significantly, thereby making it possible to brew sake with good flavor. It is something that

本発明の方法は、精米歩合70φ程度の通常の清酒醸造
用白米に用いて極めて良好な結果を得られるが、特(こ
脂質含量の高い精米歩合75φ以上の粗白米を処理する
ことにより精米歩合70多以下の高精白米を用いた清酒
の香味に近い清酒が製造できる等時をこ良好な結果が得
られ、清酒製造コストの60多以上を占める米の利用率
を上げることによりコストを大きく下げることができる
ものであり、捷た、軍法によるもろみは対照に比べて米
の消化、酵母の発酵が良く、もろみ日数が短縮されるこ
とが多い。
The method of the present invention can obtain very good results when used with ordinary white rice for sake brewing with a milling ratio of about 70φ, but it can be used to improve the polishing ratio by treating coarse white rice with a polishing ratio of 75φ or more that has a high lipid content. Good results can be obtained by producing sake with a flavor similar to that of refined sake using highly polished rice of 70% or less, and costs can be increased by increasing the utilization rate of rice, which accounts for 60% or more of the sake production cost. Compared to the control, rice is digested better, yeast ferments better, and the number of days required for mashing is often shortened.

試験例 精米歩合75φの原料米(銘柄:日本晴)を1、Ohづ
つ用意し、2を容浸漬槽3ヶに1tづつ水を入れ、それ
ぞれ仕込16.1 、 A 2 、 A 3とし、A2
にのみリパーゼ(3X10’単位/グ)を50■添加し
た。
Test Example Prepare raw rice (Brand: Nipponbare) with a rice polishing ratio of 75 φ in 1 and 2 Ohms, and put 1 ton of water into 3 soaking tanks, and make the preparations 16.1, A 2, and A 3, respectively.
Only 50 μ of lipase (3×10′ units/g) was added.

仕込Alは対照として、6時間原料米を浸漬し、後蒸き
ようし、常法により清酒を醸造した。
As a control for the preparation Al, raw rice was soaked for 6 hours, post-steamed, and sake was brewed in a conventional manner.

仕込履2は、6時間原料米をリパーゼ添加水中に浸漬し
、後蒸きようし、常法により清酒を醸造した。
For preparation 2, raw rice was soaked in lipase-added water for 6 hours, then steamed, and sake was brewed in a conventional manner.

仕込A3は、6時間原料米を浸漬し、後蒸きようし、常
法により清酒を醸造したが、その間、留後3日目にもろ
みにリパーゼ(3X10’単位/グ)50■を添加した
For preparation A3, raw rice was soaked for 6 hours, and then steamed and brewed using the conventional method. During this period, 50 μm of lipase (3 x 10' units/g) was added to the mash on the 3rd day after distillation. .

以上の仕込Al 、 A、2 、 A3 &こついて、
留後18日目のもろみ中の各脂肪酸含量をそれぞれ測定
し、かつ、これより常法により裂取した清酒の品質を分
析した。
The above preparation Al, A, 2, A3 & stuck,
The content of each fatty acid in the mash was measured on the 18th day after distillation, and the quality of the sake separated from this by a conventional method was analyzed.

その結果は次の各表に示される。The results are shown in the following tables.

次(こ本発明の実施例を示す。The following is an example of the present invention.

実施例 1゜ 新潟県産越路早生(精米歩合75%)100f’を洗米
後、それぞれリパーゼ100単位、2,000単位を溶
解した水中に15℃、20時間浸漬し、次いで30分間
蒸きようして蒸米を調製し、その粗脂肪含量、脂肪酸組
成を対照と比較した結果は次の表に示すと釦りで、リパ
ーゼ処理試料は浸漬、蒸きよう後いずれも粗脂肪含量が
低下し、特にり**ノール酸の減少が大きい。
Example 1 After washing 100f' of Koshiji Wase from Niigata Prefecture (polishing ratio 75%), it was soaked in water containing 100 units of lipase and 2,000 units of lipase for 20 hours at 15°C, and then steamed for 30 minutes. The results of comparing the crude fat content and fatty acid composition of the steamed rice prepared with the control are shown in the table below. **The decrease in nolic acid is large.

実施例 2゜ 越路早生精米歩合70%1本と80多2本それぞれ総米
400kqの清酒仕込を行い、80多の1本は米の浸漬
水(こ白米1を当り50fのリパーゼ(力価3X10’
単位/1)を添加して浸漬処理を行った。
Example 2゜One bottle of Koshiji Wase with a 70% polishing ratio and two bottles of 80 tai were used to prepare sake with a total of 400 kq of rice. '
Unit/1) was added and immersion treatment was performed.

結果は次の表に示すとかりて、もろみ日数は精米歩合7
0多仕込1の20田こ対し、精米歩合80%仕込2が1
5日と短かく、リパーゼ処理仕込3では14日と更に1
日短縮された。
The results are shown in the table below.
For 20 rice fields with 0 and 1 rice polishing ratio, 80% rice polishing 2 is 1
It is as short as 5 days, and for lipase treatment preparation 3 it takes 14 days and an additional 1 day.
day was shortened.

製成酒の暉1酒結果ば1が最も良く、次いで3,2の順
となり、特に3は香が高く、酢酸イ゛ノアミル含量が高
く、リパーゼ処理によりもろみ日数が短縮されると同時
に粗白米仕込の酒質を高精白米に近付けることができた
According to the results of sake production, 1 is the best, followed by 3 and 2. In particular, 3 has a high aroma, a high content of ionamyl acetate, and the lipase treatment shortens the time required for mashing, and at the same time improves the quality of coarse white rice. We were able to bring the quality of the brewed sake closer to that of highly polished white rice.

実施例 3゜ 麹米70多、揚米75多と異なる精米歩合のニホンバレ
2.8を仕込2本と揚米の浸漬Gこ実施例2(こ記した
と同様にリパーゼを用いた仕込2本の醸造過程と製成酒
を比較した。
Example 3 Two bottles of Nihonbare 2.8 with a different rice polishing ratio of 70% koji rice and 75% aged rice and soaked aged rice Example 2 (2 bottles prepared using lipase in the same way as described here) A comparison was made between the brewing process and the production of sake.

結果は次の表に示すと釦りで、リパーゼ処理酒はいずれ
も対照に比べ酢酸イソアミル含量が高く、香味が優れて
いた。
The results are shown in the table below: All lipase-treated sake had higher isoamyl acetate content and better flavor than the control.

Claims (1)

【特許請求の範囲】[Claims] 1 原料米の浸漬水にリパーゼを添加して米を浸漬し、
蒸きようし、得られた蒸きよう米を用いて醸造すること
を特徴とする香味の良い清酒等の醸造法。
1 Add lipase to the soaking water of raw rice and soak the rice,
A method of brewing sake, etc. with a good flavor, which is characterized by brewing using steamed soybean flour and the steamed rice obtained.
JP51070429A 1976-06-17 1976-06-17 A method of brewing sake, etc., in which lipase is added during soaking of rice. Expired JPS5835674B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP51070429A JPS5835674B2 (en) 1976-06-17 1976-06-17 A method of brewing sake, etc., in which lipase is added during soaking of rice.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP51070429A JPS5835674B2 (en) 1976-06-17 1976-06-17 A method of brewing sake, etc., in which lipase is added during soaking of rice.

Publications (2)

Publication Number Publication Date
JPS52154597A JPS52154597A (en) 1977-12-22
JPS5835674B2 true JPS5835674B2 (en) 1983-08-04

Family

ID=13431218

Family Applications (1)

Application Number Title Priority Date Filing Date
JP51070429A Expired JPS5835674B2 (en) 1976-06-17 1976-06-17 A method of brewing sake, etc., in which lipase is added during soaking of rice.

Country Status (1)

Country Link
JP (1) JPS5835674B2 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5655192A (en) * 1979-10-08 1981-05-15 Yagi Jozo Kk Production of mineral-containing japanese sake
KR100364452B1 (en) * 2000-08-31 2002-12-16 대한민국 Methods for preparing mash improving flavor by using enzyme preparation
JP2003023982A (en) * 2001-07-11 2003-01-28 Katayama Chem Works Co Ltd Cooked rice with improved variability and method for improving variability of cooked rice
KR100460646B1 (en) * 2001-08-06 2004-12-09 류이하 Estery distilled spirit making with esterification during distillation

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5147230B2 (en) * 1971-08-07 1976-12-14
JPS4961395A (en) * 1972-10-16 1974-06-14

Also Published As

Publication number Publication date
JPS52154597A (en) 1977-12-22

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