JPH0772676B2 - Method of filling working medium into heat pipe - Google Patents
Method of filling working medium into heat pipeInfo
- Publication number
- JPH0772676B2 JPH0772676B2 JP2185775A JP18577590A JPH0772676B2 JP H0772676 B2 JPH0772676 B2 JP H0772676B2 JP 2185775 A JP2185775 A JP 2185775A JP 18577590 A JP18577590 A JP 18577590A JP H0772676 B2 JPH0772676 B2 JP H0772676B2
- Authority
- JP
- Japan
- Prior art keywords
- working medium
- heat pipe
- heat
- pipe
- filling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Landscapes
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Description
【発明の詳細な説明】 「産業上の利用分野」 本発明はヒートパイプへの作動媒体の充填方法に関する
ものである。The present invention relates to a method for filling a heat pipe with a working medium.
「従来の技術」 従来は、真空ポンプによりヒートパイプ内から排気した
後、液相の作動媒体を計量しながら当該ヒートパイプへ
定量供給してこれを封止している。"Prior Art" Conventionally, after exhausting from the inside of a heat pipe by a vacuum pump, the liquid-phase working medium is metered and quantitatively supplied to the heat pipe to seal it.
「発明が解決しようとする課題」 従来の方法によれば、液相の作動媒体を計量しながらヒ
ートパイプへ供給するので、計量差が大きく、同一使用
のヒートパイプ間における作動媒体の充填量のバラツキ
が大きくなる。[Problems to be Solved by the Invention] According to the conventional method, since the liquid-phase working medium is supplied to the heat pipe while being measured, the difference in measurement is large, and the filling amount of the working medium between the heat pipes of the same use is large. The variation increases.
また、ヒートパイプ内から排気すると、そのパイプ内の
内部の不純物も同時に排出されるが、例えばヒートパイ
プコンテナが銅管である場合、脱気してもパイプの内壁
には酸素分子や水素分子その他の不純物が付着残留して
おり、このような残留不純物によって作動が不安定にな
り易い。Further, when exhausted from the heat pipe, impurities inside the pipe are also exhausted at the same time, but for example, when the heat pipe container is a copper pipe, even if it is degassed, oxygen molecules, hydrogen molecules and other Impurities remain attached, and such residual impurities tend to cause unstable operation.
本発明の第1の目的は、作動媒体の充填量のバラツキが
より小さいヒートパイプへの作動媒体の充填方法を提供
することにある。A first object of the present invention is to provide a method for filling a working pipe with a working medium in which variations in the amount of the working medium filled are smaller.
本発明の第2の目的は、作動がより安定したヒートパイ
プを製造することができる作動媒体の充填方法を提供す
ることにある。It is a second object of the present invention to provide a working medium filling method capable of producing a heat pipe with more stable operation.
「課題を解決するための手段」 本発明による第1の充填方法は、前述の第1の目的を達
成するため、ヒートパイプ内から排気する工程と、気相
の作動媒体を計量しながら、前記ヒートパイプ側へ送
り、この作動媒体を凝縮させながら前記ヒートパイプへ
の定量供給する工程とを含むことを特徴としている。[Means for Solving the Problems] In order to achieve the above-mentioned first object, the first filling method according to the present invention is characterized in that the step of exhausting from the heat pipe and the measurement of the working medium in the gas phase are performed. A step of sending the working medium to the heat pipe side and condensing the working medium to supply a fixed amount to the heat pipe.
本発明による第2の充填方法は、前述の目的を達成する
ため、前記第1の充填方法における最終工程の後に、前
記ヒートパイプ内の作動媒体を蒸発させてその一部を計
量しながら排出する工程を備えたことを特徴としてい
る。In order to achieve the above-mentioned object, the second filling method according to the present invention evaporates the working medium in the heat pipe after the final step of the first filling method and discharges a part of the working medium while measuring it. It is characterized by having a process.
前記ヒートパイプから蒸発させながら排出した気相の作
動媒体は、これを凝縮させつつ回収タンクへ回収するの
が好ましい。It is preferable that the vapor-phase working medium discharged from the heat pipe while being evaporated is collected in the collection tank while being condensed.
前記発明方法において、気相の作動媒体の計量には質量
流量計が使用される。In the method of the invention, a mass flow meter is used to measure the working medium in the gas phase.
また、気相の作動媒体を計量しながら前記ヒートパイプ
側へ送り、この作動媒体を凝縮させながら前記ヒートパ
イプへ定量供給する工程においては、多数のヒートパイ
プに対し順次作動媒体を供給し、前記ヒートパイプ内の
作動媒体を蒸発させてその一部を計量しながら排出する
工程においては、前工程において全部のヒートパイプに
対する作動媒体の供給が終了した後その多数のヒートパ
イプから作動媒体を順次排出するように構成するのが好
ましい。In addition, while feeding the working medium in the gas phase to the heat pipe side while metering the working medium, in the step of quantitatively supplying the working medium to the heat pipe while condensing the working medium, the working medium is sequentially fed to a large number of heat pipes, In the process of evaporating the working medium in the heat pipes and discharging a part of the working medium, the working medium is sequentially discharged from the large number of heat pipes after the supply of the working medium to all the heat pipes is completed in the previous process. It is preferable to configure so that
「作用」 本発明による第1の充填方法は、ヒートパイプへ作動媒
体を供給する際に、蒸発させて気相の作動媒体を計量し
ながら供給するものであるが、気相の作動媒体は液相の
作動媒体に比して著しく膨張しているので、液相の作動
媒体を計量しながら供給するのと比較して、計量誤差は
はるかに小さくなる。[Operation] In the first filling method according to the present invention, when the working medium is supplied to the heat pipe, the working medium in the vapor phase is vaporized and supplied while being measured. Since the working medium in the phase is significantly expanded compared with the working medium in the phase, the metering error is much smaller than that in the case where the working medium in the liquid phase is metered.
前記第2の充填方法によれば、ヒートパイプ内に一度供
給されて液相になっている作動媒体は、蒸発した状態で
その一部を排出することによって蒸留され、ヒートパイ
プ内に残留している酸素ガスや水素ガスその他の不純物
は、この蒸留によってヒートパイプから排出される。According to the second filling method, the working medium once supplied to the heat pipe and in the liquid phase is distilled by discharging a part of the working medium in an evaporated state, and remains in the heat pipe. Oxygen gas, hydrogen gas and other impurities present are discharged from the heat pipe by this distillation.
したがって、作動媒体の純度が一層高まる。Therefore, the purity of the working medium is further increased.
「本発明方法を実施するための装置例」 第1図は本発明方法を実施するための装置の一例を示す
配管図である。"Example of apparatus for carrying out the method of the present invention" Fig. 1 is a piping diagram showing an example of an apparatus for carrying out the method of the present invention.
多数のヒートパイプHP1,HP2〜HPnは、バルブV1,V2〜Vn
を介して第1の排気用配管1及び供給用配管2に接続さ
れている。第1の排気用配管1のヒートパイプ側寄りに
はバルブV3が、また、供給用配管2のヒートパイプ側寄
りにはバルブV4がそれぞれ設けられている。Many heat pipes HP1, HP2-HPn are valves V1, V2-Vn
Is connected to the first exhaust pipe 1 and the supply pipe 2 via. A valve V3 is provided near the heat pipe side of the first exhaust pipe 1, and a valve V4 is provided near the heat pipe side of the supply pipe 2.
第1の排気用配管1には、バルブV5及び流量計F1を設け
るとともに、バルブV6を有するバイパス管11が接続され
ている。この排気用配管1は、バルブV10を介して排気
ポンプ6に接続されている。The first exhaust pipe 1 is provided with a valve V5 and a flow meter F1 and is connected to a bypass pipe 11 having a valve V6. The exhaust pipe 1 is connected to an exhaust pump 6 via a valve V10.
供給用配管2の途中には流量計F2が設けられており、こ
の供給用配管2はバルブVV7,V8を介して作動媒体の供給
タンク4と接続している。A flow meter F2 is provided in the middle of the supply pipe 2, and the supply pipe 2 is connected to a working medium supply tank 4 via valves VV7 and V8.
タンク4は、上部に水冷式の冷却手段41を、下部にヒー
タ42をそれぞれ有しており、バルブV8,V9,第2の排気用
配管5及びバルブV10を介して排気ポンプ6に接続して
いる。The tank 4 has a water-cooling type cooling means 41 in the upper part and a heater 42 in the lower part, and is connected to the exhaust pump 6 via the valves V8, V9, the second exhaust pipe 5 and the valve V10. There is.
排気用配管1及び5のバルブ10を挟む位置には、バルブ
V11,V12を介して回収タンク7を接続し、この回収タン
ク7の上部には冷却手段71を設けている。At the position where the valve 10 of the exhaust pipes 1 and 5 is sandwiched, the valve
The recovery tank 7 is connected via V11 and V12, and a cooling means 71 is provided above the recovery tank 7.
この装置の例では、各バルブにはベローバルブを、流量
計F1,F2には質量計量計を、排気ポンプ6には乾式排気
ポンプをそれぞれ使用している。In the example of this device, a bellows valve is used for each valve, a mass meter is used for the flow meters F1, F2, and a dry exhaust pump is used for the exhaust pump 6.
「実施例」 この実施例において、ヒートパイプHP1〜HPnは、内径16
mm,肉厚0.7mm,容量600の銅管であり、作動媒体はフレ
オン113(沸点48℃)、ヒートパイプへの作動媒体の初
期充填量35g,最終充填量30gである。"Example" In this example, the heat pipes HP1 to HPn have an inner diameter of 16
mm, wall thickness 0.7 mm, capacity 600 copper tube, working medium is Freon 113 (boiling point 48 ° C.), initial filling amount of working medium to heat pipe is 35 g, final filling amount is 30 g.
配管1,2,5は、図示しないヒータ等の加熱手段により60
℃程度に加熱して、内部を流れる気相の作動媒体の凝縮
を防止している。The pipes 1, 2, and 5 are connected by heating means such as a heater (not shown).
It is heated to about ℃ to prevent the vapor-phase working medium flowing inside from condensing.
事前にバルブV12のみを開にして、排気ポンプ6により
回収タンク7から排気する。Only the valve V12 is opened in advance, and the exhaust tank 6 exhausts air from the recovery tank 7.
作動媒体の供給タンク4内の作動媒体はヒータ42の加熱
(55℃)によって蒸発し、同タンク4の上部の冷却手段
41によって凝縮する。酸素や窒素その他の不純物は蒸留
によりタンク4内の上部に溜まるので、バルブV8,V9,V1
0を開、他のバルブを閉にして時々これらの不純物を排
気ポンプ6によって排出する。The working medium in the tank 4 for supplying the working medium is evaporated by the heating (55 ° C.) of the heater 42, and the cooling means at the upper part of the tank 4
Condenses by 41. Oxygen, nitrogen and other impurities are accumulated in the upper part of the tank 4 by distillation, so valves V8, V9, V1
When 0 is opened and other valves are closed, these impurities are occasionally discharged by the exhaust pump 6.
先ず、バルブV1,V2,Vn,V3,V6,V10を開、他のバルブを閉
にし、排気ポンプ6を作動させてヒートパイプHP1〜HPn
内から排気する。First, the valves V1, V2, Vn, V3, V6, V10 are opened, the other valves are closed, and the exhaust pump 6 is operated to heat the heat pipes HP1 to HPn.
Exhaust from inside.
次にバルブV1,V4,V7,V8のみを開にし、タンク内の気相
の作動媒体を、途中の流量計F2で計量しながら供給用配
管2を通じて、ヒートパイプHP1内に35g供給する。次い
で、バルブV1を閉、バルブV2を開にしてヒートパイプHP
2内へ同量の作動媒体を供給し、以下同様なバルブ操作
により、最後のヒートパイプHPnまで順次同量の作動媒
体を供給する。Next, only the valves V1, V4, V7, V8 are opened, and 35 g of the gas-phase working medium in the tank is supplied into the heat pipe HP1 through the supply pipe 2 while being measured by the flow meter F2 on the way. Then, close the valve V1 and open the valve V2 to set the heat pipe HP.
The same amount of working medium is supplied into 2, and the same amount of working medium is sequentially supplied to the last heat pipe HPn by the same valve operation.
各ヒートパイプHP1〜HPnに供給される気相の作動媒体
は、これらのヒートパイプの上部に設けられているそれ
ぞれの水冷式の冷却手段81〜8nによって冷却され、凝縮
しつつ各ヒートパイプHP1〜HPn内に供給される。The gas-phase working medium supplied to each of the heat pipes HP1 to HPn is cooled by the respective water-cooling type cooling means 81 to 8n provided at the upper part of these heat pipes, and each heat pipe HP1 to HPn while being condensed. Supplied within HPn.
また、各ヒートパイプHP1〜HPnの下部に設けられたそれ
ぞれの加熱手段91〜9nにより、これらのヒートパイプ内
の作動媒体を蒸発させる。この状態で、バルブV3,V5,V1
0,V11のみを開にし、バルブV1,V2,Vnを順次開閉するこ
とにより、ヒートパイプHP1〜HPn内の蒸発した作動媒体
を、流量計F1で計量しながら第1の排気用配管1を通じ
て5gずつ順次回収タンク7へ回収する。しかる後に、各
ヒートパイプHP1〜HPnを封じる。The heating means 91 to 9n provided below the heat pipes HP1 to HPn evaporate the working medium in these heat pipes. In this state, valves V3, V5, V1
By opening only 0, V11 and sequentially opening and closing valves V1, V2, Vn, the evaporated working medium in the heat pipes HP1 to HPn is metered by the flow meter F1 while measuring 5 g through the first exhaust pipe 1. Collected one by one into the recovery tank 7. Then, the heat pipes HP1 to HPn are sealed.
このように、ヒートパイプHP1〜HPn内の作動媒体の蒸留
により、ヒートパイプHP1〜HPn内に残留していた酸素分
子や水素分子その他の不順物は排出される。In this way, by distilling the working medium in the heat pipes HP1 to HPn, oxygen molecules, hydrogen molecules and other irregular substances remaining in the heat pipes HP1 to HPn are discharged.
回収タンク7内に回収される作動媒体は、上部の冷却手
段71により、凝縮しつつタンク7に溜まる。回収タンク
7内に所定量以上の作動媒体が溜まったならば、バルブ
V11,V12を閉にし、バルブV13,V14を開にして不活性ガス
等を回収タンク7内に導入することにより、配管3を通
じて回収タンク7内の作動媒体をタンク4内へ圧送す
る。The working medium recovered in the recovery tank 7 is condensed in the tank 7 by the upper cooling means 71. If a predetermined amount or more of working medium is accumulated in the recovery tank 7, the valve
V11 and V12 are closed, valves V13 and V14 are opened, and an inert gas or the like is introduced into the recovery tank 7, whereby the working medium in the recovery tank 7 is pumped into the tank 4 through the pipe 3.
以上の要領により、15本のヒートパイプに作動媒体を充
填したが、各ヒートパイプ間の作動媒体充填量の誤差は
±0.5g以内であって、特性がより安定したヒートパイプ
を生産性よく製造することができた。According to the above procedure, 15 heat pipes were filled with the working medium, but the error of the working medium filling amount between each heat pipe was within ± 0.5 g, and the heat pipe with more stable characteristics was manufactured with high productivity. We were able to.
例えば作動媒体がフレオン113である場合、その液相状
態における1モル=119ccに対し、その気相状態におけ
る1モル=22400ccであるが、両相のフレオン113を各別
の配管中で流しながら、例えば数cc〜10cc単位で計量す
ると、後者の測定精度がはるかに高くなる。ちなみに、
フレオン113の30gはおよそ1/6モル程度であるが、その
気相状態のときは、例えば質量流量計により数cc単位で
計量できる。For example, when the working medium is Freon 113, 1 mol = 119 cc in the liquid phase state and 1 mol = 22400 cc in the gas phase state, while flowing Freon 113 of both phases in separate pipes, For example, when measuring in units of several cc to 10 cc, the latter measurement accuracy is much higher. By the way,
Although 30 g of Freon 113 is about 1/6 mol, in the gas phase state, it can be measured in units of several cc by a mass flow meter, for example.
気相の作動媒体を凝縮させながらヒートパイプへ供給す
るとき、ヒートパイプの上部へ前述のように冷却手段を
設けて冷却することに代えて、例えばヒートパイプに近
い上方の配管中に図示しない冷却アキュムレータを設
け、この部分で冷却しても実施することができる。When supplying the working medium in the vapor phase to the heat pipe while condensing it, instead of providing cooling means on the upper part of the heat pipe as described above, for example, cooling not shown in the upper pipe near the heat pipe It can also be implemented by providing an accumulator and cooling at this portion.
「発明の効果」 本発明の充填方法によれば、極めて高精度で作動媒体を
計量しながらヒートパイプへ充填することができるの
で、同一使用のヒートパイプ間における作動媒体の充填
量のバラツキが従来方法に比べてはるかに小さくなる。
したがって、より均質なヒートパイプを製造することが
できる。"Effect of the Invention" According to the filling method of the present invention, since it is possible to fill the heat pipe while measuring the working medium with extremely high accuracy, there is a variation in the filling amount of the working medium between the heat pipes of the same use. Much smaller than the method.
Therefore, a more homogeneous heat pipe can be manufactured.
第1図は本発明方法を実施するための装置の一例を示す
配管図である。 主要図中符号の説明 1は第1の排気用配管、11はバイパス管、2は供給用配
管、4は作動媒体の供給タンク、5は第2の排気用配
管、6は排気ポンプ、7は回収タンク、V1〜Vnはバル
ブ、HP1〜HPnはヒートパイプ、F1,F2は流量計である。FIG. 1 is a piping diagram showing an example of an apparatus for carrying out the method of the present invention. DESCRIPTION OF SYMBOLS IN THE MAIN FIGURES 1 is a first exhaust pipe, 11 is a bypass pipe, 2 is a supply pipe, 4 is a working medium supply tank, 5 is a second exhaust pipe, 6 is an exhaust pump, and 7 is Recovery tanks, V1 to Vn are valves, HP1 to HPn are heat pipes, and F1 and F2 are flow meters.
Claims (3)
の作動媒体を計量しながら前記ヒートパイプ側へ送り、
この作動媒体を凝縮させながら前記ヒートパイプへ定量
供給する工程とを含むことを特徴とする、ヒートパイプ
への作動媒体の充填方法。1. A step of exhausting air from the inside of a heat pipe, and feeding a working medium in a gas phase to the heat pipe side while measuring
And a step of quantitatively supplying the working medium to the heat pipe while condensing the working medium, the method for filling the working medium into the heat pipe.
いて、作動媒体を凝縮させながら前記ヒートパイプへ定
量供給する工程の後に、当該ヒートパイプ内の作動媒体
を蒸発させてその一部を計量しながら排出する工程を含
むことを特徴とする、ヒートパイプへの作動媒体の充填
方法。2. The working medium filling method according to claim 1, wherein after the step of quantitatively supplying the working medium to the heat pipe while condensing the working medium, the working medium in the heat pipe is evaporated and a part thereof is evaporated. A method of filling a heat pipe with a working medium, the method comprising discharging while measuring.
パイプ側へ送り、この作動媒体を凝縮させながら前記ヒ
ートパイプへ定量供給する工程においては、多数のヒー
トパイプに対し順次作動媒体を供給し、前記ヒートパイ
プ内の作動媒体を蒸発させてその一部を計量しながら排
出する工程においては、前工程において全部のヒートパ
イプに対する作動媒体の供給が終了した後その多数のヒ
ートパイプから作動媒体を順次排出することを特徴とす
る、請求項2に記載のヒートパイプへの作動媒体の充填
方法。3. A step of feeding a working medium in a vapor phase to the heat pipe side while measuring the working medium and supplying the working medium to the heat pipe while condensing the working medium in a fixed amount, the working medium is sequentially supplied to a large number of heat pipes. However, in the step of evaporating the working medium in the heat pipe and discharging a part of the working medium while measuring it, after the working medium has been supplied to all the heat pipes in the previous step, the working medium is removed from the large number of heat pipes. The method for filling a working medium with a heat pipe according to claim 2, wherein the heat medium is sequentially discharged.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2185775A JPH0772676B2 (en) | 1990-07-13 | 1990-07-13 | Method of filling working medium into heat pipe |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2185775A JPH0772676B2 (en) | 1990-07-13 | 1990-07-13 | Method of filling working medium into heat pipe |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0473596A JPH0473596A (en) | 1992-03-09 |
| JPH0772676B2 true JPH0772676B2 (en) | 1995-08-02 |
Family
ID=16176677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2185775A Expired - Lifetime JPH0772676B2 (en) | 1990-07-13 | 1990-07-13 | Method of filling working medium into heat pipe |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0772676B2 (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103335548A (en) * | 2013-06-11 | 2013-10-02 | 大连理工大学 | Temperature control gas phase working medium perfusion method for micron heat pipe |
| CN106698309B (en) * | 2015-07-20 | 2018-11-09 | 江苏宏力光电科技有限公司 | A kind of new heat pipe liquid-injection equipment |
| CN110949715B (en) * | 2019-12-21 | 2020-11-17 | 西安交通大学 | High-precision quantitative filling device and method for liquid sodium metal |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5652189U (en) * | 1979-09-27 | 1981-05-08 |
-
1990
- 1990-07-13 JP JP2185775A patent/JPH0772676B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0473596A (en) | 1992-03-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5354433A (en) | Method for producing a flow of triisobutylaluminum from liquid triisobutylaluminum containing isobutene | |
| Vieth et al. | Dual sorption mechanisms in glassy polystyrene | |
| Elgin et al. | Thermodynamic study of the He 4 monolayer adsorbed on Grafoil | |
| Drain et al. | Thermodynamic properties of argon adsorbed on rutile | |
| JP5583121B2 (en) | Purified liquefied gas supply method | |
| Witzenburg et al. | Density measurements of compressed solid and liquid argon | |
| CN104973629B (en) | A kind of method of purification of tungsten hexafluoride | |
| JP3123020B2 (en) | Method and apparatus for boosting high purity gas to ultra high pressure | |
| JP2007516396A (en) | Method for filling a compressed gas container with gas | |
| US2959926A (en) | Generation of cold or cooling by evaporation of a liquid evaporating at a very low temperature | |
| US2938360A (en) | Anhydrous ammonia storage tank | |
| JPH0772676B2 (en) | Method of filling working medium into heat pipe | |
| JP7019726B2 (en) | Analysis method for trace pollutants in cryogenic liquids | |
| Ancsin | Dew points, boiling points and triple points of" pure" and impure oxygen | |
| Elsworth et al. | The sorption of N2, H2 and D2 on titanium films at 20° C and− 190° C | |
| Price et al. | The use of gas chromatography to study solubility in polymeric systems | |
| JP4036618B2 (en) | Method and apparatus for measuring mixed gas | |
| Higuti et al. | Calorimetric evidence for the capillary condensation theory | |
| Akhtar et al. | The hydrogen/oxygen titration on platinum films. Determination of the catalytically-active area | |
| JPH04265213A (en) | Storage method for phosphorus pentafloride | |
| CN117059521A (en) | Thin film deposition equipment, vaporization detection device and vaporization detection method | |
| CN116242178A (en) | Heat pipe working medium filling device and method | |
| Machin | Hysteresis and irreversible phase transitions: xenon adsorbed on a mesoporous silica gel | |
| JPH10239223A (en) | Method and apparatus for analyzing siloxane in silicon compound gas | |
| Swenson | The Catalysis of the Ortho‐Para Conversion in Liquid Hydrogen |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20070802 Year of fee payment: 12 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20080802 Year of fee payment: 13 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20080802 Year of fee payment: 13 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090802 Year of fee payment: 14 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090802 Year of fee payment: 14 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20100802 Year of fee payment: 15 |
|
| EXPY | Cancellation because of completion of term |