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JPS637748B2 - - Google Patents
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JPS637748B2 - - Google Patents

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Publication number
JPS637748B2
JPS637748B2 JP58169990A JP16999083A JPS637748B2 JP S637748 B2 JPS637748 B2 JP S637748B2 JP 58169990 A JP58169990 A JP 58169990A JP 16999083 A JP16999083 A JP 16999083A JP S637748 B2 JPS637748 B2 JP S637748B2
Authority
JP
Japan
Prior art keywords
crystalline cellulose
fur
drink
cerelan
observed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP58169990A
Other languages
Japanese (ja)
Other versions
JPS6062967A (en
Inventor
Hideaki Yoshida
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fuji Oil Co Ltd (fka Fuji Oil Holdings Inc)
Original Assignee
Fuji Oil Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuji Oil Co Ltd filed Critical Fuji Oil Co Ltd
Priority to JP58169990A priority Critical patent/JPS6062967A/en
Publication of JPS6062967A publication Critical patent/JPS6062967A/en
Publication of JPS637748B2 publication Critical patent/JPS637748B2/ja
Granted legal-status Critical Current

Links

Landscapes

  • Non-Alcoholic Beverages (AREA)
  • Confectionery (AREA)

Description

【発明の詳細な説明】 本発明は、ココア粉末を水溶液に溶解乃至分散
させて安定な懸濁状態を示す飲料を製造する方法
に関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for producing a beverage exhibiting a stable suspended state by dissolving or dispersing cocoa powder in an aqueous solution.

従来ココア末等の粉末材料を使用した飲料、例
えばチヨコレートドリンク等が市販されている
が、この種の飲料は保存中に内容分散物が凝集し
沈降するため、その防止が最大の解決課題となつ
ている。このようなチヨコレートドリンクの沈降
防止に対し例えば特開昭50−132160号では、植物
ガム等の乳化分散安定剤の小量存在下における水
溶液中でココア蛋白質を予め酸で凝固させた後、
50Kg/cm2以上の圧力をかけ物理的に破砕分散せし
めて均質化する方法を開示している。又特開昭50
−157564号では、親油性乳化剤を添加後アルギン
酸ナトリウム、アルギン酸プロピレングライコー
ルエステル、ペクチン、カラギーナン等の糊料を
添加し、次いでさらに親水性乳化剤とキレート剤
を添加する方法を開示している。このように従来
はガム類、ペクチン類、カラギーナン等を用い、
それらの増粘性を利用して内容分散物を沈降させ
ない方法がとられてきた。その為、清涼飲料とし
ては程遠い、口当たりの粘つこい飲料しか得られ
なかつた。一方、最近開発された結晶セルロース
(アビセル 旭化成工業(株))は、それ自体粘性を
示さず特異な網目構造により数多くの機能を発揮
するため、各種食品に使用した際サツパリした食
感を与え、上記チヨコレートドリンクのような粉
末材料の沈降防止に対しても有効であるといわれ
ている。しかしながら、かかる結晶セルロースは
高価であり、かつ、沈降防止効果の得られる量
も、例えば1%のココア末水溶液の懸濁状態を安
定に維持させるために0.8〜1.0%の使用量が必要
であつて、この使用量を経済性の面から0.2〜0.6
%程度に減ずると最早沈降防止効果が得られず下
層に内容分散物が分離する(後記比較例1参照)。
Traditionally, beverages made from powdered materials such as cocoa powder, such as tyokolate drinks, have been commercially available, but the dispersion content of these types of beverages aggregates and settles during storage, so preventing this is the biggest problem to be solved. ing. In order to prevent the sedimentation of such a tyokolate drink, for example, in JP-A-50-132160, after coagulating cocoa protein with an acid in an aqueous solution in the presence of a small amount of an emulsifying dispersion stabilizer such as a vegetable gum,
It discloses a method of applying a pressure of 50 kg/cm 2 or more to physically crush and disperse the material to homogenize it. Also published in 1977
No. 157564 discloses a method in which a lipophilic emulsifier is added, a thickening agent such as sodium alginate, alginate propylene glycol ester, pectin, carrageenan, etc. is added, and then a hydrophilic emulsifier and a chelating agent are further added. In this way, conventionally gums, pectins, carrageenan, etc. are used,
Methods have been taken to utilize their thickening properties to prevent the content dispersion from settling. As a result, the result was a drink with a sticky texture that was far from being suitable as a soft drink. On the other hand, the recently developed crystalline cellulose (Avicel, manufactured by Asahi Kasei Industries, Ltd.) does not exhibit viscosity and exhibits many functions due to its unique network structure, giving it a crispy texture when used in various foods. It is also said to be effective in preventing sedimentation of powdered materials such as the above-mentioned Thiyocolate drink. However, such crystalline cellulose is expensive, and the amount necessary to obtain the anti-sedimentation effect is, for example, 0.8 to 1.0% in order to stably maintain a suspended state of a 1% aqueous cocoa powder solution. Therefore, from an economical point of view, the amount used should be reduced to 0.2 to 0.6.
%, the anti-sedimentation effect can no longer be obtained and the content dispersion separates into the lower layer (see Comparative Example 1 below).

本発明者は、この結晶セルロースに代わる安価
な他の乳化分散安定剤につき種々検討したが適当
な該安定剤は見つからず、更に該結晶セルロース
を少量併用する形で他の乳化分散安定剤を種々検
討した結果、結晶セルロースとフアーセレランと
の併用が極めて有効であるとの知見を得た。本発
明は、かかる知見に基づいて完成されたものであ
つて、ココア粉末を水溶液に溶解乃至分散させて
飲料を製造する方法において、結晶セルロース及
びフアーセレランを併用することを特徴とする飲
料の製造法である。
The present inventor investigated various other inexpensive emulsion dispersion stabilizers to replace this crystalline cellulose, but could not find any suitable stabilizers, and furthermore, various other emulsion dispersion stabilizers were used in combination with a small amount of the crystalline cellulose. As a result of the study, it was found that the combined use of crystalline cellulose and fur-cerelan is extremely effective. The present invention has been completed based on such knowledge, and is a method for producing a beverage by dissolving or dispersing cocoa powder in an aqueous solution, which is characterized in that crystalline cellulose and fur-celleran are used together. It is.

フアーセランとは、デンマーク近海に生育する
紅藻、ススカケベニ科のフアセラリヤ
〔Furcellaria fastigiata〕から抽出される一種の
ゲル化剤であり、カラギーナンに近い性質を有し
ているが、カラギーナンが結晶セルロースとの併
用においても良好な結果が得られないのに対し、
フアーセレランは結晶セルロースとの併用におい
て極めて有効であり、且つ、添加量も極く少量で
効果的に作用する。
Furcellan is a type of gelling agent extracted from Furcellaria fastigiata, a red alga that grows in the sea near Denmark, and has properties similar to carrageenan, but carrageenan is used in combination with crystalline cellulose. Although good results were not obtained in
Fur-cerelan is extremely effective when used in combination with crystalline cellulose, and works effectively even when added in a very small amount.

本発明によれば、フアーセレランの添加量は
0.05〜0.2%の範囲内で使用するのでが良く、上
限を越えると増粘傾向を示すので好ましくなく、
逆に下限末満では効果が得られない。他方、結晶
セルロースは0.2〜0.6%の範囲内で用いればよい
ので、経済的に極めて有利である。なお、本発明
における飲料は、製品として120℃30〜40分とい
う厳しいレトルト殺菌条件の工程を経ても、充分
に安定な懸濁状態を維持することが出来、長期保
存に耐え得る製品が得られるのである。
According to the present invention, the amount of fur-cerelan added is
It is best to use it within the range of 0.05 to 0.2%; exceeding the upper limit is not preferable as it tends to thicken.
On the other hand, no effect can be obtained at the lower limit. On the other hand, since crystalline cellulose can be used within a range of 0.2 to 0.6%, it is extremely advantageous economically. Furthermore, the beverage of the present invention can maintain a sufficiently stable suspended state even after going through the process of severe retort sterilization at 120°C for 30 to 40 minutes, resulting in a product that can withstand long-term storage. It is.

以下に本発明の実施例及び比較例を例示して本
発明の効果をより一層明瞭にする。
Examples and comparative examples of the present invention will be illustrated below to further clarify the effects of the present invention.

実施例 1 ココア粉末1%(重量基準、以下同じ)グラニ
ユー糖9%、脱脂粉乳1%、庶糖脂肪酸エステル
0.1%及び結晶セルロース(アビセルRC、商品
名、旭化成工業(株))0.5%、フアーセレラン0.15
%を全量が100%となる量の水に加え、ホモミキ
サーにて撹拌しながら80℃になるまで加熱して予
備乳化した後、更に加熱を続け一旦沸騰させた後
ホモゲナイザーにて300Kg/cm2の圧力下で均質化
後、充罐し、120℃40分間レトルト殺菌し、冷却
してチヨコレートドリンクを得た。
Example 1 Cocoa powder 1% (by weight, same below) 9% granulated sugar, 1% skim milk powder, sucrose fatty acid ester
0.1% and crystalline cellulose (Avicel RC, trade name, Asahi Kasei Industries, Ltd.) 0.5%, Faseleran 0.15
% to 100% water, pre-emulsify by heating to 80℃ while stirring with a homomixer, then continue heating and boil once, then use a homogenizer to make 300Kg/cm 2 After homogenization under the pressure of

斯くして得たチヨコレートドリンクの罐製品を
常温(約25℃)に2週間放置後、開罐して懸濁状
態を観察したところ、対照として結晶セルロース
を1%使用(フアーセレランを用いず)したもの
に比べ、両者とも全く分離現象が見られず、また
試飲したところ粘度も低く、極めて口当たりのよ
い清涼感を呈していて、対照品と差異がなかつ
た。
After leaving the thus obtained canned product at room temperature (approximately 25°C) for two weeks, the can was opened and the state of suspension was observed. As a control, 1% crystalline cellulose was used (no fur-celleran was used). Compared to the original product, no separation phenomenon was observed in either product, and when sampled, the viscosity was low and the taste was extremely pleasant and refreshing, with no difference from the control product.

比較例 1 実施例1において、フアーセレランを添加せず
他は全て同様に実施して得たチヨコレートドリン
クの罐品を常温に2週間放置後、開罐して懸濁状
態を観察したところ、罐の底から全体の約3割に
当たる部分にココア粒子の凝集沈澱物が分離沈降
していた。但し、容器を振ると凝集沈澱物は、或
る程度再分散した。
Comparative Example 1 A can of thiyocolate drink obtained by carrying out the same procedure as in Example 1 without adding fur-cerelan was left at room temperature for two weeks, and then the can was opened to observe the suspension state. An agglomerated precipitate of cocoa particles was separated and settled in about 30% of the total area from the bottom. However, when the container was shaken, the flocculated precipitate was redispersed to some extent.

比較例 2 実施例1において、結晶セルロースを用いず、
他は全て同様にして実施して得たチヨコレートド
リンクを観察したところ、罐の底から約3割に当
たる部分にココア粒子の凝集沈澱物が分離沈降し
ていた。この凝集沈澱物はかなり固化しており、
容器を振つた程度ではほぐれずに小切片が残り、
均一に分散しなかつた。
Comparative Example 2 In Example 1, without using crystalline cellulose,
When the thiokolate drink obtained in the same manner as above was observed, it was found that agglomerated precipitates of cocoa particles had separated and settled in about 30% of the bottom of the can. This coagulated precipitate has solidified considerably,
Even if you shake the container, it won't loosen and small pieces will remain.
It was not evenly dispersed.

比較例 3 実施例1において、結晶セルロースとフアーセ
レランの代わりに、カラギーナン0.02%、ローカ
ストビーンガム0.2%を使用し、他は全て同様に
して実施して得たチヨコレートドリンクは粘度が
上昇してネトツキを感じ、また罐品を常温に2週
間放置後、開罐して懸濁状態を観察したところ、
比較例2と同様の状態であつた。
Comparative Example 3 In Example 1, 0.02% of carrageenan and 0.2% of locust bean gum were used in place of crystalline cellulose and fur-cerelan, and the other things were the same, but the obtained thiokolate drink had increased viscosity and did not become sticky. After leaving the can at room temperature for two weeks, we opened the can and observed the suspended state.
The condition was similar to that of Comparative Example 2.

実施例2及び3 フアーセレランをそれぞれ0.1%及び0.05%使
用した以外、他は全て実施例1と同様にして得た
チヨコレートドリンクを観察した結果、前者は実
施例1と同様に良好であつたが、後者は罐の底に
僅かに凝集物がみられた。但し、この場合罐を軽
く振るだけで直ちに均一に分散した。この結果、
フアーセレランの添加量は0.05%が限界と考えら
れた。
Examples 2 and 3 Thiyocolate drinks obtained in the same manner as in Example 1 except that 0.1% and 0.05% of furcerelan were used were observed. As a result, the former was as good as in Example 1, but In the latter case, a slight amount of aggregate was observed at the bottom of the can. However, in this case, the mixture was immediately and uniformly dispersed by simply shaking the can. As a result,
It was thought that 0.05% was the limit for the amount of fur-celleran added.

実施例4及び5 結晶セルロースの使用量を両者とも0.3%とし、
一方にフアーセレラン1.0%、他方にフアーセレ
ラン0.05%を使用して実施例1と同様に実施して
得たチヨコレートドリンクを観察した結果、前者
は実施例1と同様に良好であつたが、後者は罐の
底に僅かに凝集がみられた。但し、この場合も罐
を振ると直ちに均一に分散した。
Examples 4 and 5 The amount of crystalline cellulose used was 0.3% in both cases,
As a result of observing the thiokolate drink obtained in the same manner as in Example 1 using 1.0% Far-Seleran on one side and 0.05% Far-Seleran on the other, it was found that the former was as good as in Example 1, but the latter was A slight amount of agglomeration was observed at the bottom. However, in this case as well, when the can was shaken, it was immediately dispersed uniformly.

Claims (1)

【特許請求の範囲】 1 ココア粉末を水溶液に溶解乃至分散させて飲
料を製造する方法において、結晶セルロース及び
フアーセレランを併用することを特徴とする飲料
の製造法。 2 結晶セルロース及びフアーセレランの添加量
が前者0.2〜0.6%(重量基準、以下同じ)及び後
者0.05〜0.2%である特許請求の範囲第1項記載
の方法。
[Scope of Claims] 1. A method for producing a beverage by dissolving or dispersing cocoa powder in an aqueous solution, characterized in that crystalline cellulose and fur-cerelan are used in combination. 2. The method according to claim 1, wherein the amounts of crystalline cellulose and furcerelan added are 0.2 to 0.6% (by weight, same hereinafter) of the former and 0.05 to 0.2% of the latter.
JP58169990A 1983-09-13 1983-09-13 Production of a drink Granted JPS6062967A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP58169990A JPS6062967A (en) 1983-09-13 1983-09-13 Production of a drink

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP58169990A JPS6062967A (en) 1983-09-13 1983-09-13 Production of a drink

Publications (2)

Publication Number Publication Date
JPS6062967A JPS6062967A (en) 1985-04-11
JPS637748B2 true JPS637748B2 (en) 1988-02-18

Family

ID=15896546

Family Applications (1)

Application Number Title Priority Date Filing Date
JP58169990A Granted JPS6062967A (en) 1983-09-13 1983-09-13 Production of a drink

Country Status (1)

Country Link
JP (1) JPS6062967A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11003192B2 (en) 2015-11-10 2021-05-11 Positec Power Tools (Suzhou) Co., Ltd. Automatic working system and control method thereof and automatic moving device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11003192B2 (en) 2015-11-10 2021-05-11 Positec Power Tools (Suzhou) Co., Ltd. Automatic working system and control method thereof and automatic moving device

Also Published As

Publication number Publication date
JPS6062967A (en) 1985-04-11

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