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JPH0742488B2 - Method for manufacturing rod-shaped body of composite sintered material - Google Patents
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JPH0742488B2 - Method for manufacturing rod-shaped body of composite sintered material - Google Patents

Method for manufacturing rod-shaped body of composite sintered material

Info

Publication number
JPH0742488B2
JPH0742488B2 JP59120219A JP12021984A JPH0742488B2 JP H0742488 B2 JPH0742488 B2 JP H0742488B2 JP 59120219 A JP59120219 A JP 59120219A JP 12021984 A JP12021984 A JP 12021984A JP H0742488 B2 JPH0742488 B2 JP H0742488B2
Authority
JP
Japan
Prior art keywords
layer
cemented carbide
composite
sintered
block
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP59120219A
Other languages
Japanese (ja)
Other versions
JPS61506A (en
Inventor
雄一郎 鴻野
昭夫 原
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Electric Industries Ltd
Original Assignee
Sumitomo Electric Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Electric Industries Ltd filed Critical Sumitomo Electric Industries Ltd
Priority to JP59120219A priority Critical patent/JPH0742488B2/en
Priority to CA000483612A priority patent/CA1286510C/en
Priority to AT85304135T priority patent/ATE49147T1/en
Priority to EP85304135A priority patent/EP0168953B2/en
Priority to KR1019850004091A priority patent/KR920001585B1/en
Priority to DE8585304135T priority patent/DE3575092D1/en
Publication of JPS61506A publication Critical patent/JPS61506A/en
Priority to US07/231,644 priority patent/US4880707A/en
Publication of JPH0742488B2 publication Critical patent/JPH0742488B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Description

【発明の詳細な説明】 産業上の利用分野 本発明は硬質な頭部を有する複合材料棒状体、好ましく
は小径の円柱体の製造方法に関する。
Description: FIELD OF THE INVENTION The present invention relates to a method for manufacturing a composite rod having a rigid head, preferably a cylinder of small diameter.

更に詳細には本発明は、ダイヤモンド焼結体或いは高圧
相窒化硼素焼結体の如き硬質な頭部と、該頭部と一体に
構成され、例えば超硬合金からなる支持部とを具備する
小断面の複合材料棒状体の製造方法に関する。
More specifically, the present invention provides a small head including a hard head such as a diamond sintered body or a high-pressure phase boron nitride sintered body, and a support portion integrally formed with the head and made of, for example, cemented carbide. The present invention relates to a method for manufacturing a composite material rod-shaped body having a cross section.

このような本発明の製造方法によって得られる複合材料
棒状体は、高性能な小径ドリルの素材或いはドットプリ
ンタへのヘッド部として用いることができる。
The composite material rod-shaped body obtained by the manufacturing method of the present invention can be used as a material for a high-performance small-diameter drill or a head portion for a dot printer.

従来技術 超硬合金よりなるドリルが金属、非金属材料の穴あけ用
に多用されている。特に近年急激に需要が伸びているプ
リント基板の穴あけには直径1mm前後の超硬合金製ドリ
ルが使われている。
2. Description of the Related Art Drills made of cemented carbide are widely used for drilling metal and non-metal materials. In particular, cemented carbide drills with a diameter of around 1 mm are used for drilling printed circuit boards, which are in rapid demand in recent years.

プリント基板には各種の材料が使われているが、主とし
て用いられているのはガラス繊維にエポキシ樹脂を含浸
させた強化樹脂で、一般にガラエポ基板と称されてい
る。
Although various materials are used for a printed circuit board, a mainly used resin is a reinforced resin obtained by impregnating glass fiber with an epoxy resin, which is generally called a glass epoxy substrate.

このようなプリント基板の穴あけは剛性の高いドリルで
通常回転数5〜6万rpmの条件で行われているが、基板
に含まれるガラス繊維は超硬工具を非常に早く摩耗させ
て、一般的に3000〜5000ヒット(ヒットとは穴あけ回数
のこと)で超硬ドリルは寿命となる。こうしたドリル盤
には自動工具交換装置がついており、寿命となったドリ
ルは自動的に交換されるが、生産効率向上のためにはこ
の自動工具交換のための時間も問題であり、ドリル寿命
をのばして工具交換回数すなわち交換時間を減少させる
という要求が強い。
Drilling of such a printed circuit board is normally performed with a high-rigidity drill at a rotation speed of 50,000 to 60,000 rpm. However, the glass fiber contained in the circuit board causes the cemented carbide tool to wear very quickly, which is common. With 3000 to 5000 hits (hits are the number of holes drilled), a carbide drill reaches its end of life. Such a drilling machine is equipped with an automatic tool changer, and the drill that has reached the end of its life is automatically replaced, but in order to improve production efficiency, the time for this automatic tool change is also a problem and There is a strong demand to extend the number of tool changes, that is, to reduce the change time.

プリント基板の特性からみると、更に耐熱性等を向上さ
せて高機能化を計りたいという要求も強く、このような
基板材料は実際に製造可能であるが、一般にこのような
高機能材料は難削で、従来の超硬合金ドリルでは非常に
短寿命となってしまい、このためこの基板材料の実用化
が出来ないのが実情である。
Considering the characteristics of printed circuit boards, there is a strong demand for further improvement in heat resistance and other functions, and such board materials can be actually manufactured, but in general, such high-performance materials are difficult to manufacture. Due to the grinding, the life of conventional cemented carbide drills becomes extremely short, and the actual situation is that this substrate material cannot be put to practical use.

更に、通常のガラエポ基板に対しても更に高能率の穴あ
けを行うため穴あけドリルの回転数の上昇が望まれてい
るが、これも従来の超硬合金製ドリルでは切削速度の上
昇と共に急激に寿命が低下してしまうためこの面から高
能率化を達成できない。
Furthermore, it is desired to increase the rotation speed of the drill to make even more efficient drilling for ordinary glass-epoxy substrates, but this is also the case with conventional cemented carbide drills, where the life is sharply increased with increasing cutting speed. Therefore, the efficiency cannot be improved from this point.

一方、近年使用量が急激に増加しつつある焼結ダイヤモ
ンド工具は超硬工具に対して飛躍的に硬度が高く、耐摩
耗性が優れており、上記強化樹脂などの切削に於いては
非常な高性能を発揮する。
On the other hand, sintered diamond tools, whose usage has been increasing rapidly in recent years, have dramatically higher hardness than cemented carbide tools and are excellent in wear resistance, and are extremely useful in cutting the above reinforced resin. Demonstrate high performance.

ところが第1図に示すように、この焼結ダイヤモンド工
具は焼結ダイヤモンド層11が超硬合金の支持部12に貼り
合わされた複合焼結体13からなる。この複合焼結体13を
使用してドリルを作製する場合には第2図に示すように
シャンク15の先端部に複合焼結体13を何らかの方法によ
り固着させて作らざるを得ない。
However, as shown in FIG. 1, this sintered diamond tool comprises a composite sintered body 13 in which a sintered diamond layer 11 is bonded to a cemented carbide support portion 12. When making a drill using this composite sintered body 13, as shown in FIG. 2, the composite sintered body 13 must be fixed to the tip of the shank 15 by some method.

ところがこのドリル先端部の径は1mm程度であり、この
ような小径のものではシャンク15と余程強力な接合強度
をもたせないと接合後の刃先研削加工で接合部16からは
ずれてしまい、良好なドリルが製造できない。特に焼結
ダイヤモンドは難研削であり、研削抵抗が高く、通常の
銀ロウ付け程度の強度では強度不足である。接合強度の
高い接合方法としては例えば電子ビーム溶接が考えられ
るが、電子ビーム溶接を実施するとなると、ドリルの製
造工程が複雑且つ原価が高くなり、高性能ドリルの需要
の近年の急激な増加に対応できなかった。
However, the diameter of the tip of this drill is about 1 mm, and with such a small diameter, unless it has a very strong joining strength with the shank 15, it will come off from the joining portion 16 in the cutting edge grinding process after joining, which is good. I can't manufacture a drill. In particular, sintered diamond is difficult to grind, has a high grinding resistance, and is insufficient in strength at the level of ordinary silver brazing. Electron beam welding can be considered as a joining method with high joining strength, but if electron beam welding is implemented, the manufacturing process of the drill will be complicated and the cost will be high, and it will respond to the recent rapid increase in demand for high-performance drills. could not.

シャンク15との接合を強固にし且つドリル自体の切削性
を高めるためには、ドリルの先端部全体が超硬合金で、
その頭部にダイヤモンドの如き硬質の焼結体を有するよ
うに構成すると理想的である。そのためには、硬質な頭
部を有し、超硬合金からなる細長の複合材料棒状体が必
要である。しかしながら、従来技術では、このような小
断面で且つ軸長の大きい複合焼結体を製造することがで
きなかった。
In order to strengthen the connection with the shank 15 and improve the machinability of the drill itself, the entire tip of the drill is cemented carbide,
It is ideal to have a hard sintered body such as diamond on its head. For that purpose, an elongated composite rod-shaped body having a hard head and made of cemented carbide is required. However, in the prior art, it was not possible to manufacture a composite sintered body having such a small cross section and a large axial length.

すなわち、断面積に対し軸方向長さの大きい製品を製造
する場合、粉末材料を軸方向に加圧してホットプレスを
行っても、粉末材料層による圧力損失が大きく、軸方向
中央部分に必要な圧力がかからず、強固な焼結体が得ら
れないからである。これをさらに軸方向に加圧して高圧
力のホットプレスを行うと、ホットプレスのコンテナ内
の圧力分布が極めて変則的となるので座屈したり、曲が
りなどの変形を起こし易く十分な寸法精度を持つ焼結体
が得られない。
That is, when manufacturing a product having a large axial length with respect to the cross-sectional area, even if the powder material is pressed in the axial direction and hot pressed, the pressure loss due to the powder material layer is large, and it is necessary for the central portion in the axial direction. This is because no pressure is applied and a strong sintered body cannot be obtained. If this is further pressed in the axial direction and hot pressed with high pressure, the pressure distribution inside the container of the hot press becomes extremely irregular, so it is easy to cause buckling, deformation such as bending, and has sufficient dimensional accuracy. A sintered body cannot be obtained.

そのため、細長の焼結材料のホットプレスでは焼結材料
の軸方向が加圧方向と直角となるよう焼結材料を寝かせ
て配置していた。このような方式で、細長の複合材料を
ホットプレスをしても、異った材料層間の境界面に垂直
な方向での圧力は小さく、材料層間の十分な強度の接合
が得られなかった。
Therefore, in the hot pressing of the elongated sintered material, the sintered material is laid out so that the axial direction of the sintered material is perpendicular to the pressing direction. In such a method, even when hot pressing was performed on the elongated composite material, the pressure in the direction perpendicular to the boundary surface between different material layers was small, and sufficient strength bonding between the material layers could not be obtained.

発明の目的 本発明は、上記従来技術の問題を解決することを目的と
し、更に詳細には、硬質焼結体の頭部を有し、該頭部と
支持部とが焼結処理により一体に接合されている小断面
且つ細長の複合材料棒状体、好ましくは小径の円柱体の
製造方法を提供し、これより耐摩耗性および剛性の優れ
たドリルを容易且つ安価に製造可能とすることを目的と
する。
OBJECT OF THE INVENTION The present invention has an object of solving the above-mentioned problems of the prior art, and more specifically, has a head of a hard sintered body, and the head and the supporting portion are integrally formed by a sintering process. An object of the present invention is to provide a method for producing a joined rod-shaped body having a small cross-section and an elongated shape, preferably a columnar body having a small diameter, thereby making it possible to easily and inexpensively produce a drill having excellent wear resistance and rigidity. And

更に本発明の目的は、ガラエポ基板の如き難削性の基板
の穴あけを容易且つ高性能で実現する、長寿命のドリル
を低価格で提供することにある。
A further object of the present invention is to provide a long-life drill at a low price, which enables easy and high-performance drilling of a difficult-to-cut substrate such as a glass epoxy substrate.

更に、本発明の目的は、ドットプリンタのヘッドの如き
硬質の先端部を必要とする細長の部材を容易に製造し得
る中間製品としての小断面の複合材料棒状体の製造方法
を提供することにある。
Further, an object of the present invention is to provide a method for manufacturing a rod-shaped composite material having a small cross section as an intermediate product capable of easily manufacturing an elongated member which requires a hard tip portion such as a head of a dot printer. is there.

発明の構成 本発明者らは、断面積の大きな複合材料ブロックのホッ
トプレスを行って複合焼結体ブロックを製造し、これを
放電ワイヤカッティングで小径の円柱体に切断すること
により小径で細長の、硬質な頭部を有する複合焼結材料
棒状体を与えることに成功したものである。
Configuration of the Invention The present inventors manufacture a composite sintered body block by hot pressing a composite material block having a large cross-sectional area, and cut it into a small-diameter columnar body by discharge wire cutting to make it small and elongated. It has succeeded in providing a rod-shaped body of a composite sintered material having a hard head.

すなわち、本発明に従い、ダイヤモンド粉末または高圧
相窒化硼素粉末を50%以上含有する硬質焼結体用の第1
の材料層と、該第1の材料層の焼結過程で該第1の材料
の硬質焼結体と接合する第2の材料層とを同一のホット
プレスコンテナ内に加圧方向に重ねて装入し、 高温高圧下でホットプレスして該第1の材料層を焼結す
るとともに、得られた硬質焼結体を該第2の材料層側と
接合せしめて、所定厚さの硬質焼結体の層を有する複合
材料ブロックを形成し、 該複合材料ブロックを放電ワイヤカッティング方法によ
り材料層厚方向に切断して、該複合材料ブロックの材料
層厚方向厚さに対して1/6以下で且つ3mm以下の相当直径
の断面を有する硬質焼結体を頭部に備える細長の複合材
料棒状体を2本以上切り取ることを特徴とする細長の複
合材料棒状体の製造方法が提供される。
That is, according to the present invention, the first for hard sintered bodies containing 50% or more of diamond powder or high-pressure phase boron nitride powder.
And a second material layer to be joined to the hard sintered body of the first material in the sintering process of the first material layer are mounted in the same hot press container in the pressing direction. Then, the first material layer is sintered by hot pressing under high temperature and high pressure, and the obtained hard sintered body is joined to the second material layer side to obtain a hard sintered body having a predetermined thickness. A composite material block having a body layer is formed, the composite material block is cut in the material layer thickness direction by a discharge wire cutting method, and the thickness is 1/6 or less with respect to the material layer thickness direction thickness of the composite material block. Also provided is a method for producing an elongated composite material rod-shaped body, which comprises cutting out two or more elongated composite material rod-shaped bodies each having a hard sintered body having a cross section of an equivalent diameter of 3 mm or less at its head.

複合材料をホットプレスして焼結にするに際し、本発明
に従うと、複合材料ブロックの軸方向長さは相当直径D
Eの3倍、好ましくは2倍以下の必要がある。3倍を越
える軸方向長さの複合材料ブロックのホットプレスを行
うと複合材料ブロック内の圧力分布が変則的となり、曲
がりなどを生ずる。本明細書中で、相当直径とは断面積
の等しい円の直径に換算した値を意味する。
In hot pressing the composite material to sinter, according to the invention, the axial length of the composite material block is the equivalent diameter D.
It should be 3 times, preferably 2 times or less than E. When hot pressing a composite material block having an axial length of more than three times, the pressure distribution in the composite material block becomes irregular and bending occurs. In the present specification, the equivalent diameter means a value converted into the diameter of a circle having the same cross-sectional area.

ダイヤモンド粉末または高圧相窒化硼素粉末の平均粒度
は好ましくは30μm以下であり、この範囲の粒度のダイ
ヤモンドまたは高圧相窒化硼素焼結体では耐摩耗性およ
び剛性に優れた複合焼結材料が得られる。
The average particle size of the diamond powder or the high-pressure phase boron nitride powder is preferably 30 μm or less, and a diamond or high-pressure phase boron nitride sintered body having a particle size within this range can provide a composite sintered material having excellent wear resistance and rigidity.

ただし、ダイヤモンド粉末を使用して切削工具のチップ
を作製するときは、平均粒度が10μmを越えるダイヤモ
ンド粉末を原料として使用すると、この複合焼結材料円
柱体を加工して得た切削工具の切刃が鋭利に成形でき
ず、このため高性能とならないので、硬質焼結部は10μ
m以下のダイヤモンドまたは高圧相窒化硼素からなるの
が好ましい。
However, when producing chips for cutting tools using diamond powder, if diamond powder with an average particle size of more than 10 μm is used as a raw material, the cutting edge of the cutting tool obtained by processing this composite sintered material cylindrical body Can not be formed sharply, and as a result, high performance cannot be achieved.
It is preferably composed of diamond or less m or high-pressure phase boron nitride.

本発明の好ましい特徴に従うと、該硬質焼結部の軸方向
長さは0.3〜2mmである。
According to a preferred feature of the invention, the axial length of the hard sintered part is 0.3-2 mm.

第1の材料層がダイヤモンド粉末を主成分とするとき
は、ダイヤモンド粉末単独、或いは70%以上のダイヤモ
ンドを含み、残部がFe、CoまたはNiを主成分とする結合
材粉末を添加した混合粉末がある。ダイヤモンド粉末の
第1の材料層の好ましい例としては、70%以上のダイヤ
モンド粉末とWC−5〜15%Co粉末との混合粉末である。
When the first material layer contains diamond powder as a main component, a diamond powder alone or a mixed powder containing 70% or more of diamond and the remainder being a binder powder containing Fe, Co or Ni as a main component is added. is there. A preferred example of the first material layer of diamond powder is a mixed powder of 70% or more diamond powder and WC-5 to 15% Co powder.

尚、第1の材料層の材料としてダイヤモンド単独の粉末
を使用する場合は、第1の材料層の焼結時に第2の材料
層の中の結合材成分が第1の材料層粉末中に溶浸するこ
とによって第1の材料層の焼結が達成される。
When powder of diamond alone is used as the material of the first material layer, the binder component in the second material layer dissolves in the powder of the first material layer when the first material layer is sintered. Sintering achieves sintering of the first layer of material.

第1の材料層が高圧相窒化硼素系の場合は、高圧相窒化
硼素粉末単独、或いは50%、以上の高圧相窒化硼素に4
a、5a、6a族元素の炭化物、窒化物、炭窒化物及びアル
ミニウムおよび/またはシリコンを結合材として添加し
て焼結したものがある。ここで、高圧相窒化硼素とは、
立方晶型窒化硼素およびウルツ鉱型窒化硼素を意味す
る。
When the first material layer is a high-pressure phase boron nitride-based material, high-pressure phase boron nitride powder alone or 50% or more of high-pressure phase boron nitride
There are those obtained by adding carbides, nitrides, carbonitrides, and aluminum and / or silicon of group a, 5a, and 6a elements as a binder and sintering them. Here, the high-pressure phase boron nitride is
It means cubic boron nitride and wurtzite boron nitride.

支持部を形成する第2の材料層は、いわゆる超硬合金す
なわち、周期律表第4a5a、6a族元素の炭化物、窒化物、
炭窒化物、硼化物、珪化物又はこれらの相互固溶体炭化
物をFe、CoまたはNiの鉄族金属で結合した焼結合金また
はサーメットあるいはそれらの粉末原料である。サーメ
ットの1例としては、(Mo,w)Cの炭化物をNiまたはCo
の鉄族金属で結合したものがある。
The second material layer forming the support portion is a so-called cemented carbide, that is, carbides or nitrides of elements of groups 4a5a and 6a of the periodic table,
It is a sintered alloy or cermet in which a carbonitride, a boride, a silicide or a mutual solid solution carbide thereof is bound by an iron group metal of Fe, Co or Ni, or a powder raw material thereof. As an example of cermet, (Mo, w) C carbide is Ni or Co.
There is one that is bound by the iron group metal.

更に別の第2の材料層としては、Wを80〜98重量%含
み、残余がNi−FeまたはNi−Fe−Cuからなるいわゆるヘ
ビー・メタルといわれる焼結合金、あるいはその粉末原
料がある。
Still another second material layer is a so-called heavy metal sintered alloy containing 80 to 98% by weight of W and the balance of Ni-Fe or Ni-Fe-Cu, or a powder raw material thereof.

第2の材料層は、既に焼結済みの固形超硬合金であって
もよく、或いは超硬合金材料の粉末であってもよい。し
かしながら、ホットプレスの際の取扱い上の便宜、さら
には高圧力の適用の容易性を考慮すると、焼結済みの超
硬合金ブロックを使用するのが好ましい。
The second material layer may be a solid cemented carbide that has already been sintered, or a powder of cemented carbide material. However, it is preferable to use a sintered cemented carbide block in consideration of handling convenience in hot pressing and ease of application of high pressure.

本発明の複合材料棒状体の製造方法の重要な特徴の1つ
は、硬質焼結部と支持部との接合を硬質焼結部の焼結過
程で行うことにある。従って、第2の材料層の成分は、
第1の材料層の焼結過程で第1の材料層と接合し得る材
料であることが必要である。
One of the important features of the method for producing a rod-shaped composite material according to the present invention is that the hard sintered portion and the support portion are joined in the sintering process of the hard sintered portion. Therefore, the components of the second material layer are
It is necessary that the material is a material that can be bonded to the first material layer during the sintering process of the first material layer.

しかしながら、上記した硬質焼結部と支持部との成分の
範囲ではこのような組み合わせは無限にあり、ダイヤモ
ンドまたは高圧相窒化硼素の高圧力および高温度下のホ
ットプレスによる焼結過程で、上記したように支持部材
中の鉄系金属の結合材が溶浸して硬質焼結部と支持部と
の接合は容易に生ずる。従って、このような硬質焼結部
と支持部の成分の選択は当業者が上記した範囲内で必要
に応じて可能であることは云うまでもない。更に高圧相
窒化硼素粉末は上記したように単独でも焼結可能であ
り、支持部との接続はその焼結過程で達成される。
However, such combinations are endless within the range of the components of the hard sintered portion and the support portion described above, and in the sintering process of diamond or high pressure phase boron nitride by hot pressing under high pressure and high temperature, Thus, the ferrous metal binder in the support member is infiltrated, so that the hard sintered portion and the support portion are easily joined. Therefore, it goes without saying that those skilled in the art can select the components of the hard sintered portion and the support portion as needed within the above-described range. Further, the high-pressure phase boron nitride powder can be sintered alone as described above, and the connection with the supporting portion is achieved during the sintering process.

更に、本発明の1つの態様に従うと、上記第1の材料層
と第2の材料層との間に厚さ0.5mm以下の中間接合層を
配置してホットプレスを行う。
Further, according to one aspect of the present invention, an intermediate bonding layer having a thickness of 0.5 mm or less is arranged between the first material layer and the second material layer, and hot pressing is performed.

中間接合層としては、70%未満の高圧相窒化硼素と残部
が周期律表第4a族のTi、Zr、Hfの炭化物、窒化物、炭窒
化物あるいはホウ化物の1種もしくはこれらの混合物ま
たは相互固溶体化合物を主体としたものと、これにAlお
よび/またはSiを0.1重量%以上含有するものが好まし
い。
As the intermediate bonding layer, a high-pressure phase boron nitride of less than 70% and the balance being one of Ti, Zr, and Hf carbides, nitrides, carbonitrides, or borides of Group 4a of the Periodic Table, or a mixture thereof or mutual mutual. It is preferable to use a solid solution compound as a main component and a material containing Al and / or Si in an amount of 0.1% by weight or more.

更に、本発明の1つの態様に従うと、上記第2の材料
層、すなわち支持部が軸方向に2以上の材料層から構成
される。このような1例として、第2の材料層の支持側
の層がWC−Coであり、硬質な頭部側の層が(Mo,w)Cの
炭化物をNiまたはCoの鉄族金属で結合したサーメットか
らなるものがある。
Furthermore, according to one aspect of the present invention, the second material layer, that is, the support portion, is composed of two or more material layers in the axial direction. As an example of such a case, the support side layer of the second material layer is WC-Co, and the hard head side layer is a (Mo, w) C carbide bonded with an iron group metal of Ni or Co. Some are made of cermet.

更に、第1の材料層を第2の材料層の上下に配置し、ホ
ットプレスを行い、得られる複合材料ブロックを同軸方
向の小断面の棒状体に切出して上下の両端に硬質な頭部
を有する棒状体を製造することも出来る。
Further, the first material layer is arranged above and below the second material layer, hot press is performed, and the obtained composite material block is cut into a rod-shaped body having a small cross section in the coaxial direction, and hard heads are provided at both upper and lower ends. It is also possible to manufacture a rod-shaped body having the same.

次に本発明の製造方法により得られる複合焼結材料棒状
体の形状を説明する。
Next, the shape of the composite sintered material rod-shaped body obtained by the manufacturing method of the present invention will be described.

添付の第3図(a)および(b)は本発明の製造方法に
よって得られる複合材料棒状体の例の斜視図である。
3 (a) and 3 (b) attached herewith are perspective views of examples of composite material rods obtained by the production method of the present invention.

第3図(a)に示す複合焼結材料棒状体は全体として円
柱形をなし、硬質焼結部21が支持部22と直接に接合され
ている。
The composite sintered material rod-shaped body shown in FIG. 3 (a) has a cylindrical shape as a whole, and the hard sintered portion 21 is directly joined to the support portion 22.

他方、第3図(b)に示す複合焼結材料棒状体では、硬
質焼結部21と支持部22とが中間接合層24を介して接合さ
れている。
On the other hand, in the composite sintered material rod-shaped body shown in FIG. 3 (b), the hard sintered portion 21 and the support portion 22 are joined via the intermediate joining layer 24.

しかしながら、本発明の製造方法によって得られる複合
材料棒状体は円柱形に限定されず、角柱形であってもよ
いことは勿論である。
However, it goes without saying that the composite material rod-shaped body obtained by the manufacturing method of the present invention is not limited to the cylindrical shape and may be a prismatic shape.

本発明の方法で得られる複合焼結材料棒状体は3mm以下
の相当直径の断面である。3mmを越える相当直径の断面
の複合材料棒状体はプリント基板の穴あけドリル用素材
としては不適格であり、また研削して使用するにしても
研削代が大きくなり不経済である。
The composite sintered material rod-shaped body obtained by the method of the present invention has a cross section with an equivalent diameter of 3 mm or less. A composite material rod having a cross section with an equivalent diameter of more than 3 mm is not suitable as a material for a drilling hole for a printed circuit board, and even if it is ground and used, the grinding allowance is large and it is uneconomical.

また、硬質焼結部21の軸方向の長さは0.3〜2mmの範囲で
ある。0.3mm未満では、ドリル先端部として使用した場
合には切削性の向上を期待できず、2mmを越える長さで
は高価なダイヤモンド粉末等を多量に使用することにな
り不経済である。また3mmを越える直径の棒状体は本発
明の方法以外の従来方法でも製造可能である。
The axial length of the hard sintered part 21 is in the range of 0.3 to 2 mm. If it is less than 0.3 mm, improvement in machinability cannot be expected when used as a drill tip, and if it exceeds 2 mm, a large amount of expensive diamond powder or the like is used, which is uneconomical. Further, a rod-shaped body having a diameter of more than 3 mm can be manufactured by a conventional method other than the method of the present invention.

更に、支持部22の長さは硬質焼結部21の長さの5倍以上
であることが必要である。ドリルを作製する場合に、ド
リルの切羽長さを確保し、末端をシャンクに埋込む必要
があるので、上記の通り、5倍以上の長さの支持部が必
要となる。
Further, the length of the support portion 22 needs to be 5 times or more the length of the hard sintered portion 21. When manufacturing a drill, it is necessary to secure the face length of the drill and bury the end in the shank, so that a supporting portion having a length of 5 times or more is required as described above.

次に、この本発明の製造方法により得られた複合材料棒
状体をドリルに適用した例を第4図に示す。
Next, FIG. 4 shows an example in which the composite material rod-like body obtained by the manufacturing method of the present invention is applied to a drill.

第4図(a)に示す如く、ドリルのシャンク25の先端
に、複合材料棒状体(図示の例では円柱体)とほゞ同一
径の孔26を穿設する。この孔26に複合材料棒状体23の支
持部側端部を押し込み、固定する。このとき、孔26は内
にロウ材を滴下しておき、ロウ付けしてもよい。
As shown in FIG. 4 (a), a hole 26 having substantially the same diameter as that of the composite material rod-shaped body (cylindrical body in the illustrated example) is formed at the tip of the shank 25 of the drill. The end of the composite material rod-shaped body 23 on the support portion side is pushed into this hole 26 and fixed. At this time, a brazing material may be dropped into the holes 26 and then brazed.

この第4図(a)に示す如く、シャンクに固定された複
合材料棒状体23を刃付け加工し、第4図(b)に示す如
きドリルを得た。
As shown in FIG. 4 (a), the composite material rod 23 fixed to the shank was bladed to obtain a drill as shown in FIG. 4 (b).

第3図および第4図に示す複合材料棒状体の切り出し方
法を説明すると、上述の如くホットプレスして得られた
複合焼結体ブロック33は、第5図(a)に示す如く、厚
さ1mmのダイヤモンド焼結体層31と、これに接合した超
硬合金層32とからなり、中間接合層を含む場合では第5
図(b)示す如くダイヤモンド焼結体層31と超硬合金層
32と中間接合層を介して接合されている。図示の例では
円柱状の複合焼結体ブロックを示しているが、複合焼結
体ブロックは円柱体でも角柱体でもよいことは勿論であ
る。
The method of cutting out the composite material rod-shaped body shown in FIGS. 3 and 4 will be described. The composite sintered body block 33 obtained by hot pressing as described above has a thickness as shown in FIG. 5 (a). It is composed of a 1 mm diamond sintered body layer 31 and a cemented carbide layer 32 bonded to the diamond sintered body layer 31, and the fifth layer in the case of including an intermediate bonding layer.
Diamond sintered body layer 31 and cemented carbide layer as shown in FIG.
It is joined to 32 with an intermediate joining layer. In the illustrated example, a cylindrical composite sintered body block is shown, but it goes without saying that the composite sintered body block may be a cylindrical body or a prismatic body.

これらの複合焼結体ブロックを第6図に示す如く、複合
焼結体ブロックと同軸方向の相当直径3mm以下の断面の
棒状体に放電ワイヤカッティング法により切断して第3
図(a)および(b)に示す如き硬質の頭部を有する複
合材料棒状体に切断する。
As shown in FIG. 6, these composite sintered body blocks were cut into a rod-shaped body having a cross-section with an equivalent diameter of 3 mm or less in the direction coaxial with the composite sintered body block by a discharge wire cutting method to form a third rod.
A composite rod having a hard head as shown in FIGS. (A) and (b) is cut.

この放電ワイヤカッティング法では、ワイヤと複合焼結
体ブロックとの間に高電圧をかけ、ワイヤを緊張した状
態で走行させてブロックを切断するものであり、その詳
細は米国特許第4,103,137号を参照されたい。
In this electric discharge wire cutting method, a high voltage is applied between the wire and the composite sintered body block, and the wire is run in a tensioned state to cut the block. For details, see U.S. Pat.No. 4,103,137. I want to be done.

以下、実施例により本発明の製造方法を説明する。ただ
し、これらの実施例は本発明の単なる例示であって、本
発明の範囲を何等制限するものではない。
Hereinafter, the production method of the present invention will be described with reference to examples. However, these examples are merely examples of the present invention and do not limit the scope of the present invention in any way.

尚、本明細書中では%の表示は、特別に示さない限り容
量パーセントで示す。
In the present specification,% is shown as a volume percentage unless otherwise specified.

実施例1 外径18mm、内径14mm、高さ15mmのWC−12%Co超硬合金製
リング、外径14mm、高さ12mmのWC−12%Co超硬合金製円
柱ブロック、外径14mm、厚さ0.5mmのWC−12%Co超硬合
金製円板と粒径0.5μmのダイヤモンド粉末85%と残余
が粒径0.5μm以下のWC−15%Co超硬合金粉末よりなる
混合粉末を用意した。
Example 1 WC-12% Co cemented carbide ring of outer diameter 18 mm, inner diameter 14 mm, height 15 mm, WC-12% Co cemented carbide column block of outer diameter 14 mm, height 12 mm, outer diameter 14 mm, thickness Prepared a mixed powder consisting of a 0.5 mm thick WC-12% Co cemented carbide disc, 85% diamond powder with a particle size of 0.5 μm, and the balance WC-15% Co cemented carbide powder with a particle size of 0.5 μm or less. .

超合金リングの内径に超合金円柱ブロックを挿入し、超
硬合金リング内面と超硬合金円柱ブロックの上面とで形
成される直径14mm、深さ3mmの凹所に前記混合ダイヤモ
ンド粉末を充填後加圧して、混合粉末の高さを1.5μm
とし、超硬合金円板で蓋をした後、超高圧焼結装置中に
配置し、圧力55kb、温度1370℃の条件で15分間焼結を行
った。冷却後、減圧して取り出した封入容器の上部超硬
合金円板を研削により除去すると高さ12mmの超硬合金支
持部の上面に厚さ1mmの焼結ダイヤモンド層が接合して
形成され周囲に超硬合金製リングがやはり支持部及び焼
結ダイヤモンド層に結合した複合体ブロックが得られ
た。
Insert the superalloy cylinder block into the inner diameter of the superalloy ring, and add the mixed diamond powder to the recess of 14mm in diameter and 3mm in depth formed by the inner surface of the superhard alloy ring and the upper surface of the superhard alloy column block, and then add. Press to raise the height of the mixed powder to 1.5 μm
After covering with a cemented carbide disc, it was placed in an ultra-high pressure sintering apparatus and sintered under conditions of a pressure of 55 kb and a temperature of 1370 ° C. for 15 minutes. After cooling, decompressing and removing the upper cemented carbide disk of the enclosed container removed by grinding, a sintered diamond layer with a thickness of 1 mm was formed on the upper surface of the cemented carbide support with a height of 12 mm and formed around it. A composite block was obtained in which the cemented carbide ring was also bonded to the support and the sintered diamond layer.

この複合体ブロックを第6図に示すように、放電ワイヤ
カット加工機に装着して、放電ワイヤカッティングし
て、複合体ブロックの軸方向より直径1mm、長さ13mmの
丸棒で支持体部はWC−12%Co超硬合金よりなり、その一
端に長さ1mmの焼結ダイヤモンド層が固着形成された棒
状体を得た。
As shown in FIG. 6, this composite block is mounted on an electric discharge wire cutting machine, and the electric discharge wire is cut. A support bar is a round bar with a diameter of 1 mm and a length of 13 mm from the axial direction of the composite block. A rod-shaped body made of WC-12% Co cemented carbide and having a 1 mm long sintered diamond layer fixedly formed on one end thereof was obtained.

実施例2 それぞれWC−12%Co超硬合金よりなる外径18mm、内径
14mm、高さ20mmのリング、外径14mm、高さ18mmの円柱
ブロック、外径14mm、厚さ0.5mmの円板と、粒径3μ
mのダイヤモンド粉末90%と残余がCo粉末よりなる混合
粉末、粒径3μmの高圧相窒化硼素(以下、立方晶型窒
化硼素をCBNと略記する)粉末60%と残余が(TiN−10重
量%Al)の組成の粉末よりなる混合粉末を用意した。
Example 2 Outer diameter 18 mm and inner diameter made of WC-12% Co cemented carbide
14mm, height 20mm ring, outer diameter 14mm, height 18mm cylinder block, outer diameter 14mm, thickness 0.5mm disc, grain size 3μ
m 90% diamond powder and the balance Co powder, 3% high-pressure phase boron nitride powder (hereinafter cubic boron nitride is abbreviated as CBN) powder 60% and the balance (TiN-10% by weight) A mixed powder composed of powder having a composition of Al) was prepared.

超硬合金製円柱ブロックの上面に前記CBN混合粉末を溶
媒に溶かしたものを厚さ50μmに塗付した後、溶媒を加
熱除去し、この処理を行った超硬合金円柱ブロックを超
硬リング内径に挿入した。
The CBN mixed powder dissolved in a solvent is applied to the upper surface of a cemented carbide column block to a thickness of 50 μm, and then the solvent is removed by heating, and the cemented carbide column block that has undergone this treatment is processed into a cemented carbide ring inner diameter. Inserted in.

次に、超硬合金リング内面とCBN混合粉末を塗布した超
硬合金円柱ブロックの上面とで形成される凹所に前記ダ
イヤモンド混合粉末を充填した後、加圧成型して厚さ1.
8mmのダイヤモンド混合粉末層を形成した後、超硬合金
円板で蓋をした。
Next, after filling the diamond mixed powder in the recess formed by the inner surface of the cemented carbide ring and the upper surface of the cemented carbide columnar block coated with the CBN mixed powder, pressure molding to a thickness of 1.
After forming an 8 mm diamond mixed powder layer, the lid was covered with a cemented carbide disc.

次にこの容器を超高圧焼結装置中に配置し、圧力55kb、
温度1400℃で10分間焼結を行った後、冷却、減圧して容
器を取り出した。容器の上部超硬合金円板を研削除去す
ると高さ18mmの超硬合金支持体の上面に厚さ1.2mmの焼
結ダイヤモンド層が厚さ25μmの焼結CBN層を介して接
合され、周囲に超硬合金リングが支持体及び焼結ダイヤ
モンド層に結合した複合体ブロックが得られた。
Next, this container was placed in an ultra-high pressure sintering machine, and the pressure was 55 kb,
After sintering at a temperature of 1400 ° C. for 10 minutes, the container was taken out by cooling and reducing the pressure. When the upper cemented carbide disk of the container is ground away, a 1.2 mm thick sintered diamond layer is bonded to the upper surface of a 18 mm high cemented carbide support via a 25 μm thick sintered CBN layer, A composite block was obtained in which the cemented carbide ring was bonded to the support and the sintered diamond layer.

この複合体ブロックを放電ワイヤカット、加工機に装着
し、放電ワイヤカッティングにより複合体の軸方向より
直径2mm、長さ19.2mmの丸棒で支持体部はWC−12%Co超
硬合金よりなり、その一端に長さ1.2mmの焼結ダイヤモ
ンド層が厚さ25μmの焼結CBN界面層を介して接合形成
された棒状体を得た。
This composite block was mounted on a discharge wire cutting and processing machine, and by discharge wire cutting, it was a round bar with a diameter of 2 mm and a length of 19.2 mm from the axial direction of the composite, and the support part was made of WC-12% Co cemented carbide. A rod-shaped body was obtained in which a sintered diamond layer having a length of 1.2 mm was joined and formed at one end thereof through a sintered CBN interface layer having a thickness of 25 μm.

実施例3 (Mo7、W3)C−11%Co超硬合金よりなり、上面に直径2
0mm、深さ3mmの円形凹所を有する外径24mm、高さ25mmの
円柱ブロック、外径20mm、厚さ0.5mmのWC−12%Co超硬
合金製円板と粒径0.5μmのダイヤモンド粉末80%と残
余が粒径0.5μm以下のWC−15%Co超硬合金粉末よりな
るダイヤモンド混合粉末を用意した。
Example 3 (Mo 7 , W 3 ) C-11% Co cemented carbide with a diameter of 2
Cylinder block with an outer diameter of 24 mm and a height of 25 mm, which has a circular recess of 0 mm and a depth of 3 mm, an outer diameter of 20 mm and a thickness of 0.5 mm, made of WC-12% Co cemented carbide disc and a diamond powder with a particle size of 0.5 μm. A diamond mixed powder consisting of WC-15% Co cemented carbide powder with a particle size of 80% and the remainder of 0.5 μm or less was prepared.

このダイヤモンド混合粉末を前記超硬合金円柱ブロック
の上面凹所に充填後加圧して高さ2.3mmのダイヤモンド
混合粉末層を形成した。次にこの上に超硬合金円板で蓋
をした後、超高圧焼結装置内に配置し、圧力55kb、温度
1400℃で15分間焼結した。
This diamond mixed powder was filled in the recess in the upper surface of the cemented carbide column block and then pressed to form a diamond mixed powder layer having a height of 2.3 mm. Next, after covering with a cemented carbide disc on this, place it in the ultra-high pressure sintering equipment, pressure 55 kb, temperature
Sintered at 1400 ° C for 15 minutes.

焼結後、封入容器を取り出し、上面の超硬合金蓋を研削
除去すると上面円形凹所に厚さ1.5mmの焼結ダイヤモン
ド層を有し、これが周囲の(Mo7、W3)C−11%Co合金
容器に強固に接合した複合体ブロックが得られた。
After sintering, the enclosure was taken out and the cemented carbide lid on the upper surface was ground and removed, and there was a sintered diamond layer with a thickness of 1.5 mm in the circular recess on the upper surface, which was around (Mo 7 , W 3 ) C-11. A composite block was obtained that was firmly bonded to the% Co alloy container.

この複合体ブロックを放電ワイヤカット加工機に装着
し、放電ワイヤカッティングにより複合体ブロックの軸
方向より直径2mm、長さ23.5mmの丸棒で支持体部は(M
o7、W3)C−11%Co超硬合金よりなり、その一端に長さ
1.5mmの焼結ダイヤモンド層が固着形成された棒状体が
得られた。
This composite block is mounted on an electric discharge wire cutting machine, and by electric discharge wire cutting, the support part is a round bar with a diameter of 2 mm and a length of 23.5 mm from the axial direction of the composite block.
o 7 , W 3 ) C-11% Co cemented carbide, with a length at one end
A rod-shaped body on which a 1.5 mm sintered diamond layer was firmly formed was obtained.

実施例4 外径18mm、内径14mm、高さ15mmのWC−12%Co超硬合金リ
ング、外径14mm、高さ12mmの96重量%W−3重量%Ni−
1重量%Cu合金よりなる円柱ブロック、外径14mm、厚さ
0.5mmのWC−12%Co超硬合金円板と粒径3μmのCBN85%
と残余がTiN0.82粉末とAl粉末を重量比で80:20として混
合した後、1000℃で30分真空炉内で加熱処理を行った
後、0.3μmに粉砕した粉末とよりなるCBN混合粉末を用
意した。
Example 4 WC-12% Co cemented carbide ring having an outer diameter of 18 mm, an inner diameter of 14 mm, and a height of 15 mm, an outer diameter of 14 mm and a height of 12 mm, 96 wt% W-3 wt% Ni-
Cylindrical block made of 1 wt% Cu alloy, outer diameter 14 mm, thickness
0.5mm WC-12% Co cemented carbide disc and 3μm grain CBN 85%
CBN mixed powder consisting of the following: TiN 0.82 powder and Al powder were mixed at a weight ratio of 80:20, heated at 1000 ° C for 30 minutes in a vacuum furnace, and then ground to 0.3 μm. I prepared.

超硬合金リングの内径にW合金円柱ブロックを挿入し
て、超硬合金リング内面とW合金円柱ブロック上面とで
形成される直径14mm、深さ3mmの凹所に前記CBN混合粉末
を充填し、加圧して高さ1.7mmのCBN混合粉末層を形成し
た。次いで、超硬合金円板をかぶせて蓋をし、超硬合金
容器全体を超高圧焼結装置中に配置し、しかる後圧力50
kb、温度1250℃で20分間焼結を行った。
Inserting the W alloy columnar block into the inner diameter of the cemented carbide ring, filling the CBN mixed powder into a recess of 14 mm in diameter and 3 mm in depth formed by the inner surface of the cemented carbide ring and the upper surface of the W alloy columnar block, A pressure was applied to form a CBN mixed powder layer having a height of 1.7 mm. Then, cover with a cemented carbide disc and cover, place the entire cemented carbide container in the ultra-high pressure sintering device, and then apply a pressure of 50.
Sintering was performed for 20 minutes at kb and a temperature of 1250 ° C.

焼結後、超硬合金容器を取り出し、上面のWC−12%Co超
硬合金蓋を研削除去すると高さ12mmのW合金支持部の上
面に厚さ1mmの焼結CBN層が接合して形成され周囲に超硬
合金製リングが支持体および焼結CBN層に接合した複合
体ブロックが得られた。
After sintering, take out the cemented carbide container and grind off the WC-12% Co cemented carbide lid on the top surface to form a 1 mm thick sintered CBN layer on the top surface of the 12 mm high W alloy support. Then, a composite block was obtained in which a cemented carbide ring was bonded to the support and the sintered CBN layer around it.

この複合体ブロックを放電ワイヤカット加工機に装着
し、放電ワイヤカッティングにより複合体ブロックの軸
方向より直径1mm、長さ13mmの丸棒で支持部は96重量%
W−3重量%Ni−1重量%Cu合金よりなり、その一端に
長さ1mmの焼結CBNが固着形成された棒状体が得られた。
This composite block was mounted on an electric discharge wire cutting machine, and by discharge wire cutting, it was a round bar with a diameter of 1 mm and a length of 13 mm from the axial direction of the composite block.
A rod-shaped body made of a W-3 wt% Ni-1 wt% Cu alloy and having a 1 mm long sintered CBN fixedly formed at one end thereof was obtained.

実施例5 外径40mm、内径36mm、高さ40mmのWC−12%Co超硬合金リ
ング、外径36mm、高さ34mmのWC−12%Co超硬合金円柱ブ
ロック、外径36mm、厚さ0.5mmのWC−12%Co超硬合金円
板と粒径3μmのCBN粉末60体積%と残余(TiN−10重量
%Al)の組成の粉末よりなるCBN混合粉末を用意した。
Example 5 WC-12% Co cemented carbide ring with outer diameter 40 mm, inner diameter 36 mm, height 40 mm, WC-12% Co cemented carbide column block with outer diameter 36 mm, height 34 mm, outer diameter 36 mm, thickness 0.5 A WC-12% Co cemented carbide disc having a diameter of 3 mm, a CBN powder having a composition of 60% by volume of a CBN powder having a particle diameter of 3 μm and a balance (TiN-10 wt% Al) was prepared.

まずCBN混合粉末を直径36mm、厚さ2.5mmの円板に加圧成
型し、前記超硬合金リングの内径に下部より超硬合金円
板、CBN成型体、超硬合金円柱ブロック、CBN成型体、超
硬合金円板の順に積層配置し、セットした容器全体を超
高圧焼結装置中に配置して圧力40kb、温度1200℃で20分
間焼結した。
First, the CBN mixed powder is pressure-molded into a disc having a diameter of 36 mm and a thickness of 2.5 mm, and the cemented carbide ring, the CBN molded body, the cemented carbide column block, and the CBN molded body are inserted into the inner diameter of the cemented carbide ring from the bottom. Then, the cemented carbide discs were laminated in this order, and the entire set container was placed in an ultrahigh pressure sintering apparatus and sintered at a pressure of 40 kb and a temperature of 1200 ° C. for 20 minutes.

焼結後取り出し、上下の超硬合金蓋を研削除去すると高
さ34mmの超硬合金円柱ブロックの上下面に直径36mm、厚
さ1.5mmの焼結CBN層が固着形成され、更に周囲が超硬合
金リングでおおわれた複合体ブロックが得られた。
After taking out after sintering and grinding and removing the upper and lower cemented carbide lids, a sintered CBN layer with a diameter of 36 mm and a thickness of 1.5 mm is fixedly formed on the upper and lower surfaces of the cemented carbide column block with a height of 34 mm. A composite block covered with an alloy ring was obtained.

次に、この複合体ブロックを放電ワイヤカット加工機に
装着し、放電ワイヤカッティングにより複合ブロック軸
方向より、直径2.5mm、長さ37mmの丸棒でその両端に長
さ1.5mmの焼結CBN層が固着形成されものが得られた。
Next, this composite block was mounted on an electric discharge wire cutting machine, and by a discharge wire cutting, from the axial direction of the composite block, a 2.5 mm diameter and 37 mm long round bar was used to form a sintered CBN layer of 1.5 mm length at both ends. Was adhered and formed.

この丸棒を更に長さ方向中央部で切断2分することによ
り直径2.5mm、長さ18mmの丸棒で支持部はWC−12%Co超
硬合金よりなり一端に長さ1.5mmの焼結CBN層が固着形成
された棒状体が得られた。
This round bar is further cut at the center in the length direction and cut into two parts. The round bar has a diameter of 2.5 mm and a length of 18 mm. The supporting part is made of WC-12% Co cemented carbide and has a length of 1.5 mm at one end A rod-shaped body on which the CBN layer was firmly formed was obtained.

【図面の簡単な説明】[Brief description of drawings]

第1図は従来技術の複合ダイヤモンド焼結体の構造を示
す。 第2図は従来技術の複合焼結体を刃先に固着したドリル
を示す。 第3図(a)及び(b)はそれぞれ本発明の方法によっ
て製造される複合焼結材料棒状体の例を示す。 第4図(a)は本発明の方法によって得られた複合材料
棒状体を使用してドリルを作る方法を図示し、第4図
(b)はそのドリルを示す。 第5図(a)は本発明の方法に従い得られた複合材料ブ
ロックの1例を示し、第5図(b)は中間接合部を有す
る複合材料ブロックの例を示す。 第6図は、本発明に従い複合材料ブロックから棒状体を
切り出す位置を示す。 (主な参照番号) 11……従来のダイヤモンド工具の焼結ダイヤモンド層、
12……超硬合金製の支持部、 13……従来の複合焼結ダイヤモンドのチップ、 15……シャンク、 21……本発明方法による複合焼結材料棒状体の硬質焼結
部、22……支持部、23……本発明の複合焼結材料棒状
体、24……中間接合部、 31……複合材料ブロックの硬質焼結部、 32……支持部、33……複合材料ブロック、 34……中間接合部、
FIG. 1 shows the structure of a prior art composite diamond sintered body. FIG. 2 shows a drill in which a composite sintered body of the prior art is fixed to the cutting edge. 3 (a) and 3 (b) each show an example of a composite sintered material rod-shaped body manufactured by the method of the present invention. FIG. 4 (a) illustrates a method of making a drill using the composite material rod obtained by the method of the present invention, and FIG. 4 (b) shows the drill. FIG. 5 (a) shows an example of a composite material block obtained according to the method of the present invention, and FIG. 5 (b) shows an example of a composite material block having an intermediate joint portion. FIG. 6 shows a position where a rod-shaped body is cut out from a composite material block according to the present invention. (Main reference number) 11 …… Sintered diamond layer of conventional diamond tool,
12 …… Cemented Carbide Support, 13 …… Conventional Composite Sintered Diamond Tip, 15 …… Shank, 21 …… Hard Sintered Part of Composite Sintered Rod by the Method of the Present Invention, 22 …… Supporting part, 23 ... Composite sintered material rod-shaped body of the present invention, 24 ... Intermediate joining part, 31 ... Hard sintering part of composite material block, 32 ... Supporting part, 33 ... Composite material block, 34 ... ... intermediate joints,

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】平均粒径が10μm以下であるダイヤモンド
粉末または高圧相窒化硼素粉末を50%以上含有する硬質
焼結体用の第1の材料の層と、周期律表第4a、5aまたは
6a族元素の炭化物あるいはこれらの相互固溶体炭化物を
鉄族金属で結合した超硬合金からなる第2の材料層とを
同一のホットプレスコンテナ内に加圧方向に重ねて装入
し、 高温高圧下でホットプレスして第1の材料の層を焼結す
るとともに、第1の材料の層の焼結過程で第1の材料の
硬質焼結体を第2の材料から得られる超硬合金層に接合
させて所定厚さの硬質焼結体の層を有する複合材料ブロ
ックを形成し、 得られた複合材料ブロックを放電ワイヤカッティング方
法で材料層厚方向に切断して、複合材料のブロックの材
料層厚方向厚さに対して1/6以下で且つ3mm以下の相当直
径の断面を有する頭部に硬質焼結体を備えた細長い複合
材料棒状体を2本以上切り取る、 ことを特徴とする細長い複合材料棒状体の製造方法。
1. A layer of a first material for a hard sintered body containing 50% or more of diamond powder or high-pressure phase boron nitride powder having an average particle size of 10 μm or less, and a periodic table 4a, 5a or
The second material layer made of cemented carbide in which the carbides of 6a group elements or their mutual solid solution carbides are bound by an iron group metal is placed in the same hot press container in the pressurizing direction and stacked under high temperature and high pressure. Hot-pressing with to sinter the layer of the first material, and in the process of sintering the layer of the first material, the hard sintered body of the first material into a cemented carbide layer obtained from the second material. A composite material block having a layer of a hard sintered body having a predetermined thickness is formed by joining, and the obtained composite material block is cut in the material layer thickness direction by a discharge wire cutting method to form a composite material block material layer. Elongated composite material characterized in that two or more elongated composite rod-shaped bodies each having a hard sintered body on the head having a cross section with an equivalent diameter of 1/6 or less and 3 mm or less with respect to the thickness direction are cut out. Material A method for manufacturing a rod-shaped body.
【請求項2】第1の材料の層と第2の材料の層との間に
厚さが0.5mm以下の中間接合層を配置してホットプレス
する特許請求の範囲第1項に記載の方法。
2. The method according to claim 1, wherein an intermediate bonding layer having a thickness of 0.5 mm or less is arranged between the first material layer and the second material layer and hot pressing is performed. .
JP59120219A 1984-06-12 1984-06-12 Method for manufacturing rod-shaped body of composite sintered material Expired - Fee Related JPH0742488B2 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
JP59120219A JPH0742488B2 (en) 1984-06-12 1984-06-12 Method for manufacturing rod-shaped body of composite sintered material
CA000483612A CA1286510C (en) 1984-06-12 1985-06-11 Stick of composite materials and process for preparation thereof
AT85304135T ATE49147T1 (en) 1984-06-12 1985-06-11 ROD MADE OF COMPOSITE MATERIALS AND METHOD FOR ITS MANUFACTURE.
EP85304135A EP0168953B2 (en) 1984-06-12 1985-06-11 Stick of composite materials and process for preparation thereof
KR1019850004091A KR920001585B1 (en) 1984-06-12 1985-06-11 Stick compositie materials and process for preparation thereof
DE8585304135T DE3575092D1 (en) 1984-06-12 1985-06-11 ROD FROM COMPOSITE MATERIALS AND METHOD FOR THEIR PRODUCTION.
US07/231,644 US4880707A (en) 1984-06-12 1988-08-10 Stick of composite materials and process for preparation thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP59120219A JPH0742488B2 (en) 1984-06-12 1984-06-12 Method for manufacturing rod-shaped body of composite sintered material

Publications (2)

Publication Number Publication Date
JPS61506A JPS61506A (en) 1986-01-06
JPH0742488B2 true JPH0742488B2 (en) 1995-05-10

Family

ID=14780829

Family Applications (1)

Application Number Title Priority Date Filing Date
JP59120219A Expired - Fee Related JPH0742488B2 (en) 1984-06-12 1984-06-12 Method for manufacturing rod-shaped body of composite sintered material

Country Status (1)

Country Link
JP (1) JPH0742488B2 (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61209821A (en) * 1985-03-13 1986-09-18 Sumitomo Electric Ind Ltd Method of manufacturing bar type body of composite sintered material
JPH0215069Y2 (en) * 1986-10-24 1990-04-24
EP3375554B1 (en) * 2016-11-15 2021-05-19 Sumitomo Electric Hardmetal Corp. Cutting tool
CN110539007A (en) * 2018-05-28 2019-12-06 上海名古屋精密工具股份有限公司 Blanks with hard materials and their use in tool manufacturing
WO2020255315A1 (en) * 2019-06-20 2020-12-24 オーエスジー株式会社 Cutting tool
CN116103529B (en) * 2023-02-16 2024-11-29 修武县鑫锐超硬材料有限公司 Preparation method of cubic boron nitride particle reinforced copper-based composite material
CN119328145A (en) * 2024-12-23 2025-01-21 陕西斯瑞铜合金创新中心有限公司 A method for quickly hot pressing and compounding copper alloy powder and matrix

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS567603U (en) * 1979-06-25 1981-01-23
JPS5672105A (en) * 1979-11-13 1981-06-16 Toshiba Tungaloy Co Ltd Composite cutting body
JPS5681605A (en) * 1979-12-06 1981-07-03 Toshiba Tungaloy Co Ltd Production of composite cutting body
JPS5681606A (en) * 1979-12-06 1981-07-03 Toshiba Tungaloy Co Ltd Production of composite cutting body

Also Published As

Publication number Publication date
JPS61506A (en) 1986-01-06

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