AU630164B2 - Method of corrosion protection at pipe junctions - Google Patents

Description

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OPI DATE 05/09/90 PCT AOJP DATE 11/10/90 APPLN. ID 51058 PCT NUMBER PCT/AU90/00055 INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (51) International Patent Classification 5 (11) International Publication Number: WO 90/09542 Fl6L 58/00, 58/02, 58/10 Al (43) International Publication Date: 23 August 1990 (23.08.90) (21) International Application Number: PCT/AU90/00055 (81) Designated States: AT, AT (European patent), AU, BB, BE (European patent), BF (OAPI patent), BG, BJ (OAPI (22) International Filing Date: 9 February 1990 (09.02.90) patent), BR, CA, CF (OAPI patent), CG (OAPI patent), CH, CH (European patent), CM (OAPI patent), DE, DE (European patent), DK, DK (European patent), ES Priority data: (European patent), FI, FR (European patent), GA (OA- PJ 2670 9 February 1989 (09.02.89) AU PI patent), GB, GB (European patent), HU, IT (European patent), JP, KP, KR, LK, LU, LU (European patent), MC, MG, ML (OAPI patent), MR (OAPI patent), (71) Applicant (for all designated States except US): TUBEMAK- MW, NL, NL (European patent), NO, RO, SD, SE, SE ERS OF AUSTRALIA LIMITED [AU/AU]; Hume (European patent), SN (OAPI patent), SU, TD (OAPI Highway, Somerton, VIC 3047 patent), TG (OAPI patent), US.

(72) Inventors; and Inventors/Applicants (for US only) MIESZELEWICZ, Gie- Published nek [AU/AU]; 9 Elwyn Street, Bentleigh East, VIC 3165 With international search report.

AYLEN, Brian, Arthur, Valentine [AU/AU]; 4/7 View Street, Surrey Hills, VIC 3165 (AU).

(74) Agent: ARTHUR S. CAVE CO.; Level 10, 10 Barrack Street, Sydney, NSW 2000 63064 (54) Title: METHOD OF CORROSION PROTECTION AT PIPE JUNCTIONS (57) Abstract A method for providing protection against corrosion of a pipe joint formed by the mating of complementary ends of two pipes comprising the steps of: applying controlled heating to a pipe body which is to be joined to an adjacent pipe, (b) applying to the ends 5) of each pipe a protective layer or coating of material to the pipe body by a time/temperature function process, allowing the pipe to cool, bevelling the terminations of the protective layer or coating mating complementary ends 5) of the pipes together to form a sealed and corrosion resistant joint c P(IIAU UVI v u V O RECEIVED 1 8 APR 1990 METHOD OF CORROSION PROTECTION AT PIPE JUNCTIONS The present invention relates to a method of producing rubber-ring steel jointed pipe junctions having high internal and external long term corrosion protection, tight pipe end tolerances and being capable of withstanding high operating pressures. Whilst the invention is according to one embodiment directed towards and primarily described for producing steel pipe to be used in underground pipelines, it is anticipated that the invention is suitable for other forms of pipelines such as overground installations.

Earlier corrosion protection methods for the outer surface of underground pipelines have utilised bituminous enamels, whilst more recently the application of high quality plastic coatings such as polyethylene (PE) have been used. Both these methods of corrosion protection have been used in conjunction with cathodic protection systems. Typical prior art corrosion protection methods also utilise epoxy or cement linings for the internal surface of the steel pipe.

Corrosion protection utilising coatings such as bituminous coatings have the major disadvantage that they create an effect known as the 'area effect' resulting in accelerated local corrosion if the coating is damaged. This often occurs as a result of abrasion or impact during laying of pipes.

Generally, a weak point in a pipeline occurs at the junction of pipes due to the fact that it is a si'e where the necessary elements to create electrolytic corrosion are present. It is critical that pipe joints be provided with effective resistance against corrosion however, in the past this has proved to be difficult.

At pipe joints it is necessary to provide means for the purpose of preventing ingress of moisture which may precipitate corrosive processes. Furthermore, it is necessary to provide means to prevent the setting up of any electrolytic corrosion process. Pipe joints typically comprise the mating of a socket end (female part) and a spigot end (male part).

The socket end preferably has an internal groove into which a rubber ring fits to effect sealing of the joint.

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Z 1923j/KW 2 which a rubber ring fits to effect sealing of the joint.

Typically, the rubber-ring socket end of the pipe has previously been uncoated causing further major problems associated with use of the above-mentioned corrosion protection methods. The failure of such pipes resulting from corrosion of the pipe ends arises from the ingress of moisture and corrosive agents at the pipe joint.

In order to overcome the problems associated with the corrosion of pipe ends, the use of plastic coatings on the outer surface of the pipe has been extended to cover the internal surface of the rubber ring socket end of the pipe.

Even though such practice has marginally improved the corrosion protection for such pipes the known methods of producing rubber ring socket ended steel pipe have not been adequate for producing economical and easy to assemble pipe having the outer plastic coating extending to the internal surface of the pipe joint. The major drawbacks stem from o o the critical tolerances required for the efficient mating of the pipe joint such that high operating pressures may be withstood and the increased difficulty associated with e• laying pipelines having the plastic coating extending to the :internal surface of the pipe joint.

Problems were previously experienced in use of rubber ring socket end joi!nt pipes which have previously utilised 25 an outer plastic coating which extends from the outer surface around the socket end to the inner surface of the socket end.

The present invention seeks to provide a method for forming a corrosion resistant pipe junction of two pipes formed by a spigot end of one pipe married to a socket end of another pipe, each of said pipe ends having its outer surface covered with a protective layer, which extends around the socket and spigot ends providing protection to the inner and outer surface of the socket and spigot ends.

In one broad form according to the method aspect, the invention comprises the steps of: a) hot rolling a pipe socket end at controlled pipe .temperature; b) quenching the pipe socket end; !sai~a 4W 1923j/KW -3c) partially re-rolling the pipe socket end if it is undersized or requenching socket end if it is oversized; d) grit blasting of the pipe outer surface and the inner surface near pipe ends; e) controlled heating of the pipe; f) applying protective layer material to the pipe body by a time/temperature function process; g) elimination of any protective layer porosity by post heating; h) allowing the pipe to cool, i) bevelling the terminations of the protective coating layer.

In another broad form, the present invention provides a method for forming a coated pipe end, said pipe having a 15 spigot end and a socket end, with its outer surface covered i with a protective layer, extending the outer surface around ee the socket end and providing protection to the inner surface c o of the socket end and spigot and; the method generally comprising the steps of: a) producing a pipe with the spigot end shell having a Sb) diameter of a predetermined tolerance; hot rolling the pipe socket end at first preferred 00 temperature whilst pipe is held by at least a first e* clamp at a first preferred distance from said socket with the area of the pipe at or near said clamnp being held at a second preferred temperature; 0 e0 c) quenching the socket end when said socket end has cooled to a third preferred temperature; d i) partially reheating the pipe socket end, if end undersized, to a fourth preferred temperature and re rolling, ii) partially reheating the socket end if end oversized thence clamping and heating to a fifth preferred temperature level followed by quenching; e) grit blasting simultaneously the pipe outer surface and inner surface near the pipe ends in a blast machine; f) heating the pipe body to a sixth preferred temperature level with the pipe body at or near said pipe ends held at a seventh preferred temperature level; L i; i 1923j/KW 3a g) immersing the pipe into the protective layer material and rotating, with the immersion process being controlled by a time/temperature function; e m **0 i i 1 J I i i i i i W 1923j/KW -4h) elimination of the protective layer porosity by infrared radiation post heating, with the socket inner surface protective layer alternatively heated by induction for pipes having small thicknesses; i) cooling the pipe by natural or fan assisted drafting; j) bevelling the coating terminations of the protective layer.

In its broadest form the present invention comprises; a method for providinig corrosion protection of a steel pipe joint which is formed by the mating of a socket end of one pipe with a complementary spigot end of a second pipe, comprising the steps of: a) applying controlled heating to the body of one pipe which is to be joined to an adjacent pipe, b) applying to the spigot end and socket end of each pipe an outer protective layer or coating of a plastics material by a time/temperature function process, such that the protective layer covers a portion of the outer surface of each pipe at or near the ends thereof and then passes continuously around the end extremitites 4nd along the internal surface terminating at a predetermined distance from the ends, c) allowing the pipe to cool, oooo d) bevelling the terminations of the protective layer, 25 e) mating complementary ends of each pipe to form a sealed corrosion resistant joint.

In the preferred embodiment the pipe coating covers the .outer surface and inner surface at the pipe ends so that the coating on the inner surface is at least partially sandwiched between the internal pipe surface and a concrete lining. A rubber ring is then inserted in a groove after application of a lubricant in the pipe end to provide a seal between it and a mating pipe.

The process is intended to be completed in the factory so no further field attention to the joint is required.

The invention will now be described by way of dxample with reference to the accompanying drawings in which: Figure 1 illustrates one embodiment of the cross section of the socket ended pipe joint prior to assembly.

Figure 2 illustrates the same embodiment of Figure 1 L off\C; 1923j/KW 4a fully assembled.

The present invention relates to an improved method for producing rubber-ring steel jointed pipe as shown according to one embodiment in Figures 1 and 2.

Referring to figures 1 and 2, two views of a cross section of the pipe joint are shown, the first view showing the joint prior to assembly and the second following

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,It 0 WO 90/09542 PC/AU90/00055 ends have the coating disposed on their external and internal surfaces as shown.

The pipes are coated externally by a polyethylene coating 2 and internally lined by a cement mortar lining 3, with the polyethylene coating 2 and cement mortar lining 3 being provided as corrosion resistant barriers for the steel pipes i. The spigot end 4 of one pipe may be joined to the socket end 5 of another pipe i. The socket end 5 is provided with an internal recess located at position 6 to accommodate a rubber ring 8. The rubber-ring 8 is lubricated prior to assembly to assist in assembly of the joint and provides a compressive water-tight seal.

The polyethylene coating 2 extends around the socket 5 end and continues internally. The socket 5 end has its inner surface coated with the polyethylene coating 2 along its length and meets the cement mortar lining 3 which protects the remaining internal length of the pipe i.

The methodology of the present invention seeks to improve the production of rubber-ring steel jointed pipes as mentioned above.

Joint formation is effected in the following manner.

The pipe is produced initially with the spigot end of the shell to nominal diameters and mechanically sized to mate the socket within 0.5mm and limiting the growth at a point, 120mm from the end of the shell. A collapse of 1 plate thickness is introduced at the very end of the spigot to permit ease of entry into the socket during assembly.

Larger growth values will cause assembly difficulties in the field that could render the joint impossible to assemble.

Diameters below nominal will reduce rubber pre-compression which provide the initial seal, controls organic root penetration through the joint, provides rounding forces on the socket to reduce localised lip gaps to below the critical level of 2 mm, and therefore eliminates the chance of rubber ring blow-out.

The diametric dimensions of the socket for each specific pipe size are designed taking into account the final nominal outside diameter of the spigot and the thickness and tolerance WO 90/09542 PCT/AU90/G0055 6 of the corrosion protection coating. The socket is hot rolled and this demands precise rolling die dimensions and settings plus an accurately controlled pipe temperature of 780 0 C for reproducibility of socket formation.

Since the pipe is held in clamps approx. 250 mm from the end that will be rolled into a socket, it is imperative that the 780 0 C 20 0 C temperature be uniform and limited in length to 200 mm with a sudden temperature gradient over the next mm so that the pipe temperature in the clamp area is held at 400 0 C max. This will avoid unacceptable shell deformation during the rolling operation.

The rate of socket material upset must be controlled to 6 mm per rolling head revolution to ensure concentricity of rolled socket with the pipe body. The socket formation must be completed in 4 1 revolutions of the rotary head followed by a controlled unloading speed of the inner die to ensure socket roundness and dimensional accuracy.

After the completion of rolling the next step is to quench the pipe. While the pipe is still held concentric and round to 0.5 mm by two clamps (relieved by 1.25% (outer) and 1.00% (inner) to match the temperature gradient of the shell), the newly rolled socket is water quenched and shrunk to size.

Quenching begins when the pipe temperature is approx. 450°C Where sockets are rolled outside specification, they can be corrected as follows: When undersized, the correction is carried out by partial re-rolling after reheating the socket to 75% of the standard rolling temperature. Great care is required when repositioning the already rolled socket into the die system. The hump must be centred evenly between the outer dies before commencing to re-roll.

Oversized product is corrected by reheating the socket to 500 0 C 25 0 C, reclamping and shrinking to size by water quenching.

'V -i i 1. iL I~ i-- WO 90/09542 PCT/AU90/00055 -7- SURFACE PREPARATION The next step in the process is to prepare the pipe surface in order to enable application of the corrosion protection layer. Sound adhesion between the corrosion protection layer and the substrate is obtained principally due to "Anchor pattern" effects. Optimum pattern conditions are achieved by the use of steel grit abrasive conforming to "running mixes" of the following graduation: mM Passing 840 12.8% 710 27.0% 600 28.5% 500 14.5% 425 9.2% 355 4.7% 300 3.3% TAKEOUT SIZE 177 As 1627 Part 4 Class 2.5 3 with profile height of um Rtm and 85 95 Rt.

The internal surfaces of the joint ends are prepared simultaneously with the external process by selective rotational/travel delays when the critical joint areas are located in the "Hot Spot" region of the blast machine. Both direct and reflective particle impingement maintains profile character in the socket region including the shadow faces.

HEATING

The next step is to heat the pipe to the correct temperature gradient prior to coating the pipe with the protective layer.

Direct propane flame impingement heating with additional and independent open flame end heaters are located at 6 o'clock providing energy at 150,000 KJ/m. Pipe rotation of 7 12 m/min is used during this heat cycle which varies from 4 min and is dependent on the pipe mass. Temperature gradients are controlled such that 1 2 m of the pipe ends are held at 5 0 C above the pipe body temperature but never exceeding 400°C, at the time of discharge from the oven.

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WO 90/09542 PCr/AU90/00055 8 To balance the pipe end cooling effects, the pipe socket end temperature must be held to 300 5°C above the pipe body temperature with a maximum of 345°C, when the pipe dipping operation commences.

The spigot end can be held at a temperature closer to the pipe body temperature as there is less internal coating applied at that end.

For sound adhesion to be obtained, it is critical that the above temperature controls and the following lower limits on dip temperature are strictly observed: 280°C and 10 mm w.t.

300°C 6 mm w.t.

320°C 5 mm w.t.

340°C 4.5 mm w.t.

COATING

The coating process step which is a time/temperature function follows.

The pipe is rotated at 5 10 m/min., while immersed to of its diameter in a fluidized polyethylene bath, held at 60°C. Higher temperatures increase the rate of fusion onto the pipe. Immersion times vary between 2.5 5 min. which provides the necessary time to deposit coating thicknesses.

POST HEATING The porosity in the coating is eliminated in a further step by post heating using infrared radiation techniques varying in time from 5 20 min. with the pipe shell temperature being held between 180 220 0 C. Radiation levels are held at a point where shell temperature will not decay more than 1°C/min. and may even rise at a nominal rate of 0.3 0 C/min.

The socket lining is treated in a similar manner internally except when shell thicknesses are 5 mm. In this case induction heating is resorted to, using the following conditions: The induction heating unit operates at 25 kw with 10 kHZ frequency and is ON for a number of seconds for five pipe revolution and OFF for number of seconds for one pipe 1- i.:i ii'- i; C I WO 90/09542 PCT/AU90/00055 -9 revolutions to hold shell temperatures at 230 0 C Parameters are: mm W.T. Post heat not required.

mm W.T. Marginal post heat required.

mm W.T. Post heat at 180 210°C Heating limit is below the onset of surface oxidation and crazing. Temperature measurements of coating surface at e 0.96.

COOLING

Cooling of the pipe is the next step and is carried out by natural or fan assisted drafting which lowers the temperature from 200 0 C 20 0 C to 60 C within a time limit of not less than 60 minutes.

BUFFING

Buff bevelling of the coating terminations at 1:5 tapers follows the cooling step.

RUBBER RINGS Rubber rings of a suitable type are utilised for the sealing means of the pipe joint.

The present invention therefore provides a method for producing corrosion barrier coated pipes.

It should be obvious to persons skilled in the art that numerous variations and modifications could be made to the method and apparatus of the present inventions as described and with reference to the drawings without departing from the overall scope or spirit of the invention.

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Claims (24)

1. A method for providing corrosion protection of a steel pipe joint which is formed by the mating of a socket end of one pipe with a complementary spigot end of a second pipe, comprising the steps of: a) applying controlled heating to the body of one pipe which is to be joined to an adjacent pipe, b) applying to the spigot end and socket end of each pipe an outer protective layer or coating of a plastics material by a time/temperature function process, such that the protective layer covers a portion of the outer surface of each pipe at or near the ends thereof and then passes continuously around the end extremitites and along the internal surface terminating at a pnedetermined distance from the ends, c) allowing the pipe to cool, d) bevelling the terminations of the protective layer, e) mating complementary ends of each pipe to form a sealed corrosion resistant joint.

2. A method according to claim 1 comprising the additional preliminary steps before controlled heating of the pipe body of: at least hot rolling the pipe at a first preferred o••e temperature whilst the pipe is held by at least a first clamp, quenching the socket end of the pipe when the socket end has cooled to a preferred temperature.

3. A method according to claim 2 comprising the additional step of grit blasting of the pipe outer surface and the S 30 inner surface near the pipe ends prior to controlled heating of the pipes.

A method according to claim 3 comprising the additional step of eliminating protective layer porosity by post heating prior to mating the pipe ends.

5. A method according to claim 4 comprising the additional steps of: partially reheating the pipe socket end if the end is undersized to a preferred temperature thence rerolling, S(b) partially reheating the socket end if the end is 6 oversized thence clamping and heating to a preferred II i. I 1923j/KW 11 temperature level followed by quenching.

6. A method according to claim 5 comprising the steps of; hot rolling a pipe having a socket end and a spigot end at the first preferred temperature whilst the pipe is held by at least the first clamp at a first prefeired distance from said socket end with the area of the pipe at or near the said first clamp being held at a second preferred temperature; quenching the socket end when said socket end has a cooled to a third preferred temperature, partially reheating the pipe socket end, if the pipe end undersized to a fourth preferred temperature thence rerolling, partially reheating the socket end if the pipe end is 15 oversized thence clamping and heating to a fifth preferred temperate level followed by quenching.

7. A method according to claim 6 wherein the heating after grit blasting comprises the step of heating the pipe body to a sixth preferred temperature level, followed by quenching.

8. A method according to claim 7 comprising the additional :step of immersing the pipe end in the protective layer material and rotating the pipe with the immersion process being controlled by a time temperature function.

9. A method according to claim 8 comprising the optional additional step of eliminating protective layer porosity by *e infrared radiation post heating, with a socket inner surface protective layer alternatively heated by induction for pipes having small thicknesses.

A method according to claim 9 wherein the hot rolling 00 temperature is controlled within the range of 760°C to 800 C and at a distance than not greater than 250mm from the heated pipe end.

11. A method according to claim 10 wherein the pipe temperature in the clamp area is not greater than 400 0 C.

12. A method according to claim 11 wherein the quenching begins when the pipe temperature falls within the range 0 0 425°C to 475°C.

13. A method according to claim 12 wherein, if the pipe is O6 T. oversized, the socket is reheated to a temperature within C, 1 i 1923j/KW 12 the range of 475 0 C to 525 0 C.

14. A method according to claim 13 wherein when the heating of the pipe takes place before immersion in the said protective layer, the pipe is rotated in an open flame.

15. A method according to claim 14 wherein the said infrared radiation post heating takes place for a period within or including the range 5 to 20 minutes and at a temperature falling within the range of 180 0 C to 220 0 C.

16. A method for producing a.plastics coating for steel pipes applied at a spigot end and socket end of each pipe so that the coating covers a portion of the outer surface of each pipe at or near the ends thereof and then passes continuously around the pipe extremities and along the internal surface for a predetermined distance thereby providing a corrosion resistant joint formed by mating of the spigot end of one pipe with the socket end of another pipe, the method comprising the steps of; Hot rolling a pipe at a first preferred temperature whilst the pipe' is held by at least a first clamp at a first preferred distance from said socket with the area of the pipe at or near the said first.clamp being held at a second preferred temperature; quenching the socket end when said socket end has cooled to a third preferred temperature; 25 partially reheating the pipe socket end, if the pipe end is undersized to a fourth preferred temperature thence rerolling, partially reheating. the socket end, if the pipe end is 6versized, thence clamping and heating to a fifth preferred temperature level followed by quenching, grit blasting simultaneously the pipe outer 'surface and inner surface near the pipe ends in a blast machine, heating the pipe body to a sixth preferred temperature level followed by quenching, immersing the pipe into a protective layer material and rotating it with the immersion process being controlled by a time/temperature function, eliminating the protective layer porosity by infrared radiation post heating, with a socket inner surface 1 1U u yl-cY uue- ena at controlled pipe temperature; b) quenching the pipe socket end; 1~i 1923j/KW 12a protective layer alternatively heated by induction for pipes having small thicknesses; cooling the pipe by natural or fan assisted drafting; bevelling the coating terminations of the protdctive layer. 0 L CI i LL I LI i level with the pipe body at or near said pipe ends held at a seventh preferred temperature level; Z S2- 0 1923j/KW 13

17. A method according to claim 16 wherein the hot rolling temperature is controlled within the range of 760 0 C to 800 C and at a distance than not greater than 250mm from the heated pipe end.

18. A method according to claim 17 wherein the pipe temperature in the clamp area is not greater than 400 0 C.

19. A method according to claim 18 wherein the quenching begins when the pipe temperature falls within the range 425 C to 475 C.

20. A method according to claim 19 wherein if the pipe is oversized the socket is reheated to a temperature within the range of 475 C to 525 0 C.

21. A method according to claim 20 wherein when the heating of the pipe takes place before immersion in the said 15 protective layer, the pipe is rotated in an open flame.

22. A method according to claim 21 wherein the Said infrared radiation post heating takes place for a period within or including the range 5 to 20 minutes and at a temperature falling within the range of 180 0 C to 220 0 C. 20

23. A method according to anyone of the foregoing claims wherein the protective layer comprises a low density polyethylene.

24. A pipe having a protective layer applied to each of its ends so as to form a corrosion resistant joint when mated to another pipe, the joint produced by application of the method according to anyone of the foregoing claims. A method for production of a pipe having a protective coating to prevent corrosion thereof as hereinbefore described and with reference to the accompanying illustrations. DATED this 29th day of May, 1992. TUBEMAKERS OF AUSTRALIA LIMITED By Its Patent Attorneys DAVIES COLLISON CAVE ii SIPCT/AU 9 0 /000 5 4 RECEIVED 1 8 APR 1990 14 .ABSTRACT A method for providing protection against corrosion of a pipe joint formed by the mating of complementry ends of two pipes comprising the steps of: applying controlled heating to a pipe body which is to be joined to an adjacent pipe, applying to the ends 5) of each pipe a protective layer or coating of material 2 to the pipe body by a time/temperature function process, allowing the pipe to cool, bevelling the terminations of the protective layer or coating mating complimentary ends 5) of the pipes together to form a sealed and corrosion resistant joint 0121j I I 1 SUBSTITUTE SHEET L- if I-