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JPS6361118B2 - - Google Patents
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JPS6361118B2 - - Google Patents

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Publication number
JPS6361118B2
JPS6361118B2 JP13724680A JP13724680A JPS6361118B2 JP S6361118 B2 JPS6361118 B2 JP S6361118B2 JP 13724680 A JP13724680 A JP 13724680A JP 13724680 A JP13724680 A JP 13724680A JP S6361118 B2 JPS6361118 B2 JP S6361118B2
Authority
JP
Japan
Prior art keywords
welding
pressure
welded
defects
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP13724680A
Other languages
Japanese (ja)
Other versions
JPS5762884A (en
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Priority to JP13724680A priority Critical patent/JPS5762884A/en
Publication of JPS5762884A publication Critical patent/JPS5762884A/en
Publication of JPS6361118B2 publication Critical patent/JPS6361118B2/ja
Granted legal-status Critical Current

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  • Turbine Rotor Nozzle Sealing (AREA)
  • Welding Or Cutting Using Electron Beams (AREA)
  • Heat Treatment Of Nonferrous Metals Or Alloys (AREA)

Description

【発明の詳細な説明】[Detailed description of the invention]

本発明は、溶融溶接後、溶接部内に存在する溶
接ミクロ欠陥を加熱加圧処理によつて消滅せしめ
る溶接処理方法に関するものである。 一般に、母材の溶接時に生ずる溶接欠陥として
は、割れ、気孔、融合不良、溶込み不足など種々
のものがあり、その欠陥の大きさも大小まちまち
である。そして、基準を越えた溶接欠陥が発生し
た場合には、従来は、欠陥発生部分の溶接部を完
全に除去し、再溶接することにより上記溶接欠陥
を補修するようにしている。 しかしながら、上記補修においては、作業が煩
雑であるとともに、母材の材料がもともと溶接性
の悪い場合には、再溶接しても同様に溶接欠陥が
再発生する恐れがある。 例えば、ガスタービンのタービンホイルは、通
常500℃以上の高温にさらされ、かつ高速回転体
であるため、高強度が要求されるものであつて、
近年その金属材料としてNi基耐熱合金が使用さ
れている。しかし、Ni基耐熱鍜造合金からなる
ガスタービンホイルのデイスクと、Ni基耐熱鋳
造合金からなるブレードとの結合を溶接によつて
行うとNi基耐熱鋳造合金は溶接性が悪く、溶接
金属凝固割れあるいは溶接熱影響部の液化割れな
どの欠陥を生じ、良好な溶接部を得ることは溶融
溶接法のいかにかかわらず困難である。これは急
熱急冷の過程において粒界に存在する炭化物、
γ′相およびγ相の間の反応等により、粒界にNb,
Al,Ti,S,O,Cが偏析して低融点相を形成
し、これが溶接時溶融し、液化するために、ミク
ロ割れが生ずるものである。この割れは幅が数ミ
クロン〜数百ミクロン、長さが数十ミクロンから
数千ミクロン程度のミクロ割れである。また、こ
の溶接欠陥の発生を溶接時に防止することは非常
に困難であり、かつ、不確実な方法である。 よつて、従来は、上記ガスタービンホイルのデ
イスクとブレードとの結合は嵌め合せによる機械
的結合により行われているものであり、その機械
加工に多大の時間と費用を要していた。 そこで、本発明者らはかかる点に鑑み、被溶接
部内部の溶接欠陥発生部分を除去することなく、
溶接欠陥を溶接後消滅せしめる方法を鋭意研究
し、上記被溶接物を高温、高圧下に数時間保持す
ることにより、溶接ミクロ欠陥を潰滅できるとと
もに、粒界近傍の偏析元素の均一化を図ることが
可能であることを確認し、本発明をなすに至つた
ものである。 すなわち、本発明は、母材を溶融溶接後、溶接
部内部に割れあるいは気孔等のミクロ欠陥が生じ
ている被溶接物を、母材が十分塑性流動あるいは
クリープ挙動を生ずる高温に加熱するとともに、
1軸方向、2軸方向、3軸方向あるいは静水圧的
に全方向から母材の塑性変形を促進するに十分な
高圧を負荷せしめ、前記欠陥が高温で熱加工プロ
セスあるいは冶金反応により潰滅する時間保持し
て加熱加圧処理した後、除荷、冷却して溶接ミク
ロ欠陥を消滅せしめる溶接処理方法である。 本発明処理方法が適用可能な溶接母材として
は、各種鋼材、アルミニウムおよびその合金、ニ
ツケルおよびその合金、銅およびその合金、ある
いはチタンおよびその合金等があるが、以下に、
Ni基耐熱合金によるガスタービンホイルのデイ
スクとブレードとの結合についての具体例を説明
する。 使用した溶接母材は、デイスク材としてNi基
耐熱鍜造合金のInconel718、ブレード材として
Ni基耐熱鋳造合金のInconel713Cである。両材料
の化学組成を表に示す。
The present invention relates to a welding treatment method for eliminating welding micro-defects existing in a welded part by heat and pressure treatment after fusion welding. Generally, there are various types of welding defects that occur during welding of base metals, such as cracks, pores, poor fusion, and insufficient penetration, and the size of these defects also varies. When a welding defect exceeding the standard occurs, conventionally, the welded portion where the defect has occurred is completely removed and rewelded to repair the welding defect. However, in the above-mentioned repair, the work is complicated, and if the base material originally has poor weldability, there is a risk that welding defects will occur again even if we re-weld. For example, the turbine foil of a gas turbine is normally exposed to high temperatures of 500°C or higher and is a high-speed rotating body, so high strength is required.
In recent years, Ni-based heat-resistant alloys have been used as the metal material. However, when the disk of the gas turbine foil made of a Ni-based heat-resistant forged alloy and the blade made of a Ni-based heat-resistant cast alloy are joined by welding, the Ni-based heat-resistant cast alloy has poor weldability and weld metal solidification cracks. Otherwise, defects such as liquefaction cracking in the weld heat-affected zone occur, and it is difficult to obtain a good weld regardless of the fusion welding method. This is caused by carbides existing at grain boundaries during the rapid heating and cooling process.
Due to the reaction between the γ′ phase and the γ phase, Nb and
Al, Ti, S, O, and C segregate to form a low melting point phase, which melts and liquefies during welding, resulting in microcracks. These cracks are micro-cracks with a width of several microns to several hundred microns and a length of several tens of microns to several thousand microns. Moreover, it is very difficult to prevent the occurrence of welding defects during welding, and it is an uncertain method. Therefore, conventionally, the disc and the blade of the gas turbine foil have been mechanically connected by fitting, and the machining thereof requires a great deal of time and cost. Therefore, the present inventors took this into account, and without removing the welding defect occurring part inside the welded part,
By intensively researching methods to eliminate welding defects after welding and holding the workpieces mentioned above under high temperature and high pressure for several hours, it is possible to eliminate welding micro-defects and to homogenize the segregated elements near grain boundaries. We have confirmed that this is possible and have come up with the present invention. That is, in the present invention, after melt welding the base metal, a workpiece having micro defects such as cracks or pores inside the welded part is heated to a high temperature at which the base metal sufficiently causes plastic flow or creep behavior, and
A high pressure sufficient to promote plastic deformation of the base material is applied from uniaxial, biaxial, triaxial, or all directions using hydrostatic pressure, and the time period during which the defects are destroyed by a thermal processing process or metallurgical reaction at high temperatures. This is a welding processing method in which the welding micro-defects are eliminated by holding and heating and pressurizing, followed by unloading and cooling. Welding base materials to which the treatment method of the present invention can be applied include various steel materials, aluminum and its alloys, nickel and its alloys, copper and its alloys, titanium and its alloys, etc.
A specific example of the connection between a disk and a blade of a gas turbine foil using a Ni-based heat-resistant alloy will be described. The welding base materials used were Inconel 718, a Ni-based heat-resistant forging alloy, as the disk material, and Inconel 718 as the blade material.
Inconel713C is a Ni-based heat-resistant casting alloy. The chemical composition of both materials is shown in the table.

【表】 上記2種の材料(母材)を試験用に、第1図に
示す如きI型突合せ継手として、表2に示す溶接
条件により電子ビーム溶接を行つた。 第1図において、1はInconel718により形成し
たデイスク材用の第1母材、2はInconel713Cに
より形成したブレード材用の第2母材、3は電子
ビーム溶接により接合された溶接部、3aは第1
母材1側の溶接熱影響部、3bは第2母材2側の
溶接熱影響部である。
[Table] Electron beam welding was performed on the two types of materials (base metals) mentioned above for testing, as I-type butt joints as shown in FIG. 1, under the welding conditions shown in Table 2. In Fig. 1, 1 is the first base material for the disk material made of Inconel 718, 2 is the second base material for the blade material made of Inconel 713C, 3 is the welded part joined by electron beam welding, and 3a is the first base material for the blade material. 1
The welding heat affected zone 3b is the welding heat affected zone on the base material 1 side, and 3b is the welding heat affected zone on the second base material 2 side.

【表】 次に、上記電子ビーム溶接を施した被溶接物に
下記条件で加熱加圧処理を施した。 加熱温度 1200℃ 加圧圧力 1200気圧 保持時間 4時間 処理方法は、前記被溶接物を圧力容器内に装入
し、該圧力容器に高圧不活性ガス(Ar,He等)
を注入しこの容器内を所定圧力に上昇させて被溶
接物に全方向から静水圧力を作用させ、圧力を負
荷するとともに、ヒータにより所定温度に加熱す
る。この状態を所定時間保持した後、容器内圧力
を低下させて除荷するとともに冷却して処理を完
了する。 上記加熱温度は、材料(母材)の塑性流動ある
いはクリープ挙動を十分促進する温度であり、絶
対温度で表示した融点の略2/3の温度以上でクリ
ープ挙動が顕著になることから、この近傍の温度
以上液化温度以下に加熱するものであつて、本例
のNi基耐熱合金の場合には1000℃〜1250℃が好
適である。また、上記加圧圧力は、材料(母材)
の塑性変形を促進するに十分な高圧であつて、本
例のNi基耐熱合金の場合には1000気圧以上の負
荷が必要である。さらに、加熱加圧の保持時間
は、溶接ミクロ欠陥が熱加工プロセスあるいは冶
金反応を生じて潰滅するのに要する時間であり、
本例のNi基耐熱合金の場合には数時間必要とさ
れる。 上記加熱加圧処理を施した被溶接物と、電子ビ
ーム溶接を行つたままの被溶接物とを、その溶接
部の溶接欠陥(主としてミクロ割れ、気孔)の発
生状況を検査した結果を表3に示す。この検査
は、両被溶接物の試験片からマクロ断面をとり、
顕微鏡観察(倍率100倍)により測定したもので
ある。
[Table] Next, the workpieces subjected to the above electron beam welding were subjected to heating and pressure treatment under the following conditions. Heating temperature: 1200°C Pressure: 1200 atm Holding time: 4 hours The processing method is to charge the workpiece to be welded into a pressure vessel, and inject high-pressure inert gas (Ar, He, etc.) into the pressure vessel.
is injected into the container to raise the pressure in the container to a predetermined level, applying hydrostatic pressure to the workpiece from all directions, applying pressure, and heating the workpiece to a predetermined temperature using a heater. After maintaining this state for a predetermined period of time, the pressure inside the container is lowered, the load is removed, and the container is cooled to complete the process. The above heating temperature is a temperature that sufficiently promotes plastic flow or creep behavior of the material (base material), and since creep behavior becomes noticeable at temperatures above approximately 2/3 of the melting point expressed in absolute temperature, The temperature is preferably from 1000°C to 1250°C in the case of the Ni-based heat-resistant alloy of this example. In addition, the above pressurizing pressure is for the material (base material)
The pressure is sufficiently high to promote plastic deformation, and in the case of the Ni-based heat-resistant alloy of this example, a load of 1000 atmospheres or more is required. Furthermore, the holding time of heating and pressurizing is the time required for welding micro defects to collapse due to the thermal processing process or metallurgical reaction,
In the case of the Ni-based heat-resistant alloy of this example, several hours are required. Table 3 shows the results of inspecting the welded parts subjected to the above heating and pressure treatment and the welded parts that had been subjected to electron beam welding for the occurrence of welding defects (mainly microcracks and pores) in the welded parts. Shown below. In this inspection, macro cross sections are taken from test pieces of both objects to be welded.
Measured by microscopic observation (100x magnification).

【表】【table】

【表】 表3に示すように、電子ビーム溶接のままで
は、いずれの溶接条件(表2参照)においてもミ
クロ割れが観察されたが、加熱加圧処理を施した
ものは溶接速度が遅い場合(試片A,B)は、ミ
クロ割れが十分消滅しなかつたが、溶接速度が速
い場合(試片C,D)は、完全にミクロ割れが消
滅している。 さらに、上記加熱加圧処理を施した被溶接物お
よび電子ビーム溶接を行つたままの被溶接物の高
温継手性能検査として、100時間クリープ・ラプ
チヤ試験を行い、高温特性を比較した。この結果
を第2図のグラフに示す。尚、この試験には、前
記被溶接物より溶接部3を中間に有する棒状の試
験片を作成し、これを使用している。 第2図に示すように、溶接のままのもの(破
線)は、いずれも溶接部破断であつたが、溶接後
加熱加圧処理したもの(実線)は、いずれも母材
側破断であり、十分な高温強度を示した。 尚、上記実施例では、母材の溶融溶接を電子ビ
ーム溶接で行つているが、その他、レーザビーム
溶接、TIG溶接あるいはプラズマ溶接によつて溶
融溶接しても同様の処理が行える。 また、加圧方式は、実施例の如く静水圧的に全
方向から負荷するほか、1軸方向、2軸方向ある
いは3軸方向から機械的に加圧する方式を採用し
てもよいが、静水圧的に高圧を負荷するのが最も
有効である。 また、溶接部の表面に割れ等のミクロ欠陥が生
じている場合には、表面を研削して上記欠陥を除
去した後、前記の加熱加圧処理を施すか、もしく
は、欠陥発生部の表面または被溶接物全体を母材
と同程度の融点および高温強度をもつ薄板のカバ
ー部材で覆つて加熱加圧処理を施すものである。 従つて、以上の如き本発明によれば、溶融溶接
後、被溶接物を母材が塑性流動あるいはクリープ
挙動する高温高圧状態で加熱加圧処理することに
より、溶接部内部のミクロ欠陥を熱加工プロセス
あるいは冶金反応により潰滅した該溶接ミクロ欠
陥を消滅せしめて溶接強度を向上するために、従
来溶接困難とされている母材を確実に溶接接合す
ることができる。よつて、従来機械的結合により
接合することを余儀なくされていたガスタービン
ホイルのデイスクとブレードとの接合を、溶融溶
接可能とするものであつて、両部材の機械加工を
簡略化し加工時間の短縮化、コストの低減を図る
ことができる利点を有する。
[Table] As shown in Table 3, micro-cracks were observed under all welding conditions (see Table 2) when electron beam welding was performed as is, but when the welding speed was slow in the case where heat and pressure treatment was applied. In specimens A and B, the microcracks were not completely eliminated, but in specimens C and D, where the welding speed was high, the microcracks were completely eliminated. Furthermore, a 100-hour creep rupture test was conducted to compare the high-temperature characteristics of the welded objects subjected to the above-mentioned heating and pressure treatment and the welded objects that had undergone electron beam welding as a high-temperature joint performance test. The results are shown in the graph of FIG. Incidentally, in this test, a rod-shaped test piece having a welded portion 3 in the middle was prepared from the object to be welded and used. As shown in Fig. 2, the as-welded specimens (broken lines) all had weld fractures, but the welded specimens (solid lines) that had been subjected to heat and pressure treatment after welding had fractures on the base metal side. It showed sufficient high temperature strength. In the above embodiment, the base metal is fused and welded by electron beam welding, but the same process can also be achieved by fusion welding by laser beam welding, TIG welding, or plasma welding. In addition, as for the pressurizing method, in addition to applying hydrostatic pressure from all directions as in the embodiment, a method of applying mechanical pressure from one, two, or three axes may also be adopted; The most effective method is to apply high pressure. In addition, if micro-defects such as cracks occur on the surface of the welded part, the above-mentioned heating and pressure treatment may be applied after the surface is ground to remove the defects, or the surface of the defect-generated part or The entire object to be welded is covered with a thin plate cover member having a melting point and high-temperature strength similar to that of the base metal, and then heated and pressurized. Therefore, according to the present invention as described above, after fusion welding, the workpiece to be welded is subjected to heating and pressure treatment at a high temperature and high pressure state where the base material exhibits plastic flow or creep behavior, thereby removing micro defects within the weld zone through thermal processing. In order to improve the welding strength by eliminating the welding micro-defects that have been destroyed by processes or metallurgical reactions, it is possible to reliably weld and join base materials that have conventionally been considered difficult to weld. Therefore, the disk and blade of the gas turbine foil, which had conventionally been forced to be joined mechanically, can be joined by fusion welding, which simplifies the machining of both parts and shortens the machining time. It has the advantage of being able to reduce costs.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は試験片の斜視図、第2図はクリープ・
ラプチヤ試験の結果を示すグラフである。
Figure 1 is a perspective view of the test piece, Figure 2 is a creep and
It is a graph showing the results of the Lapture test.

Claims (1)

【特許請求の範囲】 1 母材を溶融溶接後、溶接部内部に割れあるい
は気孔等のミクロ欠陥が生じている被溶接物を、
母材が十分塑性流動あるいはクリープ挙動する高
温に加熱するとともに、1軸方向、2軸方向、3
軸方向あるいは静水圧的に全方向から母材の塑性
変形を促進するに十分な高圧を負荷せしめ、前記
欠陥が高温で熱加工プロセスあるいは冶金反応に
より潰滅する時間保持して加熱加圧処理した後、
除荷、冷却して溶接ミクロ欠陥を消滅せしめるこ
とを特徴とする溶接処理方法。 2 Ni基耐熱合金を母材として溶融溶接した後、
被溶接物に、温度が1000℃〜1250℃、圧力が1000
気圧以上で数時間加熱加圧処理を施すことを特徴
とする特許請求の範囲第1項記載の溶接処理方
法。 3 Ni基耐熱鍛造合金からなるガスタービンホ
イルのデイスクと、Ni基耐熱鋳造合金からなる
ブレードの結合において、該デイスクとブレード
とを電子ビーム溶接、レーザビーム溶接、TIG溶
接あるいはプラズマ溶接により突合せ溶融溶接し
た後、前記ガスタービンホイルに、温度が1000℃
〜1250℃、圧力が1000気圧以上の静水圧不活性ガ
ス中で、数時間の加熱加圧処理を施すことを特徴
とする特許請求の範囲第2項記載の溶接処理方
法。
[Claims] 1. A welded object that has micro-defects such as cracks or pores inside the welded part after fusion welding the base metal,
The base material is heated to a high temperature where it exhibits sufficient plastic flow or creep behavior, and
After applying a high pressure sufficient to promote plastic deformation of the base material from all directions, either axially or hydrostatically, and holding it for a period of time during which the defects are destroyed by a thermal processing process or metallurgical reaction at high temperature, and then subjected to heat and pressure treatment. ,
A welding processing method characterized by unloading and cooling to eliminate weld micro defects. 2 After melt welding Ni-based heat-resistant alloy as a base material,
The temperature of the object to be welded is 1000℃~1250℃ and the pressure is 1000℃.
2. The welding process according to claim 1, wherein the welding process is performed at a pressure above atmospheric pressure for several hours. 3. When joining a gas turbine foil disk made of a Ni-based heat-resistant forged alloy and a blade made of a Ni-based heat-resistant cast alloy, the disk and blade are butt-fused and welded by electron beam welding, laser beam welding, TIG welding, or plasma welding. After that, the gas turbine foil has a temperature of 1000℃
The welding processing method according to claim 2, characterized in that the heating and pressurizing treatment is performed for several hours in a hydrostatic inert gas at a temperature of ~1250°C and a pressure of 1000 atmospheres or more.
JP13724680A 1980-09-30 1980-09-30 Treatment of welding Granted JPS5762884A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP13724680A JPS5762884A (en) 1980-09-30 1980-09-30 Treatment of welding

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP13724680A JPS5762884A (en) 1980-09-30 1980-09-30 Treatment of welding

Publications (2)

Publication Number Publication Date
JPS5762884A JPS5762884A (en) 1982-04-16
JPS6361118B2 true JPS6361118B2 (en) 1988-11-28

Family

ID=15194180

Family Applications (1)

Application Number Title Priority Date Filing Date
JP13724680A Granted JPS5762884A (en) 1980-09-30 1980-09-30 Treatment of welding

Country Status (1)

Country Link
JP (1) JPS5762884A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0498811A (en) * 1990-08-16 1992-03-31 Matsushita Electric Ind Co Ltd Electric double-layer capacitor and manufacture thereof
JPH0562026U (en) * 1992-01-28 1993-08-13 富士電気化学株式会社 Electric double layer capacitor

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6124568A (en) * 1998-12-31 2000-09-26 General Electric Company Heating apparatus for a welding operation and method therefor
JP4468082B2 (en) 2004-06-11 2010-05-26 株式会社東芝 Material degradation / damage recovery processing method for gas turbine parts and gas turbine parts
JP4488830B2 (en) * 2004-08-03 2010-06-23 株式会社東芝 Regeneration treatment method of gas turbine stationary blade
JP2009285664A (en) 2008-05-27 2009-12-10 Toshiba Corp Braze-repairing material, and braze-repairing method using the material

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0498811A (en) * 1990-08-16 1992-03-31 Matsushita Electric Ind Co Ltd Electric double-layer capacitor and manufacture thereof
JPH0562026U (en) * 1992-01-28 1993-08-13 富士電気化学株式会社 Electric double layer capacitor

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