JPS6344800B2 - - Google Patents
Info
- Publication number
- JPS6344800B2 JPS6344800B2 JP1912584A JP1912584A JPS6344800B2 JP S6344800 B2 JPS6344800 B2 JP S6344800B2 JP 1912584 A JP1912584 A JP 1912584A JP 1912584 A JP1912584 A JP 1912584A JP S6344800 B2 JPS6344800 B2 JP S6344800B2
- Authority
- JP
- Japan
- Prior art keywords
- plants
- volatile components
- temperature
- room
- fresh
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 241000196324 Embryophyta Species 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 150000001299 aldehydes Chemical class 0.000 description 4
- 150000003505 terpenes Chemical class 0.000 description 4
- 235000007586 terpenes Nutrition 0.000 description 4
- 238000007791 dehumidification Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000003287 bathing Methods 0.000 description 2
- FUWUEFKEXZQKKA-UHFFFAOYSA-N beta-thujaplicin Chemical compound CC(C)C=1C=CC=C(O)C(=O)C=1 FUWUEFKEXZQKKA-UHFFFAOYSA-N 0.000 description 2
- 229930002875 chlorophyll Natural products 0.000 description 2
- 235000019804 chlorophyll Nutrition 0.000 description 2
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 description 1
- BQACOLQNOUYJCE-FYZZASKESA-N Abietic acid Natural products CC(C)C1=CC2=CC[C@]3(C)[C@](C)(CCC[C@@]3(C)C(=O)O)[C@H]2CC1 BQACOLQNOUYJCE-FYZZASKESA-N 0.000 description 1
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 241000269817 Centrarchidae Species 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241000209504 Poaceae Species 0.000 description 1
- 241000219492 Quercus Species 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- TUFYVOCKVJOUIR-UHFFFAOYSA-N alpha-Thujaplicin Natural products CC(C)C=1C=CC=CC(=O)C=1O TUFYVOCKVJOUIR-UHFFFAOYSA-N 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 235000019477 peppermint oil Nutrition 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 229930007845 β-thujaplicin Natural products 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Description
【発明の詳細な説明】
新鮮な植物には蛋白質、炭水化物、ビタミン、
クロロフイルのほか、精油に包含される揮発成分
を多数含んでいる。これらの物質は熱の作用で変
質するものが多いため効果的な利用をはかる上か
ら、できだけ自然に近い状態で捕集することが望
まれている。[Detailed Description of the Invention] Fresh plants contain proteins, carbohydrates, vitamins,
In addition to chlorophyll, it contains many other volatile components found in essential oils. Since many of these substances change in quality due to the action of heat, it is desirable to collect them in conditions as close to their natural state as possible in order to use them effectively.
本発明は新鮮な植物に含有する揮発成分をでき
る限り変質させずに簡易な方法で捕集することを
目的とする。 The object of the present invention is to collect volatile components contained in fresh plants using a simple method without deteriorating their quality as much as possible.
従来、新鮮な葉に高温の水蒸気を吹きこみ、葉
に含有する精油を水蒸気と共に留出する方法が水
蒸気蒸留法として知られており、現在でもハツカ
油やヒノキチオールの捕集に利用されている。し
かし、この方法では試料が常に水の沸点近くの温
度に保持されるため、アルデヒドのような反応活
性の高いものは熱変性をうけやすく、また、不揮
発成分でもビタミンCのような熱に弱い物質は破
壊されるため、留出液、残渣とも利用価値がそれ
だけ減少するのが実情である。 Conventionally, the method of blowing high-temperature steam into fresh leaves and distilling the essential oil contained in the leaves along with the steam is known as steam distillation, and is still used today to collect peppermint oil and hinokitiol. However, in this method, the sample is always kept at a temperature close to the boiling point of water, so substances with high reaction activity such as aldehydes are easily denatured by heat, and even non-volatile components are susceptible to heat-sensitive substances such as vitamin C. The reality is that the utility value of both the distillate and the residue decreases accordingly.
本発明は以上のような実情に鑑みてなされたも
のであり、その特徴とすることろは新鮮な植物を
外部から水蒸気を供給することなく、中温高湿下
に保持して、揮発成分を冷却して捕集するもので
ある。使用する植物は新鮮なものであることが望
ましく、草、潅木樹木など、いずれにも適用でき
る効率的な捕集をはかる意味から、試料の植物は
圧砕、切削などにより細胞を破壊し、できるだけ
表面積を大きくする。これらの処理をした植物試
料を密閉した室内に入れる。入れる量はその室内
容積の8割程度とする。ついで、室内の温度を30
〜50℃に保ち、内部の空気を撹拌する。試料から
はアルコール、アルデヒド、テルペンの他に水も
揮発し、室内の湿度は100%近くにまで達する。
湿度が90%を越えた時点で室内の空気を少しずつ
冷却し、屋外に取出す。アルコール、アルデヒ
ド、テルペンなどの溶解した水溶液が得られる。
室内の試料が次第に乾燥し、その含水率が通常の
大気中の湿度と平衡する15%前後になつたところ
で捕集を終了する。断熱材で周囲を囲い、内部に
低温除湿セツトを入れた内容積96.5m3の部屋で厚
さ3cm×長さ1.8m×幅30cmのミズナラの挽き板
を20パレツト、マンボウを間にはさんで積み重ね
る。ついで、内部の温度が30℃になるようヒータ
ーで加温し、内部の空気をフアンで撹拌する。三
日後には内部の湿度が90%に達したのでトラツプ
で凝縮しつつ、1日に20c.c.の水を捕集した。この
ようにして30日間放置し、板が乾燥したところで
捕集を終了した。全捕集液量は600であつた。 The present invention was made in view of the above circumstances, and its characteristics are that fresh plants are kept at medium temperature and high humidity without supplying water vapor from the outside, and volatile components are cooled. It is collected by It is desirable that the plants used be fresh, and in order to achieve efficient collection that can be applied to grasses, shrubs, trees, etc., the sample plants should be crushed, cut, etc. to destroy their cells and reduce the surface area as much as possible. Make it bigger. Place the treated plant samples in a sealed room. The amount to be filled should be about 80% of the indoor volume. Then, reduce the temperature in the room to 30
Keep at ~50℃ and stir the air inside. In addition to alcohol, aldehydes, and terpenes, water also evaporates from the sample, and the humidity in the room reaches nearly 100%.
When the humidity exceeds 90%, the indoor air is cooled little by little and taken outside. An aqueous solution containing dissolved alcohols, aldehydes, terpenes, etc. is obtained.
The sample in the room gradually dries, and collection ends when its moisture content reaches around 15%, which is in equilibrium with normal atmospheric humidity. In a room with an internal volume of 96.5m3 , surrounded by insulation and containing a low-temperature dehumidification set, 20 pallets of sawn Quercus oak boards measuring 3cm thick x 1.8m long x 30cm wide were sandwiched between sunfish. Stack. Next, the inside temperature is heated to 30℃ using a heater, and the air inside is stirred with a fan. Three days later, the internal humidity reached 90%, so the trap condensed and collected 20 c.c. of water per day. This was left for 30 days, and the collection was completed when the board was dry. The total amount of collected liquid was 600.
なお、上記低温除湿セツトについては上述のも
ののほか、除湿乾燥機、ソーラー乾燥機を使用し
てもよい。 In addition to the above-mentioned low-temperature dehumidification set, a dehumidification dryer or a solar dryer may also be used.
本方法は植物自身のもつ多量の水分を利用して
アルデヒド、テルペンなどの揮発成分を緩和な条
件で捕集するものである。捕集の過程では高熱に
保持しないために熱分解による損失がなく残渣の
乾燥物も含めて効果的な利用がはかれる。例え
ば、新鮮な植物として針葉樹の鋸挽きした板や葉
を用いた場合、アルプアーピネンやアビエチン酸
のようなテルペンを含む水溶液が得られる。この
液は山中の森林浴で味わうものとほぼ同じ成分を
含んでおり、家庭で居室や浴槽、サウナに散布し
て使えば森林浴の雰囲気にひたることができ、健
康の保持に役立つ。残留物である乾燥した葉はビ
タミンやクロロフイルに富むので栄養強化物とし
て飼料に混入できる。本法は植物のもつ生理活性
物質をほとんど損うことなく安価に捕集して有効
に利用できるという経済性のすぐれた方法であ
る。 This method uses the large amount of water contained in plants to collect volatile components such as aldehydes and terpenes under mild conditions. During the collection process, the material is not kept at high temperatures, so there is no loss due to thermal decomposition, and the dried residue can be effectively utilized. For example, if sawn boards or leaves of coniferous trees are used as fresh plants, an aqueous solution containing terpenes such as alpinene and abietic acid can be obtained. This liquid contains almost the same ingredients as those enjoyed during forest bathing in the mountains, and by spraying it in your room, bathtub, or sauna at home, you can immerse yourself in the atmosphere of forest bathing and help maintain your health. The remaining dried leaves are rich in vitamins and chlorophyll and can be added to feed as a nutritional fortifier. This method is an economical method that allows the physiologically active substances of plants to be collected at low cost and effectively utilized with almost no damage.
Claims (1)
関係湿度が90〜100%の中温高湿下に放置し、揮
発する成分を冷却しつつ収集することを特徴とす
る植物の揮発成分の捕集法。1 Fresh plant leaves, stems, and trunks at a temperature of 30 to 50℃.
A method for collecting volatile components of plants, which is characterized by leaving the plants under a medium temperature and high humidity environment with relative humidity of 90 to 100%, and collecting volatile components while cooling them.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1912584A JPS60161929A (en) | 1984-02-02 | 1984-02-02 | Collection of volatile component of plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1912584A JPS60161929A (en) | 1984-02-02 | 1984-02-02 | Collection of volatile component of plant |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60161929A JPS60161929A (en) | 1985-08-23 |
| JPS6344800B2 true JPS6344800B2 (en) | 1988-09-06 |
Family
ID=11990738
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1912584A Granted JPS60161929A (en) | 1984-02-02 | 1984-02-02 | Collection of volatile component of plant |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60161929A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0251100U (en) * | 1988-10-04 | 1990-04-10 |
-
1984
- 1984-02-02 JP JP1912584A patent/JPS60161929A/en active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0251100U (en) * | 1988-10-04 | 1990-04-10 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60161929A (en) | 1985-08-23 |
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