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JPH0225988B2 - - Google Patents
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JPH0225988B2 - - Google Patents

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Publication number
JPH0225988B2
JPH0225988B2 JP58111849A JP11184983A JPH0225988B2 JP H0225988 B2 JPH0225988 B2 JP H0225988B2 JP 58111849 A JP58111849 A JP 58111849A JP 11184983 A JP11184983 A JP 11184983A JP H0225988 B2 JPH0225988 B2 JP H0225988B2
Authority
JP
Japan
Prior art keywords
target
electromagnet
current
substrate
discharge impedance
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP58111849A
Other languages
Japanese (ja)
Other versions
JPS605878A (en
Inventor
Hisaharu Obinata
Tomohisa Sawada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ulvac Inc
Original Assignee
Ulvac Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ulvac Inc filed Critical Ulvac Inc
Priority to JP11184983A priority Critical patent/JPS605878A/en
Publication of JPS605878A publication Critical patent/JPS605878A/en
Publication of JPH0225988B2 publication Critical patent/JPH0225988B2/ja
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/54Controlling or regulating the coating process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physical Deposition Of Substances That Are Components Of Semiconductor Devices (AREA)
  • Physical Vapour Deposition (AREA)
  • Electrodes Of Semiconductors (AREA)

Description

【発明の詳細な説明】 本発明はマグネトロン型のスパツタリング装置
の放電インピーダンス制御方法に関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for controlling discharge impedance of a magnetron type sputtering device.

従来この種装置は真空室内のSiウエハ等の基板
が取付けられる基板ホルダに対向させてAlその
他のターゲツトを設け、例えば該ホルダと該ター
ゲツトの間にDC電源により電位差を与えると共
に該ターゲツトの前面に電磁石或は永久磁石の磁
界を作用させてマグネトロン放電を生じさせ、該
ターゲツトの物質をスパツタして基板表面に該物
質の薄膜を形成するを一般とする。而してターゲ
ツトはスパツタに伴なうエロージヨンの進行で次
第に飛散して薄くなるものであり、その薄化に伴
ないターゲツトの前面に於ける実質的な電磁石の
磁束密度が増大し、次のような不都合を生ずる。
即ち磁束密度が増大すると放電インピーダンスが
小さくなり、この時スパツタ電流は次第に増加
し、しまいにはスパツタ電源の定格値に達してし
まうので一定の定電力制御が難しく、多数枚の基
板に一定時間で順次薄膜を形成した場合初期に処
理された基板の膜厚と終期に処理された基板の膜
厚とが大きく異なる不都合があり、1枚のターゲ
ツトで多くの基板を処理出来ず経済的でない。
Conventionally, this type of device has an Al or other target placed opposite to a substrate holder to which a substrate such as a Si wafer is attached in a vacuum chamber, and, for example, a potential difference is applied between the holder and the target by a DC power supply, and a voltage is applied to the front side of the target. Generally, a magnetic field of an electromagnet or a permanent magnet is applied to generate a magnetron discharge, and the target material is sputtered to form a thin film of the material on the surface of the substrate. The target gradually scatters and becomes thinner due to the progress of erosion accompanying the spatter, and as the target becomes thinner, the actual magnetic flux density of the electromagnet in front of the target increases, as follows. causing inconvenience.
In other words, as the magnetic flux density increases, the discharge impedance decreases, and at this time the sputtering current gradually increases, and eventually reaches the rated value of the sputtering power supply, making it difficult to control a constant power, and it is difficult to control a constant power, and it is difficult to control the sputtering current in a fixed amount of time. When thin films are sequentially formed, there is a disadvantage that the film thickness of the initially processed substrate and the film thickness of the final processed substrate differ greatly, and it is not economical because many substrates cannot be processed with one target.

本発明はこうした不都合等を解決することを目
的としたもので真空室内の基板が取付けられる基
板ホルダに対向させてターゲツトを設け、該ター
ゲツトにスパツタ電源により負電位を与えると共
に該ターゲツトの前面に電磁石の磁界を作用させ
てマグネトロン放電を生じさせ、該ターゲツトを
スパツタする式のものに於て、放電インピーダン
スを略一定に維持するように前記電磁石に流す電
流を漸次下げることを特徴とする。
The present invention is aimed at solving these inconveniences, and includes providing a target opposite to a substrate holder to which a substrate is attached in a vacuum chamber, applying a negative potential to the target by a sputter power source, and installing an electromagnet in front of the target. In this method, a magnetron discharge is generated by applying a magnetic field to sputter the target, and the current flowing through the electromagnet is gradually lowered so as to maintain the discharge impedance substantially constant.

本発明の実施例を図面につき説明すると1は真
空排気された真空室、2は薄膜が形成される基
板、3は該基板2を取付ける基板ホルダ、4はタ
ーゲツトを示し、該ホルダ3とターゲツト4は該
真空室1内に対向して設けられ、図示のような
DC或はRFのスパツタ電源5を接続して例えばホ
ルダ3とターゲツト4の間に電位差が与えられ
る。6は該ターゲツト4の背後にバツキングプレ
ート7を介して設けた電磁石、8は該電磁石6を
励磁するDCの電源である。
An embodiment of the present invention will be described with reference to the drawings. Reference numeral 1 indicates an evacuated vacuum chamber, 2 a substrate on which a thin film is formed, 3 a substrate holder to which the substrate 2 is attached, and 4 a target. are provided facing each other in the vacuum chamber 1, as shown in the figure.
A DC or RF sputter power supply 5 is connected to provide a potential difference between the holder 3 and the target 4, for example. 6 is an electromagnet provided behind the target 4 via a bucking plate 7, and 8 is a DC power source for exciting the electromagnet 6.

以上の構成のスパツタリング装置は従来より知
られたものであり、真空室1を真空化すると共に
Arその他の希ガスを注入し、電磁石6を励磁す
ると共にスパツタ電源5を入れるとターゲツト4
の前面にマグネトロン放電が生じ、励起されたイ
オンによりスパツタされたターゲツト4の物質が
基板2の表面に薄膜状に付着する。該ターゲツト
4は例えば厚さ3cmのAlで構成され、その表面
には水平磁束密度で例えば約250ガウスの磁界が
電磁石6により与えられる。また基板2は順次交
代でターゲツト4と対向して位置される。
The sputtering device with the above configuration is conventionally known, and is capable of evacuating the vacuum chamber 1 and
When Ar or other rare gas is injected, the electromagnet 6 is excited, and the sputter power source 5 is turned on, the target 4 is
A magnetron discharge occurs in front of the substrate 2, and the substance of the target 4 sputtered by the excited ions adheres to the surface of the substrate 2 in the form of a thin film. The target 4 is made of Al with a thickness of, for example, 3 cm, and a magnetic field with a horizontal magnetic flux density of, for example, about 250 Gauss is applied to its surface by an electromagnet 6. Further, the substrates 2 are positioned facing the target 4 in turn.

ターゲツト4はスパツタのエロージヨンで次第
に点線9で示すように薄くなり、その表面の磁束
密度が高まる結果放電インピーダンスが小さくな
つて定電力動作をさせる場合スパツタ電源5が電
流定格一杯になる。
The target 4 gradually becomes thinner as shown by the dotted line 9 due to the erosion of the sputter, and the magnetic flux density on its surface increases, resulting in a decrease in discharge impedance, so that the sputter power supply 5 reaches its full current rating when operating at constant power.

本発明はターゲツト4の薄化に伴なう放電イン
ピーダンスの変化をスパツタ電源5の電流或は電
圧の変化に於て注視し、実施例では該電流が定格
電流一杯に近ずくまで増大するか或は該電圧が設
定値まで下降したとき電磁石6の電流を下げ、放
電インピーダンスを略一定に制御するようにし
た。
The present invention pays close attention to changes in discharge impedance due to thinning of the target 4 through changes in the current or voltage of the sputter power source 5, and in the embodiment, it is determined whether the current increases until it approaches the full rated current or not. When the voltage drops to a set value, the current of the electromagnet 6 is lowered to control the discharge impedance to be approximately constant.

これを更に説明すれば、ターゲツト4のエロー
ジヨンの進行に伴ないスパツタ電源5の電流及び
電圧は夫々第2図のA及びBで示すように次第に
上昇及び下降する変化が見られ、該電流Aが点C
で示した定格一杯か、もしくは一杯に近い電流値
に達するか或は該電圧Bが点Dで示すように設定
値Eよりも下降したことを回路10の電流計11
或は電圧計12で検知し、電磁石6の電流Fを点
Gで示すように下げる。これによつて放電インピ
ーダンスは曲線Hで示したように略一定に制御さ
れ、スパツタ電源5の定格出力を越えることなく
多数の基板2を処理出来曲線で示したように基
板2の膜厚も略一定に得られる。これを従来の場
合と比較すれば、従来は基板2を200Å/secの成
膜速度で約1400枚の処理枚数を越えると放電イン
ピーダンスが小さくなりスパツタ電源5は定格電
流出力一杯になるので、ターゲツト4を新品に交
換する必要があつたが、本発明のように電磁石6
の電流を下げれば放電インピーダンスを1400枚の
処理枚数を越えても略一定となし得、ターゲツト
4が非常に薄くなるまで有効に使用することが出
来る。
To further explain this, as the erosion of the target 4 progresses, the current and voltage of the sputter power source 5 gradually rise and fall as shown by A and B in FIG. 2, respectively, and the current A Point C
The ammeter 11 of the circuit 10 indicates that the current reaches the full rated value or close to the full rating as shown by , or that the voltage B has fallen below the set value E as shown by point D.
Alternatively, it is detected by the voltmeter 12 and the current F of the electromagnet 6 is lowered as shown by point G. As a result, the discharge impedance is controlled to be approximately constant as shown by the curve H, and a large number of substrates 2 can be processed without exceeding the rated output of the sputter power supply 5. As shown by the curve, the film thickness of the substrate 2 is also approximately constant. You can get a certain amount. Comparing this with the conventional case, when the number of processed substrates 2 exceeds about 1400 at a film formation rate of 200 Å/sec, the discharge impedance decreases and the sputter power supply 5 reaches its rated current output, so the target 4 had to be replaced with a new one, but as in the present invention, the electromagnet 6
By lowering the current, the discharge impedance can be kept approximately constant even when the number of sheets processed exceeds 1400, and the target 4 can be used effectively until it becomes extremely thin.

電磁石6の電流を下げることにより放電インピ
ーダンスが略一定となる理由は、該電流を下げる
ことでターゲツト4の前面の磁束密度が小さくな
ることが原因である。
The reason why the discharge impedance becomes substantially constant by lowering the current of the electromagnet 6 is that the magnetic flux density in front of the target 4 decreases by lowering the current.

実施例ではスパツタ回路10の電圧が500V以
下に下つた時電磁石6の電流を1Aだけ下げて制
御したが、回路10の電流計11或は電圧計12
に接続した計算器13により電磁石6の電源8の
電流を制御するようにしてもよく、また電磁石6
の電流をより多くの回路で漸次下げることも可能
であり、連続的に下げることも可能である。この
ように本発明によるときは電磁石の電流を漸次下
げて放電インピーダンスを略一定に維持するよう
にしたのでターゲツトのエロージヨンが進行して
もスパツタ電源の電力に不足を来たすことなく定
電力でスパツタリングを行なえ、ターゲツトを交
換することなく長時間多数枚の基板を処理出来、
作業能率が向上し、ターゲツトを有効利用し得て
経済的であり、基板に形成される薄板の厚さも略
一定の良好なものが得られる等の効果がある。
In the embodiment, when the voltage of the sputter circuit 10 fell below 500V, the current of the electromagnet 6 was controlled to be lowered by 1A.
The current of the power source 8 of the electromagnet 6 may be controlled by a calculator 13 connected to the electromagnet 6.
It is also possible to gradually lower the current in more circuits, and it is also possible to lower the current continuously. In this way, according to the present invention, the current of the electromagnet is gradually lowered to maintain the discharge impedance approximately constant, so that even if the erosion of the target progresses, sputtering can be performed with constant power without causing a shortage of power in the sputtering power supply. It is possible to process a large number of substrates for a long time without changing the target.
This method improves work efficiency, makes effective use of the target, is economical, and allows the thin plate formed on the substrate to have a substantially constant thickness.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明の実施例の線図、第2図は基板
処理枚数と、電流、電圧及び放電インピーダンス
の関係を示す線図である。 1……真空室、2……基板、3……基板ホル
ダ、4……ターゲツト、5……スパツタ電源、6
……電磁石。
FIG. 1 is a diagram of an embodiment of the present invention, and FIG. 2 is a diagram showing the relationship between the number of processed substrates, current, voltage, and discharge impedance. 1... Vacuum chamber, 2... Substrate, 3... Substrate holder, 4... Target, 5... Sputter power supply, 6
……electromagnet.

Claims (1)

【特許請求の範囲】[Claims] 1 真空室内の基板が取付けられる基板ホルダに
対向させてターゲツトを設け、該ターゲツトにス
パツタ電源により負電位を与えると共に該ターゲ
ツトの前面に電磁石の磁界を作用させてマグネト
ロン放電を生じさせ、該ターゲツトをスパツタす
る式のものに於て、放電インピーダンスを略一定
に維持するように前記電磁石に流す電流を漸次下
げることを特徴とするスパツタリング装置の放電
インピーダンス制御方法。
1. A target is provided facing the substrate holder to which the substrate is mounted in the vacuum chamber, and a negative potential is applied to the target by a sputter power supply, and a magnetic field of an electromagnet is applied to the front surface of the target to generate a magnetron discharge, thereby causing the target to 1. A method for controlling discharge impedance of a sputtering apparatus, characterized in that, in a sputtering type apparatus, a current flowing through the electromagnet is gradually lowered so as to maintain a substantially constant discharge impedance.
JP11184983A 1983-06-23 1983-06-23 Control method of discharge impedance of sputtering device Granted JPS605878A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11184983A JPS605878A (en) 1983-06-23 1983-06-23 Control method of discharge impedance of sputtering device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11184983A JPS605878A (en) 1983-06-23 1983-06-23 Control method of discharge impedance of sputtering device

Publications (2)

Publication Number Publication Date
JPS605878A JPS605878A (en) 1985-01-12
JPH0225988B2 true JPH0225988B2 (en) 1990-06-06

Family

ID=14571701

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11184983A Granted JPS605878A (en) 1983-06-23 1983-06-23 Control method of discharge impedance of sputtering device

Country Status (1)

Country Link
JP (1) JPS605878A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1088341A (en) * 1996-09-11 1998-04-07 Anelva Corp Low pressure discharge sputtering apparatus and sputtering control method

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008156708A (en) * 2006-12-25 2008-07-10 Idemitsu Kosan Co Ltd Method for producing transparent conductive film

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58110872A (en) * 1981-12-23 1983-07-01 Hitachi Ltd Vacuum exhauster

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1088341A (en) * 1996-09-11 1998-04-07 Anelva Corp Low pressure discharge sputtering apparatus and sputtering control method

Also Published As

Publication number Publication date
JPS605878A (en) 1985-01-12

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