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JPH0429331B2 - - Google Patents
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JPH0429331B2 - - Google Patents

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Publication number
JPH0429331B2
JPH0429331B2 JP58154941A JP15494183A JPH0429331B2 JP H0429331 B2 JPH0429331 B2 JP H0429331B2 JP 58154941 A JP58154941 A JP 58154941A JP 15494183 A JP15494183 A JP 15494183A JP H0429331 B2 JPH0429331 B2 JP H0429331B2
Authority
JP
Japan
Prior art keywords
minutes
soymilk
soy milk
temperature
hours
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP58154941A
Other languages
Japanese (ja)
Other versions
JPS6047648A (en
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Priority to JP58154941A priority Critical patent/JPS6047648A/en
Publication of JPS6047648A publication Critical patent/JPS6047648A/en
Publication of JPH0429331B2 publication Critical patent/JPH0429331B2/ja
Granted legal-status Critical Current

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  • Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
  • Dairy Products (AREA)
  • Beans For Foods Or Fodder (AREA)

Description

【発明の詳細な説明】 本発明は、大豆に由来する芽胞を形成する細菌
(以下芽胞菌と記載する)を完全に死滅させた滅
菌豆乳の製造法に係るものであり、特に長期間保
持し得る豆腐の製造にも使用できる滅菌された豆
乳の製造法に関する。 〔技術の背景及び先行技術〕 滅菌豆乳又は長期保存可能な豆腐を製造する場
合、豆乳中の大豆に由来する芽胞菌を完全に死滅
させることが不可欠である。 従来、豆乳の芽胞菌を死滅させる技術として種
種の方法が知られているが、化学薬品等を使用せ
ずに加熱のみによる方法としては、特開昭51−
22845号公報、特開昭51−44663号公報及び特開昭
52−148647号公報がある。第二者は豆腐の製造方
法に関する発明であり、その一部の工程としてご
又は豆乳を115゜〜160℃で2秒〜5分間加熱し、
20゜〜40℃で2〜30時間保持することを開示して
いる。後者は豆乳の製造において常法により調製
した豆乳を約30℃に急冷し、80゜〜100℃で1分間
以上加熱し、20゜〜40℃で0〜18時間保持し、80゜
〜100℃で1分間以上加熱することを開示してい
る。しかしながらこれらの発明に開示されている
方法は、10℃以下の低温に長時間保持していない
ため、後述する試験結果から明らかなように芽胞
菌を完全に死滅させ得ない。 更に本発明者らの一部が先に特許を取得した特
許第1048808号及び特許第1079790号の工程の一部
に採用されている方法がある。これらの方法は、
「豆乳を70゜〜85℃の温度で10〜20分間加熱し、の
ち30゜〜45℃の温度で20〜80分間保持する工程と
この処理を経た豆乳を80゜〜90℃の温度で1〜10
分間保持し、のち122゜〜128℃の温度で1〜4秒
間加熱する工程」(以下これらの工程を滅菌工程
と記載する)とを包含している。 前記特許取得後、本発明者らはこれらの特許に
包含されている前記の滅菌工程により種々の芽胞
菌について試験を行なつた。即ち豆乳に種々の芽
胞菌を添加し、前記の滅菌工程により処理し、芽
胞菌の生残を試験した。その結果芽胞菌の種類に
よつては前記滅菌工程で完全に死滅しないことが
判明した。もつともその芽胞菌が豆乳中に必ずし
も存在するとは限らないので、前記滅菌工程は商
業的滅菌として充分であるが、本発明者らは更に
完全な豆乳の滅菌処理について研究を継続した。 その結果、本発明者らは10℃以下の低温に長時
間豆乳を保持することが芽胞菌の完全な滅菌に有
効であることを発見し、本発明を完成した。 〔発明の目的及び発明の要約〕 本発明の目的は、芽胞菌をほぼ完全に死滅させ
た豆乳の製造法を提供することにある。 本発明の他の目的は、長時間保存し得る豆乳を
提供することにある。 更に本発明の他の目的は、長期間保存し得る豆
腐の製造にも使用できる滅菌された豆乳を提供す
ることにある。 本発明は、豆乳を10℃以下の温度で少なくとも
10時間保持し、70゜〜80℃で10〜20分間保持し、
30゜〜45℃で20〜80分間保持し、更に80゜〜90℃で
1〜10分間保持し、次いで加熱滅菌することを特
徴とする滅菌された豆乳の製造法である。 〔発明の具体的な説明〕 本発明の方法に使用する豆乳は、常法により次
のようにして調製される。水で洗浄した丸大豆を
流水中で5℃16時間浸漬し、水切り後吸水大豆の
約1.9倍量の水を加え、グラインダー等で磨砕し、
100℃で4分間蒸煮し、不溶物を濾別し、豆乳を
得る。このようにして調製された豆乳は、通常PH
6.6、糖度計で測定したブリツクス糖度が10.5で
ある。以上のようにして調製された豆乳を10℃以
下の温度で少なくとも10時間、望ましくは5℃で
17時間、保持する。この10℃以下の低温で長時間
保持する工程が滅菌豆乳を製造するために極めて
重要である。 次いで豆乳を70゜〜80℃の温度で10〜20分間、
望ましくは80℃で10分間、保持し、冷却して30゜
〜45℃の温度で20〜80分間、望ましくは37℃で30
分間、保持し、更に80゜〜90℃で1〜10分間保持
する。尚これらの保持温度及び保持時間の範囲に
ついては本発明者らの一部が先きに特許出願して
特許された特許第1048808号及び特許第1079790号
の明細書に詳細に記載されている。 以上のように処理した豆乳を加熱滅菌する。加
熱滅菌は、牛乳の加熱滅菌と同一の方法、即ち超
高温加熱滅菌法、により行なわれ、通常120゜〜
150℃で1〜数秒間加熱される。しかしながら滅
菌豆乳を豆腐の製造に使用する場合には得られる
豆腐のカードテンシヨン及び色調の点から122゜〜
128℃で1〜4秒間加熱するのが望ましい。加熱
滅菌された豆乳は、冷却され、無菌的に容器に充
填され、長期保存可能な滅菌豆乳製品が得られ
る。又加熱滅菌され、冷却された豆乳を、豆腐製
造のための原料として使用することもできる。 次に試験例を示し、本発明の方法を更に詳述す
る。 試験 1 この試験は本発明の方法及び従来技術における
豆乳の滅菌効果を比較する目的で実施された。 (1) 豆乳の調製 常法により次のようにして豆乳を調製した。米
国産大豆を洗穀機で洗浄し、5℃で16時間浸漬槽
で流水浸漬し、水切り後吸水大豆の約1.9倍量の
水を加え、グラインダーで磨砕し、煮釜で約100
℃で3分間加熱し、絞り機で粕を除き、更にバイ
ブロスクリーンでみじんを除去し、豆乳を得た。
このようにして得られた豆乳の固形分含量を10.2
%(重量。以下同じ)に調整した。大豆から分離
し、バチルス属に属し、そして強い耐熱性の芽胞
を形成する2種類の芽胞菌(以下A株及びB株と
記載する)を、この豆乳1ml当りそれぞれ2×
106の割合で添加した。 (2) 豆乳の滅菌 次の〜の4種の方法により上記の豆乳を滅
菌した。 本発明の方法 上記の豆乳を5℃で15時間保持し、のち80℃
で10分間加熱し、37℃で60分間保持し、次いで
90℃で6分間加熱し、122℃で4秒間加熱した。 特許第1048808号及び特許第1079790号の方法 上記の豆乳を80℃で10分間保持し、次いで37
℃で60分間保持し、90℃で6分間加熱し、122
℃で4秒間加熱した(これらの特許発明の実施
例1と同一の方法)。 特開昭51−22845号及び特開昭51−44663号の
方法 上記の豆乳を120℃で3分間加熱し、30℃で
6時間保持した(これらの発明の実施例1と同
一の方法)。 特開昭52−148647号の方法 上記の豆乳を30℃に急冷し、90℃で5分間加
熱し、30℃に急冷して6時間保持し、次いで90
℃で5分間加熱し、30℃に急冷した(1次加熱
試料)。尚この操作を反復した試料(2次加熱
試料)も調製した(この発明の実施例2と同一
の方法)。 (3) 試験方法 ○…
[Detailed Description of the Invention] The present invention relates to a method for producing sterilized soymilk that completely kills spore-forming bacteria derived from soybeans (hereinafter referred to as spore bacteria), and particularly relates to a method for producing sterilized soymilk that can be kept for a long period of time. The present invention relates to a method for producing sterilized soy milk that can also be used to produce tofu. [Technical background and prior art] When producing sterilized soy milk or long-term shelf-stable tofu, it is essential to completely kill the spore-forming bacteria derived from soybeans in soy milk. Conventionally, various methods have been known as techniques for killing spore bacteria in soy milk, but a method using only heating without using chemicals is disclosed in Japanese Patent Application Laid-open No. 1973-
Publication No. 22845, Japanese Patent Publication No. 51-44663, and Japanese Patent Application Publication No. 1987-44663
There is a publication No. 52-148647. The second invention relates to a method for manufacturing tofu, in which part of the process involves heating rice or soy milk at 115° to 160°C for 2 seconds to 5 minutes.
It discloses holding at 20° to 40°C for 2 to 30 hours. The latter is made by rapidly cooling soymilk prepared by a conventional method in the production of soymilk to about 30°C, heating it at 80° to 100°C for 1 minute or more, holding it at 20° to 40°C for 0 to 18 hours, and then heating it to 80° to 100°C. It discloses heating for 1 minute or more. However, since the methods disclosed in these inventions do not maintain the temperature at a low temperature of 10° C. or lower for a long period of time, the spore-forming bacteria cannot be completely killed, as is clear from the test results described below. Furthermore, there is a method adopted as part of the process of Patent No. 1048808 and Patent No. 1079790, which were previously patented by some of the present inventors. These methods are
``The process of heating soy milk at a temperature of 70° to 85°C for 10 to 20 minutes, and then holding it at a temperature of 30° to 45°C for 20 to 80 minutes, and the process of heating the soymilk that has undergone this process at a temperature of 80° to 90°C. ~Ten
122° to 128° C. for 1 to 4 seconds (hereinafter, these steps will be referred to as sterilization steps). After obtaining the patents, the inventors conducted tests on various spore-forming bacteria using the sterilization process covered in these patents. That is, various spore-forming bacteria were added to soybean milk, treated by the above-mentioned sterilization process, and the survival of the spore-forming bacteria was tested. As a result, it was found that some types of spore-forming bacteria were not completely killed during the sterilization process. Since the spore bacteria are not necessarily present in soymilk, the above sterilization process is sufficient for commercial sterilization, but the present inventors continued their research on a more complete sterilization process for soymilk. As a result, the present inventors discovered that keeping soy milk at a low temperature of 10° C. or lower for a long period of time is effective in completely sterilizing spore-forming bacteria, and completed the present invention. [Object of the Invention and Summary of the Invention] An object of the present invention is to provide a method for producing soymilk in which spore-forming bacteria are almost completely killed. Another object of the present invention is to provide soymilk that can be stored for a long time. Yet another object of the present invention is to provide sterilized soymilk that can be used to produce tofu that can be stored for a long period of time. The present invention provides soy milk at a temperature of 10°C or less.
Hold for 10 hours, hold at 70° to 80°C for 10 to 20 minutes,
This is a method for producing sterilized soymilk, which is characterized by holding at 30° to 45°C for 20 to 80 minutes, further holding at 80° to 90°C for 1 to 10 minutes, and then heat sterilizing. [Detailed Description of the Invention] The soybean milk used in the method of the present invention is prepared by a conventional method as follows. The whole soybeans that have been washed with water are soaked in running water at 5℃ for 16 hours, and after draining, approximately 1.9 times the amount of water as water-absorbed soybeans is added and ground using a grinder.
Steam at 100°C for 4 minutes, filter out insoluble matter, and obtain soy milk. Soy milk prepared in this way usually has a pH of
6.6, the Brix sugar content measured with a sugar meter is 10.5. The soymilk prepared as above is kept at a temperature of 10℃ or less for at least 10 hours, preferably at 5℃.
Hold for 17 hours. This process of holding the soybean at a low temperature of 10°C or less for a long time is extremely important for producing sterilized soymilk. Next, soy milk is heated to a temperature of 70° to 80°C for 10 to 20 minutes.
Preferably held at 80°C for 10 minutes, cooled and heated at a temperature of 30° to 45°C for 20 to 80 minutes, preferably at 37°C for 30 minutes.
Hold for 1 minute, and then hold at 80° to 90°C for 1 to 10 minutes. The ranges of these holding temperatures and holding times are described in detail in the specifications of Japanese Patent No. 1048808 and Japanese Patent No. 1079790, which were previously filed by some of the present inventors. The soymilk treated as described above is heat sterilized. Heat sterilization is carried out using the same method as for milk sterilization, that is, ultra-high temperature heat sterilization, and is usually carried out at temperatures of 120° to
Heated at 150°C for 1 to several seconds. However, when sterilized soymilk is used to produce tofu, the curd tension and color tone of the resulting tofu should be 122°~
It is desirable to heat at 128°C for 1 to 4 seconds. The heat-sterilized soy milk is cooled and aseptically filled into containers to obtain a sterilized soy milk product that can be stored for a long time. Heat-sterilized and cooled soymilk can also be used as a raw material for producing tofu. Next, test examples will be shown to further explain the method of the present invention in detail. Test 1 This test was conducted for the purpose of comparing the effectiveness of sterilizing soy milk using the method of the present invention and the prior art. (1) Preparation of soy milk Soy milk was prepared in the following manner using a conventional method. Wash soybeans produced in the United States in a grain washing machine, soak them in running water in a soaking tank at 5℃ for 16 hours, drain them, add about 1.9 times the amount of water to the absorbed soybeans, grind them in a grinder, and boil them in a boiling pot to reduce the
The mixture was heated at ℃ for 3 minutes, the lees were removed using a squeezing machine, and the crumbs were further removed using a vibroscreen to obtain soymilk.
The solid content of the soymilk thus obtained was 10.2
% (weight, same below). Two types of spore-forming bacteria (hereinafter referred to as strain A and strain B), which belong to the genus Bacillus and are isolated from soybeans and form strong heat-resistant spores, were added at 2x each per ml of soymilk.
It was added at a ratio of 10 6 . (2) Sterilization of soy milk The above soy milk was sterilized using the following four methods. Method of the present invention The above soymilk is kept at 5°C for 15 hours, and then heated to 80°C.
Heat for 10 minutes at 37°C, hold for 60 minutes, then
Heated at 90°C for 6 minutes and then at 122°C for 4 seconds. Method of Patent No. 1048808 and Patent No. 1079790 The above soy milk was held at 80℃ for 10 minutes, and then
℃ for 60 minutes, heated to 90℃ for 6 minutes, 122
℃ for 4 seconds (same method as Example 1 of these patented inventions). Methods of JP-A-51-22845 and JP-A-51-44663 The above soymilk was heated at 120°C for 3 minutes and held at 30°C for 6 hours (same method as in Example 1 of these inventions). Method of JP-A No. 52-148647 The above soymilk was rapidly cooled to 30℃, heated at 90℃ for 5 minutes, rapidly cooled to 30℃ and held for 6 hours, and then heated to 90℃ for 5 minutes.
It was heated at ℃ for 5 minutes and rapidly cooled to 30 ℃ (first heating sample). A sample (secondary heating sample) was also prepared by repeating this operation (the same method as in Example 2 of the present invention). (3) Test method○…

Claims (1)

【特許請求の範囲】 1 豆乳を10℃以下の温度で少なくとも10時間保
持し、70゜〜80℃で10〜20分間保持し、30゜〜45℃
で20〜80分間保持し、更に80゜〜90℃で1〜10分
間保持し、次いで加熱滅菌することを特徴とする
滅菌された豆乳の製造法。 2 豆乳を5℃で17時間保持し、80℃で10分間保
持し、37℃で30分間保持し、更に85℃で6分間保
持することを特徴とする特許請求の範囲第1項に
記載の製造法。 3 加熱滅菌が122゜〜128℃で1〜4秒間行なわ
れることを特徴とする特許請求の範囲第1項又は
第2項に記載の製造法。
[Claims] 1. Soy milk is kept at a temperature of 10°C or lower for at least 10 hours, held at a temperature of 70° to 80°C for 10 to 20 minutes, and heated to a temperature of 30° to 45°C.
A method for producing sterilized soymilk, which comprises holding at a temperature of 80° to 90°C for 20 to 80 minutes, further holding at 80° to 90°C for 1 to 10 minutes, and then heat sterilizing. 2. The method according to claim 1, characterized in that soy milk is held at 5°C for 17 hours, 80°C for 10 minutes, 37°C for 30 minutes, and further held at 85°C for 6 minutes. Manufacturing method. 3. The manufacturing method according to claim 1 or 2, wherein the heat sterilization is carried out at 122° to 128°C for 1 to 4 seconds.
JP58154941A 1983-08-26 1983-08-26 Preparation of soybean milk Granted JPS6047648A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP58154941A JPS6047648A (en) 1983-08-26 1983-08-26 Preparation of soybean milk

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP58154941A JPS6047648A (en) 1983-08-26 1983-08-26 Preparation of soybean milk

Publications (2)

Publication Number Publication Date
JPS6047648A JPS6047648A (en) 1985-03-15
JPH0429331B2 true JPH0429331B2 (en) 1992-05-18

Family

ID=15595276

Family Applications (1)

Application Number Title Priority Date Filing Date
JP58154941A Granted JPS6047648A (en) 1983-08-26 1983-08-26 Preparation of soybean milk

Country Status (1)

Country Link
JP (1) JPS6047648A (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6287069A (en) * 1985-10-15 1987-04-21 Yamasa Shoyu Co Ltd Production of seasoning liquid
JPS62163666A (en) * 1986-01-14 1987-07-20 Kikkoman Corp Grinding of soybean
JP7649909B1 (en) * 2024-07-08 2025-03-21 キッコーマン株式会社 Soymilk manufacturing method and soymilk
WO2026014349A1 (en) * 2024-07-08 2026-01-15 キッコーマン株式会社 Method for producing soy milk and soy milk

Also Published As

Publication number Publication date
JPS6047648A (en) 1985-03-15

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