JPS6043416B2 - Method for producing cold-rolled steel sheets with excellent workability - Google Patents
Method for producing cold-rolled steel sheets with excellent workabilityInfo
- Publication number
- JPS6043416B2 JPS6043416B2 JP56002730A JP273081A JPS6043416B2 JP S6043416 B2 JPS6043416 B2 JP S6043416B2 JP 56002730 A JP56002730 A JP 56002730A JP 273081 A JP273081 A JP 273081A JP S6043416 B2 JPS6043416 B2 JP S6043416B2
- Authority
- JP
- Japan
- Prior art keywords
- temperature
- solal
- coarse grains
- steel sheets
- excellent workability
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/46—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals
- C21D9/48—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals deep-drawing sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Heat Treatment Of Steel (AREA)
- Heat Treatment Of Sheet Steel (AREA)
Description
【発明の詳細な説明】
本発明は熱延ストリップの巻取方法に関するものであり
、熱延粗大粒の発生を適切に防止することをその目的と
するものである。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for winding a hot-rolled strip, and an object of the present invention is to appropriately prevent the generation of hot-rolled coarse grains.
連続焼鈍法において、深絞り用鋼板を製造する場合、軟
質化及びに値を向上させるために熱延における高速巻取
を実施することは周知の事実てある。It is a well-known fact that when producing a steel plate for deep drawing using a continuous annealing method, high-speed winding is carried out in hot rolling in order to soften the steel sheet and improve the strength.
一方、この巻取温度の設定は一般的に高くなればなるほ
ど軟化することも周知でり、軟質鋼板を得るためには出
来る限りの高温巻取が実施される。この巻取温度を規制
する項目として、1スケール剥離不良による規制、2巻
取、抜き出し時のコイル変形、3熱延粗大粒発生による
品質低下などがあげられる。On the other hand, it is well known that the higher the winding temperature is set, the softer the steel becomes, and in order to obtain a soft steel sheet, winding is performed at the highest temperature possible. Items that regulate the winding temperature include: 1. Regulation due to poor scale peeling, 2. Coil deformation during winding and extraction, and 3. Quality deterioration due to generation of hot rolled coarse grains.
この内1については酸洗前のスキンバス及びロールペン
ディングなどによりほとんど解消される。2の問題につ
いてはコイル変形が問題となる温度はかなり高い温度て
あり、それ以下の温度で十分軟化させることは可能であ
る。Of these, 1 can be almost eliminated by skin bathing and roll pending before pickling. Regarding problem 2, the temperature at which coil deformation becomes a problem is quite high, and it is possible to sufficiently soften the coil at a temperature lower than that.
これに対し3の問題については各種の要素が入り乱れ、
非常に不安定な状態にある。従来これを安定させるため
には、かなりの安全サイドまで温度レベルを下げた運用
がなされており、これが高加工性鋼板製造のネックとな
つていた。このようなことから、連続焼鈍において従来
から高加工性鋼板を製造するために種々の検討がなされ
てきた。On the other hand, regarding problem 3, various factors are mixed,
It is in a very unstable state. Conventionally, in order to stabilize this, the temperature level has been lowered to a considerably safe side, and this has been a bottleneck in the production of highly formable steel sheets. For this reason, various studies have been made in the past in order to produce highly formable steel sheets using continuous annealing.
この高加工性用素材としては鋼種的には時効劣化が少な
く、かつ介在物が少ないため延性(特に2軸延性)の優
れたアルミキルド鋼が主体に考えられている。一方、成
分的には強度を下げに値の向上及び粒成長性向上のため
に〔Mn〕及び〔C〕〔N〕の低下などのアクションが
とられ、結晶粒は大きくなるように考慮されてきた。)
本発明はこのような状況を背景に、さらに研究を重ね
た結果提案されたものであつて、連続焼鈍で高加工性鋼
板を安定して製造するための方法を堤供するものであり
、特に高品質を得るための素材を使用し、十分な巻取温
度て巻取ることによつ5て粗大粒の発生を防止しようと
するものである。As a material for this high workability, aluminum killed steel is mainly considered as a steel type that exhibits less aging deterioration and has excellent ductility (particularly biaxial ductility) because it has few inclusions. On the other hand, in terms of components, actions such as lowering [Mn], [C], and [N] have been taken to reduce strength, improve values, and improve grain growth, and consideration has been given to increasing crystal grain size. Ta. )
Against this background, the present invention was proposed as a result of further research, and it provides a method for stably manufacturing high-formability steel sheets by continuous annealing, and in particular, The purpose is to prevent the generation of coarse grains by using materials with high quality and by winding at a sufficient winding temperature.
以下本発明につき詳細に説明する。一般に、高温巻取時
における粗大粒の発生の主要因は、熱延時及び巻取時に
発生する残留歪が高温下て回復する時に生じる粒成長に
よるものと考えられ、歪が発生しなければ粗大粒は発生
し難いものである。しかし、これらの残留歪を残さない
ようにすることは一般的な製造条件下では非常に難しい
問題であり、その他の条件により防止する必要がある。
そこで、本発明者等は種々の項目について検討した結果
、アルミキルド鋼における粗大粒の発生と成分の間に密
接な関係があることを発見した。The present invention will be explained in detail below. In general, the main cause of the generation of coarse grains during high-temperature coiling is thought to be due to grain growth that occurs when the residual strain generated during hot rolling and coiling recovers at high temperatures. is unlikely to occur. However, preventing these residual strains from remaining is a very difficult problem under typical manufacturing conditions, and it is necessary to prevent them under other conditions.
Therefore, the inventors of the present invention investigated various items and discovered that there is a close relationship between the occurrence of coarse grains and the components in aluminum killed steel.
即ち、アルミキルド鋼の高温巻取における粗大粒の発生
は〔N〕 〔SOlAl〕量に影響を受け、A1一N
の析出物が存在する領域においてはh影響は少ないこと
である。この〔N〕と〔SOlAl)の粗大粒発生に対
する効果を示したものが第1図である。In other words, the generation of coarse grains during high-temperature coiling of aluminum-killed steel is affected by the amount of [N] and [SOlAl].
The effect of h is small in areas where precipitates exist. FIG. 1 shows the effects of [N] and [SOlAl] on the generation of coarse grains.
同図に示されるごとく、〔N〕はある程度以下に低くな
ると粗大粒が発生しやすくなり、この時〔N〕量に対し
て〔SOlAl)量が高くなつても粗大粒が発生しやす
くなることがわかる。また巻取温度と降状点(YP)、
全伸び(El)、平均ランクフオード値(〒)は第2図
(同図では代表例としてYPとの関係を示した)に示す
ような関係にあり、粗大粒が発生しないかぎり、これら
の値は高い方が良い。このことから粗大粒の発生を防止
するめには、熱延後の巻取温度を〔N〕量と〔SOlA
l)量との関係で、次式を満足せしめるようにすればよ
いことを知得した。本発明において、連続焼鈍で高加工
性鋼板を得.るために銅成分範囲はSOl,Al:0.
020〜0.100%,〔C〕 :0.06%以下、〔
Mn〕 :0.30%以下、〔P〕 :0.020%以
下、〔S〕 :0.025%以下、〔N〕 :0.00
70%以下とちることが推奨される。As shown in the figure, when [N] decreases below a certain level, coarse particles tend to occur, and even if the amount of [SOLAl] increases relative to the amount of [N], coarse particles also tend to occur. I understand. Also, the winding temperature and descending point (YP),
The total elongation (El) and the average Rankford value (〒) have a relationship as shown in Figure 2 (the figure shows the relationship with YP as a representative example), and unless coarse grains occur, these values The higher the value, the better. Therefore, in order to prevent the generation of coarse grains, the coiling temperature after hot rolling should be adjusted to the amount of [N] and [SOlA].
l) I learned that the following formula should be satisfied in relation to the quantity. In the present invention, a highly formable steel plate is obtained by continuous annealing. In order to achieve this, the copper component range is SOl, Al: 0.
020-0.100%, [C]: 0.06% or less, [
Mn]: 0.30% or less, [P]: 0.020% or less, [S]: 0.025% or less, [N]: 0.00
It is recommended to reduce the amount to 70% or less.
即ち、〔C〕は0.06%を超えると強度が増加し、〒
値が低下するためであり、〔Mn〕についても〔C〕と
同様の理由及び製品長手方向の均一性から規制される。
〔P〕は強度の増加と伸びの低下から0.020%以下
に限定され、〔S〕は固溶〔S〕を残さないため上限を
0.025%と限定したものである。またSOlAlの
下限を0.020%とした理由は、これ以下だど熱延の
高温巻取時及びその後の工程でも〔N〕がAl−Nとし
て固定されず、固溶状態となり、時効性及び加工性に悪
影響を与えるためであり、上限を0.100%としたの
は、これ以上になるとSOlAl量増大による強度の増
加、表面性状の悪化などが発生し、かつコスト的にも高
くなるためである。〔N〕については0.0070%を
)超えるとAl−Nの析出物の数が増え、粒の成長性が
阻害され、また析出物による強度、伸びの低下などが発
生するためである。また、本発明において〔N〕量が0
.0070%以下の場合、〔N〕/〔SOlAl〕≦0
.067になると粗大・粒が発生しやすくなる。That is, when [C] exceeds 0.06%, the strength increases;
This is because the value decreases, and [Mn] is also regulated for the same reason as [C] and for uniformity in the longitudinal direction of the product.
[P] is limited to 0.020% or less because it increases strength and reduces elongation, and [S] does not leave solid solution [S], so the upper limit is limited to 0.025%. The reason why the lower limit of SOlAl was set to 0.020% is that even if it is less than this, [N] will not be fixed as Al-N during high-temperature coiling of hot rolling and in subsequent steps, but will be in a solid solution state, resulting in poor aging properties. This is because it adversely affects workability, and the reason why the upper limit was set at 0.100% is because if it exceeds this, the strength will increase due to an increase in the amount of SOlAl, the surface quality will deteriorate, and the cost will also increase. It is. This is because if [N] exceeds 0.0070%, the number of Al--N precipitates increases, grain growth is inhibited, and the precipitates cause a decrease in strength and elongation. Further, in the present invention, the amount of [N] is 0.
.. If 0070% or less, [N]/[SOlAl]≦0
.. When it reaches 067, coarse grains tend to occur.
このことから粗大粒が特に発生しやすい〔N〕 :0.
0040%以下のものについては、〔N〕/SOIAI
の比を0.067以上とすることで、粗大粒の発生を防
止することがてきる。このような効果が得られる理由に
ついては次のように考えられる。即ち、高温巻取時のA
I−Nの析出物の大きさと数が粒成長性に影響を及ほし
、〔N〕が多い場合は析出物の数が多く、全体的な粗大
長を阻害すことにより粗大粒が発生し難くなる。一方、
析出物の数が少なく大きさが大きい場合(低NでもSO
lAlが低い場合に相当)は粒の成長性が良く、均一に
粒成長を起こすため、逆に粗大粒は発生し難い。これら
中間にある領域では粒の成長を阻害する部分と成長しや
すい部分が混在しているため、成長しやすい部分のが極
端に大きくなる結果、粗大粒が発生するものと思われる
。なお、上式において巻取温度の上限を780℃に限定
した理由は、これ以上になると、いわゆるコイルツブレ
を生じる危険性があるためである。For this reason, coarse particles are particularly likely to occur [N]: 0.
For those below 0040%, [N]/SOIAI
By setting the ratio to 0.067 or more, it is possible to prevent the generation of coarse particles. The reason why such an effect can be obtained is considered as follows. That is, A during high temperature winding
The size and number of I-N precipitates affect grain growth, and when [N] is large, the number of precipitates is large and the overall coarse length is inhibited, making it difficult to form coarse grains. on the other hand,
When the number of precipitates is small and large (SO
Corresponding to the case where lAl is low), grain growth is good and grains grow uniformly, so on the contrary, coarse grains are less likely to occur. In the region between these regions, there are a mixture of areas that inhibit grain growth and areas where grain growth is easy, so it is thought that the areas that are easy to grow become extremely large, resulting in the generation of coarse grains. The reason why the upper limit of the winding temperature is limited to 780° C. in the above formula is that if it exceeds this value, there is a risk of so-called coil breakage.
〔実施例〕本発明の実施例として表1に、各種成分を組
合せたものをAr′3以上の温度で仕上げ、その後、水
冷により700℃〜750℃の範囲で巻取温度を変化さ
せた時の粗大粒の発生状況を示す。[Example] As an example of the present invention, as shown in Table 1, when a combination of various components was finished at a temperature of Ar'3 or higher, and then the winding temperature was varied in the range of 700 ° C to 750 ° C by water cooling. This shows the occurrence of coarse grains.
また第2表にこれらの材料についてスケールを剥離後、
圧延率60%以上で冷延を行い、連続焼鈍炉にて690
〜720℃×15m11n加熱し、急速冷却後350〜
500℃×1min以上オーバーエツジングを行ない1
.0%前後の伸長率をかけたものの機械的性質を示す。
以上の実施例からも明らかなように、本発明によれば、
特ににキルド鋼を熱延後所定の巻取温度て巻取ることに
より、粗大粒の発生を防止し、加工性の優れた冷延鋼板
を安定して製造することが可能となり、その効果の優れ
た発明である。Table 2 also shows the results of these materials after removing scale.
Cold rolling is performed at a rolling reduction of 60% or more, and 690% is applied in a continuous annealing furnace.
〜720℃×15m11n heating, 350℃ after rapid cooling
Perform over-edging at 500℃ x 1 min or more 1
.. Mechanical properties are shown after applying an elongation rate of around 0%.
As is clear from the above examples, according to the present invention,
In particular, by coiling killed steel at a predetermined coiling temperature after hot rolling, it is possible to prevent the generation of coarse grains and to stably produce cold rolled steel sheets with excellent workability. This is a great invention.
第1図は〔N〕と〔SOlAl〕の粗大粒発生に及ぼす
影響を説明するためのグラフ、第2図は、?取温度とY
P及び粗大粒発生面積の関係を示すクラブである。Figure 1 is a graph to explain the influence of [N] and [SOlAl] on the generation of coarse grains, and Figure 2 is a graph for explaining the influence of [N] and [SOlAl] on the generation of coarse grains. Temperature and Y
This is a club showing the relationship between P and the area where coarse grains are generated.
Claims (1)
延後のストリップを下式を満足する巻取温度で巻取り、
次いで通常の冷延及び連続焼鈍を行なうことを特徴とす
る加工性の優れた冷延鋼板の製造方法。 T≦15×10^3(〔N〕−0.067〔solAl
〕+720℃<780℃ただし、T:巻取温度(℃) 〔N〕:N濃度(%) 〔solAl〕:solAl濃度(%)[Claims] 1. In Al-killed steel that is hot-rolled and coiled at a high temperature, the hot-rolled strip is coiled at a coiling temperature that satisfies the following formula,
A method for producing a cold-rolled steel sheet with excellent workability, which is then subjected to normal cold rolling and continuous annealing. T≦15×10^3([N]-0.067[solAl
] +720℃<780℃ However, T: Coiling temperature (℃) [N]: N concentration (%) [solAl]: solAl concentration (%)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56002730A JPS6043416B2 (en) | 1981-01-13 | 1981-01-13 | Method for producing cold-rolled steel sheets with excellent workability |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56002730A JPS6043416B2 (en) | 1981-01-13 | 1981-01-13 | Method for producing cold-rolled steel sheets with excellent workability |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS57116729A JPS57116729A (en) | 1982-07-20 |
| JPS6043416B2 true JPS6043416B2 (en) | 1985-09-27 |
Family
ID=11537428
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP56002730A Expired JPS6043416B2 (en) | 1981-01-13 | 1981-01-13 | Method for producing cold-rolled steel sheets with excellent workability |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6043416B2 (en) |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5316465B2 (en) * | 1972-04-24 | 1978-06-01 | ||
| JPS5166220A (en) * | 1974-12-06 | 1976-06-08 | Nippon Kokan Kk | RENZOKUSHODONNYORUARUMINIUMUKIRUDOREIENKOHANNO SEIZOHOHO |
| JPS51101715A (en) * | 1975-03-06 | 1976-09-08 | Nippon Kokan Kk | RENZOKUSHODONNYORUKOIRUNAGATEHOKONO ZAISHITSUKINITSUSEINISUGURETA ARUMINIUMUKIRUDOREIENKOHANNOSEIZOHOHO |
| JPS5558328A (en) * | 1978-10-24 | 1980-05-01 | Nippon Steel Corp | Production of cold rolled steel plate and surface treated type steel plate |
-
1981
- 1981-01-13 JP JP56002730A patent/JPS6043416B2/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPS57116729A (en) | 1982-07-20 |
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