JPH072430B2 - Recording sheet - Google Patents
Recording sheetInfo
- Publication number
- JPH072430B2 JPH072430B2 JP1121414A JP12141489A JPH072430B2 JP H072430 B2 JPH072430 B2 JP H072430B2 JP 1121414 A JP1121414 A JP 1121414A JP 12141489 A JP12141489 A JP 12141489A JP H072430 B2 JPH072430 B2 JP H072430B2
- Authority
- JP
- Japan
- Prior art keywords
- ink
- pseudo
- boehmite
- recording sheet
- receiving layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Ink Jet Recording Methods And Recording Media Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Description
【発明の詳細な説明】 ［産業上の利用分野］ 本発明は、水性および油性のいずれのインクでも記録可
能な透明シートに関するものである。TECHNICAL FIELD The present invention relates to a transparent sheet capable of recording with both water-based and oil-based inks.
［従来の技術］ 近年、各種学会、会議等のプレゼンテーション用とし
て、従来のスライドプロジェクターに替わり、オーバー
ヘッドプロジェクターが用いられる機会が多くなってい
る。また、印刷の分野でも、各種の出版物や、包装等の
用途で、透明な印刷物が求められるようになっている。[Prior Art] In recent years, an overhead projector has been increasingly used in place of a conventional slide projector for presentations at various academic conferences and conferences. Also in the field of printing, transparent printed materials are required for various publications and applications such as packaging.
これらの透明なシートへの印字、印刷は、基材であるシ
ートそれ自体に吸収性が無いため、一般の紙面上に行な
う印刷に比べ印刷の速度や乾燥の面で特別な配慮が必要
である。Printing and printing on these transparent sheets require special consideration in terms of printing speed and drying, as compared with printing performed on general paper, because the sheet itself, which is the base material, has no absorbability. .
また、オーバーヘッドプロジェクター用のシート等の、
ごく少量の印刷物を得るために、パーソナルコンピュー
ターやワープロを用いて原稿を編集し、プリンターによ
って印字する方法が広く行なわれており、そのプリンタ
ーとして、フルカラー化が容易なことからインクジェッ
ト方式が注目されている。Also, such as seats for overhead projectors,
In order to obtain a very small amount of printed matter, a method of editing an original with a personal computer or a word processor and printing it with a printer is widely used, and as the printer, an inkjet method has been attracting attention because it is easy to make full color. There is.
また、インク受容層中に半径40〜1000Åの細孔を持つ多
孔性アルミナキセロゲルを有するインクジェット記録媒
体も知られている。（特開昭60−245588号公報参照） ［発明の解決しようとする問題点］ しかしながら、透明シートに対して従来の如きインクジ
ェット方式を採用すると、多量のインクが取り扱われる
ため、吸収性の乏しい透明シートへの印字はごく低品位
の場合のみ可能であり、フルカラー化は殆ど不可能に近
かった。Further, an ink jet recording medium having a porous alumina xerogel having pores with a radius of 40 to 1000Å in an ink receiving layer is also known. (See Japanese Patent Laid-Open No. 60-245588) [Problems to be Solved by the Invention] However, when a conventional ink jet method is used for a transparent sheet, a large amount of ink is handled, and thus the transparency is poor. Printing on a sheet was possible only when the quality was very low, and full-color printing was almost impossible.
また、特開昭60−245588号に示されたインクジェット記
録媒体においては、インクの受容体としてアルミナキセ
ロゲルが用いられているため、粒子径が比較的大きくな
り、従って、粒子間間隙も大きくなる。この結果、光の
散乱が生じ、透明性が損なわれ、像が白っぽくなる欠点
を有している。そしてこの傾向は基材が透明材である程
著しくなる。Further, in the ink jet recording medium disclosed in JP-A-60-245588, since the alumina xerogel is used as the ink receptor, the particle size becomes relatively large, and therefore the interparticle gap becomes large. As a result, light is scattered, the transparency is impaired, and the image becomes whitish. This tendency becomes more remarkable as the base material is a transparent material.
［問題点を解決するための手段］ 本発明者はこれら従来法が有する諸欠点を排除し、透明
基材上にインクジェットプリントを施しても透明性を失
わず、かつ充分にフルカラー発色し得る記録用シートを
得ることを目的として種々の研究、検討した結果、特定
のアルミナを特定の細孔容積に揃えて透明シート上にイ
ンクの受容層として用いることにより前記目的を達成し
得ることを見出した。[Means for Solving Problems] The present inventor eliminates various drawbacks of the conventional methods, does not lose transparency even when inkjet printing is performed on a transparent substrate, and is capable of full color development. As a result of various studies for the purpose of obtaining a sheet for use, it was found that the above object can be achieved by aligning a specific alumina with a specific pore volume and using it as an ink receiving layer on a transparent sheet. .
かくして本発明は、透明な基材上に多孔質のインク受容
層を設けた記録用シートにおいて、インク受容層が主と
して擬ベーマイトよりなり、そのインク受容層の半径10
0〜1000Åを有する細孔の全容積が0.1cc/g以下であるこ
とを特徴とする記録用シートを提供するにある。Thus, the present invention provides a recording sheet in which a porous ink-receiving layer is provided on a transparent substrate, the ink-receiving layer mainly consisting of pseudo-boehmite and having a radius of 10 mm.
Another object of the present invention is to provide a recording sheet characterized in that the total volume of pores having 0 to 1000Å is 0.1 cc / g or less.
本発明に用いられる基材としては、透明であれば特に限
定はされず、例えばポリエチレンテレフタレート、ポリ
エステル、ジアセテート等の有機フィルムやシート、各
種ガラス等を用い得る。The substrate used in the present invention is not particularly limited as long as it is transparent, and for example, an organic film or sheet of polyethylene terephthalate, polyester, diacetate or the like, various glasses and the like can be used.
また、基材の厚さは目的により選ばれ、特に限定されな
い。これら基材は、使用に際し、後述するインク受容層
との接着性を良好ならしめるため、コロナ放電処理等の
表面処理を行なったり、プレコート層を設けることも出
来る。The thickness of the base material is selected according to the purpose and is not particularly limited. These substrates may be subjected to surface treatment such as corona discharge treatment or may be provided with a precoat layer in order to improve the adhesiveness to the ink receiving layer described later when used.
本発明におけるインク受容体としては擬ベーマイトが用
いられる。かかる擬ベーマイトとしては、半径100〜100
0Åを有する細孔の全容積が0.1cc/g以下である必要があ
る。かかる半径およびその全容積が前記範囲を超過する
場合には、光の散乱が生じ、印刷された像が白っぽくな
りフルカラー化が困難となるので不適当である。Pseudo-boehmite is used as the ink receptor in the present invention. Such pseudo-boehmite has a radius of 100-100
The total volume of pores having 0Å must be 0.1 cc / g or less. When the radius and the total volume thereof exceed the above range, light scattering occurs, and the printed image becomes whitish, which makes it difficult to form a full color image.
望ましくはこれらの物性に加え、インク受容体の半径40
〜100Åを有する細孔の全容積が0.1〜0.4cc/g、更に望
ましくはこれに加うるに半径10〜40Å未満を有する細孔
の全容積が0.2〜1.0cc/gが好ましい。かくすることによ
り、いずれの色においても十分発色し、鮮明な像を得る
ことができる。Desirably, in addition to these physical properties, the radius of the ink receiver is 40
It is preferable that the total volume of the pores having a volume of -100 liters is 0.1 to 0.4 cc / g, and more desirably, the total volume of the pores having a radius of 10 to less than 40 liters is 0.2 to 1.0 cc / g. By doing so, it is possible to obtain a clear image with sufficient color development in any color.
そして、本発明においてはこれら物性を有するインクの
受容体として擬ベーマイトを用いる場合に限り、インク
中の染料を十分吸着し、透明性を損なわない程度の細孔
容積でも十分な発色効果が得られ、他のアルミナ物質で
は困難である。And, in the present invention, only when using pseudo-boehmite as the receptor of the ink having these physical properties, a sufficient coloring effect can be obtained even with a pore volume that sufficiently adsorbs the dye in the ink and does not impair the transparency. , It is difficult with other alumina materials.
更に具体的には後述する実施例に示した如き触媒化成工
業（株）から市販されている商品名「カタロイドAS−
３」の如き擬ベーマイトゾルに代表される様な、Al2O3
固形分に換算して７重量％を含有するアルミナゾルを純
水により100倍に稀釈し、これを親水化したコロジオン
膜上に滴下して乾燥せしめた場合、一定方向に配向した
毛束状のアルミナ水和物の集合体を形成する様なアルミ
ナゾルから得られる擬ベーマイトが最適である。More specifically, the trade name "Cataloid AS-", which is commercially available from Catalyst Kasei Kogyo Co., Ltd., as shown in Examples described later.
Al 2 O 3 as represented by pseudo-boehmite sol
Alumina sol containing 7% by weight in terms of solid content was diluted 100 times with pure water, and when this was dropped on a hydrophilized collodion film and dried, hair bundle-shaped alumina oriented in a fixed direction Pseudo-boehmite obtained from an alumina sol which forms a hydrate aggregate is the most suitable.
かかる擬ベーマイトの層厚は印刷、印字に用いられるイ
ンク量により適宜選択されるが、一般には１〜20μ程度
を採用するのが適当である。層厚が前記範囲を逸脱する
と発色性が不安定になったり透明性が損なわれたりする
恐れがあるので好ましくない。擬ベーマイト層を透明基
材上に設ける手段としては、擬ベーマイトとバインダー
の混合スラリーをロールコーター、エアナイフコータ
ー、ブレードコーター、ロッドコーター、バーコーター
等の各種コーターにより基材上に塗布し、乾燥する手段
が主として用いられる。擬ベーマイトとしては、そのゾ
ルを用いると好ましいインク受容層を容易に得ることが
できるので望ましい。The layer thickness of such pseudo-boehmite is appropriately selected depending on printing and the amount of ink used for printing, but it is generally suitable to employ about 1 to 20 μm. If the layer thickness deviates from the above range, the color developability may become unstable or the transparency may be impaired, such being undesirable. As means for providing the pseudo-boehmite layer on the transparent substrate, a mixed slurry of the pseudo-boehmite and the binder is applied onto the substrate by various coaters such as a roll coater, an air knife coater, a blade coater, a rod coater and a bar coater, and dried. Means are mainly used. As the pseudo-boehmite, it is desirable to use the sol because a preferable ink receiving layer can be easily obtained.
バインダーとしては、一般にデンプンやその変性物、PV
Aやその変性物、SBRラテックス、NBRラテックス、ヒド
ロキシセルロース、ポリビニルピロリドン等の有機物を
用いることができる。As a binder, starch, its modified products, PV
Organic substances such as A and its modified products, SBR latex, NBR latex, hydroxycellulose, and polyvinylpyrrolidone can be used.
また、その使用量は、余り少ないと受容層の強度が不十
分となり、逆に余り多すぎるとインクの吸収性を阻害す
るので好ましくなく、一般に擬ベーマイトの10〜50重量
％程度を採用するのが適当である。尚、本発明における
細孔径分布の測定は窒素吸脱着法（オミクロンテクノロ
ジー社製オムニソープ100」）により行なった。If the amount used is too small, the strength of the receptive layer will be insufficient, and on the contrary, if the amount is too large, the ink absorbency will be impaired. Is appropriate. The pore size distribution in the present invention was measured by a nitrogen adsorption / desorption method (Omnisorb 100 manufactured by Omicron Technology).
以下に実施例に示すが、本発明による記録シートはイン
クジェット方式のみに用い得るものではない。Examples will be shown below, but the recording sheet according to the present invention cannot be used only for the ink jet system.
［実施例］ 尚、実施例、比較例で得られた記録用シートの評価方法
は次に示す方法で行なった。[Examples] The recording sheets obtained in Examples and Comparative Examples were evaluated by the following methods.
印字：シャープ社カラーイメージジェットプリンター
IO-735を用いて、黒色で1cm×1cmのパターンを印字し
た。Printing: Sharp Color Image Jet Printer
A 1 cm x 1 cm pattern was printed in black using IO-735.
色濃度：で印字したシートに白紙で裏あてをして、
黒色の反射色濃度をサクラデンシトメータPDA45で測定
した。Color density: Back the sheet printed with with a blank sheet,
The black reflection color density was measured with a Sakura Densitometer PDA45.
解像度：で印字したシートのパターンのにじみ具合
から４段階で評価した。Resolution: The degree of bleeding of the pattern of the sheet printed with was evaluated in four levels.
（0:最悪、3:最良） 透明性：印字していない部分に黒紙で裏あてをして色
濃度を測定した。黒紙そのものの色濃度を100とし、％
で表したものを評価値とした。(0: Worst, 3: Best) Transparency: The non-printed part was backed with black paper and the color density was measured. The color density of the black paper itself is 100, and%
What was represented by was made into the evaluation value.
ヘイズ:JIS K-7105によった。Haze: According to JIS K-7105.
実施例 擬ベーマイトゾル（触媒化成社製カタロイドAS-3）５重
量部（固形分）、ポリビニルアルコール（クラレ社製PV
A117）１重量部（固形分）および水からなる固形分約10
重量％のコート液を調整し、ポリエチレンテレフタレー
トフィル（東レ社製、厚さ100μ）に、バーコーターに
より乾燥時の膜厚が５μとなるよう塗布し乾燥して記録
用シートを得た。Example 5 parts by weight (solid content) of pseudo-boehmite sol (Cataloid AS-3 manufactured by Catalyst Kasei), polyvinyl alcohol (PV manufactured by Kuraray Co., Ltd.)
A117) Solid content consisting of 1 part by weight (solid content) and water about 10
A coating liquid of weight% was prepared and applied to polyethylene terephthalate fill (manufactured by Toray Industries, Inc., thickness 100 μm) by a bar coater so that the film thickness when dried was 5 μm, and dried to obtain a recording sheet.
比較例１ 実施例１の擬ベーマイトゾルの代わりにアモルファスア
ルミナゾル（日産化学社製アルミナゾル100）を用いた
以外は実施例１と同様の方法でシートを得た。Comparative Example 1 A sheet was obtained in the same manner as in Example 1 except that an amorphous alumina sol (Alumina sol 100 manufactured by Nissan Chemical Industries, Ltd.) was used in place of the pseudo-boehmite sol of Example 1.
比較例２ 実施例１の擬ベーマイトゾルの代わりにシリカゾル（触
媒化成社製カタロイドSI-40）を用いた以外は実施例１
と同様の方法でシートを得た。Comparative Example 2 Example 1 except that silica sol (Cataloid SI-40 manufactured by Catalyst Kasei) was used in place of the pseudo-boehmite sol of Example 1.
A sheet was obtained in the same manner as in.
これらのシートのインク受容層の物性および評価結果を
表１に示す。Table 1 shows the physical properties and evaluation results of the ink receiving layer of these sheets.
Claims (3)
けた記録用シートにおいて、インク受容層が主として擬
ベーマイトよりなり、そのインク受容層の半径100〜100
0Åを有する細孔の全容積が0.1cc/g以下であることを特
徴とする記録用シート。1. A recording sheet in which a porous ink-receiving layer is provided on a transparent substrate, the ink-receiving layer mainly consisting of pseudo-boehmite, and the radius of the ink-receiving layer is 100 to 100.
A recording sheet characterized in that the total volume of pores having 0Å is 0.1 cc / g or less.
細孔の全容積が0.2〜1.0cc/g、かつ、半径40〜100Åを
有する細孔の容積が0.1〜0.4cc/gである請求項１の記録
用シート。2. The ink receiving layer has pores having a radius of 10 to 40 Å, the total volume of pores is 0.2 to 1.0 cc / g, and the volume of pores having a radius of 40 to 100 Å is 0.1 to 0.4 cc / g. The recording sheet according to claim 1.
７重量％を含有するアルミナゾルを純水により100倍に
稀釈し、これを親水化したコロジオン膜上に滴下して乾
燥せしめた場合、一定方向に配向した毛状束のアルミナ
水和物の集合体を形成する様なアルミナゾルから得られ
る擬ベーマイトである請求項１または請求項２の記録用
シート。3. Pseudo-boehmite is prepared by diluting an alumina sol containing 7% by weight in terms of Al 2 O 3 solid content with pure water 100 times, and dropping this on a hydrophilized collodion film to dry it. The recording sheet according to claim 1 or 2, which is a pseudo-boehmite obtained from an alumina sol that forms an aggregate of alumina hydrates of hair-like bundles oriented in a certain direction.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP31644488 | 1988-12-16 | ||
| JP1-19829 | 1989-01-31 | ||
| JP1982989 | 1989-01-31 | ||
| JP63-316444 | 1989-01-31 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02276670A JPH02276670A (en) | 1990-11-13 |
| JPH072430B2 true JPH072430B2 (en) | 1995-01-18 |
Family
ID=26356688
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1121414A Expired - Fee Related JPH072430B2 (en) | 1988-12-16 | 1989-05-17 | Recording sheet |
| JP1180563A Pending JPH02276671A (en) | 1988-12-16 | 1989-07-14 | Recording sheet |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1180563A Pending JPH02276671A (en) | 1988-12-16 | 1989-07-14 | Recording sheet |
Country Status (1)
| Country | Link |
|---|---|
| JP (2) | JPH072430B2 (en) |
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|---|---|---|---|---|
| JPH11321070A (en) * | 1988-12-20 | 1999-11-24 | Asahi Glass Co Ltd | Manufacturing method of recording sheet and recording sheet |
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| EP0507255B1 (en) * | 1991-04-05 | 1997-10-01 | Asahi Glass Company Ltd. | Electrostatic image transfer recording sheet |
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| CA2122099C (en) * | 1993-04-28 | 1999-08-17 | Hitoshi Yoshino | Recording medium, ink-jet recording method using the same, and dispersion of alumina hydrate |
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| JP2887098B2 (en) * | 1994-10-26 | 1999-04-26 | キヤノン株式会社 | Recording medium, manufacturing method thereof, and image forming method |
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| JP2877740B2 (en) * | 1994-10-27 | 1999-03-31 | キヤノン株式会社 | Recording medium, image forming method using the same, and printed matter |
| JPH09150570A (en) * | 1994-10-31 | 1997-06-10 | Canon Inc | Recording medium, dispersion liquid for the medium, method for producing the medium, and image forming method using the medium |
| JP2921785B2 (en) | 1995-04-05 | 1999-07-19 | キヤノン株式会社 | Recording medium, method for manufacturing the medium, and image forming method |
| JP2921786B2 (en) * | 1995-05-01 | 1999-07-19 | キヤノン株式会社 | Recording medium, method for manufacturing the medium, and image forming method using the medium |
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| TW498054B (en) | 1998-09-10 | 2002-08-11 | Nissan Chemical Ind Ltd | Moniliform silica sol and process for producing the same, and coating composition for ink receiving layer and ink jet recording medium having ink receiving layer |
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Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6050721B2 (en) * | 1980-02-19 | 1985-11-09 | 千代田化工建設株式会社 | Method for producing porous inorganic oxide |
| JPS58110287A (en) * | 1981-12-24 | 1983-06-30 | Mitsubishi Paper Mills Ltd | Sheet for recording |
| JPS60232990A (en) * | 1984-05-02 | 1985-11-19 | Mitsubishi Paper Mills Ltd | inkjet recording medium |
| JPS60245588A (en) * | 1984-05-21 | 1985-12-05 | Mitsubishi Paper Mills Ltd | inkjet recording medium |
-
1989
- 1989-05-17 JP JP1121414A patent/JPH072430B2/en not_active Expired - Fee Related
- 1989-07-14 JP JP1180563A patent/JPH02276671A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11321070A (en) * | 1988-12-20 | 1999-11-24 | Asahi Glass Co Ltd | Manufacturing method of recording sheet and recording sheet |
| CN104921959A (en) * | 2014-03-18 | 2015-09-23 | 松下知识产权经营株式会社 | Skin sticking sheet manufacturing method, cosmetic method, and skin sticking sheet |
| CN104921959B (en) * | 2014-03-18 | 2020-03-06 | 松下知识产权经营株式会社 | Method for producing sheet for skin adhesion, method for beautifying skin, and sheet for skin adhesion |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02276670A (en) | 1990-11-13 |
| JPH02276671A (en) | 1990-11-13 |
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