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JP6418636B2 - Creep characteristic value acquisition method - Google Patents
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JP6418636B2 - Creep characteristic value acquisition method - Google Patents

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JP6418636B2
JP6418636B2 JP2014231947A JP2014231947A JP6418636B2 JP 6418636 B2 JP6418636 B2 JP 6418636B2 JP 2014231947 A JP2014231947 A JP 2014231947A JP 2014231947 A JP2014231947 A JP 2014231947A JP 6418636 B2 JP6418636 B2 JP 6418636B2
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creep
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stress relaxation
stress
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JP2016095241A (en
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吉田 誠
吉田  誠
卓大 明石
卓大 明石
利光 岡根
利光 岡根
雄一 本山
雄一 本山
葉椰 福田
葉椰 福田
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Waseda University
Kimura Foundry Co Ltd
National Institute of Advanced Industrial Science and Technology AIST
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Kimura Foundry Co Ltd
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Description

本発明は、歪速度依存性を考慮したクリープ構成式に用いるクリープ特性値取得方法に関するものである。   The present invention relates to a creep characteristic value acquiring method used in a creep constitutive equation taking strain rate dependency into consideration.

鋳造品など、高温で加工された金属が常温に至る過程で発生する残留応力や変形を予測するため、従来から、解析プログラムにおいて金属の力学挙動を数式上で表現する構成式が用いられてきた。
その際、精度よく残留応力および変形を予測するためには、高温時に生じる歪速度依存性を考慮可能な構成式を用いるべきだと明らかにされている。また、歪速度依存性はクリープ特性の取得によって考慮可能となるものの、従来、その取得には任意の温度で複数回の引張試験、もしくはクリープ試験の実施が必要となるため、試験時間や、試験コスト、試験片本数等がかかる問題があった。
In order to predict residual stress and deformation that occur when a metal processed at high temperature, such as cast products, reaches room temperature, conventionally, a constitutive equation that expresses the mechanical behavior of the metal in mathematical expressions has been used in analysis programs. .
At that time, in order to predict residual stress and deformation with high accuracy, it has been clarified that a constitutive equation that can take into consideration the strain rate dependency occurring at high temperature should be used. Although strain rate dependency can be taken into consideration by acquiring creep characteristics, conventionally, it is necessary to carry out multiple tensile tests or creep tests at any temperature for acquisition, so test time, test, or test There is a problem that the cost, the number of test pieces, and the like are required.

これに対し、近年、様々な合金種で、クリープ特性を迅速に取得する手段として応力緩和法が提案されている。
例えば、横浜国立大学の谷村ら(非特許文献1)の報告や、非特許文献2、さらには特許文献1の例が挙げられる。これらの提案では、応力緩和法でのクリープ特性取得に対する有効性を示していたが、本来、引張試験やクリープ試験で取得されるクリープ特性とは全く異なる値を取得しているおそれがある。
以下に、当該発明に関係する従来の知見の問題点を述べる。
On the other hand, in recent years, a stress relaxation method has been proposed as a means for rapidly acquiring creep characteristics with various alloy types.
For example, a report of Tanimura et al. Of Yokohama National University (Non-Patent Document 1), a non-patent document 2, and an example of Patent Document 1 can be given. In these proposals, although the effectiveness to the creep property acquisition by the stress relaxation method was shown, there is a possibility that the value originally different from the creep property acquired by the tensile test or the creep test may be acquired.
The problems of the conventional findings related to the invention will be described below.

特開2008−209262号公報JP 2008-209262 A

谷村 利伸、于 強、澁谷 忠弘、白鳥 正樹:エレクトロニクス実装学会誌、Vol.10、No.1、2007、Pages 52-61「応力緩和法を用いたはんだの弾塑性・クリープ・粘塑性の物性値取得の効率化」Toshinobu Tanimura, Toshio Tatsuhiro, Tadahiro Tsujitani, Masaki Shiratori: Electronics Packaging Society Journal, Vol. 10, No. 1, 2007, Pages 52-61 “Elasto-plastic / creep / viscoplastic physical properties of solder using stress relaxation method” Acquisition efficiency " 大口 健一、瀧田 敦子、木村 光彦:J.JF、Vol.84、No.10、2012、Pages 569-576「ステンレス鋼鋳鋼の弾・塑性・クリープ特性の効率的評価と熱変形FEM解析」Kenichi Oguchi, Atsuko Shibata, Mitsuhiko Kimura: J. JF, Vol. 84, No. 10, 2012, Pages 569-576 “Efficient Evaluation of Elastic-Plastic-Creep Properties of Stainless Steel Cast Steel and Thermal Deformation FEM Analysis” 阿部勝憲、吉永日出男、諸星正太郎:日本金属学会誌、Vol.4、Issue4、1976、393-399「応力緩和試験による内部応力と摩擦応力の識別」Katsunori Abe, Hideo Yoshinaga, Shotaro Moroshi: Journal of the Metals Society of Japan, Vol. 4, Issue 4, 1976, 393-399 “Determination of internal stress and frictional stress by stress relaxation test”

Figure 0006418636
Figure 0006418636

Figure 0006418636
Figure 0006418636

Figure 0006418636
Figure 0006418636

Figure 0006418636
Figure 0006418636

Figure 0006418636
Figure 0006418636

ここで、変形応力に対し、摩擦応力が無視できない場合は、

Figure 0006418636
Here, when the frictional stress can not be ignored for the deformation stress,
Figure 0006418636

また、変形応力に対し、摩擦応力が無視できる場合は、

Figure 0006418636
となる。 Also, if the frictional stress can be ignored for the deformation stress,
Figure 0006418636
It becomes.

上掲した非特許文献1では、はんだ合金においては、応力緩和法を用いることで、従来の引張試験と比べてクリープ特性取得に要する試験回数を低減させることができると報告している。しかし、応力緩和前後のクリープ歪速度の比較は行っておらず、応力緩和法の成立条件を満たしていないおそれがある。   Non-Patent Document 1 mentioned above reports that, in a solder alloy, by using a stress relaxation method, it is possible to reduce the number of tests required to obtain creep characteristics as compared with a conventional tensile test. However, comparison of creep strain rates before and after stress relaxation is not performed, and there is a possibility that the conditions for establishing the stress relaxation method are not satisfied.

また、非特許文献2や特許文献1は、ステンレス鋼鋳鋼において、谷村ら(非特許文献1)と同様に応力緩和法を用いることで、クリープ特性取得に要する試験回数を低減させることができると報告しているが、応力緩和前後のクリープ歪速度の比較は行っていないため、応力緩和法の成立条件を満たしていないおそれがある。   In Non-Patent Document 2 and Patent Document 1, it is possible to reduce the number of tests required to obtain creep characteristics by using a stress relaxation method in stainless steel cast steel as in Tanimura et al. (Non-Patent Document 1). Although we report it, we do not compare creep strain rates before and after stress relaxation, so it may not meet the conditions for stress relaxation method.

以上述べたように、クリープ特性取得に要する時間やコスト、試験片本数の削減のために様々な合金種で応力緩和法を用いることが提案されているが、金属の変形機構解明を主眼とした研究から、応力緩和法が成立しない場合があることが示されている。
従って、現状、引張試験などのクリープ特性取得方法の代替としての応力緩和法の適応範囲は限定的なものとなっている。
As described above, it has been proposed to use the stress relaxation method with various alloy types in order to reduce the time and cost required for acquiring the creep characteristics and the number of test pieces, but the main objective was to elucidate the deformation mechanism of the metal. Studies have shown that stress relaxation may not hold.
Therefore, the applicable range of the stress relaxation method as a substitute for creep property acquisition methods such as tensile tests is currently limited.

また、現行の応力緩和法を用いたクリープ特性の取得おいては、応力緩和法成立の可不可は考慮されておらずに、応力緩和前後のクリープ歪速度が一致しているとの前提のもとに実施されている。ゆえに、本来、引張試験で得られるクリープ特性とは異なった値を取得している可能性がある。   In addition, in acquisition of creep characteristics using the current stress relaxation method, it is also assumed that creep strain rates before and after stress relaxation match, without considering whether the stress relaxation method is established or not. And has been implemented. Therefore, it may be possible to obtain a value different from the creep property obtained by the tensile test.

さらに、引張試験で得られるクリープ特性とは異なった値を取得している場合における従来試験の代替としてのクリープ特性取得方法についての知見も、同様に存在しないため、その場合に対する新たなクリープ特性の取得方法が必要となる。   Furthermore, since knowledge on a method for acquiring creep characteristics as an alternative to conventional tests in the case where values different from creep characteristics obtained in tensile tests are obtained does not exist either, there is a new creep characteristic for that case. Acquisition method is required.

本発明は、上記の現状に鑑み開発されたもので、歪速度依存性を考慮したクリープ構成式に用いるクリープ特性値:n値およびA値の取得方法であって、現行の応力緩和法が成立しない場合に対しても、現在用いられている応力緩和法と比べ、引張試験やクリープ試験により近い正確性をもってクリープ特性を取得することができるので、上述した種々の問題の解決を図ることができる。   The present invention has been developed in view of the above-mentioned present conditions, and is a method of acquiring creep characteristic values: n value and A value used in creep constitutive equation considering strain rate dependency, and the current stress relaxation method is established. Even in the case of not being used, creep characteristics can be obtained with close accuracy by tensile test and creep test as compared with the stress relaxation method currently used, so that the various problems described above can be solved. .

加えて、本発明では、引張試験やクリープ試験と比べ、現在用いられている応力緩和法の利点である、時間や、コスト、試験片本数の削減などを損なうことなくクリープ特性の取得が行うことができる。   In addition, in the present invention, acquisition of creep characteristics is performed without impairing time, cost, reduction in the number of test pieces, etc., which are advantages of the stress relaxation method currently used compared to tensile tests and creep tests. Can.

Figure 0006418636
Figure 0006418636

本発明を用いれば、従来の引張試験などのクリープ特性取得方法に相当する正確性と、現行の応力緩和法が有する、時間や、コスト、試験片本数の削減効果を併せ持ち、高温で加工された金属が常温に至る過程で発生する残留応力や変形を、より正確にシミュレーションする構成式構築のためのクリープ特性値を得ることが可能になる。   By using the present invention, it is processed at high temperature, which has the accuracy equivalent to the conventional creep property acquisition method such as tensile test and the reduction effect of time, cost and the number of test specimens that the current stress relaxation method has. It is possible to obtain a creep characteristic value for constructing a constitutive equation that simulates more accurately the residual stress and deformation generated when the metal reaches the normal temperature.

応力緩和試験の概要図である。なお、(a)は、歪-時間の関係を示し、(b)は、応力-時間の関係を示す。It is a schematic diagram of a stress relaxation test. Note that (a) shows the strain-time relationship, and (b) shows the stress-time relationship. 応力緩和法が成立しない場合における応力緩和試験で得られるクリープ歪速度と応力の関係の概念図である。It is a conceptual diagram of the relationship between the creep strain rate and stress which are obtained by the stress relaxation test when the stress relaxation method does not hold. 引張試験と応力緩和試験の結果における、クリープ歪速度と応力の関係を示したグラフである。It is the graph which showed the relationship between creep strain rate and stress in the result of a tension test and a stress relaxation test.

以下、本発明を具体的に説明する。
応力緩和試験は、図1に示したように、引張、歪保持の各ステージから成り、引張時から応力緩和直前の歪速度を測定する。さらに、歪保持部分から応力緩和速度とヤング率によって応力緩和直後を含む応力緩和中のクリープ歪速度を求める。
Hereinafter, the present invention will be specifically described.
The stress relaxation test, as shown in FIG. 1, comprises stages of tension and strain holding, and measures the strain rate immediately before stress relaxation from the time of tension. Furthermore, the creep strain rate during stress relaxation including immediately after stress relaxation is determined from the strain holding portion by stress relaxation rate and Young's modulus.

ここで、サンディア国立研究所のR.W.Rohdeらの非特許文献4は、応力緩和試験での応力緩和中とクリープ試験中の変形機構は同一であるとしている。
非特許文献4では、クリープ特性値のうちn値は金属の変形機構の判断基準として広く用いられている。したがって、応力緩和中とクリープ試験中の変形機構が同一である以上、応力緩和法とクリープ試験や引張試験といった従来試験で取得されるn値は、いずれも同一であることを示している。
Here, Non-Patent Document 4 of RWRohde et al. Of Sandia National Laboratory, assumes that the deformation mechanism is the same during stress relaxation in the stress relaxation test and in the creep test.
In Non-Patent Document 4, n value among creep characteristic values is widely used as a judgment standard of the deformation mechanism of metal. Therefore, as long as the deformation mechanism is the same during stress relaxation and during the creep test, it is indicated that the n values obtained in the conventional tests such as the stress relaxation method and the creep test and the tensile test are the same.

R.W.Rohde、J.C.Swearengen:ASTM、1979、Pages 21-35「Metal Deformation Modeling-Stress Relaxation of Aluminum」R. W. Rohde, J. C. Swearengen: ASTM, 1979, Pages 21-35 "Metal Deformation Modeling-Stress Relaxation of Aluminum"

また、図2は、現行の応力緩和試験から得られるクリープ歪速度と応力の関係を示す図である。
被測定物の引張時に、歪速度と定常応力の関係を1点取得することができるが、応力緩和直前と直後のクリープ歪速度の不一致に起因する、応力緩和曲線から得られる傾きnの直線とギャップが生じる。
FIG. 2 is a view showing the relationship between the creep strain rate and the stress obtained from the current stress relaxation test.
The relationship between strain rate and steady state stress can be acquired at one point when the object to be measured is tensioned, but with a straight line of slope n obtained from the stress relaxation curve due to the mismatch of creep strain rate immediately before and after stress relaxation There is a gap.

Figure 0006418636
Figure 0006418636

以下、本発明のクリープ特性取得方法の手順を説明する。
まず、被対象物たる金属(合金)を、試験片として鋳造し、引張試験片形状に加工する。この形状は、特に限定されないが、JIS Z 2201の4号試験片が好ましい。
Hereinafter, the procedure of the creep characteristic acquisition method of the present invention will be described.
First, a metal (alloy) which is a target object is cast as a test piece and processed into a tensile test piece shape. This shape is not particularly limited, but JIS Z 2201 No. 4 test piece is preferable.

試験温度は、応力緩和法は定常クリープ則であるNorton則で表現できる定常クリープ状態での実施を想定しているため、一般的に定常クリープが支配的になる温度を考慮して、融点をTmとすると0.4Tm〜Tmの間で選定すれば良い。例えば、アルミニウムダイカスト合金であるJIS ADC12であれば、300℃から450℃程度の範囲である。
応力緩和試験を実施する歪速度は、取得目的のクリープ特性における歪速度の範囲に依り、その範囲以上の歪速度を選定すれば良い。
Since the test temperature assumes implementation in a steady state creep condition that can be expressed by the stress relaxation method and a steady state creep law, the Norton Law, the melting point is generally Tm considering the temperature at which the steady state creep becomes dominant. Then, it may be selected between 0.4Tm and Tm. For example, if it is JIS ADC12 which is an aluminum die-cast alloy, it is the range of about 300 degreeC to 450 degreeC.
The strain rate at which the stress relaxation test is performed depends on the range of strain rates in the creep characteristics for acquisition, and the strain rate above that range may be selected.

応力緩和の開始歪量は、定常応力状態に達する歪量の範囲で選定すれば良い。例えば、上記JIS ADC12であれば、4.0%がその範囲内である。   The starting strain amount of stress relaxation may be selected in the range of the strain amount reaching the steady state stress state. For example, if it is said JIS ADC12, 4.0% is in the range.

次に、上記の試験からクリープ特性値:n値とA値を取得する手順を記載する。
まず、n値は、前掲非特許文献4から、現行の応力緩和法のn値の求め方に依ることができる。本発明においても、n値は、金属の変形機構に依存するものだからである。
Next, the procedure for acquiring the creep characteristic value: n value and A value from the above test will be described.
First, the n value can be determined by the method of obtaining the n value of the current stress relaxation method from Non-Patent Document 4 mentioned above. Also in the present invention, the n value depends on the deformation mechanism of the metal.

Figure 0006418636
Figure 0006418636

そして、本発明では、上記クリープ特性値:n値とA値を利用して以下の式(2)から被対象物の任意の温度におけるクリープ特性を求めることができる。

Figure 0006418636
And in this invention, the creep characteristic in the arbitrary temperature of a target object can be calculated | required from the following formula (2) using the said creep characteristic value: n value and A value.
Figure 0006418636

本発明が、応力緩和法を用いたクリープ特性よりも、従来試験により近いクリープ特性を従来試験より少ない試験回数で取得することが可能なことを以下に実施例として示す。   It will be shown below as an example that the present invention can obtain creep characteristics closer to the conventional test with less number of tests than the conventional test than the creep characteristics using the stress relaxation method.

まず、代表的なアルミニウムダイカスト合金であるJIS ADC12を対象として、従来試験である引張試験と応力緩和試験でクリープ特性の取得を行った。
試験片は、JIS ADC12を銅舟型で鋳造し、引張試験片形状に加工した。
引張試験では、試験温度をJIS ADC12において定常クリープが支配的になる温度である300℃と450℃に設定した。
歪速度は1.0×10-2から1.0×10-5/sの範囲におけるクリープ特性の取得を目的としたため、1.0×10-2/s、1.0×10-4/sおよび1.0×10-5/sに設定した。
応力緩和試験では、同じ試験温度で、試験実施の容易さから歪速度を1.0×10-3/sとし、与える歪量が定常応力状態にある4.0%に達した後、歪を保持し、試験片の応力を緩和させた。
First, creep characteristics were acquired by a tensile test and a stress relaxation test, which are conventional tests, targeting JIS ADC12 which is a typical aluminum die-cast alloy.
The test piece was manufactured by casting JIS ADC 12 with a copper rod shape and processing it into a tensile test piece shape.
In the tensile test, the test temperature was set to 300 ° C. and 450 ° C. at which steady-state creep becomes dominant in JIS ADC12.
Since strain rate for the purpose of acquisition of creep characteristics in a range from 1.0 × 10 -2 of 1.0 × 10 -5 / s, 1.0 × 10 -2 /s,1.0×10 -4 / s and 1.0 × 10 -5 / Set to s.
In the stress relaxation test, at the same test temperature, the strain rate is set to 1.0 × 10 -3 / s from the ease of test implementation, and after the amount of applied strain reaches 4.0% in the steady state stress, the strain is maintained and the test The stress of the piece was relaxed.

本応力緩和試験における、応力緩和直前と直後の歪速度を表1に示す。   The strain rates immediately before and after stress relaxation in this stress relaxation test are shown in Table 1.

Figure 0006418636
Figure 0006418636

表1からJIS ADC12において、上述した試験条件では、応力緩和前後の歪速度が一致しないため、従来の応力緩和法が成立しないと判断することができる。
実際に、それぞれの試験のクリープ歪速度と応力の関係を取得した結果である図3を見ると、引張試験と応力緩和試験で得られたクリープ歪速度と応力の関係を表す直線にはギャップが生じている。
そのため、A値とn値を比較した表2から分かるように、n値は誤差10%程度の範囲内で一致しているが、A値は誤差60〜90%程度の誤差となっている。
In Table 1 to JIS ADC 12, the strain rates before and after stress relaxation do not match under the test conditions described above, so it can be judged that the conventional stress relaxation method does not hold.
Actually, looking at FIG. 3 which is the result of acquiring the relationship between the creep strain rate and the stress of each test, it is clear that the gap is a straight line representing the relationship between the creep strain rate and the stress obtained by the tensile test and the stress relaxation test. It is happening.
Therefore, as can be seen from Table 2 in which the A value and the n value are compared, the n value agrees within about a 10% error, but the A value is an about 60 to 90% error.

Figure 0006418636
Figure 0006418636

次に、上記の試験で取得した応力緩和直前のクリープ歪速度とn値を利用して前掲式(1)から取得したクリープ特性を表3に示す。   Next, Table 3 shows creep characteristics obtained from the above equation (1) using the creep strain rate immediately before the stress relaxation obtained in the above test and the n value.

Figure 0006418636
Figure 0006418636

同表より、従来の応力緩和法を用いるよりも、本発明に従うことで、引張試験で得られるクリープ特性に近い値の取得ができていることが分かる。   From the table, it can be seen that, according to the present invention, it is possible to obtain a value close to the creep characteristics obtained in the tensile test, rather than using the conventional stress relaxation method.

実際に、従来の応力緩和法と本発明で取得したクリープ特性を用いて構築した次の式(2)に示すNorton則によって、[0035]で実施した高温引張試験で得られた定常応力とその計算値の比較を表4および5に示す。

Figure 0006418636
In fact, the steady stress obtained by the high temperature tensile test carried out in [0035] and its stress according to the Norton law shown in the following equation (2) constructed using the conventional stress relaxation method and the creep characteristics obtained in the present invention Comparisons of calculated values are shown in Tables 4 and 5.
Figure 0006418636

Figure 0006418636
Figure 0006418636

Figure 0006418636
表4および5から、現行の応力緩和法による計算値よりも、本発明によって構築された構成式を用いた計算値の方が、より精度よく引張試験で得られる定常応力を予測できていることが分かる。
Figure 0006418636
From Tables 4 and 5, it is possible to predict the steady-state stress obtained in the tensile test more accurately by the calculated value using the constitutive equation constructed according to the present invention than the calculated value by the current stress relaxation method I understand.

また、本実施例で、従来行われてきた試験方法では、任意の温度におけるクリープ特性取得に、試験片本数が4本、試験時間が約2000秒必要であったのに対し、本発明では、クリープ特性取得に対して試験片本数が1本、試験時間が約1000秒で済み、クリープ特性取得に要する時間や、コスト、試験片本数などを削減することが可能となったことを併せて確認している。   Further, in the present embodiment, in the test method conventionally conducted, although the number of test pieces required is four and the test time is about 2000 seconds to obtain the creep characteristics at an arbitrary temperature, The number of test pieces was only one for creep property acquisition and the test time was about 1000 seconds, and it was confirmed that it was possible to reduce the time required for creep property acquisition, cost, the number of test pieces, etc. doing.

本発明を用いることで、鋳造および熱間塑性加工を行う際に発生する熱応力や、残留応力、変形の予測などを、より簡便かつ正確に行うことができるので、試験時間や、試験コスト、試験片本数などに係る問題が解消することが可能となる。   By using the present invention, it is possible to more simply and accurately predict thermal stress, residual stress, deformation, etc. generated when performing casting and hot plastic working, so that test time, test cost, It becomes possible to solve the problem concerning the number of test pieces etc.

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Figure 0006418636
Figure 0006418636
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