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JPH035481B2 - - Google Patents
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JPH035481B2 - - Google Patents

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Publication number
JPH035481B2
JPH035481B2 JP15110783A JP15110783A JPH035481B2 JP H035481 B2 JPH035481 B2 JP H035481B2 JP 15110783 A JP15110783 A JP 15110783A JP 15110783 A JP15110783 A JP 15110783A JP H035481 B2 JPH035481 B2 JP H035481B2
Authority
JP
Japan
Prior art keywords
liquid
steam
funnel
container
shaped cylinder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP15110783A
Other languages
Japanese (ja)
Other versions
JPS6044702A (en
Inventor
Yoshio Iwamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shinryo Air Conditioning Co Ltd
Original Assignee
Shinryo Air Conditioning Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shinryo Air Conditioning Co Ltd filed Critical Shinryo Air Conditioning Co Ltd
Priority to JP15110783A priority Critical patent/JPS6044702A/en
Publication of JPS6044702A publication Critical patent/JPS6044702A/en
Publication of JPH035481B2 publication Critical patent/JPH035481B2/ja
Granted legal-status Critical Current

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  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)

Description

【発明の詳細な説明】 発明の属する技術分野 本発明は、一定濃度の蒸気を発生させる方法お
よびその装置に関する。
DETAILED DESCRIPTION OF THE INVENTION Field of the Invention The present invention relates to a method and apparatus for generating steam at a constant concentration.

従来技術とその問題点 有機溶媒等常温常圧で液体として存在する有害
物質の毒性評価のための動物吸入試験あるいはこ
れら有害物質の除去試験等において、低濃度の有
機溶媒蒸気を発生させる必要がある。
Prior art and its problems In animal inhalation tests to evaluate the toxicity of organic solvents and other harmful substances that exist as liquids at room temperature and normal pressure, or in tests for the removal of these harmful substances, it is necessary to generate low-concentration organic solvent vapors. .

従来、この種の蒸気発生装置は強制気化式ある
いはバブリング式が採用されている。強制気化式
蒸気発生装置を第1図に示す。この方式では、加
熱手段2により蒸発釜1を所定温度に加熱しなが
ら、蒸発させる液体をライン3から蒸発釜1に添
加するとともに気体をライン4から蒸発釜1内に
送気し、蒸発釜1の内面で液体を気化させて発生
した蒸気をライン5から生成蒸気として取出す。
Conventionally, this type of steam generator employs a forced vaporization type or a bubbling type. Figure 1 shows a forced vaporization steam generator. In this method, while heating the evaporator 1 to a predetermined temperature by the heating means 2, the liquid to be evaporated is added to the evaporator 1 from a line 3, and gas is sent into the evaporator 1 from a line 4. The vapor generated by vaporizing the liquid on the inner surface of the tube is taken out from line 5 as generated vapor.

バブリング蒸気発生装置では、蒸発釜内に所定
量の蒸発させる液体を装填し、この液体を加熱し
ながらこの液体中に気体を吹込んで気泡を形成す
ることにより蒸気を発生させる。
In a bubbling steam generator, a predetermined amount of liquid to be evaporated is loaded into an evaporating pot, and while heating the liquid, gas is blown into the liquid to form bubbles to generate steam.

強制気化装置では、生成蒸気濃度の制御は、主
として液送ポンプの吐出流量を変化させることに
より行なわれる。液送ポンプの吐出流量の変動
は、生成蒸気濃度の変動へと直接影響するため、
ポンプの脈流等により蒸気濃度が変動してしま
う。また、10ppm以下と低濃度の蒸気を発生させ
るための送液ポンプは相当小型のものとなり、こ
の種のポンプは安定した給液が困難である。ま
た、生成蒸気濃度はこのポンプ流量調節範囲内で
しか変化させることができない。その他、蒸発釜
内壁に滴下された液体により、蒸発釜内壁の温度
分布が不均一になりこれにより生成蒸気濃度も変
動してしまう。このように強制気化式蒸気発生装
置では所望の蒸気濃度を長期間にわたり安定して
得ることはできない。
In a forced vaporizer, the concentration of generated vapor is controlled mainly by changing the discharge flow rate of the liquid feed pump. Fluctuations in the discharge flow rate of the liquid pump directly affect fluctuations in the concentration of generated steam, so
The vapor concentration fluctuates due to the pulsating flow of the pump, etc. In addition, a liquid pump for generating low-concentration steam of 10 ppm or less is quite small, and it is difficult for this type of pump to supply liquid stably. Furthermore, the concentration of generated vapor can only be changed within this pump flow rate adjustment range. In addition, the liquid dripped onto the inner wall of the evaporating pot causes the temperature distribution on the inner wall of the evaporating pot to become non-uniform, thereby causing fluctuations in the concentration of generated vapor. As described above, the forced vaporization type steam generator cannot stably obtain a desired steam concentration over a long period of time.

バブリング式蒸気発生装置では、生成蒸気濃度
の変動は、バブリング状態に依存する。バブリン
グ状態は、気体流量、吹込み圧力、液深、液温度
等種々の因子により影響を受ける。これらの因子
の変動を完全になくすことはできないため、バブ
リング式蒸気発生装置では生成蒸気濃度は大幅に
変動する。
In a bubbling steam generator, fluctuations in the concentration of generated steam depend on the bubbling state. The bubbling state is influenced by various factors such as gas flow rate, blowing pressure, liquid depth, and liquid temperature. Since fluctuations in these factors cannot be completely eliminated, the concentration of generated steam in a bubbling steam generator varies considerably.

発明の目的 本発明は、従来技術の欠点を解消し低濃度から
高濃度までの蒸気を簡便かつ安定して生成するこ
とのできる蒸気発生方法およびその装置を提供す
ることを目的とする。
OBJECTS OF THE INVENTION An object of the present invention is to provide a steam generation method and an apparatus therefor that can eliminate the drawbacks of the prior art and easily and stably generate steam from low to high concentrations.

発明の要点 すなわち本発明は、横断面積が下向きに減少す
る漏斗状筒体に含まれている液体の表面に、前記
液体と間接熱交換されて前記液体とほぼ同温度の
気体を、前記液体の表面の高さを一定に保持しつ
つ吹付け;前記液体を蒸発させ;および発生した
蒸気を系外に取出す;ことからなる、蒸気発生方
法であり、 蒸発させる液体を含む容器、横断面積が下向き
に減少する漏斗状筒体、気体導入管、および溢流
部から構成される蒸気発生装置であつて、 前記漏斗状筒体は前記容器内に位置し、前記気
体導入管が前記液体中を通過し、前記気体導入管
の放出口が前記漏斗状筒体内の前記液体の表面に
向いており、前記容器と前記溢流部は連通してお
り、 前記気体導入管に導入した気体を前記気体導入
管の前記放出口から前記液体の前記表面に吹付
け、生成した蒸気を前記容器から生成蒸気として
取出す、蒸気発生装置である。
Summary of the Invention In other words, the present invention provides indirect heat exchange with the liquid and a gas having approximately the same temperature as the liquid onto the surface of the liquid contained in a funnel-shaped cylinder whose cross-sectional area decreases downward. A steam generation method that involves spraying while keeping the surface height constant; evaporating the liquid; and taking the generated vapor out of the system. The container containing the liquid to be evaporated has a cross-sectional area facing downward. A steam generating device comprising a funnel-shaped cylinder, a gas introduction pipe, and an overflow part, wherein the funnel-shaped cylinder is located in the container, and the gas introduction pipe passes through the liquid. and the outlet of the gas introduction tube faces the surface of the liquid in the funnel-shaped cylinder, the container and the overflow part communicate with each other, and the gas introduced into the gas introduction tube is transferred to the gas introduction tube. This is a steam generating device that sprays the liquid from the discharge port of the pipe onto the surface of the liquid and extracts the generated steam from the container.

発明の実施態様 以下、添付図面に従い本発明を詳細に説明す
る。第2図は本発明により蒸気を発生させる概略
系統図であり、第3図および第4図は本発明の効
果を示す線図である。
Embodiments of the Invention The present invention will be described in detail below with reference to the accompanying drawings. FIG. 2 is a schematic system diagram for generating steam according to the present invention, and FIGS. 3 and 4 are diagrams showing the effects of the present invention.

第2図において、メインダクト11からの空気
を本発明に係る蒸気発生装置に供給し、得られた
蒸気をメインダクト11に戻す系統図を示してい
る。本発明にて使用する空気は大気から採取され
たものであつてもよい。これらの空気を直接蒸気
発生装置に供給してもよいが、所望によりシリカ
ゲル等を充填した水分吸着塔12、活性炭吸着塔
13、および除塵フイルタ14を通して空気を精
製してもよい。このように精製された空気をポン
プ15により圧送する。圧送された空気はライン
16を経て、質量流量計17により流量調整され
る。質量流量計17はノーマルオープンであるか
ら、ポンプ15の作動時に過大流量が流れること
により質量流量計17が作動する。このため起動
時に過大流量の空気が液面21に吹付けられて設
定値よりも高い濃度が発生する。この場合は、発
生蒸気を三方弁18によりライン19に導いて排
気し、蒸気濃度が一定になつてからライン10に
蒸気を気換えてメインダクト11に供給する。こ
の過度時間は1分以内である。質量流量計17を
用いず本発明を実施することもできるが、設定蒸
気濃度が低い場合は、質量流量計17を使用して
蒸気濃度をより安定にするのが好ましい。
FIG. 2 shows a system diagram in which air from the main duct 11 is supplied to the steam generator according to the present invention and the obtained steam is returned to the main duct 11. The air used in the present invention may be collected from the atmosphere. This air may be directly supplied to the steam generator, but if desired, the air may be purified through a moisture adsorption tower 12 filled with silica gel or the like, an activated carbon adsorption tower 13, and a dust removal filter 14. The air thus purified is pumped by the pump 15. The pressure-fed air passes through line 16, and its flow rate is adjusted by mass flow meter 17. Since the mass flow meter 17 is normally open, the mass flow meter 17 is activated due to excessive flow when the pump 15 is activated. Therefore, at startup, an excessive flow rate of air is blown onto the liquid surface 21, resulting in a concentration higher than the set value. In this case, the generated steam is guided to a line 19 by a three-way valve 18 and exhausted, and after the steam concentration becomes constant, the steam is transferred to a line 10 and supplied to the main duct 11. This transient time is less than 1 minute. Although it is possible to practice the invention without the mass flow meter 17, if the set steam concentration is low, it is preferable to use the mass flow meter 17 to make the steam concentration more stable.

質量流量計により流量調整された空気は必要に
応じて設置した浮子式流量計20を経て空気導入
管22に入る。加熱手段付の容器24には蒸発す
べき液体23が装填されている。液体23の温度
は温度調整器33により所望値に設定される。液
体23は常温常圧で液体として存在すれば発生蒸
気の使用目的により何れの液体でもよいが、例え
ばCH3CCl3(1,1,1−トリクロルエタン)、
CCl2=CCl2(テトラクロルエチレン)、CH3CH
(OH)CH2OH(1,2−プロバンジオール)等
あらゆる沸点の有機物質を使用することができ
る。その他、アンモニア水等の無機物質も使用で
きる。空気導入管22は容器24内の液体23に
浸漬しており、ここで精製空気の温度は液体23
の温度とほぼ等しくなる。空気導入管の吹出口2
5は液面21に対して垂直方向に向けられ、吹出
口25から吹出された空気は液面21に吹付けら
れて液体23が蒸発する。吹出口25を液面21
に対し傾斜角度を設けてもよい。この角度を変え
ることにより蒸気濃度の微量調整が可能である。
吹出口25と液面21との距離は任意の値であつ
てよい。この距離の調整によつても蒸気濃度を調
整できる。
The air whose flow rate has been adjusted by the mass flow meter enters the air introduction pipe 22 via a float type flow meter 20 installed as necessary. A container 24 equipped with heating means is filled with a liquid 23 to be evaporated. The temperature of the liquid 23 is set to a desired value by a temperature regulator 33. The liquid 23 may be any liquid depending on the purpose of use of the generated vapor as long as it exists as a liquid at normal temperature and normal pressure; for example, CH 3 CCl 3 (1,1,1-trichloroethane),
CCl 2 = CCl 2 (tetrachlorethylene), CH 3 CH
Organic substances of any boiling point can be used, such as (OH) CH2OH (1,2-probanediol). In addition, inorganic substances such as aqueous ammonia can also be used. The air introduction pipe 22 is immersed in the liquid 23 in the container 24, and the temperature of the purified air is lower than that of the liquid 23.
is almost equal to the temperature of Air intake pipe outlet 2
5 is oriented perpendicularly to the liquid level 21, and the air blown out from the air outlet 25 is blown onto the liquid level 21 to evaporate the liquid 23. The air outlet 25 is connected to the liquid level 21.
An inclination angle may be provided for the By changing this angle, the vapor concentration can be finely adjusted.
The distance between the outlet 25 and the liquid level 21 may be any value. The vapor concentration can also be adjusted by adjusting this distance.

容器24内には漏斗状筒体26が設置されてお
り、また漏斗状筒体26内の液体23と漏斗状筒
体26外の液体23とは漏斗状筒体26下部の連
通部により連通されており海面21の高さを変え
ることにより蒸発有効面積が変化して蒸気濃度を
調整する。漏斗状筒体は図示の如く、その断面積
が下方に向かつて漸減している。液面21の高さ
を低くすると、漏斗状筒体26内の液表面積は減
少する。
A funnel-shaped cylindrical body 26 is installed inside the container 24, and the liquid 23 inside the funnel-shaped cylindrical body 26 and the liquid 23 outside the funnel-shaped cylindrical body 26 are communicated through a communication portion at the bottom of the funnel-shaped cylindrical body 26. By changing the height of the sea surface 21, the effective evaporation area changes and the vapor concentration is adjusted. As shown in the figure, the cross-sectional area of the funnel-shaped cylinder gradually decreases downward. When the height of the liquid level 21 is lowered, the liquid surface area within the funnel-shaped cylinder 26 is reduced.

容器24と溢流部27とは、連通管28により
連通されている。タンク29に貯留されている液
体23をポンプ30によりくみ上げて溢流部27
に送り、ポンプ30により供給された液体23の
一部は連通管28を通して容器内に蒸発した液体
と同量の液体を補給するとともに、残りの液体2
3は堰31より溢流してタンク29に循環する。
堰31の高さと液面21の高さは等しい。堰31
の高さを変えることにより、液面21の高さを変
えることができ、これにより蒸気濃度を制御でき
る。
The container 24 and the overflow part 27 are communicated with each other by a communication pipe 28. The liquid 23 stored in the tank 29 is pumped up by the pump 30 to the overflow part 27.
A part of the liquid 23 supplied by the pump 30 passes through the communication pipe 28 to replenish the same amount of liquid as the evaporated liquid in the container, and the remaining liquid 2
3 overflows from the weir 31 and circulates to the tank 29.
The height of the weir 31 and the height of the liquid level 21 are equal. Weir 31
By changing the height of the liquid level 21, the height of the liquid level 21 can be changed, thereby controlling the vapor concentration.

容器24の上部空間に発生した蒸気をライン3
2を経てメインダクト11に供給する。
The steam generated in the upper space of the container 24 is transferred to the line 3.
2 to the main duct 11.

本発明の他の態様として、漏斗状筒体26と容
器24を一体化させたものであつてもよい。すな
わち、容器24を漏斗状筒体の形状とし、漏斗状
筒体26を省略する。この場合においても、空気
導入管22を液体23に浸漬させる。
As another aspect of the present invention, the funnel-shaped cylinder 26 and the container 24 may be integrated. That is, the container 24 is shaped like a funnel-shaped cylinder, and the funnel-shaped cylinder 26 is omitted. Also in this case, the air introduction pipe 22 is immersed in the liquid 23.

第3図に、1,1,1−トリクロルエタンを使
用した場合の空気流量と生成蒸気濃度との関係を
本発明の装置と従来型装置(バブリング式)を比
較して示す。本発明に係る装置では、従来型装置
よりも空気流量の増加に対する生成蒸気濃度の増
加率が大きい。これより、本発明に係る装置は広
範囲の生成蒸気濃度を設定できる。
FIG. 3 shows the relationship between the air flow rate and the concentration of generated vapor when 1,1,1-trichloroethane is used, comparing the apparatus of the present invention and the conventional apparatus (bubbling type). In the device according to the present invention, the rate of increase in the concentration of produced steam with respect to the increase in air flow rate is greater than in the conventional device. As a result, the device according to the present invention allows a wide range of product vapor concentrations to be set.

第4図に、使用する液体の飽和蒸気圧とその液
体を使用して得られる生成蒸気濃度の関係を示
す。本発明の装置を用いると、10ppm以下と低濃
度の蒸気を得ることができる。特に揮発性液体に
対し本発明は顕著な効果を奏する。
FIG. 4 shows the relationship between the saturated vapor pressure of the liquid used and the concentration of vapor produced using that liquid. Using the device of the present invention, it is possible to obtain steam with a low concentration of 10 ppm or less. In particular, the present invention has remarkable effects on volatile liquids.

第5図は、第2図に示す装置において漏斗状筒
体26の使用の有無による生成蒸気濃度に与える
影響を示す線図である。漏斗状筒体を使用するこ
とにより、より低濃度の蒸気を安定して得ること
ができる。
FIG. 5 is a diagram showing the influence of whether or not the funnel-shaped cylinder 26 is used on the generated steam concentration in the apparatus shown in FIG. 2. By using a funnel-shaped cylinder, lower concentration steam can be stably obtained.

本発明の効果 本発明によれば、表面吹付方式を採用すること
により濃度変動の少ない蒸気を得ることができ
る。特に本発明では、漏斗状筒体内の液面を有効
蒸発面積としているので、液面の高さを変えるこ
とにより蒸気濃度の変更を簡便にできる。従来型
装置では送液ポンプとして高価な微量定量ポンプ
を使用しなければならないが、本発明ではこのよ
うな高価なポンプを使用する必要はなく経済的な
蒸気発生装置となる。
Effects of the present invention According to the present invention, steam with less concentration fluctuation can be obtained by employing a surface spraying method. In particular, in the present invention, since the liquid level inside the funnel-shaped cylinder is used as the effective evaporation area, the vapor concentration can be easily changed by changing the height of the liquid level. In conventional devices, an expensive minute metering pump must be used as a liquid pump, but in the present invention, there is no need to use such an expensive pump, resulting in an economical steam generating device.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は、従来型蒸気発生装置の概略断面図で
ある。第2図は、本発明により蒸気を発生させる
概略系統図である。第3図は空気流量と生成蒸気
濃度の関係を示す線図である。第4図および第5
図は、使用する液体の飽和蒸気圧とその液体を使
用して得られる生成蒸気濃度の関係を示す線図で
ある。 1……蒸発釜、3……液供給ライン、4……空
気供給ライン、22……空気導入管、24……伝
熱手段付容器、25……吹出口、26……漏斗状
筒体、27……溢流部。
FIG. 1 is a schematic cross-sectional view of a conventional steam generator. FIG. 2 is a schematic system diagram for generating steam according to the present invention. FIG. 3 is a diagram showing the relationship between air flow rate and generated vapor concentration. Figures 4 and 5
The figure is a diagram showing the relationship between the saturated vapor pressure of the liquid used and the concentration of vapor produced using the liquid. DESCRIPTION OF SYMBOLS 1... Evaporation pot, 3... Liquid supply line, 4... Air supply line, 22... Air introduction pipe, 24... Container with heat transfer means, 25... Air outlet, 26... Funnel-shaped cylinder, 27... Overflow part.

Claims (1)

【特許請求の範囲】 1 横断面積が下向きに減少する漏斗状筒体に含
まれている液体の表面に、前記液体と間接熱交換
されて前記液体とほぼ同温度の気体を、前記液体
の表面の高さを一定に保持しつつ吹付け;前記液
体を蒸発させ;および発生した蒸気を系外に取出
す;ことからなる、蒸気発生方法。 2 蒸発させる液体を含む容器、横断面積が下向
きに減少する漏斗状筒体、気体導入管、および溢
流部から構成される蒸気発生装置であつて、 前記漏斗状筒体は前記容器内に位置し、前記気
体導入管が前記液体中を通過し、前記気体導入管
の放出口が前記漏斗状筒体内の前記液体の表面に
向いており、前記容器と前記溢流部は連通してお
り、 前記気体導入管に導入した気体を前記気体導入
管の前記放出口から前記液体の前記表面に吹付
け、生成した蒸気を前記容器から生成蒸気として
取出す、蒸気発生装置。
[Scope of Claims] 1. A gas having approximately the same temperature as the liquid through indirect heat exchange with the liquid is applied to the surface of the liquid contained in a funnel-shaped cylinder whose cross-sectional area decreases downward. A method for generating steam, comprising: spraying while maintaining a constant height; evaporating the liquid; and taking out the generated steam outside the system. 2. A steam generator comprising a container containing a liquid to be evaporated, a funnel-shaped cylinder whose cross-sectional area decreases downward, a gas introduction pipe, and an overflow part, wherein the funnel-shaped cylinder is located within the container. the gas introduction tube passes through the liquid, the outlet of the gas introduction tube faces the surface of the liquid in the funnel-shaped cylinder, and the container and the overflow part communicate with each other, A steam generation device that sprays the gas introduced into the gas introduction tube onto the surface of the liquid from the discharge port of the gas introduction tube, and extracts the generated vapor from the container as generated vapor.
JP15110783A 1983-08-19 1983-08-19 Method and device for generating steam by surface evaporation Granted JPS6044702A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP15110783A JPS6044702A (en) 1983-08-19 1983-08-19 Method and device for generating steam by surface evaporation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP15110783A JPS6044702A (en) 1983-08-19 1983-08-19 Method and device for generating steam by surface evaporation

Publications (2)

Publication Number Publication Date
JPS6044702A JPS6044702A (en) 1985-03-09
JPH035481B2 true JPH035481B2 (en) 1991-01-25

Family

ID=15511500

Family Applications (1)

Application Number Title Priority Date Filing Date
JP15110783A Granted JPS6044702A (en) 1983-08-19 1983-08-19 Method and device for generating steam by surface evaporation

Country Status (1)

Country Link
JP (1) JPS6044702A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7615640B2 (en) 2002-07-29 2009-11-10 Mitsubishi PaperMillsLtd. Organic dye, photoelectric conversion material, semiconductor electrode and photoelectric conversion device

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61272503A (en) * 1985-05-24 1986-12-02 日本科学工業株式会社 High-temperature saturated steam feeder
JPH0725224Y2 (en) * 1989-02-20 1995-06-07 大同ほくさん株式会社 Evaporative gas quantitative extraction device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7615640B2 (en) 2002-07-29 2009-11-10 Mitsubishi PaperMillsLtd. Organic dye, photoelectric conversion material, semiconductor electrode and photoelectric conversion device

Also Published As

Publication number Publication date
JPS6044702A (en) 1985-03-09

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