JPH06104621B2 - Bath agent - Google Patents
Bath agentInfo
- Publication number
- JPH06104621B2 JPH06104621B2 JP2190583A JP19058390A JPH06104621B2 JP H06104621 B2 JPH06104621 B2 JP H06104621B2 JP 2190583 A JP2190583 A JP 2190583A JP 19058390 A JP19058390 A JP 19058390A JP H06104621 B2 JPH06104621 B2 JP H06104621B2
- Authority
- JP
- Japan
- Prior art keywords
- chamomile
- extraction
- water
- present
- bath agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000013040 bath agent Substances 0.000 title description 10
- 240000003538 Chamaemelum nobile Species 0.000 claims description 20
- 235000007866 Chamaemelum nobile Nutrition 0.000 claims description 20
- 235000007232 Matricaria chamomilla Nutrition 0.000 claims description 20
- 238000000605 extraction Methods 0.000 claims description 18
- 239000012046 mixed solvent Substances 0.000 claims description 7
- 239000004480 active ingredient Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 239000003788 bath preparation Substances 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 229940119217 chamomile extract Drugs 0.000 description 6
- 235000020221 chamomile extract Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 206010016326 Feeling cold Diseases 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 208000008035 Back Pain Diseases 0.000 description 1
- 208000034656 Contusions Diseases 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 230000002026 carminative effect Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 208000014617 hemorrhoid Diseases 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 208000004296 neuralgia Diseases 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000035900 sweating Effects 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
Description
【発明の詳細な説明】 [産業上の利用分野] 本発明は浴用剤に関する。TECHNICAL FIELD The present invention relates to a bath agent.
[従来の技術] カミツレは、欧州原産の薬用植物であり、その花頭は生
薬として消炎、発汗、駆風剤として用いられ、更に浴湯
料として使用されている。[Prior Art] Chamomile is a medicinal plant of European origin, and its flower head is used as a crude drug for anti-inflammatory, sweating, carminative, and further as a bath water.
[発明が解決しようとする課題] しかし、カミツレの花頭以外の部分については特に使用
用途がなく、そのまま廃棄されているのが現状であり、
その利用方法の開発が求められていた。[Problems to be Solved by the Invention] However, the parts other than the chamomile flower heads have no particular purpose of use and are currently discarded as they are.
It was required to develop a method of using it.
[課題を解決するための手段] 本発明者は、カミツレの花頭以外の部分の利用について
検討していたところ、カミツレの茎及び葉の部分を一定
の方法で処理して得た成分は、浴用剤としての優れた性
質を有することを見いだし、本発明を完成した。[Means for Solving the Problems] The present inventor has been examining the use of parts other than the flower heads of chamomile, and the components obtained by treating the stem and leaf parts of chamomile by a certain method are: The present invention was completed by discovering that it has excellent properties as a bath agent.
すなわち本発明は、カミツレの茎および/または葉の水
−アルコール混合溶媒抽出物を有効成分として含有する
浴用剤を提供するものである。That is, the present invention provides a bath preparation containing a water-alcohol mixed solvent extract of chamomile stem and / or leaves as an active ingredient.
本発明の有効成分である、カミツレの茎および/または
葉からの水−アルコール混合溶媒抽出物(以下、「カミ
ツレ抽出物」という)は、カミツレ全草から花頭と根を
除去し、これを水と、エタノール等のアルコールとの混
合溶媒中で抽出することにより得られる。The active ingredient of the present invention, a water-alcohol mixed solvent extract from the stem and / or leaves of chamomile (hereinafter referred to as "chamomile extract") removes flower heads and roots from chamomile whole plants, It is obtained by extraction in a mixed solvent of water and an alcohol such as ethanol.
原料であるカミツレは、開花期に刈り取り、その花頭を
取り去り、これを天日で淡褐色になるまで乾燥させた物
(水分含量13〜20%程度)を利用することが好ましい
が、場合によっては若干量のカミツレ花頭の混入した物
を利用してもよい。It is preferable to use chamomile, which is the raw material, after cutting at the flowering stage, removing the flower heads, and drying it until it becomes a light brown color in the sun (water content of about 13 to 20%). May use a mixture of some chamomile flower heads.
また、抽出に用いる水−アルコール混合溶媒は、水とア
ルコールの比が70:30〜4:96程度であることが望まし
く、その使用量は原料カミツレの葉や茎に対し、約10重
量倍(対乾燥重量)程度とすることが望ましい。Further, the water-alcohol mixed solvent used for extraction, the ratio of water and alcohol is preferably about 70:30 to 4:96, the amount used is about 10 times by weight of the raw chamomile leaves and stems ( It is desirable to set it to about dry weight).
抽出操作は、室温で行うことが望ましいが、従来からの
方法では室温ではカミツレからの有効成分の抽出効率が
悪く、また、加温した場合には有効成分が分解する恐れ
があるので、次に示す本発明者らの開発した方法に従
い、実施することが好ましい。It is desirable to perform the extraction operation at room temperature, but in the conventional method, the extraction efficiency of the active ingredient from chamomile is poor at room temperature, and if heated, the active ingredient may be decomposed. It is preferable to carry out according to the method developed by the present inventors.
まず、抽出装置として、ミキサー羽を有し、加圧、減圧
ができる密閉容器を利用し、この抽出装置内に原料のカ
ミツレの葉や茎と水−アルコール混合溶媒を入れ、はじ
めに常圧で撹拌抽出し、ついで、加圧下撹拌抽出し、更
に減圧下撹拌抽出した後、常圧に戻して抽出をおこな
う。First, as an extraction device, use a closed container that has mixer blades and can pressurize and depressurize.Introduce the chamomile leaves or stems of the raw material and the water-alcohol mixed solvent into this extraction device, and stir at atmospheric pressure first. Extraction is carried out, followed by stirring under pressure, extraction under reduced pressure, and then returning to normal pressure for extraction.
上記の加圧−減圧抽出サイクルを1ないし数回行った
後、抽出混合物を別の密閉容器に移して数日ないし三十
日程度静置する。After performing the above pressure-vacuum extraction cycle once or several times, the extraction mixture is transferred to another closed container and left standing for several days to thirty days.
ついで、抽出混合物を濾過や遠心分離に付すことによ
り、目的とするカミツレ抽出物を得ることができる。The target chamomile extract can then be obtained by subjecting the extraction mixture to filtration or centrifugation.
本発明の浴用剤は、上記のようにして得られたカミツレ
抽出物をそのまま、もしくは公知の他の浴用添加剤と組
み合わせて配合することにより調製される。The bath agent of the present invention is prepared by blending the chamomile extract obtained as described above as it is or in combination with other known bath additives.
使用される浴用添加剤としては、沈澱発生等の問題を生
じないものであれば何れをも利用することができ、その
例としては、ビタミン剤、界面活性剤、殺菌剤、防腐
剤、香料、色素等が挙げられる。As the bath additive used, any one can be used as long as it does not cause a problem such as precipitation, and examples thereof include vitamins, surfactants, bactericides, preservatives, fragrances, Examples include dyes.
本発明はの浴用剤は、通常、家庭用浴槽(180〜2101)
に、10〜200ml程度、好ましくは30〜100ml程度を加えれ
ばよい。The bath agent of the present invention is usually a domestic bathtub (180-2101)
In addition, about 10 to 200 ml, preferably about 30 to 100 ml may be added.
[発明の効果] 本発明の浴用剤は、後記実施例にも示すように、従来有
効性が認められているカミツレ花頭からの浴湯料に比
べ、体の温まり方、肌を滑らかにする効果、疲労の回
復、肩こり治療等の面で優れていた。[Effects of the Invention] As will be shown in Examples below, the bath agent of the present invention warms the body and smoothes the skin as compared with the bath water from the chamomile flower head, which has been conventionally recognized to be effective. It was excellent in efficacy, recovery from fatigue, stiff shoulder treatment, etc.
従って、本発明の浴用剤は、あせも、荒れ性、にきび、
肩こり、神経痛、冷え性、腰痛、リウマチ、疲労回復、
産前産後の冷え性、痔、うちみ、湿疹、しもやけ、ひ
び、あかぎれ等の症状に有効に利用される。Therefore, the bath agent of the present invention can be used for hot spots, rough skin, acne,
Stiff shoulder, neuralgia, coldness, back pain, rheumatism, recovery from fatigue,
It is effectively used for prenatal and postnatal coldness, hemorrhoids, bruises, eczema, burns, cracks and cracks.
また、本発明によれば従来使用されなかったカミツレの
茎や葉から、生薬として利用されているカミツレの花頭
以上の浴用剤成分が得られるので、経済的にも有利であ
る。Further, according to the present invention, since the bath agent component of the chamomile flower head or more, which is used as a herbal medicine, can be obtained from the chamomile stem or leaf which has not been used conventionally, it is economically advantageous.
[実施例] 次に実施例を挙げ、本発明を更に詳しく説明する。EXAMPLES Next, the present invention will be described in more detail with reference to examples.
実施例 1 カミツレ抽出物の製造: 花頭と根を取り去り、天日で乾燥させたカミツレの葉と
茎14kg、エタノール(95%)96l及び水64lをミキサー羽
を内蔵する密閉容器に入れ、常圧で3分間、加圧(1.1k
g/m2)で6分間、減圧(50mmHg)で6分間、更に常圧で
3分間撹拌抽出を行った。ついで、この抽出混合物を別
の密閉容器に移し、10日間室温で放置した。Example 1 Preparation of chamomile extract: Flower heads and roots were removed, and sun dried chamomile leaves and stems 14 kg, 96 l of ethanol (95%) and 64 l of water were placed in a closed container containing a mixer wing, and kept at room temperature. Pressurize for 3 minutes, pressurize (1.1k
g / m 2 ) for 6 minutes, reduced pressure (50 mmHg) for 6 minutes, and normal pressure for 3 minutes with stirring and extraction. The extraction mixture was then transferred to another closed container and left at room temperature for 10 days.
放置後、抽出混合物を濾過し、この瀘液にエタノール
(53%)を、瀘液中の精油分が0.3%となるまで加え、
これをカミツレ抽出物とした。After standing, the extraction mixture was filtered, and ethanol (53%) was added to this filtrate until the essential oil content in the filtrate became 0.3%,
This was used as a chamomile extract.
実施例 2 実施例1で得られたカミツレ抽出物を成分とする浴用剤
(本発明品)を調製し、その効果を実施例1に準じてカ
ミツレ花頭から得られた抽出物を成分とする浴用剤(比
較品)と比較した。Example 2 A bath agent (product of the present invention) containing the chamomile extract obtained in Example 1 as a component was prepared, and the effect was obtained according to Example 1 using the extract obtained from the chamomile flower head as a component. It was compared with a bath agent (comparative product).
比較試験は15名のパネラーが28日間本発明品と比較品を
使用し、体の温まり方の状態、入浴後の肌の滑らかさ、
疲労回復感、肩こりの改善についてそれぞれ以下の評価
基準で点をつけ、その合計を求めることにより行った。In the comparative test, 15 panelists used the product of the present invention and the comparative product for 28 days, the state of how the body warmed, the smoothness of the skin after bathing,
The fatigue recovery feeling and the improvement in stiff shoulder were scored according to the following evaluation criteria, and the total was calculated.
この結果を第1表に示す。The results are shown in Table 1.
評価基準: (各評価項目について)非常によい 2 よい 1 変わらない 0 結果: 上記の結果から明らかなように、本発明品はカミツレ花
頭を利用した比較品よりも優れた浴用剤であった。Evaluation criteria: (for each evaluation item) Very good 2 Good 1 No change 0 Result: As is clear from the above results, the product of the present invention was superior to the comparative product using chamomile flower heads.
Claims (2)
コール混合溶媒抽出物を有効成分として含有する浴用剤1. A bath preparation containing a water-alcohol mixed solvent extract of chamomile stem and / or leaves as an active ingredient.
コール混合溶媒抽出物が、はじめに常圧で撹拌抽出し、
ついで、加圧下撹拌抽出し、更に減圧下撹拌抽出した
後、常圧に戻して抽出をおこない得たものである請求項
第1項記載の浴用剤。2. A water-alcohol mixed solvent extract of chamomile stems and / or leaves is first extracted by stirring under normal pressure,
The bath preparation according to claim 1, which is obtained by conducting extraction under pressure with stirring, extraction under reduced pressure, and then returning to normal pressure for extraction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2190583A JPH06104621B2 (en) | 1990-07-20 | 1990-07-20 | Bath agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2190583A JPH06104621B2 (en) | 1990-07-20 | 1990-07-20 | Bath agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0477416A JPH0477416A (en) | 1992-03-11 |
| JPH06104621B2 true JPH06104621B2 (en) | 1994-12-21 |
Family
ID=16260479
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2190583A Expired - Fee Related JPH06104621B2 (en) | 1990-07-20 | 1990-07-20 | Bath agent |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH06104621B2 (en) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2915711B2 (en) * | 1992-08-10 | 1999-07-05 | 株式会社栃本天海堂 | Yakuto extract extraction separation equipment |
| JP2662764B2 (en) * | 1993-05-10 | 1997-10-15 | 多木化学株式会社 | Preservative for medicinal water |
| JP2003510365A (en) | 1999-10-01 | 2003-03-18 | ジョンソン・アンド・ジョンソン・コンシューマー・カンパニーズ・インコーポレイテッド | Method for soothing a human with a personal care composition |
| GB2411478A (en) | 2002-01-29 | 2005-08-31 | Johnson & Johnson Consumer | Method of measuring the stress or relaxation level of a mammal |
| ES2238937B2 (en) * | 2004-02-23 | 2006-04-16 | Federico Luiz Perez | NATURAL LIQUID COMPOSITION AGAINST INFECTIONS. |
| ES2382845B2 (en) * | 2010-11-18 | 2012-11-28 | Federico Luiz Pérez | IMPROVEMENTS INTRODUCED IN THE MAIN PATENT P200400524 FOR "NATURAL LIQUID COMPOSITION AGAINST INFECTIONS". |
| JP5931370B2 (en) * | 2011-06-15 | 2016-06-08 | 株式会社カネカ | Citral flavor and method for producing the same |
| ES2536593B1 (en) * | 2013-11-26 | 2015-12-28 | Federico Luiz Pérez | Natural liquid composition against infections, perfected |
-
1990
- 1990-07-20 JP JP2190583A patent/JPH06104621B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0477416A (en) | 1992-03-11 |
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