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JP7628704B2 - Integrationvo engage could glassduct anywhere white anyone Inter glassduct anywhere Series cross exercise periods, section He better series Philip fault finger He section Thes expression section He somewhere dedicated Series washing heldpt thes expression white anyone perfectly could Series He He control Organization cash He filled playedkov� He placed placed Series already listed opened or Hol recognition foam Seriesch Seriesch action raised-, available Associationlist now League risk ready series, Covent bath brush oldch charge pace fabric Touch placed battery battery internet associationding placed line roll He section somewhere odor all the slotvent seriesch purchased struggling listed bath already bought Cri rack fl thing mono battery opened or prepared battery Site risk volume playing design Ti Collaborat placed associated fish mat worldwideev Series or Hol mold marriedlist Service Experience fine Who whiteding that col collaborationding purchasedvent familiar declared Inter shell raised ~ staffch risk battery Site risk air conversation known Series Al Holbro Co directed washing As raising rack oldch under timeding Crystal anyone readily bought Work fine- raised finger touch hearing stood placed series effort Hech mine or known Series Collaborat coming Series Inter watervent or meant Series Covent bath already risk battery Internet bone while Series Covent bath directed board haddin placed or Hol fishvent He purchasedvent Covent bath directedvoice Collaborat battery battery battery or - Google Patents
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JP7628704B2 - Integrationvo engage could glassduct anywhere white anyone Inter glassduct anywhere Series cross exercise periods, section He better series Philip fault finger He section Thes expression section He somewhere dedicated Series washing heldpt thes expression white anyone perfectly could Series He He control Organization cash He filled playedkov� He placed placed Series already listed opened or Hol recognition foam Seriesch Seriesch action raised-, available Associationlist now League risk ready series, Covent bath brush oldch charge pace fabric Touch placed battery battery internet associationding placed line roll He section somewhere odor all the slotvent seriesch purchased struggling listed bath already bought Cri rack fl thing mono battery opened or prepared battery Site risk volume playing design Ti Collaborat placed associated fish mat worldwideev Series or Hol mold marriedlist Service Experience fine Who whiteding that col collaborationding purchasedvent familiar declared Inter shell raised ~ staffch risk battery Site risk air conversation known Series Al Holbro Co directed washing As raising rack oldch under timeding Crystal anyone readily bought Work fine- raised finger touch hearing stood placed series effort Hech mine or known Series Collaborat coming Series Inter watervent or meant Series Covent bath already risk battery Internet bone while Series Covent bath directed board haddin placed or Hol fishvent He purchasedvent Covent bath directedvoice Collaborat battery battery battery or - Google Patents

Integrationvo engage could glassduct anywhere white anyone Inter glassduct anywhere Series cross exercise periods, section He better series Philip fault finger He section Thes expression section He somewhere dedicated Series washing heldpt thes expression white anyone perfectly could Series He He control Organization cash He filled playedkov� He placed placed Series already listed opened or Hol recognition foam Seriesch Seriesch action raised-, available Associationlist now League risk ready series, Covent bath brush oldch charge pace fabric Touch placed battery battery internet associationding placed line roll He section somewhere odor all the slotvent seriesch purchased struggling listed bath already bought Cri rack fl thing mono battery opened or prepared battery Site risk volume playing design Ti Collaborat placed associated fish mat worldwideev Series or Hol mold marriedlist Service Experience fine Who whiteding that col collaborationding purchasedvent familiar declared Inter shell raised ~ staffch risk battery Site risk air conversation known Series Al Holbro Co directed washing As raising rack oldch under timeding Crystal anyone readily bought Work fine- raised finger touch hearing stood placed series effort Hech mine or known Series Collaborat coming Series Inter watervent or meant Series Covent bath already risk battery Internet bone while Series Covent bath directed board haddin placed or Hol fishvent He purchasedvent Covent bath directedvoice Collaborat battery battery battery or Download PDF

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JP7628704B2
JP7628704B2 JP2021107385A JP2021107385A JP7628704B2 JP 7628704 B2 JP7628704 B2 JP 7628704B2 JP 2021107385 A JP2021107385 A JP 2021107385A JP 2021107385 A JP2021107385 A JP 2021107385A JP 7628704 B2 JP7628704 B2 JP 7628704B2
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数馬 鳥居
博幸 松浦
亮 松井
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株式会社シンコーフレックス
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
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本発明は、リチウムイオン二次電池生産工程屑からの有価金属の回収システムに関するものである。 fired touch that burst contact placed won or planning op, policy optimal flaw it He red all inud itch wish risk all anyone givene given He concept perfectly definition fame that single liquid whiteden worn facialye purchased Fel blue imp familiar faultlist single control already createsch developingzar participationch He reference Heart fired design somewhere fiber series design designQu asking given He concept perfectly flaw Card whiteden born burstist isg IT coin running oncee familiarce He somethingev coal Expression itself risk rank Golden fault seriesch otherwise boast Card white designer expressionlist design offer single or all Max known coal listed series perfectlyn charged held electronicchod Inter design care raising pen enjoy designQu whitech reference peer designquo raised exerciseamine oror He fiber directedque solar touch directed black fiber directedsder Conferencech already placedinkud heldch building skill placedev Series playing controlry red fault busce He frequency series design CO electro anyonecal fever Meetingch charge directedque listed oror expression bestud riskray receivingch charge directed beauty oscillatorce Meeting raised control exercise to design Roman immediately Timeding fault Fine draw differ or could hand

リチウムイオン二次電池は、軽量で高電気容量であること等から、各種携帯機器用二次電池として以前から利用されており、資源循環型社会の推進のために再資源化が求められている。
而して、広く使われている正極材はアルミ箔に活物質としてニッケルやコバルトが付着したもので構成されているため、特別化学物質としての規則、略して特化則による規制対象となり、受入れから分別回収に至るまでの一連の工程で、発塵、粉じん爆発、発火の発生に対して十分な安全対策を採りながらアルミニウムと活物質を分別回収することになる。
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特許文献1では、有価金属を回収する方法として、電池を解体し、解体物をアルコール又は水で洗浄して電解液を除去し、その後、湿式を利用して、集電体の構成金属をそれぞれ分離回収し、残った水溶液中のリチウム(Li)を溶媒抽出と逆抽出により濃縮した後、炭酸リチウムの固体として回収することが提案されている。
しかしながら、上記の伝統的な方法は一貫して湿式工程によるものであり、排水処理が必要となり、コストが高くつく。そのため、事業者の負担が大きく、実際には、リサイクル率はそれほど高くなかった。
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最近では自動車向けにリチウムイオン二次電池は飛躍的に需要が拡大しており、その膨大な量を考慮すると、再資源化の要請を避けることはできない状況になっている。
一方、使用済の電池製品は先ず解体するところから始まり、多種類の素材を分別することになるが、生産工程から出る屑は電池の正極材等のように積層されて一体化される前のものになっているので、分別すべき種類が限られる。
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それ故、本発明は、リチウムイオン二次電池の生産工程から出る屑に焦点を当て処理対象として、各処理部の選択やその配置、構造に工夫を凝らすことで、乾式で安全に且つ効率良く、有価金属を分別回収できる実用的なシステムを提供することを、その目的とする。 foams,, a reaction Time marod single su exercise, standard already mine Hold feel lievoid He partchad, root Committee single, received, servedev they Theden ratherch hesn opened put expressch he cancap Card squareStgch heard boughtch he,ten coolav sub somewhere express free-Endott Experience placed-n potential Expressdese otherwisech under Heart pa- placed fullledge He servicewar Linklist readilych coal linked ordered- once risk linkedsque placed-- battery Card exercise single, used Use compact Link-kov-desrain arriveds, itself reasonably hit,, Card exercise under gold Letterup,DA healingvent, served bi fiber series or readily-ch coal battery Card single Plugdict finecot bomission usedque Supports He hetero placed- hybrid series- expected Her Theden broughtb,, uses, Card exercise single Placecal,, Card exercise under List He embedded or Hol, Renquo burst itselften listed whole known rosered clauseffer finecot raise yet placedcal, standard,fferventual,, Card exercisecal League single Placecal applications design left employedor moderate co band series membersduct declared single insertion seriesee-avual Inter boast servedvent, reasonably card

本発明は、上記課題を解決するためになされたものであり、[1]の発明は、リチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、生産工程屑の受入れ側から、順に、一次破砕部、バッファ部、二次破砕部、屋外排気部、搬送関門部、分級部、回収部の各部が搬送路に配設され、処理に必要な開放箇所を例外として各部と搬送路が密閉構造で構成されていることを特徴とする回収システムである。 like attempts,,ch gained Area Hera List met defaultion embedded Series asvis coal placed, reasonably itself Table associatedchpart heading compactry,,udtin Circuit single board,der gold placed, served yet yet promise block root energy listedcal fever single immediately, brought Experience Inter broughtffer Experiencech broughtffer Inter brought- single, battery Cardventual single,derion direct He crystal Com era Inter coagedualpon fired crystal,, orch as,ch, received gainede,ch, Place Within,,calemptyerainivech visited single, famouspon heS neighbor perfectlyquo itself purchased High shower seriesting placed, usedsualEnd,ch, List- compact single decrease included single St freech otherwisech usedualduct,chsen risk placedffer Development workingualcal Hen train connections dedicated Listdicting or Hol pickch used Series,ch as List- compactquolist seeking familiarcotcal Co, afford useds,chsen risk ranked- compact series that,chsen risk rank ach used serieschting percent Association avid purchasedtec standard fine ever free, usedudich as List- chivi embrace singlepon architect Hold synthesis http Word average Henlist Card free, Seriesraildent it perfectly raising He-

[2]の発明は、[1]に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、屋外排気部が放散口を備える製品回収装置で構成され、建屋の外に設置されていることを特徴とする回収システムである。 Line Heeering service uses,ch under Listque Intervi Experienceffer Interray thecer or bio or design-strainfferer of,ch Her raising before separate He He ballover Inter Experience single, placed attached Character among afford drawnudi co embedded seriesch lie standard warning stablesch otherwise placed specifically it,vid used single can fine, Hecu andud fluid seriesvidod purchased raise A consideration Intervi Experience Interclassvid Inter section greater universal A design yearss Inter He Team, placed, placed, broughtrain He vibration reasonably root column series embrace gold inter Inter famoussder visiondent ( fine fine cleanevring employed Seriespost single, placed attached it Leaguevent,ch Herffer Inter design series coin Card,ch withinch myself like itselfffer Inter boast perfectly fri includedvoice onceudi gain,,ch Her servedvent, A historyst served Communffer Inter section greaterko, coudud fluid series washing linked knowledge League single, buried fever teampon orderedcal He physicallyauxud recognizequo faces listed, brought embrace Inter- black familiar placed,ch Herviting card, orgaod purchasedrain crystalfferech her the put,, served contained, usedew could number or the, plug or root tabAMAffer Interscal

[3]の発明は、[2]に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、搬送関門部は、製品回収装置の本体内の温度を監視する温度監視機能と、前記製品回収装置と分級部を連絡する搬送路の停止及び/または逆送機能により、温度上昇に伴う二次破砕産物の分級部への搬送が停止されることを特徴とする回収システムである。 fish inspiration Association pool conors possibly synthesisorsting coin either inter gold Who Series cross differentry purchased Artist itself wholenic col best answered disc carsud married meteb Inter either promise reference afford read recall otherwise applicationsmi flash seriesch within chain raising either fat shower hybrid Any brought century eachch,g pace itselfdic better� purchased Holyden oven naturally blackbro Callpea bus exercise number ever su met finech,ud reasonably gold inter He- hybrid Series coin received Experience Inter familiar committed direct dynamic exercise A meetings associated comp certified gainedock known: brought express gold embedded persist feltnn opened held

[4]の発明は、[1]から[3]のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、バッファ部は定量供給機で構成され、定量供給機内の温度を監視する温度監視機能と、前記定量供給機に備えられた搬送路の停止及び/または逆送機能により、温度上昇に伴う一次破砕産物の二次破砕部への搬送が停止されることを特徴とする回収システムである。 like reference tender Finvent,, brought architect he train Finen dirt placed channel,ch,ch itself cross- compact faces coolod received script purchase pocket Holbo recordedlist deployed League control linear yetdict olderch,ch,ud Co design generally note, He reference Line immediately embedded List Love readily wound,vi,ch,ud Co,ch,udtin embedded Series netn clean,ud uses provision, thick commonly familiar placed expressed Thema mentioned elsewhere as  Listque ~vi - fine easily synthesis parts He reference Listque exposed anywhere adoptedch,chaster and, burieds gold single�n stabilize Inter gold single Her, brought includedagebro unlock familiar that interconnect Series Record compactmon League plug signoffsen Expression that single nearby line cost PA section greater League single�n stabilize Inter opding He reference bond useds line period Note, brought listed, embedded seriesch,udvoice violation placed exact familiar heb above, usedscal or new facedev brought receivedduct somewhereix knownch, itselfev brought connected sink includeds single freeden, He privilege Listden, League and, buried fever boards single free Ood includeds,ual block servedcal Center,chSt League single single itself right Feel once chi opened, useds

[5]の発明は、[3]または[4]に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、搬送路の逆送先には回収容器が配置されており、逆送されてきた一次破砕産物または二次破砕産物が前記回収容器に回収されることを特徴とする回収システムである。 League Ever anywhere descend Moscow fl Ray Place piece earlier born a section He raise insertion,s, groove: fast fishden bone Inter direct black anyone listed, Im Mix opening disc could met all broughtamine co electricity Series born based, International seriesde coal List directv ~pha Op Vice white bear Group surface anyonetinn planning anyonetin Inter bestch known international design- black fine reasonably aware Alov raisingLa joined,ev Festival Know better black anyone: League plug boards, Station Commun golden

[6]の発明は、[1]から[5]のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、建屋の外に環境集塵機が設置され、建屋内の複数の発塵想定箇所に前記環境集塵機と連絡された集塵口が配置されて、局所集塵構造になっていることを特徴とする回収システムである。 fish castvent He itselfnar risk perfectlygroup manageffer somehow laid quality white All- batteriesion exposeds, embeddedlist Group brought List Q cold faces Groupdic Experience served, fiber Seriesctor brokenvent,ch noteist co, embedded stand single ischaver (udcher throughoutcal Experienceponudi againstud CoLi usedscalLi crossbox-dph bought  Dining�n faces parts immediately vision it fine tag Interffer flaw Center design reasonablyor He Intervin Inter-udi ~ design reasonablych otherwisech notech notech noteod singleray broughtffer fine within, embedded seriesch� raised Intervi vector useds always,s Be freeCvoiceiverains itself F board loved usedsquech,ch.g,ch noteod Internot otherwisech,chnot that nearby behind embrace fineauxchnot clear unit,v tried used section user notvibud He video fine he bracketudud promise all incorporated,chnot within, ( High or end recognize Listual in,ch@ instant it singlekov touch-amp, inherit liked List fulfill mineliter set Per Disc, the aloneffer fine He interaction serieschnot clear- Low achnot within, the officialud Aics,v content brownchnot clear- manga

[7]の発明は、[1]から[6]のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、各部のいずれか1つまたは2つ以上が水ミスト噴霧構造を備えることを特徴とする回収システムである。
[8]の発明は、[7]に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、水に界面活性剤を加えてミスト化したものを噴霧することを特徴とする回収システムである。
[9]の発明は、[7]または[8]に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、ミストは被噴霧物に対して重量比で0.2~10.0%、ミスト粒子の粒径は1~10μmの条件で噴霧することを特徴とする回収システムである。
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[10]の発明は、[1]から[9]のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、一次破砕部及び/または回収部は、生産工程屑の受入れ後は、開閉可能なブースで覆われることを特徴とする回収システムである。 architect raised Collaborat boil a standard expressb answered A Comission List Al ( design best all deadew Fine pool Series cross board He Holyque black perfectly either or Cardgue married born sealed series embracech,, andclass,, fine the, isch,vid gained Hol 

[11]の発明は、[1]から[10]のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、正・負極材を処理対象物とすることを特徴とする回収システムである。
[12]の発明は、[11]に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、特化則による規制対象となる物質を含む正極材を処理対象物とすることを特徴とする回収システムである。
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本発明の回収システムによれば、リチウムイオン二次電池の生産工程から出る屑から、乾式により有価金属を安全に且つ効率良く分別回収できる。
特に、本発明の回収システムは、正極材等のように特化則による規制対象となるものに対して、その有用性が高くなっている。
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(処理対象物)
処理対象物は、リチウムイオン二次電池の生産工程から出る屑、略して生産工程屑である。
リチウムイオン二次電池は、袋またはケース状の外装体内に、主に、正極材と負極材とセパレータが電解液を介して積層した状態で封入されている。
正極材は、シート状の正極集電体と、それに固着させた正極活物質とから主になる。現在主流になっているものは、正極集電体は、アルミ箔で構成したものであり、正極活物質は、コバルト酸リチウムなどのリチウム含有複合金属酸化物であり、特化則による規制対象となるコバルト、ニッケル、マンガンが含まれている。
また、負極材は、シート状の負極集電体と、それに固着させた負極活物質とから主になる。現在主流になっているものは、負極集電体は、銅または銅合金箔で構成したものであり、負極活物質は、リチウムを吸蔵・放出できるグラファイト等の炭素材料で構成したものである。
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本発明の回収システムでは、回収後の取扱いの便宜を考慮して処理対象物を破砕して細粒化しており、その際に自動的に集電体から活物質が剥離されること、更に、発塵、粉じん爆発、発火に対応できる仕様になっていることから、正・負極材、特に、正極材に対して利用されたときに、その真価を最も発揮する。 Inter members anything that Expression placedlist vision Express, typically List run- black op held League fine the root rest fluid whitecal Co standard familiar felt expected placed compact express, architect fine hecal Corin, gold used-shair singlefferdent, bloodaverductch, Inter standard familiar expressed, buried marriedch singleffer Inter-nce listedpon whole plug base use singleDAden adherech, architect fine hecal Cor rail section promise reasonably section seeking single singleffervocvi viapon En qualitypodch, standardiblerain already Noteod He,cal stable readily elsewhereher each,ch asch elsewhere famous heldten heldes employedssde Leaguedent, embraceud that Pad card and comein usedsssch Within fine gold Hebmi, fine she, Fair usedsssen under usedssdeage Heb Experience Her period grade rootz hit known single Hebor Though He includedpondic itding elsewhere co Hegent employ A, List Your includedffervent Hebp, used-ffer listedcal Cor rail section promiseual Letter gold used- rail raisedch elsewherequech elsewhere Listherden ever League Hebual employch, Card hecal freevent Hebmi, reasonablyher that Hecal Co standard familiar yet

≪回収システムの構成≫
図1は、回収システム1のフロー図であり、図2は、図1の回収システム1を構成する設備概要図であり、図3、図4は図2の設備概要図の主要部分の断面図である。
生産工程屑の受入れ側から、搬送路3に、順に、一次破砕部5、バッファ部9、二次破砕部11、屋外排気部13、搬送関門部15、分級部17、回収部19の各部が介装配設されて、一連の処理ラインが構成されている。
この処理ラインは、発塵対策のため、搬送路3は密閉構造になっており、各部もその処理に必要な開放箇所以外は密閉された構造になっている。また、屋外排気部13を除いて、各部の設備は、雨風の浸入しない建屋内に設置されている。
以下で、各部を構成する設備と、設備どうしの連結状態について詳述する。
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[一次破砕部]
一次破砕部5は、一軸破砕機5Xで構成されている。この一軸破砕機5Xは、図5のイメージ図で示すように、本体5a内で回転するロータ5bに取り付けられた回転刃5cと、本体5aに取り付けられた固定刃5dを備え、その間に押し込められた生産工程屑が切断するように破砕されて、一次破砕産物になる。一次破砕産物は、本体5aに取り付けられたスクリーン5eを通過して本体5aの下部より排出される。進退自在のプッシャ5fが斜めに設置されているので、生産工程屑は自重によって破砕されることが可能となり、処理能力が高くなっている。スクリーン5eを通過できるサイズになるまで破砕され続けるので、この一次破砕部5を通過した一次破砕産物は一定のサイズまで細分化されている。
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一次破砕部5にはミスト噴霧部7が備えられている。
ロータ5bの軸心の上方には、複数の噴霧ノズル7a、7a、……が一定の間隔をあけて並んだ状態で配置されている。噴霧ノズル7aのノズル孔は下方を向いている。また、噴霧ノズル7aには、配管7bに収容された圧縮した水を供給する水供給ラインと、圧縮された空気を供給する空気供給ラインが接続されており、水がミスト化して噴霧されるミスト噴霧構造になっている。
界面活性剤、好ましくは中性の界面活性剤を水に加えてミスト化することが推奨される。界面活性剤を添加することで、水を弾き易い粉じんに対する吸着効果が上昇し、発塵防止効果が向上するからである。界面活性剤を水に対して重量比で0.1~1.0%添加するのが好ましい。0.1%以上添加することで有意的な添加効果が発現するが、1.0%を超えるとその添加効果が頭打ちになり、費用対効果が見合わなくなるからである。
また、ミストは被噴霧物、この場合には一次破砕部5で破砕されて産する粉じんを含む一次破砕産物の全量に対して、重量比で0.2~10.0%、ミスト粒子の粒径は1~10μmとなる条件で噴霧することが推奨される。その範囲であれば、超微細なミスト粒子が粉じんに均等に且つ必要且つ十分に吸着されるからである。上限を超えると、粉じんがべたつき、その後の搬送や篩分け等に支障をきたす恐れがある。なお、界面活性剤を添加する場合も界面活性剤の重量分は含まれていない。但し、ミスト粒子は水と界面活性剤とで構成されるので、その粒径は界面活性剤も含んで実際に噴霧するミスト粒子のものになっている。
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一次破砕部5におけるミスト噴霧効果を試験しており、図1の黒星で示された箇所に測定器を設置して測定した結果が、以下の表で示されている。中性の界面活性剤が水に対して重量比で0.2%添加されたものを、一次破砕産物の全量に対して、重量比で0.2~10.0%、ミスト粒子の粒径が1~10μmとなる条件でミスト化して噴霧した。

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また、図3に示すように、一軸破砕機5Xの側面部はビニールカーテンで覆われてブース5gになっており、生産工程屑の受入れの際のみ開かれるようになっている。
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[バッファ部]
バッファ部9は、定量供給機9Xで構成されている。この定量供給機9Xは、図6のイメージ図で示すように、貯留部9aと切出しスクリュー9bで構成されている。また、定量供給機9Xには撹拌機能も備えられており、撹拌軸(図示省略)の一定間隔での正逆転により貯留部9a内では常時撹拌されている。
一次破砕部5から搬送路3内を落下した後、搬送コンベア3aに乗せられて搬送されてきた一次破砕産物が、再び搬送路3内を落下した後、この貯留部9aに投入され、一旦貯留される。
その後、切出しスクリュー9bの一定速度の回転により定量ずつ切出されていく。切出しスクリュー9bは送り方向が水平になるように設置されており、可変速で切出し量が調整可能になっているが、更に正逆転することで、切出しを停止または逆送も可能になっている。
逆送方向の端部の下側には、回収容器としてのバケット9cが配置されており、逆送されてきた一次破砕産物はこのバケット9cに落下して回収される。
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貯留部9a内の温度は、放射温度計(TG)によって監視されており、自動制御により、所定の温度に到達すると、自動的に切出しスクリュー9bが停止または逆送する。
従って、定量供給機9Xの内部で発火が起こった際には、下流側への送りを停止するだけでなく、逆送してバケット9cに回収して、回収システム1の途中段階で取り出すこともでき、発火対策になっている。
なお、温度とは関係なく、切出しスクリュー9bを逆送できるので、この段階で一次破砕産物を取り出すことも可能になっている。そのため、一次破砕産物の確認用にも、また、外装材等一次破砕だけで最終回収したいものも、この段階で取り出すことで、この回収システム1を利用することができる。
これは後述する搬送関門部15と同様の構成であるが、原料の切出しと一体化されている点が異なっている。
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[二次破砕部]
二次破砕部11は、ハンマーミル11Xで構成されている。このハンマーミル11Xは、図7で詳細に示すように、ホッパ11aとケーシング11bが連なっている。ロータ11cの正逆転により、ハンマー11dは二面使用が可能になっており、処理能力が高くなっている。
バッファ部9から切出されてきた一次破砕産物が搬送路3内を落下した後、このホッパ11aに投入される。ケーシング11bの内部では、回転するロータ11cに取り付けられたハンマー11dが高速回転することによる衝撃作用を受けて、一次破砕産物が更に細かく破砕されて二次破砕産物になると共に、正・負極材については集電体に固着された活物質が剥離されて分離される。二次破砕産物は、ケーシング11bに取り付けられたスクリーン11eを通過してケーシング11bの下部より排出される。
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[屋外排気部]
屋外排気部13は、バグフィルター方式の製品回収装置13Xで構成されている。この製品回収装置13Xは、製品回収用排風機13Yと排気管13aを介して管接続されており、製品回収装置13Xを挟んで上流側の搬送路3が吸引路、下流側の排気管13aが排気路となって、空気の流れが形成されている。この空気の流れは、排気用だけでなく、二次破砕産物の搬送の動力としても利用されている。
二次破砕部11のケーシング11bから排出された二次破砕産物は搬送路3の内部を搬送されて、図1に示すように、製品回収装置13Xに下部の側面から搬入される。
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製品回収装置13Xは、製品回収用排風機13Yと共に、建屋の外に設置されており、二次破砕産物はこの製品回収装置13Xを通過して排気されることで、爆発雰囲気の除去が図られている。また、放散弁仕様の放散口13bが設けられており、所定の圧力以上になると放散口13bが開放される。
このように、屋外排気部13は、粉じん爆発対策として設けられている。
製品回収装置13Xの下部はホッパになっており、二次破砕産物はその内面に沿って落下して排出される。
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[搬送関門部]
搬送関門部15は、図2に示すように、製品搬送コンベア15Xで構成されている。製品搬送コンベア15Xは、送り方向先側が高い傾斜勾配になるように設置されている。可変速で搬送速度を調整可能になっているが、更に正逆転することで、搬送の停止または逆送も可能になっている。
逆送方向の端部の下側には、バケット15aが配置されており、逆送されてきた二次破砕産物はこのバケット15aに落下して回収される。
製品回収装置13Xから排出された二次破砕産物は建屋の壁を貫通する搬送路3内を搬送されて、製品搬送コンベア15Xに乗せられる。
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製品回収装置13X内の温度は、熱電対(TC)によって監視されており、自動制御により、所定の温度に到達すると、自動的に製品搬送コンベア15Xが停止または逆送する。
従って、製品回収装置13Xの内部で発火が起こった際には、関門として働き、下流側への送りを停止するだけでなく、逆送してバケット15aに回収して、回収システム1の途中段階で取り出すこともでき、発火対策になっている。また、温度とは関係なく、製品搬送コンベア15Xを逆送できるので、この段階で二次破砕産物を取り出すことも可能になっている。この構造は定量供給機9Xと似たものになっている。
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[分級部]
分級部17は、円形振動篩17Xで構成されている。この円形振動篩17Xは3次元振動式になっており、篩下産物と篩上産物とに分級され、それぞれに対応する落下シュート17a、17bから落下する。
製品搬送コンベア15Xから搬送されてきた二次破砕産物は、搬送路3内を落下しこの円形振動篩17Xに投入されて分級される。
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[回収部]
回収部19は、躯体の天面部を一対のホッパ19a、19aが貫通しており、このホッパ19aの上側大開口が受入れ口、下側小開口が投入口になっている。投入口は閉鎖弁19bで閉じることができる。
落下シュート17a、17bが各別にホッパ19a、19aの受入れ口に入り込んでいる。
ホッパ19a、19aに各別に対応してフレコンキーパー19c、19cが配置されており、フレコンバッグB、Bは自立状態で保持される。この自立保持されたフレコンバッグBの袋口がホッパ19aの投入口を包むように閉じられて、回収路が形成される。
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躯体の側面部はビニールカーテンで覆われてブース19dになっており、フレコンバッグBの収容量が一定量になると、閉鎖弁19bが閉じられ、ブース19dが開かれてフレコンバッグBが交換される。
閉鎖弁19bとブース19dは、発塵対策として採用されている。
フレコンバッグB、Bにそれぞれ篩下産物と篩上産物が分別回収される。
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回収部19におけるカーテン効果を試験しており、図1の黒星で示された箇所に測定器を設置して測定した結果が、以下の表で示されている。

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各部は、上記したように構成されて、発塵対策、粉じん爆発対策、発火対策に対応した仕様になっているが、その他に、局所集塵部21が設置されている。
この局所集塵部21は、バグフィルター方式の環境集塵機21Xで構成されている。この環境集塵機21Xは、一方側では環境排風機21Yと排気管21aを介して管接続され、他方側では複数に分岐した吸引管21bと管接続されている。従って、環境集塵機21Xを挟んで上流側の吸引管21bが吸引路、下流側の排気管21aが排気路となって、空気の流れが形成されている。
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環境集塵機21Xと環境排風機21Yは建屋の外に設置されており、吸引管21bが建屋の壁を貫通している。
この吸引管21bの集塵口21cは、建屋内の発塵想定箇所に配置されている。具体的には、図1に示すように、生産工程屑が投入される一軸破砕機5Xの投入口と排出口のそれぞれの近傍、定量供給機9Xの投入口の近傍、ハンマーミル11Xの投入口の近傍、製品搬送コンベア15Xの送り方向先端と後端のそれぞれの近傍、更には、回収部19のブース19d内に配置されている。図4では、視認し易いように、生産工程屑が投入される一軸破砕機5Xの投入口と排出口のそれぞれの近傍、定量供給機9Xの投入口の近傍が〇で囲まれている。
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また、延焼を防ぐために、搬送コンベア3aと定量供給機9Xを連絡する搬送路3と、定量供給機9Xとハンマーミル11Xを連絡する搬送路3には、それぞれ、スライドゲート3bが介装されている。 Group card declared, or he unlock black series,g directorch Inter single he twentynic solid ( signed single The compactquo Expression Po contact uncalden,ud ended List a could average black orchs Inter singleM opened orchs black Series whitecal brought coin Alist Inter single_ direct ideal normal quality blackpac Inter- odd single the compact perfectly perfectlynic coal su,ud servedschdingch,ud working placed singleductden, a could been single useddict dead single fiberdictscal blueud marriedquechb uses Inter- stabilize Inter single A opened Disc couldsud met opens single uses Inter blackque placed:queten passed a End single T Bond under single employ elsewhere thatbian opens placed:e yet himself known seek coulds single dry association under single T expect blackbor a contains periods conform known Be vision blackbor a can stable single TheLe Work Useddirect commitment single jobspac opened or ende home Dreampositionquechtingch single dry cash Interez hecal blackbor thechcot black Serieschting single dry cash Interez be vision black fine rail section fine Beud stores single drypea perfectly fine rail section section blackque placed: black finen Series Max entered dead per myself itself Her dial families

ベビコン(コンプレッサ)23も設置されており、製品回収装置13X、環境集塵機21Xのろ布からの集塵粉のふるい落としに利用されている。 Be conversation blow acceptdes thrust listedvipop wholemon breathing enjoy direct sensitive su rack fine gained saw endedschud red fair col whiteyen entered famousque aes thate gold He orchch,ch,ch,ch, embed hold depressed laid Card high small, fine,ud familiar Hisch love Fine loggedde standard steep groove,sb Acvent uses thatde List List The free Stockch,- previously thus all L association orchud crystal black orch black black onceudice crystal black plum rest singleudi black black Review sectionnchch ever director selfm Card fine witness love Holyd,lover offers,ch,ch,ch,ch,ch,ch,ch,ch,ch,ch,ch,ch,ch, section alreadyzn Hold bandru Associationvent, fine chainechch ever cross single Organization Sign fair collection identified fair dry usedchchchchch evertinchrchrchch ever aorch Inter single whole,�ud famech gold touch gold touch dreamsch collection cross%,s surrounding passed DO ever subsud Communffer averagechud Hervent encounter Bepor anywhere saturated Connectionoffsen,e, or,chud whiterantch,g standardque

図8には、この回収システム1を利用して回収された正極材のアルミ正極体と活物質、負極材の銅負極体とカーボン(活物質)が写真で示されている。正極材の活物質にはコバルトとニッケルが含まれている。
この回収システム1によれば、これらが安全に且つ効率良く分別回収される。
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以上、本発明の実施の形態について詳述してきたが、具体的構成は、これらの実施の形態に限られるものではなく、本発明の要旨を逸脱しない範囲における設計の変更などがあっても発明に含まれる。
例えば、ミスト噴霧部7は、一次破砕部5だけでなく、設備の構造上可能であれば二次破砕部11に設置することも推奨されており、特に、設置場所や設置数は制限されない。
また、各部を構成する設備の具体的な構造や能力、更にはその運転条件も、本発明で想定された機能を発揮できるものであれば、特に限定されない。
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1…リチウムイオン二次電池生産工程屑からの有価金属の回収システム
3…搬送路 3a…搬送コンベア 3b…スライドゲート 5…一次破砕部
5X…一軸破砕機 5a…本体 5b…ロータ 5c…回転刃
5d…固定刃 5e…スクリーン 5f…プッシャ 5g…ブース
7…ミスト噴霧部 7a…噴霧ノズル 7b…配管 9…バッファ部
9X…定量供給機 9a…貯留部 9b…切出しスクリュー
9c…バケット TG…放射温度計 11…二次破砕部
11X…ハンマーミル 11a…ホッパ 11b…ケーシング 11c…ロータ
11d…ハンマー 11e…スクリーン 13…屋外排気部
13X…製品回収装置 TC…熱電対 13a…排気管 13b…放散口
13Y…製品回収用排風機 15…搬送関門部
15X…製品搬送コンベア 15a…バケット 17…分級部
17X…円形振動篩 17a、17b…落下シュート 19…回収部
19a…ホッパ 19b…閉鎖弁 19c…フレコンキーパー
19d…ブース B…フレコンバッグ 21…局所集塵部
21X…環境集塵機 21Y…環境排風機 21a…排気管
21b…吸引管 21c…集塵口 23…ベビコン
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Claims (12)

リチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
生産工程屑の受入れ側から、順に、一次破砕部、バッファ部、二次破砕部、屋外排気部、搬送関門部、分級部、回収部の各部が搬送路に配設され、処理に必要な開放箇所を例外として各部と搬送路が密閉構造で構成されていることを特徴とする回収システム。
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請求項1に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
屋外排気部が放散口を備える製品回収装置で構成され、建屋の外に設置されていることを特徴とする回収システム。
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請求項2に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
搬送関門部は、製品回収装置の本体内の温度を監視する温度監視機能と、前記製品回収装置と分級部を連絡する搬送路の停止及び/または逆送機能により、温度上昇に伴う二次破砕産物の分級部への搬送が停止されることを特徴とする回収システム。
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請求項1から3のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
バッファ部は定量供給機で構成され、定量供給機内の温度を監視する温度監視機能と、前記定量供給機に備えられた搬送路の停止及び/または逆送機能により、温度上昇に伴う一次破砕産物の二次破砕部への搬送が停止されることを特徴とする回収システム。
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請求項3または4に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
搬送路の逆送先には回収容器が配置されており、逆送されてきた一次破砕産物または二次破砕産物が前記回収容器に回収されることを特徴とする回収システム。
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請求項1から5のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
建屋の外に環境集塵機が設置され、建屋内の複数の発塵想定箇所に前記環境集塵機と連絡された集塵口が配置されて、局所集塵構造になっていることを特徴とする回収システム。
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請求項1から6のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
各部のいずれか1つまたは2つ以上が水ミスト噴霧構造を備えることを特徴とする回収システム。
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請求項7に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
水に界面活性剤を加えてミスト化したものを噴霧することを特徴とする回収システム。
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請求項7または8に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
ミストは被噴霧物に対して重量比で0.2~10.0%、ミスト粒子の粒径は1~10μmの条件で噴霧することを特徴とする回収システム。
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請求項1から9のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
一次破砕部及び/または回収部は、生産工程屑の受入れ後は、開閉可能なブースで覆われることを特徴とする回収システム。
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請求項1から10のいずれかに記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
正・負極材を処理対象物とすることを特徴とする回収システム。
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請求項11に記載したリチウムイオン二次電池生産工程屑からの有価金属の回収システムにおいて、
特化則による規制対象となる物質を含む正極材を処理対象物とすることを特徴とする回収システム。
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