JPS6056224B2 - Metal vapor deposition method on the inner surface of a vacuum vessel for a torus-shaped fusion device - Google Patents
Metal vapor deposition method on the inner surface of a vacuum vessel for a torus-shaped fusion deviceInfo
- Publication number
- JPS6056224B2 JPS6056224B2 JP54086508A JP8650879A JPS6056224B2 JP S6056224 B2 JPS6056224 B2 JP S6056224B2 JP 54086508 A JP54086508 A JP 54086508A JP 8650879 A JP8650879 A JP 8650879A JP S6056224 B2 JPS6056224 B2 JP S6056224B2
- Authority
- JP
- Japan
- Prior art keywords
- vapor deposition
- vacuum vessel
- metal wire
- torus
- fusion device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/24—Vacuum evaporation
- C23C14/26—Vacuum evaporation by resistance or inductive heating of the source
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E30/00—Energy generation of nuclear origin
- Y02E30/10—Nuclear fusion reactors
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physical Vapour Deposition (AREA)
Description
【発明の詳細な説明】
本発明はトーラス形核融合装置用真空容器の内面にチタ
ン、モリブデンなどの金属を蒸着する方法に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for depositing metals such as titanium and molybdenum on the inner surface of a vacuum vessel for a toroidal fusion device.
核融合炉を実現するためには、プラズマ中の不純物の量
を少なくすることが不可欠である。In order to realize a nuclear fusion reactor, it is essential to reduce the amount of impurities in plasma.
このためにはプラズマとの相互作用が大きい核融合装置
用真空容器の内壁面を吸着分子の少ない清浄な状態にし
なければならない。そこで最近、真空容器内を真空に引
いた状態で、チタン、モリブデンなどの金属を真空容器
内壁面に蒸着する方法が採用され、きわめて効果の大き
いことが実験的に確かめられている。この蒸着を行なう
方法としては、従来、チタン、モリブデンなどの金属線
や中空の金属球をドーナツ状の真空容器に設けられてい
る各ポート毎に各別に取り付け、これらを各ポートから
引出されたリード線を介して外部電源に接続し、抵抗加
熱して蒸着する方法が用いられている。For this purpose, the inner wall surface of the vacuum vessel for the fusion device, which has a large interaction with the plasma, must be kept in a clean state with few adsorbed molecules. Recently, a method has been adopted in which metals such as titanium and molybdenum are deposited on the inner wall of the vacuum chamber while the chamber is evacuated, and this method has been experimentally confirmed to be highly effective. Conventionally, the method for performing this vapor deposition is to attach metal wires or hollow metal balls made of titanium, molybdenum, etc. to each port of a donut-shaped vacuum container, and then connect them to leads pulled out from each port. A method is used in which the material is connected to an external power source via a wire and vapor-deposited by resistance heating.
この方法では、真空に引いたままの状態で蒸着できるが
、一方いくつかのポートを使うにしても、金属線や金属
球が各ポート毎に各別に取り付けられているため、真空
容器のトロイダル方向に一様に蒸着することが困難であ
る。With this method, vapor deposition can be performed while the vacuum is drawn, but even if several ports are used, metal wires and metal balls are attached to each port separately, so the toroidal direction of the vacuum vessel It is difficult to deposit uniformly on the surface.
また、一様に蒸着しようとすれば、相当多くの金属線、
金属球を使わなければならず、これに伴つて多くのポー
トが必要となり、さらに加熱用電源も必要で、経済的で
ない。本発明の目的は、上記した従来技術の欠点を除き
、ドーナツ状の真空容器内面にチタン、モリブデンなど
のような金属をトロイダル方向に一様に蒸着することの
できる方法を提供するにある。Also, if you try to deposit it uniformly, you will need quite a lot of metal wires,
A metal bulb must be used, which requires many ports and a heating power source, which is not economical. An object of the present invention is to provide a method capable of uniformly depositing metals such as titanium, molybdenum, etc. in a toroidal direction on the inner surface of a donut-shaped vacuum container, while eliminating the drawbacks of the prior art described above.
この目的を達成するため、本発明は、チタン、モリブデ
ンなどからなる金属線をドーナツ状の真空容器のトロイ
ダル方向のほぼ全周にわたつて巻回し、真空容器内を真
空に引いた状態で、前記金属線に電流を流してこれを抵
抗加熱し、真空容器内面にチタン、モリブデンなどの金
属を蒸着することを特徴とする。以下、本発明の一実施
例を第1図および第2図について詳細に説明する。In order to achieve this object, the present invention involves winding a metal wire made of titanium, molybdenum, etc. over almost the entire circumference in the toroidal direction of a donut-shaped vacuum container, and then, while the inside of the vacuum container is evacuated, It is characterized by passing a current through a metal wire to heat it resistance, and depositing metals such as titanium and molybdenum on the inner surface of the vacuum container. Hereinafter, one embodiment of the present invention will be described in detail with reference to FIGS. 1 and 2. FIG.
第1図は本発明の一実施例に係る蒸着法を実施するため
の装置全体を示す概略構成図、第2図はこの装置におけ
る真空容器のポロイダル断面を示す要部拡大断面図であ
る。FIG. 1 is a schematic configuration diagram showing an entire apparatus for carrying out a vapor deposition method according to an embodiment of the present invention, and FIG. 2 is an enlarged sectional view of essential parts showing a poloidal cross section of a vacuum container in this apparatus.
これらの図において、1はトーラス形核融合装置に使用
されるドーナツ状の真空容器で、この中にはチタン、モ
リブデンなどからなる金属線2がトロイダル方向に1周
するように巻回配置されている。In these figures, reference numeral 1 denotes a donut-shaped vacuum container used in a toroidal fusion device, in which a metal wire 2 made of titanium, molybdenum, etc. is wound around once in a toroidal direction. There is.
3は真空容器1内にプラズマ電流を流すための変流器で
、真空容器1と鎖交する閉磁路を形成する鉄心4と、こ
の鉄心に巻回された1次コイル5より構成されている。3 is a current transformer for flowing a plasma current into the vacuum vessel 1, and is composed of an iron core 4 that forms a closed magnetic path interlinking with the vacuum vessel 1, and a primary coil 5 wound around this iron core. .
真空容器1は、トロイダル方向に電流が流れないように
、一部にセラミックなどの絶縁物を設けてトロイダル方
向に完全に絶縁するか、あるいは真空容器の一部を薄肉
のベローズなどで形成して適当な抵抗値(通常は1mΩ
程度以上)を持たせるようにしているが、この実施例で
は、トロイダル方向に完全に絶縁されているものとする
。真空容器1には、そのトロイダル方向に互に間隔をあ
けて4〜8個程度の円筒状ボート6が設けられており、
このボート6には、絶縁フランジ7を介して、ベローズ
8が取り付けられ、さらにこのベローズ8には、金属線
2を支持する支持棒9が気密に取り付けられている。な
お第2図中、CLはセンタラインを示す。したがつて、
真空容器1内を真空に引いた状態で、変流器3の1次コ
イル5に電流を流すと、金.属線2は変流器3の2次コ
イルに相当するので、誘導電流が流れ、抵抗加熱されて
、真空容器1内面にチタン、モリブデンなどの金属がト
ロイダル方向に一様に蒸着される。In order to prevent current from flowing in the toroidal direction, the vacuum container 1 may be completely insulated in the toroidal direction by providing an insulating material such as ceramic in a part thereof, or a part of the vacuum container may be formed with a thin bellows or the like. Appropriate resistance value (usually 1mΩ
However, in this embodiment, it is assumed that the toroidal direction is completely insulated. The vacuum container 1 is provided with about 4 to 8 cylindrical boats 6 spaced apart from each other in the toroidal direction.
A bellows 8 is attached to the boat 6 via an insulating flange 7, and a support rod 9 for supporting the metal wire 2 is attached to the bellows 8 in an airtight manner. Note that in FIG. 2, CL indicates the center line. Therefore,
When a current is passed through the primary coil 5 of the current transformer 3 while the inside of the vacuum container 1 is evacuated, gold. Since the metal wire 2 corresponds to the secondary coil of the current transformer 3, an induced current flows through it, resistance heating occurs, and metals such as titanium and molybdenum are uniformly deposited in the toroidal direction on the inner surface of the vacuum vessel 1.
なお、金属線2は支持棒9によつて4〜8個所.程度支
持されているので、上記の如く抵抗加熱されても、余り
垂れ下がることはない。Note that the metal wire 2 is connected to 4 to 8 locations by the support rod 9. Since it is supported to a certain extent, it will not sag much even if it is resistively heated as described above.
また、金属線2は蒸着後、そのままの状態にしておくと
、プラズマを生成するときの邪魔になるので、ボート6
の所まで下げる必要があるが、こ−のためには、例えば
各支持棒9を上下方向に移動するモータ駆動機構を各ボ
ート6毎に設け、これらのモータ駆動機構を互に同期を
とつて動作させることにより、リング状の金属線2をほ
ぼ水平状態を保つたままで下げるようにすればよい。In addition, if the metal wire 2 is left as it is after vapor deposition, it will get in the way of plasma generation, so the boat 6
To do this, for example, a motor drive mechanism for moving each support rod 9 in the vertical direction is provided for each boat 6, and these motor drive mechanisms are synchronized with each other. By operating it, the ring-shaped metal wire 2 may be lowered while maintaining a substantially horizontal state.
さらに、真空容器1がトロイダル方向に絶縁されている
ので、金属線2はその抵抗値を前述の如く1mΩ以上と
すれば、プラズマの生成に何ら悪影響を及ぼすことがな
く、またプラズマを生成させるときは、プラズマの抵抗
の方が桁違いに小さいので、金属線2に電流が流れるこ
とはない。本実施例によれば、金属線2を真空容器1の
トロイダル方向に1周するように巻回配置し、これlを
抵抗加熱して蒸着するので、真空容器1の内面にチタン
、モリブデンなどの金属をトロイダル方向に一様に蒸着
することができる。さらに、プラズマ電流を流すための
既設の変流器3を用いて金属線2に誘導電流を流すので
、専用の加熱用電源を設置する必要がなく、また各ボー
ト6からリード線を引出すこともなく、安価な装置で容
易に蒸着を行なうことができる。また、第3図は、一部
が薄肉のベローズなどで形成されて適当な抵抗値を持ち
、トロイダル方向に完全に絶縁されていない真空容器に
本発明の蒸着法を適用する場合の装置を示す概略構成図
で、ここではプラズマ電流を流すための変流器3の図示
が省略されている。Furthermore, since the vacuum container 1 is insulated in the toroidal direction, if the metal wire 2 has a resistance value of 1 mΩ or more as described above, it will not have any adverse effect on plasma generation, and when generating plasma. Since the resistance of the plasma is orders of magnitude smaller, no current flows through the metal wire 2. According to this embodiment, the metal wire 2 is wound around the vacuum vessel 1 in the toroidal direction, and the metal wire 2 is resistance-heated and vapor-deposited, so that titanium, molybdenum, etc. are deposited on the inner surface of the vacuum vessel 1. Metal can be uniformly deposited in a toroidal direction. Furthermore, since the induced current is passed through the metal wire 2 using the existing current transformer 3 for passing the plasma current, there is no need to install a dedicated heating power supply, and lead wires can be drawn out from each boat 6. evaporation can be easily performed using inexpensive equipment. Furthermore, FIG. 3 shows an apparatus in which the vapor deposition method of the present invention is applied to a vacuum container that is partially formed of thin-walled bellows, etc., has an appropriate resistance value, and is not completely insulated in the toroidal direction. This is a schematic configuration diagram, and illustration of a current transformer 3 for flowing plasma current is omitted here.
この実施例が前記実施例と異なる点は、前記実施例が金
属線2をトロイダル方向に1周するように巻回し、リン
グ状に閉成しているのに対し、この実施例では、金属線
2をトロイダル方向において少なくとも1個所、破線で
示すように切断し、その両端を導電材料からなる支持棒
9で支持するとともに、これらの両支持棒9の真空容器
1外に突出した端部間を導電材料からなる接続棒10に
よつて電気的に接続したことである。The difference between this embodiment and the previous embodiment is that in the above embodiment, the metal wire 2 is wound around the metal wire 2 in a toroidal direction and closed in a ring shape. 2 is cut in at least one place in the toroidal direction as shown by the broken line, both ends of which are supported by support rods 9 made of a conductive material, and the ends of these support rods 9 that protrude outside the vacuum vessel 1 are cut. Electrical connection is made by a connecting rod 10 made of a conductive material.
したがつて、真空容器1内を真空に引いた状態で、図示
しない変流器の1次コイルに電流を流せば、前記実施例
と同様に、真空容器1の内面にチタン、モリブデンなど
の金属をトロイダル方向に一様に蒸着することができる
。Therefore, if a current is passed through the primary coil of a current transformer (not shown) while the inside of the vacuum container 1 is evacuated, metals such as titanium, molybdenum, etc. can be uniformly deposited in the toroidal direction.
ところで、真空容器1がトロイダル方向に完全に絶縁さ
れていない場合、金属線2に誘導電流を流すためには、
金属線2の抵抗値を真空容器1の抵抗値よりも小さくし
なければならないが、このようにすると、プラズマを生
成させる場合にプラズマ電流を有効に流せなくなる。By the way, if the vacuum container 1 is not completely insulated in the toroidal direction, in order to cause an induced current to flow through the metal wire 2,
The resistance value of the metal wire 2 must be made smaller than the resistance value of the vacuum vessel 1, but if this is done, the plasma current will not be able to flow effectively when plasma is generated.
したがつて、プラズマを生成させるときには、金属線2
をトロイダル方向において少なくとも1個所電気的に切
断する必要がある。しかし、この実施例では、蒸着後、
接続棒10を取り外すことによつて、金属線2を電気的
に切断することができるので、トロイダル方向に完全に
絶縁されていない真空容器の蒸着にも容易に適用するこ
とができる。Therefore, when generating plasma, the metal wire 2
It is necessary to electrically disconnect at least one place in the toroidal direction. However, in this example, after deposition,
Since the metal wire 2 can be electrically disconnected by removing the connecting rod 10, it can be easily applied to vapor deposition in a vacuum container that is not completely insulated in the toroidal direction.
なお、この実施例の場合にも、蒸着後、金属線2をボー
トのところまで下げることは勿論である。以上説明した
ように、本発明によれば、真空に引いた状態で、ドーナ
ツ状の真空容器内面にチタン、モリブデンなどの金属を
トロイダル方向に一様に蒸着することができる。In this embodiment as well, it goes without saying that the metal wire 2 is lowered to the boat after the vapor deposition. As described above, according to the present invention, metals such as titanium and molybdenum can be uniformly deposited in the toroidal direction on the inner surface of the doughnut-shaped vacuum container in a vacuum state.
【図面の簡単な説明】
第1図は本発明の一実施例に係る蒸着法を実施するため
の装置全体を示す概略構成図、第2図はこの装置におけ
る真空容器のポロイダル断面を示す要部拡大断面図、第
3図は本発明の他の実施例に係る蒸着法を実施例するた
めの装置を示す概略構成図である。
1・・・・・・真空容器、2・・・・・・金属線、3・
・・・・・プラズマ電流を流すための変流器。[BRIEF DESCRIPTION OF THE DRAWINGS] Fig. 1 is a schematic configuration diagram showing the entire apparatus for carrying out a vapor deposition method according to an embodiment of the present invention, and Fig. 2 is a main part showing a poloidal cross section of a vacuum container in this apparatus. The enlarged sectional view and FIG. 3 are schematic configuration diagrams showing an apparatus for carrying out a vapor deposition method according to another embodiment of the present invention. 1... Vacuum container, 2... Metal wire, 3.
・・・・・・Current transformer for flowing plasma current.
Claims (1)
の真空容器内に配置された金属体に電流を流してこれを
抵抗加熱し、この真空容器内面に前記金属体の金属を蒸
着するものにおいて前記金属体として金属線を用い、こ
の金属線を前記真空容器のトロイダル方向のほぼ全周に
わたつて巻回したことを特徴とするトーラス形核融合装
置用真空容器内面への金属蒸着法。 2 特許請求の範囲第1項において、変流器を用いて前
記金属線に誘導電流を流すことを特徴とするトーラス核
融合装置用真空容器内面への金属蒸着法。 3 特許請求の範囲第2項において、前記変流器として
プラズマ電流を流すための変流器を用いたことを特徴と
するトーラス形核融合装置用真空容器内面への金属蒸着
法。[Claims] 1. With the inside of a doughnut-shaped vacuum container being evacuated, a current is passed through a metal body placed in the vacuum container to heat it resistance, and the metal body is placed on the inner surface of the vacuum container. An inner surface of a vacuum vessel for a torus-shaped nuclear fusion device, characterized in that a metal wire is used as the metal body, and the metal wire is wound almost the entire circumference of the vacuum vessel in the toroidal direction. metal vapor deposition method. 2. The method of metal vapor deposition on the inner surface of a vacuum vessel for a torus fusion device, characterized in that an induced current is passed through the metal wire using a current transformer according to claim 1. 3. A metal vapor deposition method on the inner surface of a vacuum vessel for a torus-shaped nuclear fusion device according to claim 2, characterized in that a current transformer for flowing a plasma current is used as the current transformer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP54086508A JPS6056224B2 (en) | 1979-07-10 | 1979-07-10 | Metal vapor deposition method on the inner surface of a vacuum vessel for a torus-shaped fusion device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP54086508A JPS6056224B2 (en) | 1979-07-10 | 1979-07-10 | Metal vapor deposition method on the inner surface of a vacuum vessel for a torus-shaped fusion device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5613476A JPS5613476A (en) | 1981-02-09 |
| JPS6056224B2 true JPS6056224B2 (en) | 1985-12-09 |
Family
ID=13888912
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP54086508A Expired JPS6056224B2 (en) | 1979-07-10 | 1979-07-10 | Metal vapor deposition method on the inner surface of a vacuum vessel for a torus-shaped fusion device |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6056224B2 (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11109692B2 (en) | 2014-11-12 | 2021-09-07 | Rtc Industries, Inc. | Systems and methods for merchandizing electronic displays |
| US11397914B2 (en) | 2004-02-03 | 2022-07-26 | Rtc Industries, Inc. | Continuous display shelf edge label device |
| US11468401B2 (en) | 2014-11-12 | 2022-10-11 | Rtc Industries, Inc. | Application system for inventory management |
| US11580812B2 (en) | 2004-02-03 | 2023-02-14 | Rtc Industries, Inc. | System for inventory management |
-
1979
- 1979-07-10 JP JP54086508A patent/JPS6056224B2/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11397914B2 (en) | 2004-02-03 | 2022-07-26 | Rtc Industries, Inc. | Continuous display shelf edge label device |
| US11580812B2 (en) | 2004-02-03 | 2023-02-14 | Rtc Industries, Inc. | System for inventory management |
| US11109692B2 (en) | 2014-11-12 | 2021-09-07 | Rtc Industries, Inc. | Systems and methods for merchandizing electronic displays |
| US11468401B2 (en) | 2014-11-12 | 2022-10-11 | Rtc Industries, Inc. | Application system for inventory management |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5613476A (en) | 1981-02-09 |
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