JPS6236652B2 - - Google Patents
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- Publication number
- JPS6236652B2 JPS6236652B2 JP55058493A JP5849380A JPS6236652B2 JP S6236652 B2 JPS6236652 B2 JP S6236652B2 JP 55058493 A JP55058493 A JP 55058493A JP 5849380 A JP5849380 A JP 5849380A JP S6236652 B2 JPS6236652 B2 JP S6236652B2
- Authority
- JP
- Japan
- Prior art keywords
- rich
- extraction
- water
- extract
- aromatic components
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 34
- 238000000605 extraction Methods 0.000 claims description 32
- 125000003118 aryl group Chemical group 0.000 claims description 24
- 235000014347 soups Nutrition 0.000 claims description 16
- 238000001704 evaporation Methods 0.000 claims description 14
- 239000000796 flavoring agent Substances 0.000 claims description 12
- 235000019634 flavors Nutrition 0.000 claims description 12
- 230000008020 evaporation Effects 0.000 claims description 11
- 239000012141 concentrate Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims 1
- 238000000034 method Methods 0.000 description 13
- 241000269851 Sarda sarda Species 0.000 description 10
- 238000009835 boiling Methods 0.000 description 9
- 241000269821 Scombridae Species 0.000 description 6
- 235000020640 mackerel Nutrition 0.000 description 6
- 241001377695 Polygonum arenastrum Species 0.000 description 3
- 235000006386 Polygonum aviculare Nutrition 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 238000003809 water extraction Methods 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
Landscapes
- Seasonings (AREA)
- Seeds, Soups, And Other Foods (AREA)
Description
本発明は風味の優れた濃厚だしの製法に関す
る。
風味の良い節類抽出液、いわゆる“だし”を作
るには大量の熱湯を用いて抽出する方法が最も良
く、一般的には節に対して20〜50倍の熱湯が用い
られる。しかしながら、この20〜50倍の熱湯によ
る抽出液である、いわゆるだし液そのものは、量
販性に欠け、また、加工食品、調味料などにおい
ても、だし液そのものよりも、これを濃縮した節
類濃厚抽出液、即ち、濃厚だしが要求される。
従来、節類より濃厚な抽出液を得る方法として
は、節類を熱湯抽出後単に濃縮する方法、節類を
酵素分解又は鉱酸分解する方法、節類を有機溶剤
で節芳香成分を抽出した後残渣を熱湯にて抽出す
るか又は鉱酸分解して呈味成分を得、両者を合せ
る方法などが知られている。
この内、鉱酸や酵素で加水分解する方法、ある
いは有機溶剤で抽出する方法では最も大切である
芳香成分等の変質が避けられず、風味の良いもの
は得られない。
また、節類を熱湯抽出後、単に濃縮する方法で
は、濃縮の際多量のエネルギーを消費し、その上
大部分の芳香成分が飛散してしまうため、風味の
良い濃厚だしは得られない。熱湯で抽出する際、
熱湯の量を少くすれば濃縮が少くてすむが、熱湯
が少いと、特に、節の芳香成分の抽出が充分に行
われないので、風味の良いだしが得られない。
本発明者らは、上記現状に鑑み、風味の優れた
濃厚だしを効率良く製造する方法を開発すべく
種々研究を重ねた結果、節類の呈味成分と芳香成
分を熱湯のみで夫々効率良く抽出する工程を組合
せることにより、風味の優れた濃厚だしが効率良
く製造できるとの知見に至り、本発明を完成した
ものである。
本発明の節類としては、かつお節、宗田節、サ
バ節などの節類、あるいは削り節が使用される。
第1工程は、節類から主として呈味成分を抽出す
る工程で、節類を小さく粉砕し、節類に対し1〜
10倍、望ましくは2〜5倍の熱湯を用いて抽出す
る。抽出は70〜98℃の温度で抽出することが望ま
しく、また、効率的に抽出する目的から、連続又
は半連続的に向流多段抽出することが望ましい。
一般に節類からだしを抽出するには、20〜50倍の
水を用いるが、本発明では1〜10倍と少い水を用
いる。本発明者らが、水の量と得られるだしの品
質について得た知見によると、だしの品質は、抽
出時の節類に対する水の量により大かく左右さ
れ、水が少くなるに従い、呈味性核酸等の呈味成
分の抽出率は変らないが、節の芳香成分の抽出率
が低下するため、節特有の芳香の乏しいだししか
得られない。また、この現象は他の抽出条件、例
えば節類の形状、粒度、抽出温度、時間、抽出残
渣との分離の条件等によつて変化しない。
抽出残渣を分離して得られる抽出液“だし”
は、呈味の強さは充分であるが、芳香は弱く、節
の芳香成分の大部分は抽出残渣に残つている。こ
の抽出残渣に、熱水抽出、蒸発濃縮、更に要すれ
ば精留工程を施すことにより、芳香成分を効率よ
く回収することができる。
抽出方法は、少い水で効率良く抽出するには向
流多段抽出法が望ましい。向流多段抽出機はどの
ようなタイプでも良いが、抽出時の芳香成分の飛
散を防ぐため密閉型とし、蒸発部は回収すること
が望ましい。
本発明の第2工程では、抽出残渣中に残存して
いる芳香成分を、熱水抽出するが、この場合、抽
出残渣乾燥物1部に対し、10〜50部の熱水を接触
させ、抽出温度70〜98℃にて1回抽出し、芳香成
分を充分に抽出することが望ましい。次いで該軸
出物を濃縮し、芳香成分に富む濃縮物を得る。濃
縮方法は、例えば蒸発濃縮で芳香成分を蒸発部に
移行させる方法によるが、この場合、望ましく
は、前記抽出物の残渣を除くことなく、減圧下で
回分又は連続的に蒸発濃縮を行い、元液の10〜50
%を蒸発させ、芳香成分を充分に移行させる。更
に望ましくは、この蒸発部を精留塔へ導き、水分
を凝縮除去して、節芳香成分を分留濃縮し、コン
デンサーを経て、元液の50〜200倍の強さの節芳
香成分濃縮物を得る。精留塔は充填塔でも段落で
も良く、理論段数5〜20程度のものを用い、還
流比もそのつど設定する。精留そのものは、常圧
下、回分精留でも可能であるが、蒸発濃縮装置と
組で行うためには、減圧下、連続的に精留を行う
ことが望ましい。尚、実際には、精留塔のコンデ
ンサーで凝縮しない不凝縮性のガス中にも、芳香
成分が存在するため、スクラバー等を設けること
により、芳香成分を捕集して精留塔へリサイクル
することが必要となる。
上記で得られた濃縮物の芳香は、芳香成分の1
部は既に第1工程の熱水抽出で抽出されてしまつ
ているため、節類の芳香成分のすべてが濃縮され
ているわけではないので、これ自体では、節類特
有の芳香を充分に有するものではない。第3工程
に於て、第1工程の呈味成分抽出液と第2工程の
芳香成分濃縮物を合せることによつて、はじめ
て、節類特有の芳香を有する濃厚だしが得られ
る。本発明の方法は、熱水抽出法と濃縮法の組合
せにより、有機溶剤等を全く使用することなく、
風味のよい濃厚だしを効率よく取得できるもので
あり、本発明の方法で得られる濃厚だしは、従来
法では得られない節特有の芳香を有し、水で希釈
することにより、通常のだしを完全に再現するこ
とができる。
以下、実施例にて、本発明を詳細に説明する。
実施例 1
かつお枯節20kgを粗砕し、密閉型のパドル型連
続向流抽出機を用い、抽出温度90℃で45分間、熱
湯60kgと節粒子を向流接触させた。次いで遠心分
離して、抽出残渣を分離し、抽出液45kgと抽出残
渣35kgを得た。
この抽出残渣35kg(乾物18kg)に熱湯360kgを
加え、凝縮器付の容器にて、95℃で30分間抽出し
た。得られた抽出液395kgを160mmHg Absの減圧
下、フィード量20kg/hrにて連続蒸留し、元液の
約30%、6kg/hrを蒸発させ、この蒸発部をその
まま精留塔(Φ4B×5m、3/8ベルルサドル、スク
ラバー付)に連続的に導き、全還流にて系内が平
衡に達するまで、水分を凝縮除去しながら運転
後、還流比140程度で精留塔頂部から芳香成分を
採取しながら運転し、最終的に芳香成分濃縮物約
1.2kgを得た。この場合、精留塔内で凝縮する水
分は塔底より連続的に除去し、又、凝縮器にて凝
縮しない不凝縮性ガスは、スクラバーにて冷水と
接触させ、その1部を連続的に精留塔へリサイク
ルした。
この芳香成分濃縮物を最初に得られた抽出液に
加えて、46.2kgの濃厚だしを得た。この濃厚だし
100gは、かつお枯節30gの有効成分を含む濃厚
だしに相当するものであることが確認された。
一方、かつお枯節を30%濃度で熱湯1回抽出し
たものを比較のため調製した。別に、コントロー
ルとして、かつお枯節の3%抽出液を調製し、前
記2種の濃厚だしについても水で10倍に希釈し、
パネル数20による官能検査を行つた。結果を第1
表に示す。
The present invention relates to a method for producing rich soup stock with excellent flavor. The best way to make a flavorful knot extract, known as ``dashi'', is to use a large amount of boiling water; generally, the amount of hot water used is 20 to 50 times as hot as the knot. However, the so-called stock itself, which is an extract made with 20 to 50 times as much hot water as this, lacks the ability to be sold in large quantities, and in processed foods and seasonings, it is used rather than the stock itself. An extract, ie, a concentrated stock, is required. Conventionally, methods for obtaining a thicker extract from knots include simply concentrating the knots after extracting them with hot water, decomposing the knots with an enzyme or mineral acid, and extracting the aromatic components of the knots with an organic solvent. There are known methods such as extracting the residue with hot water or decomposing it with mineral acid to obtain flavor components and combining the two. Among these methods, the methods of hydrolysis using mineral acids or enzymes, or the methods of extraction using organic solvents, cannot avoid deterioration of the most important aromatic components, making it impossible to obtain products with good flavor. Furthermore, simply concentrating joints after extracting them with boiling water consumes a large amount of energy during concentration, and most of the aromatic components are scattered, making it impossible to obtain a rich and flavorful soup stock. When extracting with boiling water,
If the amount of boiling water is reduced, there will be less concentration, but if the amount of boiling water is too small, the aromatic components of the knots will not be extracted sufficiently, making it impossible to obtain a stock with good flavor. In view of the above-mentioned current situation, the present inventors have conducted various studies to develop a method for efficiently producing rich soup stock with excellent flavor. The present invention was completed based on the finding that a rich soup stock with excellent flavor can be efficiently produced by combining the extraction steps. As the bonito flakes of the present invention, bonito flakes, Sota bonito flakes, mackerel bonito flakes, etc., or shaved bonito flakes are used.
The first step is to mainly extract flavor components from the knots, which involves crushing the knots into small pieces and
Extract using 10 times more hot water, preferably 2 to 5 times more hot water. Extraction is preferably performed at a temperature of 70 to 98°C, and for the purpose of efficient extraction, continuous or semi-continuous countercurrent multi-stage extraction is desirable.
Generally, 20 to 50 times as much water is used to extract dashi from knotweed, but in the present invention, 1 to 10 times as much water is used. According to the knowledge obtained by the present inventors regarding the amount of water and the quality of the resulting dashi, the quality of the dashi is greatly influenced by the amount of water relative to the joints at the time of extraction, and as the amount of water decreases, the flavor changes. Although the extraction rate of flavor components such as sexual nucleic acids remains the same, the extraction rate of aromatic components from knots decreases, resulting in a stock that lacks the characteristic aroma of knots. Furthermore, this phenomenon does not change depending on other extraction conditions, such as the shape of the knots, particle size, extraction temperature, time, and conditions for separation from extraction residue. Extract liquid “Dashi” obtained by separating the extraction residue
The taste is strong enough, but the aroma is weak, and most of the aromatic components of the knots remain in the extraction residue. The aromatic components can be efficiently recovered by subjecting this extraction residue to hot water extraction, evaporation concentration, and further, if necessary, a rectification step. As for the extraction method, a countercurrent multistage extraction method is desirable for efficient extraction with a small amount of water. Any type of countercurrent multistage extractor may be used, but it is preferable to use a closed type to prevent aroma components from scattering during extraction, and to recover the evaporation section. In the second step of the present invention, the aromatic components remaining in the extraction residue are extracted with hot water. In this case, 1 part of the dried extraction residue is brought into contact with 10 to 50 parts of hot water, and It is desirable to extract once at a temperature of 70 to 98°C to sufficiently extract the aromatic components. The extract is then concentrated to obtain a concentrate rich in aroma components. The concentration method is, for example, a method in which the aroma components are transferred to the evaporation section by evaporation concentration. In this case, desirably, the evaporation concentration is performed batchwise or continuously under reduced pressure without removing the residue of the extract, and the original 10-50 of liquid
% is evaporated and the aroma components are sufficiently transferred. More preferably, this evaporation section is led to a rectification column, water is condensed and removed, the aromatic components are fractionally concentrated, and the aromatic components are concentrated through a condenser to form a concentrated aromatic component that is 50 to 200 times stronger than the original liquid. get. The rectification column may be a packed column or a stage column, and the number of theoretical plates is about 5 to 20, and the reflux ratio is set each time. The rectification itself can be carried out by batch rectification under normal pressure, but in order to carry out the rectification in combination with an evaporative concentration device, it is desirable to carry out the rectification continuously under reduced pressure. In reality, aromatic components are present even in the non-condensable gas that does not condense in the condenser of the rectification tower, so by installing a scrubber etc., the aromatic components are collected and recycled to the rectification tower. This is necessary. The aroma of the concentrate obtained above is based on 1 of the aroma components.
Since the knots have already been extracted in the first step of hot water extraction, not all of the aromatic components of the knots have been concentrated. isn't it. In the third step, by combining the taste component extract from the first step and the aromatic component concentrate from the second step, a rich soup stock having the aroma characteristic of knotweed can be obtained. The method of the present invention uses a combination of hot water extraction method and concentration method, without using any organic solvents, etc.
It is possible to efficiently obtain a rich and flavorful soup stock.The rich soup stock obtained by the method of the present invention has a unique aroma of knotweed that cannot be obtained by conventional methods. can be completely reproduced. Hereinafter, the present invention will be explained in detail with reference to Examples. Example 1 20 kg of dried bonito flakes were roughly crushed, and 60 kg of boiling water was brought into countercurrent contact with 60 kg of hot water for 45 minutes at an extraction temperature of 90° C. using a closed paddle type continuous countercurrent extractor. Then, the mixture was centrifuged to separate the extraction residue, yielding 45 kg of extract liquid and 35 kg of extraction residue. 360 kg of boiling water was added to 35 kg of this extraction residue (18 kg of dry matter), and the mixture was extracted at 95°C for 30 minutes in a container equipped with a condenser. 395 kg of the obtained extract was continuously distilled under a reduced pressure of 160 mmHg Abs at a feed rate of 20 kg/hr, evaporating approximately 30% of the original liquid, 6 kg/hr, and the evaporation section was directly transferred to a rectification column (Φ4 B × 5 m, 3/8 Berl saddle, with scrubber), and after operating the system while condensing and removing water until equilibrium is reached in the system with total reflux, the aromatic components are removed from the top of the rectification column at a reflux ratio of about 140. Driving while collecting, the final aroma component concentrate is approximately
Gained 1.2 kg. In this case, the moisture that condenses in the rectification column is continuously removed from the bottom of the column, and the non-condensable gas that does not condense in the condenser is brought into contact with cold water in a scrubber, and a part of it is continuously removed. It was recycled to the rectification tower. This aroma component concentrate was added to the initially obtained extract to obtain 46.2 kg of concentrated stock. It's this rich
It was confirmed that 100g corresponds to a rich soup stock containing the active ingredients of 30g of dried bonito flakes. On the other hand, for comparison, bonito dried bonito flakes were extracted once with boiling water at a concentration of 30%. Separately, as a control, a 3% extract of dried bonito flakes was prepared, and the two types of concentrated stock were also diluted 10 times with water.
A sensory test was conducted using 20 panels. Results first
Shown in the table.
【表】
尚、評点は、コントロールのだしと比較してコ
ントロールより良いとき5点、同等であるとき4
点、やや劣るとき3点、劣るとき2点、非常に劣
るとき1点として評点した。
実施例 2
さば節20kgを原料とし、実施例1と同様にして
得た節抽出液42kg及び芳香成分濃縮物1.5kgを混
合し、さば節を原料とした濃厚だし43.5kgを調製
した。この濃厚だし100gは、さば節30gの有効
成分を含む濃厚だしに相当するものであることが
確認された。
別に、さば節を30%濃度で熱湯1回抽出したも
の及びコントロールとして、さば節の3%抽出液
を調製した。前記2種の濃厚だしを水で10倍に希
釈したものにつき、実施例1と同一の評点基準に
より、パネル数20で官能検査を行つた。結果を第
2表に示す。[Table] The rating is 5 points when it is better than the control stock compared to the control stock, and 4 points when it is equal to the control stock.
The score was rated as 3 points for slightly inferior, 2 points for inferior, and 1 point for very inferior. Example 2 Using 20 kg of mackerel flakes as a raw material, 42 kg of a mackerel flake extract obtained in the same manner as in Example 1 and 1.5 kg of aromatic component concentrate were mixed to prepare 43.5 kg of concentrated stock using mackerel flakes as a raw material. It was confirmed that 100g of this rich soup stock is equivalent to a rich stock containing 30g of active ingredients from mackerel flakes. Separately, mackerel flakes were extracted once with boiling water at a concentration of 30%, and a 3% extract of mackerel flakes was prepared as a control. A sensory test was conducted on 20 panels using the same scoring criteria as in Example 1 for the two types of concentrated soup stock diluted 10 times with water. The results are shown in Table 2.
【表】
上記結果から明かなように本発明の方法により
得られる濃厚だしは、むしろ通常のだしより、そ
の風味が好まれる傾向になり、充分満足できる質
であつた。[Table] As is clear from the above results, the flavor of the rich soup stock obtained by the method of the present invention was more preferred than that of ordinary soup stock, and the quality was sufficiently satisfactory.
Claims (1)
法。 節類1部に水1〜10部を接触させて呈味成分を
抽出し、抽出残渣を分離し、所望により抽出液を
濃縮する第1工程、該抽出残渣を水と接触させて
得た抽出物を蒸発濃縮して芳香成分を得る第2工
程、 第2工程で得られる芳香成分を第1工程の抽出
液に加えて風味の良い濃厚だしを製造する第3工
程。 2 節類からの呈味成分の抽出が、向流多段抽出
によるものであることを特徴とする特許請求の範
囲第1項記載の濃厚だしの製法。 3 前記第1工程において、節類1部に対し、接
触させる水の量が2〜5部であることを特徴とす
る特許請求の範囲第1項記載の濃厚だしの製法。 4 前記第2工程における蒸発濃縮が、抽出残渣
を水と接触させて得た抽出物を蒸発濃縮して芳香
成分に富む蒸発部を得、所望により該蒸発部を更
に精留塔を用いて濃縮するものであることを特徴
とする特許請求の範囲第1項記載の濃厚だしの製
法。 5 前記第2工程が、抽出残渣乾燥物1部に対
し、10〜50部の水と接触させ、抽出温度70〜98℃
にて1回抽出を行つて芳香成分に富む、元液の10
〜50%の蒸発部を得るものであることを特徴とす
る特許請求の範囲第1項記載の濃厚だしの製法。 6 前記第2工程が、芳香成分に富む蒸発部を更
に精留塔を用いて、元液の50〜200倍の強さまで
芳香成分を濃縮するものであることを特徴とする
特許請求の範囲第1項記載の濃厚だしの製法。[Claims] 1. A method for producing rich and flavorful soup stock comprising the following three steps: A first step of contacting 1 part of joints with 1 to 10 parts of water to extract flavor components, separating the extraction residue, and optionally concentrating the extract; an extraction obtained by contacting the extraction residue with water; The second step involves evaporating and concentrating the substance to obtain aromatic components, and the third step involves adding the aromatic components obtained in the second step to the extract from the first step to produce a rich and flavorful soup stock. 2. The method for producing a rich stock according to claim 1, wherein the extraction of flavor components from joints is carried out by multi-stage countercurrent extraction. 3. The method for producing a rich stock according to claim 1, wherein in the first step, the amount of water brought into contact with 1 part of the joints is 2 to 5 parts. 4 The evaporative concentration in the second step involves evaporating and concentrating the extract obtained by contacting the extraction residue with water to obtain an evaporation section rich in aromatic components, and if desired, further concentrating the evaporation section using a rectification column. A method for producing a thick soup stock according to claim 1, characterized in that: 5 In the second step, 1 part of the dried extraction residue is brought into contact with 10 to 50 parts of water, and the extraction temperature is 70 to 98°C.
10% of the original liquid rich in aromatic components is extracted once at
A method for producing a concentrated stock according to claim 1, characterized in that an evaporation rate of ~50% is obtained. 6. The second step is characterized in that the evaporation section, which is rich in aromatic components, further uses a rectification column to concentrate the aromatic components to a strength 50 to 200 times that of the original liquid. The method for producing rich soup stock as described in Section 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5849380A JPS56154977A (en) | 1980-05-01 | 1980-05-01 | Preparation of concentrated soup stock |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5849380A JPS56154977A (en) | 1980-05-01 | 1980-05-01 | Preparation of concentrated soup stock |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS56154977A JPS56154977A (en) | 1981-11-30 |
| JPS6236652B2 true JPS6236652B2 (en) | 1987-08-07 |
Family
ID=13085942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5849380A Granted JPS56154977A (en) | 1980-05-01 | 1980-05-01 | Preparation of concentrated soup stock |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS56154977A (en) |
-
1980
- 1980-05-01 JP JP5849380A patent/JPS56154977A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS56154977A (en) | 1981-11-30 |
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