JPH0667441B2 - Gas-liquid dispersion plate - Google Patents
Gas-liquid dispersion plateInfo
- Publication number
- JPH0667441B2 JPH0667441B2 JP61033023A JP3302386A JPH0667441B2 JP H0667441 B2 JPH0667441 B2 JP H0667441B2 JP 61033023 A JP61033023 A JP 61033023A JP 3302386 A JP3302386 A JP 3302386A JP H0667441 B2 JPH0667441 B2 JP H0667441B2
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- gas
- dispersion plate
- passage hole
- liquid passage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Landscapes
- Gas Separation By Absorption (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、向流形の気液接触装置に使用される通気及び
通液用の分散板(気液分散板)に係り、特に液体を均一
に流下せしめるための通液孔の構造に関する。TECHNICAL FIELD The present invention relates to a dispersion plate (gas-liquid dispersion plate) for ventilation and liquid passage used in a countercurrent type gas-liquid contact device, and particularly to a liquid. The present invention relates to the structure of liquid passage holes for allowing the liquid to flow uniformly.
気体と液体を向流で接触させ、物質移動或いは熱移動の
操作を行わせる気液接触装置では気体と液体とを均一に
分散させることが大切である。特に気液接触装置が充て
ん塔である場合には液体の分散性がその性能を大きく左
右する。このため、従来より液体の分散性を均一にする
ために多くの形状の気液分散板が提案されている。例え
ば特公昭57−1281号公報に記載の気液分散板の構造があ
る。しかし、従来はその構造が複雑であった。また、構
造が簡単な気液分散板に対しては、通気管の他に通液孔
として単に気液分散板の平面に液孔をあけたのみという
気液分散板が一般的である。しかし、この構造では気液
分散板の下面が液切れに悪影響を及ぼし、良好な液分散
が行なわれない欠点があった。It is important to uniformly disperse the gas and the liquid in a gas-liquid contacting device in which the gas and the liquid are brought into countercurrent contact with each other to perform mass transfer or heat transfer operation. Especially when the gas-liquid contactor is a packed column, the dispersibility of the liquid greatly affects its performance. For this reason, gas-liquid dispersion plates having many shapes have been conventionally proposed in order to make the dispersibility of the liquid uniform. For example, there is a structure of a gas-liquid dispersion plate described in Japanese Patent Publication No. 57-1281. However, in the past, its structure was complicated. Further, for a gas-liquid dispersion plate having a simple structure, a gas-liquid dispersion plate is generally used in which a liquid hole is simply formed in the plane of the gas-liquid dispersion plate as a liquid passage hole in addition to the ventilation pipe. However, in this structure, the lower surface of the gas-liquid dispersion plate has an adverse effect on liquid breakage, and there is a drawback that good liquid dispersion is not performed.
〔発明が解決しようとする問題点〕 気液分散板により液体を均一に流下させるためには液体
の物性等を考慮し、通液孔を通った液体が他の通液孔よ
りの液体と互いに干渉することもなく流下し、更に通液
孔を通った液体が分散板下面より離脱する際、分散板下
面を移動することなく流下することが重要な課題とな
る。しかし、良好な液分散性を得ようとすれば、上記従
来技術のように構造が複雑となり、製造価格が高価にな
る問題点があった。また、逆に簡易な構造の気液分散板
にすれば良好な液体の分散性が得られず、気液接触装置
の性能を十分に引き出すことができない問題があった。
本発明の目的は、構造が簡単で、更に良好な液分散性を
得ることができる気液分散板を提供することにある。[Problems to be Solved by the Invention] In order to allow the liquid to flow down uniformly by the gas-liquid dispersion plate, considering the physical properties of the liquid, etc. An important issue is that the liquid flows down without any interference, and when the liquid that has passed through the liquid passage holes is separated from the lower surface of the dispersion plate, it flows down without moving on the lower surface of the dispersion plate. However, in order to obtain good liquid dispersibility, there is a problem that the structure becomes complicated and the manufacturing cost becomes high as in the above-mentioned conventional technique. On the other hand, if a gas-liquid dispersion plate having a simple structure is used, good liquid dispersibility cannot be obtained, and there is a problem that the performance of the gas-liquid contact device cannot be sufficiently brought out.
An object of the present invention is to provide a gas-liquid dispersion plate having a simple structure and capable of obtaining good liquid dispersibility.
上記問題点を解決するためには、通液孔を通った液体が
気液分散板下面より離脱する際に、気液分散板下面の影
響、あるいは他の通液孔より流下する液体との干渉を防
ぐことが重要である。上記目的は、気液分散板の通液孔
の下面側に各々の通液孔の周囲に液切り用の溝を設ける
ことにより達成される。In order to solve the above problems, when the liquid that has passed through the liquid passage hole is separated from the lower surface of the gas-liquid dispersion plate, the influence of the lower surface of the gas-liquid dispersion plate or the interference with the liquid flowing down from other liquid passage holes It is important to prevent The above object is achieved by providing a groove for draining liquid around each liquid passage hole on the lower surface side of the liquid passage hole of the gas-liquid dispersion plate.
通液孔の周囲に設けられた溝は、他の通液孔より流下す
る液体の液切りとして作用する。このため、通液孔を通
って、気液分散板下面より流下する液体は他の通液孔よ
り流下する液体により干渉されることなく流下する。ま
た、分散板下面での液の横方向への移動が溝によりさえ
ぎられるため良好な液体の分散性を得ることができる。The groove provided around the liquid passage hole acts as a drain for the liquid flowing down from the other liquid passage holes. Therefore, the liquid flowing down from the lower surface of the gas-liquid dispersion plate passes through the liquid passage holes, and flows down without being interfered with by the liquid flowing down from the other liquid passage holes. Further, since the lateral movement of the liquid on the lower surface of the dispersion plate is blocked by the groove, good liquid dispersibility can be obtained.
以下、本発明の第1の実施例を第1A図および第1B図によ
って説明する。第1A図は断面図,第1B図は下方からの平
面図を示す。1は下方からの気体を上方に流す通気管、
2は上方から流下する液体を下方に流下せしめる通液孔
であり、気液分散板4に均一に、あるいはランダムに設
置されている。5は気液接触装置の外壁である。気液分
散板4の下面の通液孔部には、通液孔2と同心円状に形
成された液切り溝3を備えている。気液分散板4は外壁
5により構成される気液接触装置内に縦方向に数か所設
置される。次に本発明の動作を説明する。ここでは気液
接触装置の内部に設置される気液接触部材が充てん物で
ある充てん塔について説明する。Hereinafter, a first embodiment of the present invention will be described with reference to FIGS. 1A and 1B. FIG. 1A shows a sectional view, and FIG. 1B shows a plan view from below. 1 is a ventilation pipe that allows gas from below to flow upward,
Reference numeral 2 is a liquid passage hole through which the liquid flowing down from above is allowed to flow downward, and is uniformly or randomly installed in the gas-liquid dispersion plate 4. 5 is the outer wall of the gas-liquid contact device. A liquid cut groove 3 formed concentrically with the liquid passage hole 2 is provided in the liquid passage hole portion on the lower surface of the gas-liquid dispersion plate 4. The gas-liquid dispersion plate 4 is installed in several places in the vertical direction in the gas-liquid contact device constituted by the outer wall 5. Next, the operation of the present invention will be described. Here, a packed column in which the gas-liquid contact member installed inside the gas-liquid contactor is a packing will be described.
充てん塔上部から供給された液体は、下部から上昇する
気体と向流接触し、個々の充てん物層を貫流する。充て
ん物層を流下する液体は自然流下であるため、充てん物
層の長さが長い場合には充てん塔の横断面に対し均一な
液体の流下が困難となる。したがって、気液分散板は液
体が充て物層を流下し、その均一性が悪くなる前に設置
され、上方からの液体を受け止め、更に充てん塔の横断
面全体に対し、均一に分配させて再び下方の充てん層内
へ供給する。気液分散板では、下方からの気体は通気管
1を通って流下する。分散板の平板上に溜る液深さは、
液体物量のほぼ2乗に比例する。また、液体の分散性を
良くするためには、通気孔より流下する液体の圧力を大
きくすればある程度改善できる。圧力を大きくすること
は分散板上の液深さを大きくすれば良い。しかし、液深
さを大きくすることは充てん塔の塔高さの増大、あるい
は、液深さが液体物量の2乗に比例することから、操作
条件又は増減運転が困難となる。このため分散板上の液
深さはできるだけ小さくすることが望ましい。上方より
気液分散板4上の平板上に流下した液体は分散板上に一
定の液深さを保ちつつ通液孔2に流入する。通液孔より
出た液は通液孔の下面で液滴を形成し分散板下面側に付
着する。更に通液孔に液体が供給されると液体の粘度あ
るいは表面張力と液滴の自重のバランスがくずれ、液体
は下方へ流下する。ここで、従来技術のように液切り溝
がない場合(つまり通液孔のみの場合)、液体が通液孔
より離脱して流下する際、分散板の下面の影響により隣
の通液孔の液体と合流して流下するため均一性が悪くな
る。これは、気液接触の効率低下の原因となる。これに
対し、第1A図,第1B図に示す実施例では、通液孔の下側
に用けた液切り溝の働きにより、通液孔からの液体は気
液分散板より離脱し易くなる。このめ、通液孔を通った
液体は、気液分散板の下面の影響を受けることなく独立
して流下する。したがって、本発明での気液分散板での
液体は充てん塔の横断面に対し均一に分散して流下す
る。また、塔の傾斜、あるいは気液分散板の取付の誤差
により気液分散板が傾斜して取付けられた場合、液切り
溝が特に有効に作用し、液切り溝のなにい場合の気液分
散板下面での傾斜方向への液体の移動がなくなり、良好
な液分散を得ることができる。The liquid supplied from the upper part of the packed column comes into countercurrent contact with the gas rising from the lower part and flows through the individual packed beds. Since the liquid flowing down the packing layer is a natural flow, if the packing layer is long, it becomes difficult to flow the liquid uniformly over the cross section of the packing column. Therefore, the gas-liquid dispersion plate is installed before the liquid fills the material layer and its uniformity deteriorates, receives the liquid from above, and distributes it evenly over the entire cross section of the packed column and again. Supply into the lower packed bed. In the gas-liquid dispersion plate, the gas from below flows down through the ventilation pipe 1. The depth of the liquid accumulated on the flat plate of the dispersion plate is
It is approximately proportional to the square of the liquid amount. Further, in order to improve the dispersibility of the liquid, it can be improved to some extent by increasing the pressure of the liquid flowing down from the ventilation hole. The pressure can be increased by increasing the liquid depth on the dispersion plate. However, increasing the liquid depth increases the tower height of the packed column, or the liquid depth is proportional to the square of the liquid amount, which makes operating conditions or increasing / decreasing operation difficult. Therefore, it is desirable to make the liquid depth on the dispersion plate as small as possible. The liquid that has flowed down onto the flat plate on the gas-liquid dispersion plate 4 from above flows into the liquid passage hole 2 while maintaining a constant liquid depth on the dispersion plate. The liquid flowing out from the liquid passage hole forms droplets on the lower surface of the liquid passage hole and adheres to the lower surface side of the dispersion plate. When the liquid is further supplied to the liquid passage hole, the balance between the viscosity or surface tension of the liquid and the weight of the liquid droplet is lost, and the liquid flows downward. Here, when there is no liquid drain groove as in the prior art (that is, in the case of only the liquid passage hole), when the liquid separates from the liquid passage hole and flows down, due to the influence of the lower surface of the dispersion plate, the adjacent liquid passage hole Since it merges with the liquid and flows down, the uniformity deteriorates. This causes a reduction in the efficiency of gas-liquid contact. On the other hand, in the embodiment shown in FIGS. 1A and 1B, due to the action of the liquid drainage groove provided on the lower side of the liquid passage hole, the liquid from the liquid passage hole is easily separated from the gas-liquid dispersion plate. Therefore, the liquid that has passed through the liquid passages flows down independently without being affected by the lower surface of the gas-liquid dispersion plate. Therefore, the liquid in the gas-liquid dispersion plate of the present invention is uniformly dispersed and flows down on the cross section of the packed column. Also, when the gas-liquid dispersion plate is installed with an inclination due to the tilt of the tower or an error in the installation of the gas-liquid dispersion plate, the liquid cutting groove works particularly effectively, and gas liquid The liquid does not move in the tilt direction on the lower surface of the dispersion plate, and good liquid dispersion can be obtained.
第2A図,第2B図に本発明の他の実施例を示す。第2A図は
断面図、第2B図は下方からの平面図ある。液切り溝3の
構成を格子状にし、その内側に通液孔を設けたものであ
る。その他の構成及び動作については第1の実施例と同
じである。Another embodiment of the present invention is shown in FIGS. 2A and 2B. FIG. 2A is a sectional view, and FIG. 2B is a plan view from below. The liquid cutting grooves 3 are formed in a lattice shape, and liquid passage holes are provided inside thereof. Other configurations and operations are the same as those in the first embodiment.
本発明によれば、気液分散板の通液孔の周囲に液切り溝
を設けるという簡単な構造で液体の気液分散板からの液
切れを良好にでき、液体の均一な分散性を得ることがで
きる。また、気液分散板の傾きに対しても液分散に悪影
響を与えることなく良好な液分散を得ることができる。According to the present invention, a simple structure of providing a liquid cutting groove around the liquid passage hole of the gas-liquid dispersion plate can satisfactorily drain the liquid from the gas-liquid dispersion plate and obtain uniform dispersion of the liquid. be able to. Also, good liquid dispersion can be obtained without adversely affecting the liquid dispersion with respect to the inclination of the gas-liquid dispersion plate.
第1A図は本発明の第1の実施例における断面図、第1B図
は本発明の第1の実施例における下方からの平面図、第
2A図は本発明の第2の実施例における断面図、第2B図は
本発明の第2の実施例における下方からの平面図であ
る。 1……通気管、2……通液孔、3……液切り溝、4……
気液分散板、5……気液接触装置外壁FIG. 1A is a cross-sectional view of the first embodiment of the present invention, and FIG. 1B is a plan view from below in the first embodiment of the present invention.
FIG. 2A is a sectional view in the second embodiment of the present invention, and FIG. 2B is a plan view from below in the second embodiment of the present invention. 1 ... Vent pipe, 2 ... Liquid passage hole, 3 ... Liquid cut groove, 4 ...
Gas-liquid dispersion plate, 5 ... Outer wall of gas-liquid contact device
───────────────────────────────────────────────────── フロントページの続き (72)発明者 山崎 正博 山口県下松市大字東豊井794番地 株式会 社日立製作所笠戸工場内 (56)参考文献 実開 昭55−21012(JP,U) ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Masahiro Yamazaki Inventor Masahiro Yamato Prefecture, Shimomatsu City, Oita 794, Higashitoyoi, Ltd. Kasado Plant, Hitachi, Ltd. (56) References
Claims (2)
入して内部の気液接触部材により気液の接触を行なう気
液接触装置の通気及び通液分散板において、前記分散板
に少なくとも1個以上設けられている通液孔の下面側に
各々の通液孔と同心円状に溝を設けたことを特徴とする
前記分散板。1. An aeration and liquid passage dispersion plate of a gas-liquid contactor for introducing a liquid from an upper part of a tower and a gas from a lower part of the tower to contact a gas-liquid with an internal gas-liquid contact member. The dispersion plate is characterized in that at least one or more liquid passage holes are provided on the lower surface side of the liquid passage holes concentrically with the respective liquid passage holes.
いて、分散板下面側に溝を格子状に設け、夫々の格子の
中心に通液孔を設置したことを特徴とする気液分散板。2. The gas-liquid dispersion plate according to claim 1, wherein grooves are provided in a grid pattern on the lower surface side of the dispersion plate, and a liquid passage hole is provided at the center of each grid. Dispersion plate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61033023A JPH0667441B2 (en) | 1986-02-19 | 1986-02-19 | Gas-liquid dispersion plate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61033023A JPH0667441B2 (en) | 1986-02-19 | 1986-02-19 | Gas-liquid dispersion plate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62193601A JPS62193601A (en) | 1987-08-25 |
| JPH0667441B2 true JPH0667441B2 (en) | 1994-08-31 |
Family
ID=12375192
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61033023A Expired - Lifetime JPH0667441B2 (en) | 1986-02-19 | 1986-02-19 | Gas-liquid dispersion plate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0667441B2 (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016064413A (en) * | 2015-11-18 | 2016-04-28 | エア プロダクツ アンド ケミカルズ インコーポレイテッドAir Products And Chemicals Incorporated | Shielding in separation column |
| JP7059063B2 (en) * | 2018-03-23 | 2022-04-25 | 株式会社東芝 | Washer, hydrogen production equipment and power supply system |
| JP7759232B2 (en) * | 2021-10-22 | 2025-10-23 | 大陽日酸株式会社 | liquid dispensing device |
-
1986
- 1986-02-19 JP JP61033023A patent/JPH0667441B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS62193601A (en) | 1987-08-25 |
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