JPH0660446B2 - High-speed bath spinning method - Google Patents
High-speed bath spinning methodInfo
- Publication number
- JPH0660446B2 JPH0660446B2 JP58160404A JP16040483A JPH0660446B2 JP H0660446 B2 JPH0660446 B2 JP H0660446B2 JP 58160404 A JP58160404 A JP 58160404A JP 16040483 A JP16040483 A JP 16040483A JP H0660446 B2 JPH0660446 B2 JP H0660446B2
- Authority
- JP
- Japan
- Prior art keywords
- yarn
- flow
- bath
- flow tube
- tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims description 26
- 238000009987 spinning Methods 0.000 title claims description 22
- 238000005345 coagulation Methods 0.000 description 28
- 230000015271 coagulation Effects 0.000 description 28
- 230000007547 defect Effects 0.000 description 15
- 230000001112 coagulating effect Effects 0.000 description 6
- 238000002166 wet spinning Methods 0.000 description 3
- 229920000297 Rayon Polymers 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000010446 mirabilite Substances 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- RSIJVJUOQBWMIM-UHFFFAOYSA-L sodium sulfate decahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])(=O)=O RSIJVJUOQBWMIM-UHFFFAOYSA-L 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
Landscapes
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
Description
【発明の詳細な説明】 本発明は、湿式紡糸に於ける流浴紡糸方法に関する。更
に詳しくは内面が平滑な流管を用いた高速流浴紡糸方法
に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a flow bath spinning method in wet spinning. More specifically, it relates to a high-speed flow bath spinning method using a flow tube having a smooth inner surface.
湿式紡糸に於て、生産性を向上する為に高速度紡糸を行
うに際しては、形成された糸条が、凝固浴中を走行する
間に、浴抵抗をできるだけ減少しておく事が好ましい。
この為、形成された糸条を流動する凝固浴中に導びき走
行せしめる流浴紡糸方法が用いられる。When performing high-speed spinning for improving productivity in wet spinning, it is preferable to reduce the bath resistance of the formed yarn as much as possible while running in the coagulation bath.
Therefore, a flow bath spinning method is used in which the formed yarn is guided and run in a flowing coagulation bath.
流浴紡糸方法では、凝固浴中を走行する糸条速度と凝固
浴流速との差、即ち糸と凝固浴の相対速度が小さけれ
ば、小さい程好ましい。In the flow bath spinning method, the smaller the difference between the yarn speed running in the coagulation bath and the coagulation bath flow velocity, that is, the smaller the relative speed between the yarn and the coagulation bath, the better.
従って、生産性向上の要請に応え、紡糸速度を高めるに
は、流浴紡糸では凝固浴の流速を高めてゆく方法があっ
た。Therefore, in order to increase the spinning speed in response to the demand for improved productivity, there has been a method of increasing the flow velocity of the coagulation bath in the flow bath spinning.
ところが、この様な方法では、糸条と凝固浴が流管を出
た後、糸条を捲取等の後工程に走行せしめる為に、糸条
と凝固浴を分離する際に問題が発生する。However, in such a method, after the yarn and the coagulating bath leave the flow tube, the yarn is allowed to run to a subsequent process such as winding, so that there is a problem in separating the yarn and the coagulating bath. .
即ち、流管を出た後に糸条を凝固浴より分離しようとし
ても、速い凝固浴流の為に、糸条が取られ切糸が発生し
たり、糸条の単糸が取られ毛羽を発生したり、糸条の単
糸が取られ切断までには至らぬが部分的に伸長された単
糸たるみが生じる欠点があった。That is, even if an attempt is made to separate the yarn from the coagulation bath after leaving the flow tube, due to the fast coagulation bath flow, the yarn is taken off and the cutting yarn is generated, or the single yarn of the yarn is taken out and fluff is generated. However, there is a drawback that a single yarn of a yarn is taken and a slack of a partially extended single yarn is generated before cutting.
この様な欠点は、単糸の自己接着性を有するキュプラア
ンモニウムセルロース原液を除き、多くの湿式紡糸方法
に出現し、且つより生産性を向上する目的で高速度運転
を目指すと障害になるものであった。Such a defect appears in many wet spinning methods except for cupraammonium cellulose stock solution having a self-adhesive property of single yarn, and becomes an obstacle when aiming at high speed operation for the purpose of improving productivity. there were.
本発明者等は、高速度で流浴紡糸を行っても、流管出口
での糸条と凝固浴流の分離が容易で、凝固浴流に糸条又
は単糸が取られない流浴紡糸方法を検討してきた結果、
本発明に到達した。The present inventors have found that even if spinning bath spinning is performed at a high speed, it is easy to separate the filament and the coagulating bath stream at the outlet of the flow tube, and the filament or single yarn is not taken in the coagulating bath stream. As a result of examining the method,
The present invention has been reached.
すなわち、本発明は、流管を用いる流浴紡糸方法におい
て、上記流管の内面がガラス製のように平滑であって、
上記流管出口の糸条が進行する側の管内面又は管外面の
少なくとも一つの面に欠損部を設けた流管を用いる事を
特徴とする高速流浴紡糸方法である。That is, the present invention, in a flow bath spinning method using a flow tube, the inner surface of the flow tube is smooth like glass,
A high-speed flow-bath spinning method, characterized in that a flow tube provided with a defect in at least one of the inner surface or the outer surface of the tube on the side where the yarn advances at the outlet of the tube is used.
本発明でいう流管出口の糸条が進行する側の管内面又は
管外面の少なくとも一つの面に設けた欠損部とは、流管
の出口面であって、出口面と管の内面又は外面とをつな
ぐものであればよく、その大きさは極めて微少のもので
充分であるが、好ましくは長さ（周方向）が０．５〜
１．０ｍｍ、巾（半径方向）が０．５〜１．０ｍｍ、深
さ（軸方向）が０．０５〜０．２ｍｍのものである。In the present invention, the defect portion provided on at least one surface of the pipe inner surface or the pipe outer surface of the flow tube outlet on the side where the yarn advances is the outlet surface of the flow tube, and the outlet surface and the inner surface or the outer surface of the pipe. It suffices as long as it can connect to and the size thereof is extremely small, but the length (circumferential direction) is preferably 0.5 to
The thickness is 1.0 mm, the width (radial direction) is 0.5 to 1.0 mm, and the depth (axial direction) is 0.05 to 0.2 mm.
流管出口の糸条が進行する側に欠損部を設けた流管を用
いて流浴紡糸を行うと、流管出口の糸条が進行する側に
おいて、流出する凝固浴内に向けて大量の大気を気泡状
で吸入する事が判った。When flow bath spinning is carried out using a flow tube having a defect on the side where the yarn at the outlet of the flow tube advances, a large amount of water is discharged toward the inside of the coagulating bath at the side where the yarn at the outlet of the flow tube advances. It was found to inhale the air in the form of bubbles.
凝固浴内に吸入された大気は、気泡状でよく分散し、光
を当てて凝固浴流を観際すると、その部分の光沢が変わ
るので判るし、又流れる凝固浴を受けて目視でもその気
泡状態は良く観察出来る。The air inhaled in the coagulation bath is well dispersed in the form of bubbles, and when observing the coagulation bath flow by shining light, it can be seen that the gloss of that part changes, and also when the coagulation bath that flows is visually inspected The condition can be observed well.
この出口面の糸条が進行する側に欠損部を設けた流管を
用いて、流浴紡糸を実施してみると、従来法に比べ、流
管を出た後に糸条と凝固浴の分離が極めてスムースに実
施出来、糸条または単糸が凝固浴に取られ難い事が判っ
た。When the flow tube spinning was carried out using a flow tube with a defect on the yarn advancing side of the exit surface, when compared with the conventional method, the separation of the thread from the coagulation bath after the flow tube was separated. However, it was found that the yarn or the single yarn was difficult to be taken in the coagulation bath.
恐らく、凝固浴中に分散した気泡が、凝固浴へ糸条、又
は単糸が取られる事を妨げている事と思われる。Possibly, the air bubbles dispersed in the coagulation bath prevent the yarn or single yarn from being taken into the coagulation bath.
本発明方法の効果は、極めて簡単な方法で凝固浴と糸条
の分離を容易にするのみならず、糸条が凝固終了した位
置、すなわち、流管の出口で凝固浴流系に外乱を与える
だけなので、糸条形成に何等悪い影響を及ぼさない点に
ある。The effect of the method of the present invention is not only to facilitate the separation of the coagulation bath and the yarn in a very simple manner, but also to give a disturbance to the coagulation bath flow system at the position where the yarn has finished coagulation, that is, at the outlet of the flow tube. Since it is only, there is no adverse effect on the yarn formation.
更に、本発明方法を図面を用いて説明する。Further, the method of the present invention will be described with reference to the drawings.
第１図は本発明の流浴紡糸方法の実施態様の例を示す図
である。紡口１より吐出された糸条２は、矢印７でその
導入方向を示す凝固浴と共に流管３に走行する。流管３
の出口の糸条の進行方向には欠損部１０が設けられてお
り、この欠損部１０より大気は大気吸入方向１５の方向
に気泡９となって、流管を出た凝固浴流中に巻きこまれ
る。糸条２は、凝固浴流４と分離され糸道８を経て糸条
の進行方向を示す矢印５の方向に進行し、捲取等の後工
程（ここでは図示されない）へと導びかれる。流管出口
面に欠損部１０を設けた流管３を用いる事により、凝固
浴流４と糸条２の分離は容易となる。６はケーシングで
ある。FIG. 1 is a diagram showing an example of an embodiment of the flow bath spinning method of the present invention. The yarn 2 discharged from the spinneret 1 travels to the flow tube 3 together with the coagulation bath whose arrow 7 indicates the direction of introduction. Flow tube 3
A defect portion 10 is provided in the advancing direction of the yarn at the outlet of the, and the atmosphere from this defect portion 10 becomes a bubble 9 in the direction of the air intake 15 and is entrained in the coagulation bath flow exiting the flow tube. Be done. The yarn 2 is separated from the coagulation bath flow 4, travels in the direction of the arrow 5 indicating the traveling direction of the yarn through the yarn path 8, and is guided to a subsequent process (not shown here) such as winding. By using the flow tube 3 having the defect portion 10 on the exit surface of the flow tube, the coagulation bath flow 4 and the yarn 2 can be easily separated. 6 is a casing.
第２図（ａ）は従来法で用いられる流管出口形状を示
し、第２図（ｂ）、（ｃ）、（ｄ）は本発明方法で用い
る流管出口形状の例を示す。FIG. 2 (a) shows a flow tube outlet shape used in the conventional method, and FIGS. 2 (b), (c), and (d) show examples of the flow tube outlet shape used in the method of the present invention.
第２図（ａ）では、出口面１１、管内面１２、管外面１
３共に平滑で欠損部はない。第２図（ｂ）では、出口面
１１と管内面１２をつなぐ欠損部１４が設けられてい
る。管外面１３は平滑である。第２図（ｃ）では、出口
面１１と管外面１３をつなぐ欠損部１４が設けられ、管
内面１２は平滑である。第２図（ｄ）では、出口面１
１、管外面１３、管内面１２をつなぐ欠損部１４が設け
られている。In FIG. 2 (a), the outlet surface 11, the pipe inner surface 12, and the pipe outer surface 1
Both 3 are smooth and have no defect. In FIG. 2 (b), a defect portion 14 that connects the outlet surface 11 and the pipe inner surface 12 is provided. The tube outer surface 13 is smooth. In FIG. 2 (c), a defect portion 14 that connects the outlet surface 11 and the tube outer surface 13 is provided, and the tube inner surface 12 is smooth. In FIG. 2 (d), the exit surface 1
1. A defect portion 14 that connects the tube outer surface 13 and the tube inner surface 12 is provided.
以下実施例により、本発明の方法を説明する。The method of the present invention will be described below with reference to examples.
実施例 ビスコースを用いて流浴紡糸を行った。ビスコースはセ
ルロース６重量％、セカイソーダ８重量％を含有するも
のを用いた。凝固浴として、硫酸１４０ｇ／、芒硝２
６０ｇ／、硫酸亜鉛１５ｇ／を含有した５５℃の酸
浴を用いた。紡糸した糸条は、７５デニールの２６フィ
ラメントの糸で、第１図に示す方法で紡糸した。比較例
として第１図に示す方法に類似するが流管の出口に欠損
部のない流管を用いない方法で紡糸した。Example Flow bath spinning was performed using viscose. The viscose used contained 6 wt% cellulose and 8 wt% Sekai soda. As a coagulating bath, sulfuric acid 140g /, Glauber's salt 2
A 55 ° C. acid bath containing 60 g / and 15 g / zinc sulfate was used. The spun yarn was a 26-filament yarn of 75 denier and was spun by the method shown in FIG. As a comparative example, spinning was performed by a method similar to the method shown in FIG. 1 but without using a flow tube having no defect at the outlet of the flow tube.
用いた流管はガラス製で、長さ１．４ｍ、厚み１mmで、
内径は３．５mmで、その欠損部の形状は第１表に示す。The flow tube used was made of glass and had a length of 1.4 m and a thickness of 1 mm.
The inner diameter is 3.5 mm, and the shape of the defect is shown in Table 1.
各例共に、糸条の引取り速度を３２０ｍ／分、流管内の
凝固浴流速を２８０ｍ／分として紡糸して、流管出口で
の糸条と凝固浴流を分離する点で、糸条および単糸が凝
固浴流に取られる頻度を測定した（測定単位：回／２４
Ｈｒｓ・錘）。その結果を第２表に示す。 In each of the examples, the yarn take-up speed was 320 m / min, the coagulation bath flow rate in the flow tube was 280 m / min, and spinning was performed to separate the yarn at the outlet of the flow tube from the coagulation bath flow. The frequency at which the single yarn was taken by the coagulation bath flow was measured (measurement unit: 24 times)
Hrs / weight). The results are shown in Table 2.
上記実施例に示す如く、本発明の方法により、わずかな
欠損部を設けた流管を用いる事により、流浴紡糸の流管
出口での糸条および単糸が凝固浴に取られる頻度を大巾
に減少できた。 According to the method of the present invention, as shown in the above Examples, by using a flow tube provided with a slight defect, it is possible to increase the frequency at which the yarns and single yarns at the flow tube outlet of the flow bath spinning are taken in the coagulation bath. I was able to reduce to the width.
【図面の簡単な説明】 第１図は、本発明の流浴紡糸方法の実施態様の一例を示
す断面図であり、第２図は、流管出口形状を示す斜視図
であり、(a) は従来法の流管出口、(b) 、（ｃ）、
（ｄ）は本発明の方法で用いる流管出口の斜視図であ
る。また（ｅ）は（ｄ）の欠損部の拡大斜視図である。 １……紡口、２……糸条、３……流管、４……凝固浴
流、５……糸条の進行方向を示す矢印、６……ケーシン
グ、７……凝固浴流の導入方向を示す矢印、８……糸
道、９……気泡、１０……欠損部、１１……出口面、１
２……管内面、１３……管外面、１４……欠損部BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a sectional view showing an example of an embodiment of a flow bath spinning method of the present invention, and FIG. 2 is a perspective view showing a flow tube outlet shape, (a) Is the conventional tube outlet, (b), (c),
(D) is a perspective view of a flow tube outlet used in the method of the present invention. Further, (e) is an enlarged perspective view of the defective portion in (d). 1 ... Spinner, 2 ... Yarn, 3 ... Flow tube, 4 ... Coagulation bath flow, 5 ... Arrow indicating the traveling direction of yarn, 6 ... Casing, 7 ... Introduction of coagulation bath flow Directional arrow, 8 ... Thread path, 9 ... Bubble, 10 ... Missing part, 11 ... Exit surface, 1
2 ... Pipe inner surface, 13 ... Pipe outer surface, 14 ... Missing part
Claims (1)
流管の内面が平滑であって、上記流管出口の糸条が進行
する側の管内面又は管外面の少なくとも一つの面に欠損
部を設けた流管を用いる事を特徴とする高速流浴紡糸方
法。1. A flow bath spinning method using a flow tube, wherein the inner surface of the flow tube is smooth and at least one of the inner surface of the flow tube outlet and the outer surface of the tube on the side where the filament advances. A high-speed flow-bath spinning method characterized by using a flow tube provided with a section.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58160404A JPH0660446B2 (en) | 1983-09-02 | 1983-09-02 | High-speed bath spinning method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58160404A JPH0660446B2 (en) | 1983-09-02 | 1983-09-02 | High-speed bath spinning method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6052610A JPS6052610A (en) | 1985-03-25 |
| JPH0660446B2 true JPH0660446B2 (en) | 1994-08-10 |
Family
ID=15714202
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58160404A Expired - Lifetime JPH0660446B2 (en) | 1983-09-02 | 1983-09-02 | High-speed bath spinning method |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0660446B2 (en) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4427123Y1 (en) * | 1967-08-05 | 1969-11-13 |
-
1983
- 1983-09-02 JP JP58160404A patent/JPH0660446B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6052610A (en) | 1985-03-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AU692086B2 (en) | Method of producing cellulose fibres | |
| JPS5950763B2 (en) | Method of spinning aromatic polyamide solution | |
| RU2132418C1 (en) | Forming apparatus | |
| JPS6122042B2 (en) | ||
| CN1425813A (en) | Synthetic fibre containing animal protein and its preparing method | |
| JPH0660446B2 (en) | High-speed bath spinning method | |
| US2440057A (en) | Production of viscose rayon | |
| JPH0370006B2 (en) | ||
| US2136464A (en) | Method of preparing tubular artificial textile threads | |
| US2136462A (en) | Method of making tubular artificial textile threads | |
| JPH0660447B2 (en) | High-speed flowing bath wet spinning method | |
| US2731667A (en) | Wet spinning apparatus | |
| US3103732A (en) | Composite bulky regenerated cellulose yarn | |
| KR840001627B1 (en) | Continuous spinning method of viscose rayon | |
| US2895790A (en) | Production and treatment of artificial filamentary materials | |
| US1583534A (en) | Manufacture of artificial silk and like materials from viscose solutions | |
| US3248466A (en) | Process for producing two component crimpable regenerated cellulose fiber | |
| US2097034A (en) | Manufacture of artificial silk | |
| JP4827321B2 (en) | Circular nozzle for wet spinning | |
| US2565908A (en) | Method of insolubilizing artificial filaments of vegetable protein | |
| GB703613A (en) | Process for spinning artificial fibres | |
| US3219740A (en) | High speed tubular spinning of fine viscose rayon yarn | |
| JP2707274B2 (en) | Method for producing porous regenerated cellulose hollow fiber | |
| US2149197A (en) | Manufacture and production of staple fiber | |
| SU1077956A1 (en) | Method of producing crimped hydrate-cellulose yarn |