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JPS6025120B2 - sugar manufacturing method - Google Patents
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JPS6025120B2 - sugar manufacturing method - Google Patents

sugar manufacturing method

Info

Publication number
JPS6025120B2
JPS6025120B2 JP14514681A JP14514681A JPS6025120B2 JP S6025120 B2 JPS6025120 B2 JP S6025120B2 JP 14514681 A JP14514681 A JP 14514681A JP 14514681 A JP14514681 A JP 14514681A JP S6025120 B2 JPS6025120 B2 JP S6025120B2
Authority
JP
Japan
Prior art keywords
sugar
concentration
acid
fatty acid
product
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP14514681A
Other languages
Japanese (ja)
Other versions
JPS5847500A (en
Inventor
義之 大山
凱生 松尾
博明 西
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Riken Vitamin Co Ltd
Original Assignee
Riken Vitamin Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Riken Vitamin Co Ltd filed Critical Riken Vitamin Co Ltd
Priority to JP14514681A priority Critical patent/JPS6025120B2/en
Publication of JPS5847500A publication Critical patent/JPS5847500A/en
Publication of JPS6025120B2 publication Critical patent/JPS6025120B2/en
Expired legal-status Critical Current

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  • Fats And Perfumes (AREA)
  • Saccharide Compounds (AREA)

Description

【発明の詳細な説明】 本発明は砂糖の製造法に関する。[Detailed description of the invention] The present invention relates to a method for producing sugar.

さらに詳しくは結晶缶を使用しない砂糖の製造方法にお
いて、グリセリンモノおよび脂肪酸ェステル、ポリグリ
セリン脂肪酸ェステル、から選ばれた1種または2種を
濃縮仕上工程の糖液に添加することを特徴とする砂糖の
製造法に関する。ビート糖工場、さとうきび原料糖工場
、さとうきび黒糖工場、再生黒糖工場、精製糖工場、ぶ
どう糖工場、水飴工場、異性化糖工場などでは糖液の精
製、濃縮、結晶化などの工程がある。
More specifically, there is a method for producing sugar that does not use a crystal can, characterized by adding one or two selected from monoglycerin, fatty acid ester, and polyglycerin fatty acid ester to the sugar solution in the concentration finishing step. Concerning the manufacturing method. Beet sugar factories, raw sugar cane sugar factories, cane brown sugar factories, recycled brown sugar factories, refined sugar factories, glucose factories, starch syrup factories, high-fructose sugar factories, etc. carry out processes such as refining, concentrating, and crystallizing sugar solutions.

糠類の製造工場において水分の蒸発濃縮は製品原単位を
左右する大きな要素である。本発明は結晶缶を使用しな
い砂糖の製造法である。
In rice bran manufacturing plants, evaporation and concentration of water is a major factor that affects the product consumption rate. The present invention is a method for producing sugar without using crystal cans.

通常の砂糖の製造法では糖液を予め予備濃縮した後結晶
缶に入れ減圧下50〜7000の温度でBx90〜難に
濃縮し、次いで助晶機に入れ結晶化を促進した後遠心分
離により結晶と蜜とを分離する。本発明では結晶缶を使
用せず、常圧下、仕上缶で100〜130oCでBx9
0〜95に濃縮後、助晶機に入れ結晶化を促進してその
ま)粉糖として得るか、遠心分離で分蜜する。この仕上
缶は加熱蒸気を使用しており、大気圧下短時間に糖液を
高濃度に濃縮することにある。
In the usual sugar production method, the sugar solution is preconcentrated in advance, then put in a crystallizer and concentrated under reduced pressure at a temperature of 50 to 7,000 to Bx90 or more, then put in a crystallizer to promote crystallization, and then crystallized by centrifugation. and honey are separated. In the present invention, without using a crystal can, Bx9 is produced at 100 to 130 oC in a finishing can under normal pressure.
After concentrating to a concentration of 0 to 95%, it is placed in a crystallizer to promote crystallization and either obtained directly as powdered sugar or separated by centrifugation. This finishing can uses heated steam to concentrate the sugar solution to a high concentration in a short time under atmospheric pressure.

しかし大気圧下であるため糖液の濃縮温度は100〜1
30ooとなり、発泡を生ずると共に砂糖分解、還元糖
分解(pH低下)、粘度増加などを派生する極めて過酷
な条件である。またこれらの条件下で得られる糠液の品
質が低下し還元糖などの不純物の生成量が増加し、二次
工程における糠液の冷却結晶化を阻害し、ダマの多い結
晶粒蓬不揃いで、ねばりや水分の多い製品糖が得られる
。また助晶後型入れしてブロックにする場合、硬度、光
沢、色価などが劣る製品糖となる。さらに糖液劣化によ
る粘度の増加は、これらの糖液が前処理工程で可成り多
量のカルシウムを残存含有するため、仕上缶のスケール
原因となり伝熱速度を低下せしめ、濃縮時間の延長、製
品劣化など悪循環を重ねる原因となる。
However, since it is under atmospheric pressure, the concentration temperature of the sugar solution is 100 to 1
30oo, which is an extremely harsh condition that causes foaming, sugar decomposition, reducing sugar decomposition (decrease in pH), and increase in viscosity. In addition, the quality of the bran obtained under these conditions deteriorates and the amount of impurities such as reducing sugars increases, which inhibits the cooling crystallization of the bran in the secondary process, resulting in lumpy and irregular grains. A sticky and watery product sugar is obtained. In addition, when the sugar is molded into blocks after auxiliary crystallization, the resulting sugar product is inferior in hardness, luster, and color value. Furthermore, the increase in viscosity due to deterioration of sugar solutions is caused by the fact that these sugar solutions contain a considerable amount of calcium remaining in the pretreatment process, which causes scaling in the finishing can and reduces the heat transfer rate, prolonging the concentration time and causing product deterioration. This causes a vicious cycle to continue.

これらの問題を解決するために、従釆消泡の目的でなた
ね油、大豆油などが使用されているが、消泡については
効果が弱く持続性に乏しく、濃縮時間の短縮や粘個性で
あるなど製品品質の向上には寄与していない。
In order to solve these problems, rapeseed oil, soybean oil, etc. are used for the purpose of defoaming, but the antifoaming effect is weak and long-lasting, and the concentration time is shortened and the oil is sticky. It does not contribute to improving product quality.

また消泡剤の添加量も1000〜200功血と比較的多
量である。
Further, the amount of antifoaming agent added is relatively large, ranging from 1000 to 200%.

本発明は前記の諸問題を解決することを目的とし種々検
討した結果、効用缶工程または仕上缶工程において、グ
リセリンモノおよび脂肪酸ェステル、ポリグリセリン脂
肪酸ェステル、より選ばれた1種または2種を糖液に添
加することにより、濃縮仕上工程における糖液の発泡や
砧鋼‘性の問題を解決すると共に濃縮時間短縮、脱スケ
ール効果を促進し、その結果製品糖はダマの生成を著し
く減少し、ね‘よりのない製品水分の少ない均一な砂糖
結晶を得ることができることを見出し、また型入れして
ブロックの砂糖を得る場合は硬度、色価、光沢などの製
品品質を著しく改善できることを見出して本発明を完成
したものである。
The present invention aims to solve the above-mentioned problems and as a result of various studies, it has been found that one or two selected from glycerin mono, fatty acid ester, polyglycerin fatty acid ester, etc. By adding it to the sugar solution, it solves the problems of foaming and slaginess of the sugar solution during the concentration finishing process, shortens the concentration time, promotes the descaling effect, and as a result, the product sugar significantly reduces the formation of lumps. They found that it is possible to obtain uniform sugar crystals with low product moisture without stirring, and that when molding is used to obtain block sugar, product qualities such as hardness, color value, and gloss can be significantly improved. This completes the present invention.

本発明でのグリセリンモノおよび脂肪酸ヱステル、ポリ
グリセリン脂肪酸ェステルに使用する脂肪酸は炭素数8
乃至22のものが適宜用いることができるが、具体的に
はカプリル酸、カプリン酸、ラゥリン酸、ミリスチン酸
、パルミチン酸、ステアリン酸、アラキン酸、べへン酸
などの飽和脂肪酸、リンデル酸、オレィン酸、リノール
酸、リシルン酸、アラキドン酸、ェルカ酸などの不飽和
脂肪酸などの単一脂肪酸および混合脂肪酸およびヤシ油
、パーム油、大豆油、綿実油、ナタネ油、牛脂、ラード
、鶏脂、魚脂及びこれらの硬化油よりの混合脂肪酸を用
いることができる。
The fatty acids used in the glycerin mono- and fatty acid esters and polyglycerin fatty acid esters of the present invention have 8 carbon atoms.
22 can be used as appropriate, specifically saturated fatty acids such as caprylic acid, capric acid, lauric acid, myristic acid, palmitic acid, stearic acid, arachidic acid, and behenic acid, Linderic acid, and oleic acid. acids, single and mixed fatty acids such as unsaturated fatty acids such as linoleic acid, lysylonic acid, arachidonic acid, erucic acid, and coconut oil, palm oil, soybean oil, cottonseed oil, rapeseed oil, beef tallow, lard, chicken fat, fish fat and mixed fatty acids from these hydrogenated oils can be used.

本発明でいうポリグリセリン脂肪酸ェステルとはグリセ
リンの重合度2〜10のものが好ましく、脂肪酸とのェ
ステル化率は高い方が好ましいが、少なくとも1ケの遊
離の水酸基がある方が良い。
The polyglycerin fatty acid ester referred to in the present invention preferably has a degree of glycerin polymerization of 2 to 10, and the higher the esterification rate with the fatty acid, the better, but it is better to have at least one free hydroxyl group.

本発明に使用するグリセリンモノおよび脂肪酸ェステル
、ポリグリセリン脂肪酸ェステルの糠液への添加量は0
.001〜0.1%で好ましい効果を示す。0.001
%以下では期待される効果を示さず、0.1%以上の添
加は効果の点と経済的な面で必要としない。
The amount of glycerin mono- and fatty acid esters and polyglycerin fatty acid esters used in the present invention added to the bran liquid is 0.
.. A preferable effect is shown at 0.001 to 0.1%. 0.001
% or less will not show the expected effect, and addition of 0.1% or more is not necessary from the viewpoint of effectiveness and economy.

添加時間は通常濃縮仕上缶の供聯合糖液に加熱開始前に
添加するのが好ましいが、あらかじめ効用缶(多重効用
缶を含む)糖液に添加してお仇よ効用缶での糖液濃縮時
の発泡を抑制し、濃縮効率を向上するとともに、仕上濃
縮でも効果が持続し目的とする良質な砂糖が得られる。
以下実施例で本発明を説明する。実施例 1 槌糖200夕、洗糖蜜206夕、水632からなる純糖
率86の糟液に下記の各試料を添加し、常圧の濃縮装置
にて品温130qo以下でBx90〜95まで濃縮し、
110〜105qoまで櫨梓冷却後型入れをした。
Regarding the addition time, it is usually preferable to add it to the combined sugar solution in the concentrated finish can before heating starts, but it is preferable to add it to the sugar solution in the can (including multi-effect can) in advance and then concentrate the sugar solution in the can. It suppresses foaming during the process, improves concentration efficiency, and maintains its effect even during final concentration, allowing the desired high-quality sugar to be obtained.
The present invention will be explained below with reference to Examples. Example 1 Each of the following samples was added to a solution with a purity rate of 86, consisting of 200 g of mallet sugar, 206 g of washed molasses, and 632 g of water, and concentrated to Bx 90 to 95 at a temperature of 130 qo or less using a normal pressure concentrator. death,
After cooling to 110 to 105 qo, molding was carried out.

その結果は表に示した。測定値はくり返し10回の平均
値 ※ 濃縮時間は品温100℃から130℃迄の所要時間
※※ 製品品質の評価は管能的に行った。
The results are shown in the table. The measured value is the average value of 10 repeated measurements.* Concentration time is the time required for the product temperature to rise from 100°C to 130°C.* Product quality was evaluated visually.

以下の実施例でも同様◎:非常に良好 ○:普通 △:
劣る ×:非常K劣るこの結果、比較例のなたね油と比
べて、本発明は製品品質は勿論のこと、消泡性、濃縮時
間、結晶化温度で極めて良好な結果を得た。実施例 2 純糖率86.5の糖液に下記試料を添加し、常圧の仕上
缶にて取付温度130午0で濃縮し黒糖を得た。
The same applies to the following examples ◎: Very good ○: Fair △:
Inferior ×: Extremely inferior K As a result, compared to the rapeseed oil of the comparative example, the present invention obtained extremely good results not only in product quality but also in antifoaming properties, concentration time, and crystallization temperature. Example 2 The following sample was added to a sugar solution with a purity rate of 86.5 and concentrated in a finishing can at normal pressure at an installation temperature of 130 pm to obtain brown sugar.

この結果は表に示した。両工場とも試験は30回行った
時の平均値この結果B上場では本発明で優れた黒糖製品
が得られた。
The results are shown in the table. The test was carried out 30 times at both factories, and the average value was obtained.As a result, in B Listing, an excellent brown sugar product was obtained using the present invention.

実施例 3 純糖率81.2の糠液に下記試料を添加し、常圧の仕上
缶にて取付温度130qoで濃縮し、次いで助晶機に入
れ結晶化させ再生黒糖を得た。
Example 3 The following sample was added to a bran liquid with a pure sugar ratio of 81.2, concentrated in a finishing can under normal pressure at an installation temperature of 130 qo, and then placed in a crystallizer for crystallization to obtain regenerated brown sugar.

Claims (1)

【特許請求の範囲】[Claims] 1 結晶缶を使用しない砂糖の製造方法において、グリ
セリンモノおよび樹脂酸エステル、ポリグリセリン脂肪
酸エステルから選ばれた1種または2種を濃縮仕上工程
の糖液に添加することを特徴とする砂糖の製造法。
1. A sugar production method that does not use a crystal can, characterized by adding one or two selected from glycerin mono, resin acid esters, and polyglycerin fatty acid esters to the sugar solution in the concentration finishing step. Law.
JP14514681A 1981-09-14 1981-09-14 sugar manufacturing method Expired JPS6025120B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP14514681A JPS6025120B2 (en) 1981-09-14 1981-09-14 sugar manufacturing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP14514681A JPS6025120B2 (en) 1981-09-14 1981-09-14 sugar manufacturing method

Publications (2)

Publication Number Publication Date
JPS5847500A JPS5847500A (en) 1983-03-19
JPS6025120B2 true JPS6025120B2 (en) 1985-06-17

Family

ID=15378477

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14514681A Expired JPS6025120B2 (en) 1981-09-14 1981-09-14 sugar manufacturing method

Country Status (1)

Country Link
JP (1) JPS6025120B2 (en)

Also Published As

Publication number Publication date
JPS5847500A (en) 1983-03-19

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